Solutions and Colloids in The Purification of Water

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\plain\pard\sl-537 \li2083 \ri1043 \expndtw0 \b \f10 \fs48 \cf1 Solutions and Co
lloids in
\plain\par
\pard\sl-560 \li2083 \ri609 \fi360 \expndtw3 \b \f10 \fs48 \cf1 the Purification
of Water
\par
\plain\sl-183\fs18\par\sl-240\fs24\par\par\pard\pard\sl-260 \li2083 \ri6373 \exp
ndtw-17 \b \f10 \fs18 \cf1 PURPOSE
\plain\par
\pard\sl-260 \li2083 \ri501 \expndtw3 \f20 \fs18 \cf1 During this lab you will i
dentify one of the chemical contaminants in a water
\plain\expndtw2 \f20 \fs18 \cf1 sample using colorimetric techniques combined wi
th absorption spectroscopy.
\plain\expndtw2 \f20 \fs18 \cf1 You will then purify your water sample using pro
cesses based on the solubility
\plain\expndtw2 \f20 \fs18 \cf1 and reactivity of those contaminants and then re
test your purified water to de\plain\expndtw2 \f20 \fs18 \cf1 termine statistically the improvement in the wat
er quality.
\plain\par
\sl-215\fs22\par\pard\pard\sl-260 \li2083 \ri5900 \expndtw-10 \b \f10 \fs18 \cf1
BACKGROUND
\plain\par
\pard\sl-260 \li2083 \ri496 \expndtw1 \f20 \fs18 \cf1 Clean water has always bee
n very important to the people of the world. Although
\plain\expndtw2 \f20 \fs18 \cf1 approximately 2/3 of the world is covered by wat
er only a small amount of that
\plain\expndtw2 \f20 \fs18 \cf1 water can be considered "drinkable". What makes
the water undrinkable is the
\plain\expndtw2 \f20 \fs18 \cf1 mixture of both chemical and biological entities
that abound in it.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li2083 \ri501 \expndtw2 \f20 \fs18 \cf1 Water
itself is a simple polar molecule, with an uneven distribution of electron
\plain\expndtw1 \f20 \fs18 \cf1 density. Water has a partial negative charge ({\
f63 \u57444\'3f}-) near the oxygen atom due to the
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e charges ({\f63 \u57444\'3f}+) near the hydrogen
\plain\expndtw2 \f20 \fs18 \cf1 atoms. The ability of ions and other molecules t
o dissolve in water is due to this
\plain\expndtw0 \f20 \fs18 \cf1 polarity.

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\sl-305\fs31\par\pard\pard\sl-255 \li2083 \ri500 \expndtw3 \f20 \fs18 \cf1 One o
f the more common contaminants in water is the phosphate ion (PO\dn5 \fs10 43-\d
n0 \fs18 ).
\plain\par
\pard\sl-218 \li2083 \ri500 \expndtw2 \f20 \fs18 \cf1 Because it is an ion, phos
phate is soluble in water. Phosphates can enter lakes,
\plain\par
\pard\sl-260 \li2083 \ri501 \expndtw3 \f20 \fs18 \cf1 ponds, rivers and oceans f
rom various sources such as fertilizers, wastewater
\plain\expndtw2 \f20 \fs18 \cf1 treatment plants, soaps and detergents and indus
trial processes. Detergents are
\plain\expndtw2 \f20 \fs18 \cf1 especially responsible for the release of phosph
ates into water. Some detergents
\plain\expndtw3 \f20 \fs18 \cf1 contain tripolyphosphates that are used to stabi
lize dirt particles to increase
\plain\expndtw3 \f20 \fs18 \cf1 their cleaning efficiency. When these detergents
are washed away they yield
\plain\expndtw4 \f20 \fs18 \cf1 high concentrations of phosphate into the enviro
nment. Phosphates act as
\plain\expndtw1 \f20 \fs18 \cf1 "nutrients" to the plants and algae that grow in
lakes and ponds. Phosphates are
\plain\expndtw2 \f20 \fs18 \cf1 the primary limiting factor in fresh water plant
and algal growth. The growth of
\plain\expndtw1 \f20 \fs18 \cf1 excess plants and algae in a lake or pond is cal
led "algal bloom". The excess plant
\plain\expndtw2 \f20 \fs18 \cf1 growth causes an ecological imbalance within the
lake or pond. Seasonal plants
\par
\plain\sl-212\fs21\par\sl-240\fs24\par\par\pard\pard\sl-257 \li8870 \ri18 \expnd
tw-12 \f10 \fs16 \cf1 15
\plain\expndtw-10 \f20 \fs26 \cf1 {\f63 \u57454\'3f}
\par
\sect\sectd\sbkpage\margtsxn1240\pard
{\shp
ffd8ffe000104a46494600010100000100010000ffdb004300010101010101010101010101010101
01010101010101010101010101010101010101010101010101010101010101010101010101010101
010101010101010101ffdb0043010101010101010101010101010101010101010101010101010101
0101010101010101010101010101010101010101010101010101010101010101010101010101ffc0
001108067204fb03012200021101031101ffc4001f00000105010101010101000000000000000001
02030405060708090a0bffc400b5100002010303020403050504040000017d010203000411051221
31410613516107227114328191a1082342b1c11552d1f02433627282090a161718191a2526272829
2a3435363738393a434445464748494a535455565758595a636465666768696a737475767778797a
0101010101010101010000000000000102030405060708090a0bffc400b511000201020404030407
05040400010277000102031104052131061241510761711322328108144291a1b1c109233352f015
6272d10a162434e125f11718191a262728292a35363738393a434445464748494a53545556575859
5a636465666768696a737475767778797a82838485868788898a92939495969798999aa2a3a4a5a6
0028a28a0028a28a0028a28a0028a28a0028a28a0028a28a0028a28a0028a28a0028af883fe0995f
f28dcff827cffd9907eca1ff00aa1bc035f6fd036acdaecec145145020a28a2800a28a2800a28a28
00a28a2800a28a2800a28a2800a28a2800a28a2803e3cff82787863c49e09fd803f619f0678cfc3d
ae7847c61e11fd8f3f666f0c78afc29e27d26ff41f127863c49a0fc15f04e95aef87bc43a16ab6f6
9aa68bae68baa5a5d69bab693a95adb5fe9d7f6d7167796f0dc43246bf61d14500f56df70a28a280
0a28a2800a28a2800a28a2800a28a2800a28a2800a28a2803fffd9
}}}

}}\margt900\margb180\margr1400\margl900
\plain\pard\sl-286 \li0 \ri3362 \expndtw-10 \f20 \fs26 \cf1 {\f63 \u57454\'3f}
\plain\tx282 \tab \expndtw8 \f10 \fs16 \cf1 Experiment
\plain\tx2239 \tab \expndtw0 \f10 \fs16 \cf1 3\i {\f63 \u8226\'3f} Solutions an
d Colloids in the Purification of Water
\par
\sect\sectd\sbknone\cols2\colno1\colw5077\colsr286\colno2\colw4575
\plain\sl-173\fs17\par\sl-240\fs24\par\par\par\pard\pard\sl-260 \li540 \ri1 \exp
ndtw3 \f20 \fs18 \cf1 that have become too abundant die during the winter
\plain\expndtw2 \f20 \fs18 \cf1 as a regular part of their life cycle, but with
too many
\plain\expndtw2 \f20 \fs18 \cf1 in the water, the aerobic (oxygen dependent) bac
teria
\plain\expndtw2 \f20 \fs18 \cf1 that digest them use up all of the oxygen in the
water.
\plain\expndtw3 \f20 \fs18 \cf1 This loss of oxygen then kills off oxygen depend
ent
\plain\expndtw3 \f20 \fs18 \cf1 plants and fish. Eventually, decomposition is ta
ken
\plain\expndtw3 \f20 \fs18 \cf1 over by anaerobic (non-oxygen dependent) bacteri
a.
\plain\expndtw1 \f20 \fs18 \cf1 The breakdown of organic materials by anaerobes
often
\plain\expndtw1 \f20 \fs18 \cf1 produces toxic materials. It is these toxic mate
rials that
\plain\expndtw2 \f20 \fs18 \cf1 make the water undrinkable.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li540 \ri4 \expndtw1 \f20 \fs18 \cf1 pH is al
so a good indicator of water contamination. The
\plain\expndtw1 \f20 \fs18 \cf1 presence of large quantities of bacteria or othe
r organic
\plain\expndtw2 \f20 \fs18 \cf1 contaminants in water can produce ammonia that w
ill
\plain\expndtw1 \f20 \fs18 \cf1 raise the pH of the water. Acidic water can indi
cate the
\plain\expndtw1 \f20 \fs18 \cf1 presence of many industrial wastes including sul
fur and
\plain\expndtw2 \f20 \fs18 \cf1 nitrogen oxides which become sulfuric and nitric
acids
\plain\expndtw2 \f20 \fs18 \cf1 when delivered by rain or runoff into lakes or s
treams.
\plain\expndtw1 \f20 \fs18 \cf1 pH is normally recorded in the field at the wate
r sources
\plain\expndtw2 \f20 \fs18 \cf1 but as long as the water sample is refrigerated
to keep
\plain\expndtw2 \f20 \fs18 \cf1 any biological entities from changing the pH it
should
\plain\expndtw2 \f20 \fs18 \cf1 be reasonably the same when taken in the lab.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li540 \ri0 \expndtw2 \f20 \fs18 \cf1 For toda
y's experiment, pH will be recorded using the
\plain\expndtw2 \f20 \fs18 \cf1 Orion\dn4 \fs10 \dn0 \fs18 pH meters and the pho
sphate concentration will
\plain\expndtw2 \f20 \fs18 \cf1 be measured using a technique called spectroscop
y.
\plain\par
\sl-215\fs22\par\pard\pard\sl-260 \li540 \ri3126 \expndtw-14 \b \f10 \fs18 \cf1
SPECTROSCOPY
\plain\par
\pard\sl-260 \li540 \ri0 \expndtw2 \f20 \fs18 \cf1 One of our most important sen
ses is vision; we rely on
\plain\expndtw3 \f20 \fs18 \cf1 our sight to perform nearly ever ything we do. E
ven
\plain\expndtw3 \f20 \fs18 \cf1 though vision is very important, our eyes only s
ee a
\plain\expndtw3 \f20 \fs18 \cf1 narrow band of the electromagnetic spectrum, fro
m
\plain\expndtw3 \f20 \fs18 \cf1 about 390 nm to 770 nm. This band has been terme
d
\plain\expndtw2 \f20 \fs18 \cf1 the\i visible region\i0 . In this discussion, l
ight and electro\plain\expndtw2 \f20 \fs18 \cf1 magnetic radiation are synonymous.
\par
\column
\plain\sl-173\fs17\par\sl-240\fs24\par\par\par\pard\pard\sl-260 \li0 \ri36 \expn
dtw2 \f20 \fs18 \cf1 of the wavelengths of light that are not being absorbed
\plain\expndtw1 \f20 \fs18 \cf1 by the substance. (Emission and absorption spect
ra of a
\plain\expndtw2 \f20 \fs18 \cf1 substance are complementary: when added together
, a
\plain\expndtw2 \f20 \fs18 \cf1 continuous spectrum is obtained.) A molecule can
ab\plain\expndtw2 \f20 \fs18 \cf1 sorb some of the light only if it can accommodat
e that
\plain\expndtw2 \f20 \fs18 \cf1 additional energy by promoting electrons to high
er en\plain\expndtw1 \f20 \fs18 \cf1 ergy levels. The energy of the light being absor
bed must
\plain\expndtw3 \f20 \fs18 \cf1 match the energy required to promote the electro
n.
\plain\expndtw3 \f20 \fs18 \cf1 Therefore, not all wavelengths of light are abso
rbed
\plain\expndtw2 \f20 \fs18 \cf1 equally by a sample. An absorbance spectrum depi
cts
\plain\par
\pard\sl-260 \li0 \ri180 \expndtw2 \f20 \fs18 \cf1 what wavelengths of light are
absorbed by a sample.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri35 \expndtw3 \f20 \fs18 \cf1 Phosphate
ion in water is colorless and therefore not
\plain\expndtw2 \f20 \fs18 \cf1 easily detected using typical spectrophotometric
tech\plain\expndtw3 \f20 \fs18 \cf1 niques (which determines concentration from colo
r
\plain\expndtw2 \f20 \fs18 \cf1 intensity). In order to observe an absorbance th
at can
\plain\expndtw4 \f20 \fs18 \cf1 be related to concentration, phosphate must be r
e\plain\expndtw2 \f20 \fs18 \cf1 acted with a coloring agent. In this experiment
we will
\plain\expndtw4 \f20 \fs18 \cf1 be reacting phosphate with ammonium molybdate
\plain\par
\pard\sl-301 \li0 \ri36 \expndtw1 \f20 \fs18 \cf1 (NH\dn5 \fs10 4\dn0 \fs18 )\dn
5 \fs10 6\dn0 \fs18 Mo\dn5 \fs10 7\dn0 \fs18 O\dn5 \fs10 24\dn0 \fs18 :4H\dn5 \f
s10 2\dn0 \fs18 O and stannous chloride (SnCl\dn5 \fs10 2\dn0 \fs18 :2H\dn5 \fs1
0 2\dn0 \fs18 O)
\plain\par
\pard\sl-218 \li0 \ri36 \expndtw2 \f20 \fs18 \cf1 in an acidic solution. When co
mbined with phosphate,
\plain\par
\pard\sl-260 \li0 \ri36 \expndtw2 \f20 \fs18 \cf1 this coloring agent produces a
blue compound whose
\plain\expndtw2 \f20 \fs18 \cf1 absorption can be observed at 650 nm.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri36 \expndtw2 \f20 \fs18 \cf1 Spectrosc
opy is the study of the interaction of electro\plain\expndtw4 \f20 \fs18 \cf1 magnetic radiation with matter. Through the many
\plain\expndtw2 \f20 \fs18 \cf1 spectroscopic techniques available, the shape, c
ompo\plain\expndtw1 \f20 \fs18 \cf1 sition and the way a compound or molecule reacts
can be
\plain\expndtw1 \f20 \fs18 \cf1 determined. In this experiment, the Beer-Lambert
Law, a
\plain\par
\pard\sl-260 \li0 \ri139 \expndtw1 \f20 \fs18 \cf1 simple, yet basic law in spec
troscopy will be explored.
\plain\par
\sl-262\fs26\par\pard\pard\sl-258 \li0 \ri36 \expndtw0 \f20 \fs18 \cf1 The\i Be
er-Lambert Law\i0 indicates that there is a correlation
\plain\expndtw2 \f20 \fs18 \cf1 between the absorbance of a sample, its concentr
ation,
\plain\par
\pard\sl-260 \li0 \ri800 \expndtw2 \f20 \fs18 \cf1 and its thickness. The law ca
n be written as:
\par
\sect\sectd\sbknone\plain\pard\sl-309 \li540 \ri157 \fi5544 \expndtw-6 \f20 \fs1
8 \cf1 A =\fs24 {\f63 \u57445\'3f}\fs18 bc
\plain\tx8674 \tab \expndtw4 \b \f20 \fs18 \cf1 Equation 1
\plain\par
\pard\sl-210 \li540 \ri4378 \expndtw3 \f20 \fs18 \cf1 When an electron drops fro
m an excited level to the
\par
\plain\pard\sl-260 \li540 \ri1 \expndtw3 \f20 \fs18 \cf1 ground state (or to a l
ower energy level) a photon is
\plain\expndtw2 \f20 \fs18 \cf1 emitted. If this photon has a wavelength in the
visible
\plain\expndtw1 \f20 \fs18 \cf1 region a color is observed, and the spectrum emi
tted by
\plain\expndtw1 \f20 \fs18 \cf1 the substance is called an emission spectrum. (E
mission
\plain\expndtw1 \f20 \fs18 \cf1 spectra of hydrogen and helium were used in the
Atomic
\plain\expndtw2 \f20 \fs18 \cf1 Spectra experiment in 1045L.) An absorption spec
trum
\plain\expndtw2 \f20 \fs18 \cf1 is produced when continuous electromagnetic radi
ation
\plain\expndtw1 \f20 \fs18 \cf1 (every wavelength, all colors) passes through a
substance
\plain\expndtw2 \f20 \fs18 \cf1 and certain wavelengths are absorbed. In other w
ords,
\plain\expndtw1 \f20 \fs18 \cf1 an observed absorption spectrum is, in reality,
made up
\par
\column
\plain\pard\sl-309 \li0 \ri35 \expndtw3 \f20 \fs18 \cf1 where\fs24 {\f63 \u5744
5\'3f}\fs18 is the molar absorptivity (this is a constant
\plain\par
\pard\sl-254 \li0 \ri35 \expndtw2 \f20 \fs18 \cf1 which depends on the nature of
the absorbing system
\plain\par
\pard\sl-260 \li0 \ri35 \expndtw2 \f20 \fs18 \cf1 and the wavelength passing thr
ough; it is determined
\plain\expndtw1 \f20 \fs18 \cf1 experimentally as the slope of the line created
when A is
\plain\expndtw2 \f20 \fs18 \cf1 plotted versus c), b is the path length (the wid
th of the
\plain\expndtw2 \f20 \fs18 \cf1 sample cell or cuvette), and c is the concentrat
ion.
\par
\sect\sectd\sbknone\plain\sl-185\fs18\par\sl-240\fs24\par\pard\pard\sl-257 \li0
\ri8585 \expndtw-6 \f20 \fs26 \cf1 {\f63 \u57454\'3f}\f10 \fs16 16
\par
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}}}
\plain\pard\sl-286 \li3744 \ri19 \expndtw8 \f10 \fs16 \cf1 Experiment
\plain\tx9733 \tab \expndtw-10 \f20 \fs26 \cf1 {\f63 \u57454\'3f}
\par
\plain\sl-218\fs22\par\sl-240\fs24\par\par\par\pard\pard\sl-214 \li0 \ri5981 \ex
pndtw1 \f20 \fs18 \cf1 Below is a schematic of a spectrometer:
\par
\plain\sl-245\fs24\par\pard\pard\sl-98 \li6475 \ri1991 \expndtw-1 \f20 \fs8 \cf1
Hayden-McNeil Publishing, Inc.
\par
\plain\pard\sl-358 \li2951 \ri4663 \expndtw-12 \f10 \fs23 \cf1 I\dn5 \fs17 O
\plain\tx4659 \tab \expndtw-1 \f10 \fs23 \cf1 I
\par
\plain\sl-297\fs30\par\sl-240\fs24\par\par\par\par\pard\pard\sl-201 \li1646 \ri2
420 \expndtw-5 \f10 \fs17 \cf1 Light source
\plain\tx3391 \tab \expndtw-6 \f10 \fs17 \cf1 Sample cell
\plain\tx5206 \tab \expndtw-7 \f10 \fs17 \cf1 Detector
\plain\tx6556 \tab \expndtw-8 \f10 \fs17 \cf1 Readout
\par
\plain\sl-174\fs17\par\sl-240\fs24\par\pard\pard\sl-214 \li0 \ri2 \expndtw3 \f20
\fs18 \cf1 Inside the spectrometer light is emitted and passed
\plain\par
\pard\sl-301 \li0 \ri0 \expndtw2 \f20 \fs18 \cf1 through the sample cell. The in
cident light (I\dn5 \fs10 o\dn0 \fs18 ) can ei\plain\par
\pard\sl-218 \li0 \ri2 \expndtw1 \f20 \fs18 \cf1 ther hit a molecule within the
sample cell and scatter, be
\plain\par
\pard\sl-260 \li0 \ri0 \expndtw2 \f20 \fs18 \cf1 absorbed by a molecule and re-e
mitted in any direction
\plain\expndtw2 \f20 \fs18 \cf1 or pass clean through the sample cell without in
teract\plain\expndtw2 \f20 \fs18 \cf1 ing with the sample at all. Obviously, the more
packed
\plain\expndtw2 \f20 \fs18 \cf1 the sample cell, the more likely the light is to
strike a
\plain\expndtw2 \f20 \fs18 \cf1 molecule. This is why the amount of light absorb
ed is
\plain\expndtw2 \f20 \fs18 \cf1 proportional to the concentration of sample. In
much
\plain\expndtw2 \f20 \fs18 \cf1 the same way, we can relate the absorption to th
e path
\plain\expndtw2 \f20 \fs18 \cf1 length (width of the sample cell). If the sample
cell is
\plain\expndtw2 \f20 \fs18 \cf1 large, the light has to travel a greater distanc
e to pass
\par
\column
\plain\sl-129\fs13\par\sl-240\fs24\par\pard\pard\sl-260 \li0 \ri506 \expndtw2 \f
20 \fs18 \cf1 with detergents containing phosphates since this could
\plain\expndtw3 \f20 \fs18 \cf1 contaminate your sample. You should make notes i
n
\plain\expndtw3 \f20 \fs18 \cf1 your lab manual regarding the location, time of
day,
\plain\expndtw3 \f20 \fs18 \cf1 temperature and general appearance of the area f
rom
\plain\expndtw1 \f20 \fs18 \cf1 which you collect your sample. The sample should
come
\plain\expndtw1 \f20 \fs18 \cf1 from a fresh water source because there are spec
ialized
\plain\expndtw2 \f20 \fs18 \cf1 tests required to analyze salt water samples tha
t we are
\plain\expndtw2 \f20 \fs18 \cf1 not equipped to run.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri3824 \expndtw-12 \b\i \f10 \fs18 \cf1
Procedure
\plain\par
\pard\sl-260 \li0 \ri535 \expndtw2 \f20 \fs18 \cf1 1. Obtain a clean and dry ~1L
glass or plastic bottle.
\par
\sect\sectd\sbknone\cols3\colno1\colw4537\colsr286\colno2\colw154\colsr205\colno
3\colw4735
\plain\pard\sl-260 \li0 \ri1 \expndtw4 \f20 \fs18 \cf1 through the cell. The lon
ger the light is within the
\plain\expndtw2 \f20 \fs18 \cf1 cell the greater the chance that the light will
interact
\plain\expndtw2 \f20 \fs18 \cf1 with a molecule within the sample. Thus the obse
rved
\plain\expndtw3 \f20 \fs18 \cf1 absorption is proportional to the path length of
the
\plain\expndtw1 \f20 \fs18 \cf1 sample cell as well.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw4 \f20 \fs18 \cf1 If the mol
ar absorptivity and the path length are
\plain\expndtw3 \f20 \fs18 \cf1 held constant, the relationship between absorban
ce
\plain\expndtw3 \f20 \fs18 \cf1 and concentration can be studied. If there is a
direct
\plain\expndtw2 \f20 \fs18 \cf1 relationship, a plot of different concentrations
of the
\plain\expndtw1 \f20 \fs18 \cf1 solution will generate a straight line. Then the
system is
\plain\expndtw1 \f20 \fs18 \cf1 said to obey the Beer-Lambert Law. When a curved
plot
\plain\expndtw1 \f20 \fs18 \cf1 is obtained, the system deviates from the law. W
hen the
\plain\expndtw2 \f20 \fs18 \cf1 plot is not linear, no correlation between conce
ntration
\plain\expndtw1 \f20 \fs18 \cf1 and absorbance can be easily established. (This
can hap\plain\par
\pard\sl-260 \li0 \ri1020 \expndtw2 \f20 \fs18 \cf1 pen at particularly high con
centrations.)
\plain\par
\sl-259\fs26\par\pard\pard\sl-216 \li0 \ri3453 \expndtw-15 \b \f10 \fs18 \cf1 PR
OCEDURE
\plain\par
\pard\sl-216 \li0 \ri1701 \expndtw0 \b \f10 \fs18 \cf1 Part 1: Collection of Sam
ples
\plain\par
\pard\sl-260 \li0 \ri1 \expndtw1 \f20 \fs18 \cf1 You will be collecting your own
water sample for use in
\par
\column
\plain\pard\sl-260 \li0 \ri0 \expndtw-12 \f20 \fs18 \cf1 2.
\plain\par
\sl-305\fs31\par\pard\pard\sl-214 \li0 \ri0 \expndtw-12 \f20 \fs18 \cf1 3.
\plain\par
\sl-85\fs9\par\sl-240\fs24\par\par\pard\pard\sl-214 \li0 \ri0 \expndtw-12 \f20 \
fs18 \cf1 4.
\plain\par
\sl-165\fs17\par\sl-240\fs24\par\par\par\par\par\par\pard\pard\sl-214 \li0 \ri0
\expndtw-12 \f20 \fs18 \cf1 5.
\plain\par
\sl-105\fs11\par\sl-240\fs24\par\par\par\pard\pard\sl-214 \li0 \ri0 \expndtw-12
\f20 \fs18 \cf1 6.
\par
\column
\plain\pard\sl-260 \li0 \ri2157 \expndtw1 \f20 \fs18 \cf1 Find a source of fresh
water.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri503 \expndtw3 \f20 \fs18 \cf1 Make cop
ious notes regarding the location and
\plain\expndtw2 \f20 \fs18 \cf1 condition of the source.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri504 \expndtw2 \f20 \fs18 \cf1 Collect
the sample by inserting the bottle upside\plain\expndtw2 \f20 \fs18 \cf1 down into the water. Rotate the open end toward
\plain\expndtw1 \f20 \fs18 \cf1 the direction of the {\f63 \u64258\'3f}ow, and a
llow the bottle to fill
\plain\expndtw2 \f20 \fs18 \cf1 under the surface. Sample about 12 inches under
\plain\expndtw2 \f20 \fs18 \cf1 the surface. Avoid surface scum and bottom sedi\plain\expndtw1 \f20 \fs18 \cf1 ment.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri503 \expndtw3 \f20 \fs18 \cf1 Label th
e bottle with the sample name, location
\plain\expndtw1 \f20 \fs18 \cf1 and time collected and the initials of who colle
cted
\plain\expndtw1 \f20 \fs18 \cf1 the sample.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri504 \expndtw2 \f20 \fs18 \cf1 Store in
a refrigerator until time for lab. (You can
\plain\expndtw2 \f20 \fs18 \cf1 bring samples by the lab early in the day or kee
p
\plain\par
\pard\sl-260 \li0 \ri1277 \expndtw2 \f20 \fs18 \cf1 them on ice in a small coole
r until lab.)
\par
\plain\pard\sl-260 \li0 \ri0 \expndtw4 \f20 \fs18 \cf1 this laboratory.\b The c
ollection should take place
\plain\expndtw3 \b \f20 \fs18 \cf1 no more than 24 hours before lab.\b0 This is
because
\plain\expndtw1 \f20 \fs18 \cf1 analysis must take place within 48 hours to be v
alid. You
\plain\expndtw2 \f20 \fs18 \cf1 will need to obtain a clean ~1L glass or plastic
bottle
\plain\expndtw0 \f20 \fs18 \cf1 fo r th e co ll ec ti on . Be ca re fu l no t to
w as h t he b ot tl e
\par
\column
\plain\sl-132\fs13\par\pard\pard\sl-256 \li0 \ri1997 \expndtw0 \b \f10 \fs18 \cf
1 Part 2: Analysis of pH and PO\dn5 \fs10 43\plain\par
\pard\sl-218 \li0 \ri503 \expndtw3 \f20 \fs18 \cf1 For water quality testing the
re are a large number of
\plain\par
\pard\sl-260 \li0 \ri504 \expndtw2 \f20 \fs18 \cf1 chemical and biological molec
ules that can be tested.
\plain\expndtw1 \f20 \fs18 \cf1 The two we have selected to test for are importa
nt indi\plain\expndtw1 \f20 \fs18 \cf1 cators of pollution. Phosphates are often compon
ents in
\par
\sect\sectd\sbknone\plain\sl-191\fs19\par\pard\pard\sl-257 \li9510 \ri18 \expndt
w-12 \f10 \fs16 \cf1 17
\par
{\shp
ffd8ffe000104a46494600010100000100010000ffdb004300010101010101010101010101010101
01010101010101010101010101010101010101010101010101010101010101010101010101010101
010101010101010101ffdb0043010101010101010101010101010101010101010101010101010101
0101010101010101010101010101010101010101010101010101010101010101010101010101ffc0
001108067204fb03012200021101031101ffc4001f00000105010101010101000000000000000001
02030405060708090a0bffc400b5100002010303020403050504040000017d010203000411051221
31410613516107227114328191a1082342b1c11552d1f02433627282090a161718191a2526272829
2a3435363738393a434445464748494a535455565758595a636465666768696a737475767778797a
0101010101010101010000000000000102030405060708090a0bffc400b511000201020404030407
05040400010277000102031104052131061241510761711322328108144291a1b1c109233352f015
6272d10a162434e125f11718191a262728292a35363738393a434445464748494a53545556575859
5a636465666768696a737475767778797a82838485868788898a92939495969798999aa2a3a4a5a6
0028a28a0028a28a0028a28a0028a28a0028a28a0028afe58bfe0eebff00946e7c12ff00b3dff86d
ff00aa1bf695afea76829ab4632beedab76b5bfcc28a28a090a28a2800a28a2800a28a2800a28a28
00a28a2800a28a2800a28a2800a28a2803cafe2efc0bf825fb41786ec7c19f1ebe0efc2bf8dde0fd
335cb6f13e9be14f8bbf0f7c25f127c37a7f892cac353d2acfc4363a178cf48d6b4bb4d72d34bd6b
58d36db5682d63bf82c356d4ece2b84b7bfba8e5f54a28a0028a28a0028a28a0028a28a0028a28a0
028a28a0028a28a0028a28a0028a28a0028a28a0028a28a00fffd9
}}}
\par
3\colw4215
ndtw1 \f20 \fs18 \cf1 fertilizers and can enter lakes and rivers through runoff
\plain\expndtw3 \f20 \fs18 \cf1 from agricultural sources. pH values which are v
ery
\plain\expndtw2 \f20 \fs18 \cf1 acidic or very basic can indicate the presence o
f other
\plain\expndtw2 \f20 \fs18 \cf1 pollutants. For the phosphate test below you wil
l use
\plain\expndtw2 \f20 \fs18 \cf1 the spectrometer to measure the absorbance of bo
th the
\plain\expndtw2 \f20 \fs18 \cf1 sample and a series of standards. The standards
can be
\plain\expndtw3 \f20 \fs18 \cf1 run by a group of students to conserve time and
then
\plain\expndtw2 \f20 \fs18 \cf1 each student will need to run their own water sa
mple.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li540 \ri2136 \expndtw-7 \b\i \f10 \fs18 \cf1
Procedure: Analysis of pH
\plain\par
\pard\sl-260 \li540 \ri1 \expndtw3 \f20 \fs18 \cf1 1. Take 50 mL of your water s
ample and place it in
\plain\par
\pard\sl-260 \li900 \ri1 \expndtw3 \f20 \fs18 \cf1 100 mL beaker that has been c
leaned and rinsed
\plain\par
\pard\sl-260 \li900 \ri126 \expndtw2 \f20 \fs18 \cf1 with the acid wash and dist
illed water provided.
\par
\column
\plain\sl-218\fs22\par\sl-240\fs24\par\par\par\pard\pard\sl-214 \li0 \ri0 \expnd
tw-12 \f20 \fs18 \cf1 4.
\plain\par
\f20 \fs18 \cf1 5.
\plain\par
\par
\column
dtw4 \f20 \fs18 \cf1 To the beakers of unknown water samples and
\plain\expndtw2 \f20 \fs18 \cf1 standard add 1 mL of the Ammonium Molybdate
\plain\par
\pard\sl-260 \li0 \ri224 \expndtw2 \f20 \fs18 \cf1 color reagent and 2 drops of
stannous chloride.
\plain\par
\sl-305\fs31\par\pard\pard\sl-214 \li0 \ri1357 \expndtw2 \f20 \fs18 \cf1 Mix the
solutions for 5 minutes.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri35 \expndtw1 \f20 \fs18 \cf1 Using the
calculations from your prelab, create the
\plain\expndtw2 \f20 \fs18 \cf1 four serial dilutions of your stock solution. Th
ese
\plain\expndtw1 \f20 \fs18 \cf1 will be used to create the standard calibration
graph
\plain\expndtw3 \f20 \fs18 \cf1 to determine the concentration of your unknown
\plain\expndtw2 \f20 \fs18 \cf1 so be meticulous in your technique when making
\plain\expndtw2 \f20 \fs18 \cf1 the dilutions.
\par
3\colw4575
2.
\par
\column
\plain\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri1 \expndtw4 \f20 \fs18 \cf1 Usin
g the Orion pH meter, take the pH of the
\plain\expndtw0 \f20 \fs10 \cf1
\plain\par
\pard\sl-338 \li0 \ri0 \expndtw1 \f20 \fs18 \cf1 sample and record it in your no
tebook (See Appen\plain\par
\pard\sl-260 \li0 \ri19 \expndtw2 \f20 \fs18 \cf1 dix 5 for Orion\dn4 \fs10 \dn0
\fs18 pH meter instructions if needed.)
\par
\column
\plain\pard\sl-260 \li0 \ri34 \expndtw1 \f20 \fs18 \cf1 NOTE: The solution absor
ptions should be read between
\plain\expndtw3 \f20 \fs18 \cf1 5-20 minutes after adding the stannous chloride,
so
\plain\expndtw1 \f20 \fs18 \cf1 work quickly. While some of your team is making
the di\plain\expndtw2 \f20 \fs18 \cf1 lutions, the others should be reading the absorb
ance.
\par
\plain\sl-304\fs30\par\pard\pard\sl-256 \li540 \ri1971 \expndtw-7 \b\i \f10 \fs1
8 \cf1 Procedure: Analysis of PO\dn5 \fs10 43\plain\par
\pard\sl-218 \li540 \ri1 \expndtw3 \f20 \fs18 \cf1 Solutions containing phosphat
es can be determined
\plain\par
\pard\sl-260 \li540 \ri0 \expndtw2 \f20 \fs18 \cf1 through the formation of a bl
ue dye. Ammonium mo\plain\expndtw2 \f20 \fs18 \cf1 lybdate reagent combined with stannous chloride
and
\plain\expndtw3 \f20 \fs18 \cf1 phosphate produces a blue color dye whose intens
ity
\plain\expndtw3 \f20 \fs18 \cf1 is concentration dependent. Once the dye forms,
its
\plain\expndtw2 \f20 \fs18 \cf1 absorbance can be measured at 650 nm and compare
d
\par
\column
\plain\sl-261\fs26\par\pard\pard\sl-260 \li0 \ri35 \expndtw5 \b\i \f20 \fs18 \cf
1 You are now ready to measure the absorbance
\plain\expndtw4 \b\i \f20 \fs18 \cf1 of your samples.
\plain\par
\sl-214\fs21\par\pard\pard\sl-260 \li0 \ri236 \expndtw0 \b \f10 \fs18 \cf1 Opera
ting the Spectrophotometer (Genesys 20)
\plain\par
\pard\sl-260 \li0 \ri36 \expndtw4 \f20 \fs18 \cf1 1. Make sure your spectrometer
has been on for a
\plain\par
\pard\sl-260 \li0 \ri1889 \fi360 \expndtw2 \f20 \fs18 \cf1 minimum of 10 minutes
.
\par
\sect\sectd\sbknone\plain\pard\sl-260 \li540 \ri36 \expndtw2 \f20 \fs18 \cf1 to
absorbances of standard phosphate solutions.
\plain\tx5364 \tab \expndtw-12 \f20 \fs18 \cf1 2.
\plain\tx5710 \tab \expndtw1 \f20 \fs18 \cf1 Obtain a cuvette from the TA. Be re
sponsible for it
\plain\par
\pard\sl-215 \li540 \ri1092 \fi5184 \expndtw2 \f20 \fs18 \cf1 and return it at t
he end of the class.
\par
\plain\tx896 \tab \expndtw2 \f20 \fs18 \cf1 Turn on your spectrometer.
\plain\par
\pard\sl-215 \li540 \ri36 \fi4824 \expndtw3 \f20 \fs18 \cf1 NOTE: Observe the wh
ite reference mark on the cu\par
\plain\pard\sl-305 \li540 \ri0 \expndtw0 \i \f20 \fs18 \cf1 For each step below,
a standard sample of phosphate should
\plain\par
\pard\sl-260 \li540 \ri1 \expndtw2 \i \f20 \fs18 \cf1 be treated in the same man
ner as your water sample. A
\plain\par
\pard\sl-300 \li540 \ri0 \expndtw1 \i \f20 \fs18 \cf1 standard stock solution (1
0 ppm PO\dn5 \fs10 43-\dn0 \fs18 ) will be provided.
\par
\column
\plain\pard\sl-260 \li0 \ri37 \expndtw3 \f20 \fs18 \cf1 vettes. Align this mark
with the one on the sample
\plain\expndtw2 \f20 \fs18 \cf1 compartment every time a measurement is taken.
\par
3\colw4215
\plain\pard\sl-219 \li540 \ri0 \expndtw1 \i \f20 \fs18 \cf1 You will need to mak
e 4 dilutions of the stock solution, as
\plain\par
\pard\sl-260 \li540 \ri0 \expndtw1 \i \f20 \fs18 \cf1 outlined in step 4 below,
in order to cover the absorption
\plain\expndtw2 \i \f20 \fs18 \cf1 range so that the concentration of your unkno
wn water
\plain\expndtw0 \i \f20 \fs18 \cf1 sample can be determined.
\par
\column
\plain\par
\f20 \fs18 \cf1 4.
\par
\column
\plain\pard\sl-214 \li0 \ri37 \expndtw3 \f20
and rinse with distilled
\plain\par
\pard\sl-260 \li0 \ri35 \expndtw2 \f20 \fs18
ash the cuvettes, as
\plain\expndtw1 \f20 \fs18 \cf1 they scratch
\plain\par
\sl-305\fs31\par\pard\pard\sl-214 \li0 \ri36
of the cuvettes to about two-thirds (2/3)
\fs18 \cf1 Wash the cell carefully

\cf1 water. Do not use brushes to w
very easily.
\expndtw3 \f20 \fs18 \cf1 Fill one
\par
3\colw154\colsr205\colno4\colw4215
\plain\par
2 \f20 \fs18 \cf1 2.
\plain\par
2 \f20 \fs18 \cf1 3.

\par
\column
\plain\pard\sl-304 \li0 \ri0 \expndtw2 \f20 \fs18 \cf1 Take 25.0 mL of your wate
r sample and place it in
\plain\par
\pard\sl-260 \li0 \ri0 \expndtw2 \f20 \fs18 \cf1 a 100 mL beaker that has been c
leaned and rinsed
\plain\expndtw2 \f20 \fs18 \cf1 with the acid wash provided.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw4 \f20 \fs18 \cf1 Take 25.0
mL of stock phosphate solution and
\plain\expndtw3 \f20 \fs18 \cf1 place it in 100 mL beaker that has been cleaned
\plain\expndtw2 \f20 \fs18 \cf1 and rinsed with the acid wash provided.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw1 \f20 \fs18 \cf1 Place 25 m
L of DI water in another beaker to act as
\plain\expndtw-2 \f20 \fs18 \cf1 the "blank".
\par
\column
\plain\sl-85\fs9\par\sl-240\fs24\par\par\pard\pard\sl-214 \li0 \ri0 \expndtw-12
\f20 \fs18 \cf1 5.
\plain\par
\f20 \fs18 \cf1 6.
\plain\par
\sl-85\fs9\par\sl-240\fs24\par\par\pard\pard\sl-214 \li0 \ri0 \expndtw-12 \f20 \
fs18 \cf1 7.
\par
\column
\plain\pard\sl-260 \li0 \ri2236 \expndtw2 \f20 \fs18 \cf1 full with your blank.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri37 \expndtw1 \f20 \fs18 \cf1 Press the
A/T/C button on the spectrometer to select
\plain\expndtw3 \f20 \fs18 \cf1 the absorbance mode. The current mode appears
\plain\expndtw1 \f20 \fs18 \cf1 on the display.
\plain\par
\sl-259\fs26\par\pard\pard\sl-260 \li0 \ri34 \expndtw1 \f20 \fs18 \cf1 Using the
nm\f10 {\f63 \u9650\'3f}\f20 nm\f10 {\f63 \u9660\'3f}\f20 controls, set the
wavelength
\plain\expndtw2 \f20 \fs18 \cf1 at 543 nm.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri39 \expndtw4 \f20 \fs18 \cf1 Insert th
e blank cuvette into the sample com\plain\expndtw2 \f20 \fs18 \cf1 partment and close the compartment's lid.
\par
\sect\sectd\sbknone\plain\sl-165\fs16\par\pard\pard\sl-257 \li0 \ri8585 \expndtw
-6 \f20 \fs26 \cf1 {\f63 \u57454\'3f}\f10 \fs16 18
\par
{\shp

ffd8ffe000104a46494600010100000100010000ffdb004300010101010101010101010101010101
01010101010101010101010101010101010101010101010101010101010101010101010101010101
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}}}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 Ha }}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 yden }}

{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 -McN }}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 eil P }}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 ublis }}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 hing }}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 , Inc }}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 .}}
\plain\pard\sl-286 \li3744 \ri19 \expndtw8 \f10 \fs16 \cf1 Experiment
\plain\tx9733 \tab \expndtw-10 \f20 \fs26 \cf1 {\f63 \u57454\'3f}
\par
tw3 \f20 \fs18 \cf1 NOTE: Always hold the cuvette near its mouth. Use
\plain\expndtw-7 \f20 \fs18 \cf1 a K i m w i p e\dn4 \fs10 \dn0 \fs18 t o c l e
a n t h e c u v e t t e a n d t o r e m o v e fin \plain\expndtw3 \f20 \fs18 \cf1 gerprints and smudges which may interfere with t
he
\plain\expndtw2 \f20 \fs18 \cf1 measurements.
\par
\column

ndtw0 \b \f10 \fs18 \cf1 Water Purification (Each student should purify
\plain\par
\pard\sl-215 \li0 \ri2486 \expndtw1 \b \f10 \fs18 \cf1 their own water sample.)
\plain\par
\pard\sl-260 \li0 \ri3824 \expndtw-12 \b\i \f10 \fs18 \cf1 Procedure
\plain\par
\pard\sl-260 \li0 \ri504 \expndtw1 \f20 \fs18 \cf1 1. Using 50 mL of your water
sample. Filter the sample
\plain\par
\pard\sl-260 \li0 \ri502 \fi360 \expndtw0 \f20 \fs18 \cf1 using a suction filtra
tion set-up (see diagram) to remove
\par
3\colw5095
\plain\par
\par
\column
\plain\pard\sl-304 \li0 \ri0 \expndtw0 \f20 \fs18 \cf1 Press 0 ABS/100%T to set
the blank to 0 absorbance.
\plain\par
\sl-305\fs30\par\pard\pard\sl-214 \li0 \ri67 \expndtw1 \f20 \fs18 \cf1 Remove th
e "blank" cuvette and discard the blank.
\par
\column
\plain\pard\sl-260 \li0 \ri1288 \fi360 \expndtw0 \f20 \fs18 \cf1 large particula
tes. Use 0.1 mm filter paper.
\plain\par
\sl-261\fs26\par\pard\pard\sl-260 \li0 \ri504 \expndtw0 \i \f20 \fs18 \cf1 After
a liquid sample has been passed through a filtration
\plain\expndtw0 \i \f20 \fs18 \cf1 system it should now be called a "filtrate".
\par
\sect\sectd\sbknone\cols3\colno1\colw4538\colsr790\colno2\colw740\colsr52\colno3
\colw3797
\plain\pard\sl-302 \li0 \ri0 \expndtw1 \f20 \fs18 \cf1 10. Rinse the sample cuve
tte with a small portion of the
\plain\par
\pard\sl-260 \li360 \ri1 \expndtw2 \f20 \fs18 \cf1 standard stock solution (2.50
g/L) and discard the
\plain\expndtw2 \f20 \fs18 \cf1 rinse. Fill the cuvette to about 2/3 with the st
ock
\plain\expndtw2 \f20 \fs18 \cf1 solution and insert into the sample compartment.
\plain\expndtw2 \f20 \fs18 \cf1 Record the absorbance.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri1 \expndtw2 \f20 \fs18 \cf1 11. Remove
the sample cuvette, discard the stock solu\plain\par
\pard\sl-260 \li360 \ri4 \expndtw1 \f20 \fs18 \cf1 tion in the waste jar and rin
se the cuvette well with
\plain\expndtw0 \f20 \fs18 \cf1 DI water.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw1 \f20 \fs18 \cf1 12. Rinse
the sample cuvette again with a small portion
\plain\par
\pard\sl-260 \li360 \ri2 \expndtw2 \f20 \fs18 \cf1 of the your next standard sol
ution and discard the
\plain\expndtw1 \f20 \fs18 \cf1 rinse. Fill the cuvette to about 2/3 with the st
andard
\plain\expndtw2 \f20 \fs18 \cf1 solution and insert into the sample compartment.
\plain\expndtw2 \f20 \fs18 \cf1 Record the absorbance.
\par
\column
\plain\sl-264\fs26\par\sl-240\fs24\par\par\par\par\par\par\pard\pard\sl-164 \li0
\ri0 \expndtw-3 \f10 \fs11 \cf1 To aspirator on
\plain\par
\pard\sl-111 \li0 \ri117 \expndtw-3 \f10 \fs11 \cf1 water faucet
\par
\column
\expndtw-5 \f10 \fs11 \cf1 Adapter
\par
\sect\sectd\sbknone\plain\pard\sl-251 \li0 \ri501 \fi4824 \expndtw-12 \f20 \fs18
\cf1 2.
\plain\tx5170 \tab \expndtw1 \f20 \fs18 \cf1 Add 1 spatula of dry lime (CaO) pow
der and 1 spat\plain\par
\pard\sl-301 \li0 \ri504 \expndtw0 \f20 \fs18 \cf1 13. Repeat steps 11 and 12 un
til all the standards and all of
\plain\tx5170 \tab \expndtw2 \f20 \fs18 \cf1 ula of dry alum (Al\dn5 \fs10 2\dn0
\fs18 SO\dn5 \fs10 4\dn0 \fs18 ) powder to the filtrate and
\plain\par
\pard\sl-226 \li0 \ri503 \fi360 \expndtw1 \f20 \fs18 \cf1 the group's unknown sa
mples have been measured.
\plain\tx5170 \tab \expndtw1 \f20 \fs18 \cf1 stir with a clean, glass stirring r
od. Allow the pow\plain\par
\pard\sl-251 \li0 \ri549 \fi5184 \expndtw2 \f20 \fs18 \cf1 ders to react for ~10
minutes. Make observations.
\par
\sect\sectd\sbknone\cols3\colno1\colw2233\colsr1782\colno2\colw336\colsr2889\col
no3\colw2678
\plain\sl-97\fs10\par\sl-240\fs24\par\par\par\par\par\pard\pard\sl-145 \li1638 \
ri78 \fi87 \expndtw-7 \f10 \fs12 \cf1 0.1 mm
\plain\par
\pard\sl-125 \li1638 \ri0 \expndtw-3 \f10 \fs12 \cf1 filter paper
\par
\column
\plain\sl-272\fs27\par\sl-240\fs24\par\par\par\par\pard\pard\sl-166 \li0 \ri0 \e
xpndtw-11 \f10 \fs14 \cf1 Sand
\par
\column
\expndtw-6 \f10 \fs14 \cf1 1 cm layer
\plain\par
\pard\sl-143 \li0 \ri1776 \expndtw-4 \f10 \fs14 \cf1 of charcoal
\par
\sect\sectd\sbknone\plain\sl-125\fs13\par\sl-240\fs24\par\par\pard\pard\sl-166 \
li3108 \ri6515 \expndtw-12 \f10 \fs14 \cf1 CaO
\plain\par
\pard\sl-164 \li3294 \ri2359 \fi3563 \expndtw-8 \f10 \fs14 \cf1 Bleach
\plain\par
\pard\sl-113 \li3108 \ri5570 \fi186 \expndtw-5 \f10 \fs14 \cf1 Al\dn3 \fs9 2\dn0
\fs14 SO\dn3 \fs9 4
\par
\plain\sl-122\fs12\par\sl-240\fs24\par\pard\pard\sl-68 \li2673 \ri2808 \fi326 \e
xpndtw-9 \f10 \fs5 \cf1 {\ul 8}{\ul 0} ml
\plain\tx6680 \tab \expndtw-9 \f10 \fs5 \cf1 {\ul 8}{\ul 0} ml
\plain\expndtw-10 \f10 \fs4 \cf1 5%
\plain\tx6700 \tab \expndtw-10 \f10 \fs4 \cf1 5%
\plain\expndtw-3 \f10 \fs4 \cf1 100 ml
\plain\tx6364 \tab \expndtw-3 \f10 \fs4 \cf1 100 ml
\plain\expndtw-4 \f10 \fs4 \cf1 PYREX
\plain\tx2991 \tab \expndtw-11 \f10 \fs5 \cf1 60
\plain\tx6355 \tab \expndtw-4 \f10 \fs4 \cf1 PYREX
\plain\expndtw0 \f10 \fs3 \cf1 USA
\plain\tx6391 \tab \expndtw0 \f10 \fs3 \cf1 USA
\plain\par
\sl-65\fs7\par\pard\expndtw-11 \f10 \fs5 \cf1 40
\par
\plain\sl-37\fs4\par\pard\pard\sl-33 \li2690 \ri3417 \expndtw-5 \f10 \fs2 \cf1 N
O
\plain\tx2744 \tab \expndtw0 \f10 \fs2 \cf1 1
\plain\expndtw0 \f10 \fs2 \cf1 .
\plain\expndtw0 \f10 \fs2 \cf1 0
\plain\tx6388 \tab \expndtw-5 \f10 \fs2 \cf1 NO
\plain\expndtw0 \f10 \fs2 \cf1 .
\plain\expndtw-11 \f10 \fs5 \cf1 20
\par
\sect\sectd\sbknone\cols5\colno1\colw1773\colsr541\colno2\colw1106\colsr740\coln
o3\colw1309\colsr523\colno4\colw1106\colsr549\colno5\colw2270
\plain\sl-197\fs20\par\sl-240\fs24\par\par\pard\pard\sl-171 \li488 \ri0 \expndtw
-3 \b \f10 \fs14 \cf1 Filter through filter
\plain\par
\pard\sl-144 \li488 \ri400 \fi447 \expndtw-9 \b \f10 \fs14 \cf1 paper
\par
\column
\plain\sl-89\fs9\par\sl-240\fs24\par\par\pard\pard\sl-171 \li0 \ri0 \expndtw-3 \
b \f10 \fs14 \cf1 Pour filtrate into
\plain\par
\pard\sl-144 \li27 \ri21 \expndtw-4 \b \f10 \fs14 \cf1 beaker and add
\plain\par
\pard\sl-167 \li13 \ri7 \expndtw-3 \b \f10 \fs14 \cf1 CaO and Al\dn3 \fs9 2\dn0
\fs14 SO\dn3 \fs9 4

\par
\column
\plain\sl-197\fs20\par\sl-240\fs24\par\par\pard\pard\sl-171 \li0 \ri0 \expndtw-3
\b \f10 \fs14 \cf1 Filter through sand
\par
\column
\plain\sl-89\fs9\par\sl-240\fs24\par\par\pard\pard\sl-171 \li0 \ri0 \expndtw-3 \
b \f10 \fs14 \cf1 Pour filtrate into
\plain\par
\pard\sl-143 \li27 \ri21 \expndtw-4 \b \f10 \fs14 \cf1 beaker and add
\plain\par
\pard\sl-144 \li0 \ri292 \fi327 \expndtw-8 \b \f10 \fs14 \cf1 bleach
\par
\column
\plain\sl-197\fs20\par\sl-240\fs24\par\par\pard\pard\sl-171 \li0 \ri976 \fi251 \
expndtw-4 \b \f10 \fs14 \cf1 Filter through
\plain\par
\pard\sl-144 \li0 \ri1132 \fi423 \expndtw-6 \b \f10 \fs14 \cf1 charcoal
\plain\par
\sl-249\fs25\par\pard\pard\sl-124 \li0 \ri924 \expndtw-1 \f20 \fs9 \cf1 Hayden-Mc
Neil Publishing, Inc.
\par
\sect\sectd\sbknone\plain\sl-244\fs24\par\sl-240\fs24\par\pard\pard\sl-257 \li95
10 \ri18 \expndtw-12 \f10 \fs16 \cf1 19
\par
{\shp
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01451450014514500145145001451450014514500145145001451450014514500145145001451450
01451450014514500145145001451450014514500145145001451450014514500145145001451450
01451450014514500145145001451450014514500145145001451450014514500145145001451450
01451450014514500145145001451450014514500145145001451450014514500145145001451450
01451450014514500145145001451450014514500145145001451450014514500145145001451450
01451450014514500145145001451450014514500145145001451450014514500145145001451450
01451450014514500145145001451450014514500145145001451450014514500145145001451450
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}}}

\par
3\colw4575
ndtw-12 \f20 \fs18 \cf1 3.
\plain\par
2 \f20 \fs18 \cf1 4.
\plain\par
\plain\par
\sl-85\fs9\par\sl-240\fs24\par\par\pard\pard\sl-214 \li540 \ri0 \expndtw-12 \f20
\fs18 \cf1 6.
\plain\par
\sl-185\fs19\par\sl-240\fs24\par\par\par\par\par\par\par\pard\pard\sl-214 \li540
\ri0 \expndtw-12 \f20 \fs18 \cf1 7.
\plain\par
\sl-125\fs13\par\sl-240\fs24\par\par\par\par\pard\pard\sl-214 \li540 \ri0 \expnd
tw-12 \f20 \fs18 \cf1 8.
\plain\par
\sl-85\fs9\par\sl-240\fs24\par\par\pard\pard\sl-214 \li540 \ri0 \expndtw-12 \f20
\fs18 \cf1 9.
\par
\column
tw2 \f20 \fs18 \cf1 Using your filter funnel again, place a filter paper
\plain\expndtw3 \f20 \fs18 \cf1 in the funnel and then add enough sand to cover
\plain\expndtw2 \f20 \fs18 \cf1 the filter paper with ~.5cm of sand.
\plain\par
\sl-305\fs31\par\pard\pard\sl-214 \li0 \ri697 \expndtw2 \f20 \fs18 \cf1 Pass the
filtrate through the sand slowly.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw3 \f20 \fs18 \cf1 Add 1 mL o
f sodium hypochlorite reagent to the
\plain\expndtw1 \f20 \fs18 \cf1 filtrate. Stir to mix completely.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri1 \expndtw2 \f20 \fs18 \cf1 Set up the
charcoal filtration funnel. Place a filter
\plain\expndtw2 \f20 \fs18 \cf1 paper in the Bchner funnel. Add a 1 cm layer of
\plain\expndtw1 \f20 \fs18 \cf1 activated charcoal on the filter and then cover
with
\plain\expndtw2 \f20 \fs18 \cf1 a second filter. Attach a hose to the side nozzl
e of
\plain\expndtw2 \f20 \fs18 \cf1 the water faucet in the sink and the side nozzle
of
\plain\expndtw2 \f20 \fs18 \cf1 a filtration {\f63 \u64258\'3f}ask. Use an adapt
or and fit the funnel
\plain\par
\pard\sl-260 \li0 \ri1657 \expndtw1 \f20 \fs18 \cf1 into the {\f63 \u64258\'3f}a
sk. (See diagram)

\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri1 \expndtw3 \f20 \fs18 \cf1 Rinse the
charcoal with distilled water until the
\plain\expndtw2 \f20 \fs18 \cf1 water in the {\f63 \u64258\'3f}ask is clear. Mak
e sure you discard
\plain\expndtw1 \f20 \fs18 \cf1 the charcoal rinse water and dry the filtration
{\f63 \u64258\'3f}ask
\plain\expndtw1 \f20 \fs18 \cf1 before filtering your water sample.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw3 \f20 \fs18 \cf1 Pass your
water sample through the fully rinsed
\plain\expndtw1 \f20 \fs18 \cf1 charcoal filter.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri0 \expndtw2 \f20 \fs18 \cf1 Make obser
vations regarding color and clarity of
\plain\expndtw0 \f20 \fs18 \cf1 the "purified" water.
\par
\column
dtw2 \f20 \fs18 \cf1 Prepare a data table listing the concentrations in both
\plain\par
\pard\sl-310 \li0 \ri35 \expndtw2 \f20 \fs18 \cf1 molarity and ppm (parts per mi
llion) of\fs20 PO\dn6 \fs11 43-\dn0 \fs18 in your
\plain\par
\pard\sl-209 \li0 \ri37 \expndtw1 \f20 \fs18 \cf1 water sample both before and a
fter purification. [1 ppm =
\plain\par
\pard\sl-301 \li0 \ri964 \expndtw1 \f20 \fs18 \cf1 1mg/1L; 1 mol PO\dn5 \fs10 43
-\dn0 \fs18 = 9.5 x 10\dn4 \fs10 4\dn0 \fs18 mg PO\dn5 \fs10 43-\dn0 \fs18 ]
\plain\par
\sl-218\fs22\par\pard\pard\sl-260 \li0 \ri35 \expndtw2 \f20 \fs18 \cf1 Using sta
tistical analysis describe how much "purer"
\plain\expndtw2 \f20 \fs18 \cf1 your water sample was after purification. E.g. I
f there
\plain\par
\pard\sl-310 \li0 \ri35 \expndtw1 \f20 \fs18 \cf1 were 50 ppm\fs20 PO\dn6 \fs11
43-\dn0 \fs18 prior to purification and only 3 ppm
\plain\par
\pard\sl-209 \li0 \ri36 \expndtw2 \f20 \fs18 \cf1 after that there is a 50 ppm-3
ppm/50 ppm {\f63 \u57395\'3f} 100% =
\plain\par
\pard\sl-260 \li0 \ri2807 \expndtw1 \f20 \fs18 \cf1 94% purification.
\plain\par
\sl-215\fs22\par\pard\pard\sl-260 \li0 \ri3658 \expndtw-11 \b \f10 \fs18 \cf1 QU
ESTION
\plain\par
\pard\sl-260 \li0 \ri36 \expndtw2 \f20 \fs18 \cf1 Look up on the internet the ma
ximum ppm values for
\plain\par
\pard\sl-310 \li0 \ri33 \expndtw1 \f20 \fs20 \cf1 PO\dn6 \fs11 43-\dn0 \fs18 io
ns in drinking water. Would your purified water
\plain\par
\pard\sl-209 \li0 \ri1863 \expndtw2 \f20 \fs18 \cf1 sample be drinkable? Explain
.
\par
\sect\sectd\sbknone\plain\sl-215\fs22\par\pard\pard\sl-260 \li540 \ri5801 \expnd
tw1 \b \f10 \fs18 \cf1 Water Quality After Purification
\plain\par
\pard\sl-260 \li540 \ri7697 \expndtw-12 \b\i \f10 \fs18 \cf1 Procedure
\plain\par
\pard\sl-260 \li540 \ri4378 \expndtw3 \f20 \fs18 \cf1 1. Repeat the pH and phosp
hate test for your water
\plain\par
\pard\sl-259 \li900 \ri4378 \expndtw1 \f20 \fs18 \cf1 sample only. You don't nee
d to repeat the measure\plain\expndtw2 \f20 \fs18 \cf1 ment for the standards.
\plain\par
\sl-216\fs22\par\pard\pard\sl-260 \li540 \ri6142 \expndtw-6 \b \f10 \fs18 \cf1 R
EPORT CONTENTS AND QUESTIONS
\plain\par
\pard\sl-260 \li540 \ri4377 \expndtw1 \f20 \fs18 \cf1 Prepare data tables for th
e absorbencies of the standard
\plain\expndtw3 \f20 \fs18 \cf1 solutions, and water samples both before and aft
er
\plain\expndtw1 \f20 \fs18 \cf1 purification.
\plain\par
\sl-260\fs26\par\pard\pard\sl-260 \li540 \ri4377 \expndtw2 \f20 \fs18 \cf1 Repor
t observations and pH readings both before and
\plain\expndtw1 \f20 \fs18 \cf1 after purification.
\plain\par
\sl-305\fs31\par\pard\pard\sl-214 \li540 \ri4381 \expndtw2 \f20 \fs18 \cf1 Prepa
re concentration vs. absorbance calibration graph
\plain\par
\pard\sl-310 \li540 \ri6668 \expndtw1 \f20 \fs18 \cf1 for the\fs20 PO\dn6 \fs11
43-\dn0 \fs18 standards.
\plain\par
\sl-252\fs25\par\pard\pard\sl-217 \li540 \ri4376 \expndtw3 \f20 \fs18 \cf1 Using
A =\fs22 {\f63 \u57445\'3f}\fs18 bc and the calibration graph, determine
\plain\par
\pard\sl-309 \li540 \ri4377 \expndtw2 \f20 \fs18 \cf1 the concentrations of\fs20
PO\dn6 \fs11 43-\dn0 \fs18 in your water sample both
\plain\par
\pard\sl-209 \li540 \ri6291 \expndtw1 \f20 \fs18 \cf1 before and after purificat
ion.
\par
{\f63 \u57454\'3f}\f10 \fs16 20
\par
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}}}
{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f12 \fs16 \cf1 {\f63 \u8226\'3f}{\f63 \
u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\
f63 \u8226\'3f} }}
\cols2\colno1\colw2213\colsr1296\colno2\colw6590
\plain\sl-100\fs10\par\sl-240\fs24\par\pard\pard\sl-360 \li5 \ri113 \expndtw-1 \
b \f10 \fs30 \cf1 Solutions and
\plain\expndtw0 \b \f10 \fs30 \cf1 Colloids in the
\plain\expndtw0 \b \f10 \fs30 \cf1 Purification of
\plain\par
\pard\sl-360 \li5 \ri1264 \expndtw0 \b \f10 \fs30 \cf1 Water
\par
\column
\plain\sl-164\fs16\par\sl-240\fs24\par\par\par\par\par\pard\pard\sl-1073 \li0 \r
i1999 \expndtw24 \f10 \fs90 \cf130 Pre-Lab
\par
\sect\sectd\sbknone\cols1\colno1\colw10100
\plain\pard\sl-2386 \li5223 \ri1090 \expndtw4 \f10 \fs200 \cf1 3
\plain\expndtw-15 {\cf1 \f0\fs24 \bullet }\f12 \fs16 \cf1 {\f63 \u8226\'3f}{\f63
\u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}
{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226
\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}{\f63 \u8226\'3f}
\par
\plain\sl-187\fs19\par\sl-240\fs24\par\par\par\pard\pard\sl-161 \li2903 \ri6831
\expndtw0 \i \f20 \fs14 \cf1 Name
\plain\par
\sl-198\fs20\par\sl-240\fs24\par\pard\pard\sl-161 \li2903 \ri5398 \expndtw0 \i \
f20 \fs14 \cf1 Lab Section and TA
\plain\par
\sl-198\fs20\par\sl-240\fs24\par\pard\pard\sl-161 \li2903 \ri6211 \expndtw-4 \i
\f20 \fs14 \cf1 Date
\par
\plain\sl-223\fs22\par\sl-240\fs24\par\pard\pard\sl-214 \li180 \ri0 \expndtw-12
\f20 \fs18 \cf1 1.
\par
\column
\plain\sl-223\fs22\par\sl-240\fs24\par\pard\pard\sl-255 \li0 \ri504 \expndtw2 \f
20 \fs18 \cf1 You are given a stock solution of 10.0 ppm of PO\dn5 \fs10 43-\dn0
\fs18 and asked to create a series of evenly divided concentra\plain\par
\pard\sl-218 \li0 \ri503 \expndtw3 \f20 \fs18 \cf1 tions that will allow you to
determine the concentration of phosphate in an unknown water sample. Each
\plain\par
\pard\sl-260 \li0 \ri504 \expndtw2 \f20 \fs18 \cf1 solution should initially be
25 mL in total volume. Using the serial dilution example below, describe how
\plain\expndtw4 \f20 \fs18 \cf1 you will do this in lab.\b Copy all of the calc
ulations and the completed table below into your lab
\plain\expndtw4 \b \f20 \fs18 \cf1 notebook.
\plain\par
\sl-300\fs30\par\pard\pard\sl-260 \li0 \ri504 \expndtw1 \f20 \fs18 \cf1 Example:
You need 25 mL of 8 ppm PO\dn5 \fs10 43-\dn0 \fs18 solution and have excess qu
antity of 10.0 ppm stock PO\dn5 \fs10 43-\dn0 \fs18 solution.
\plain\expndtw1 \f20 \fs18 \cf1 Using M\dn5 \fs10 1\dn0 \fs18 V\dn5 \fs10 1\dn0
\fs18 = M\dn5 \fs10 2\dn0 \fs18 V\dn5 \fs10 2\dn0 \fs18 : (25 mL)( 8 ppm PO\dn5
\fs10 43-\dn0 \fs18 ) = (x)( 10.0 ppm stock PO\dn5 \fs10 43-\dn0 \fs18 ); x = 2
0 mL. So you will take 20 mL
\plain\expndtw2 \f20 \fs18 \cf1 of 10.0 ppm stock PO\dn5 \fs10 43-\dn0 \fs18 so
lution and add 5.0 mL (for a total volume of 25 mL) of water to make the 8 ppm
\plain\expndtw2 \f20 \fs18 \cf1 PO\dn5 \fs10 43-\dn0 \fs18 solution. Now repeat
the process, but use the 8 ppm PO\dn5 \fs10 43-\dn0 \fs18 solution as the conc
entration M\dn5 \fs10 2\dn0 \fs18 . Continue
\plain\par
\pard\sl-218 \li0 \ri647 \expndtw2 \f20 \fs18 \cf1 to repeat this serial dilutio
n until all of the solutions you need are made. Show work to receive full credit
.
\par
\sect\sectd\sbknone\plain\sl-126\fs13\par\sl-240\fs24\par\par\par\par\par\par\pa
r\par\par\par\par\par\par\par\par\par\par\par\par\par\pard\pard\sl-257 \li9690 \
ri18 \expndtw-12 \f10 \fs16 \cf1 21
\par
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\plain\sl-218\fs22\par\sl-240\fs24\par\par\par\pard\pard\sl-214 \li540 \ri3589 \
expndtw-12 \f20 \fs18 \cf1 2.
\plain\tx896 \tab \expndtw2 \f20 \fs18 \cf1 Based on your calculations above, co
mplete the table below:
\par
\plain\sl-102\fs10\par\sl-240\fs24\par\par\pard\pard\sl-215 \li1634 \ri388 \fi20
35 \expndtw0 \b \f10 \fs18 \cf1 Solution Diluted
\plain\tx5904 \tab \expndtw-4 \b \f10 \fs18 \cf1 Volume
\plain\tx9025 \tab \expndtw-5 \b \f10 \fs18 \cf1 Total
\plain\par
\pard\sl-134 \li1634 \ri1299 \expndtw0 \b \f10 \fs18 \cf1 Concentration of
\plain\tx7162 \tab \expndtw0 \b \f10 \fs18 \cf1 Concentration
\plain\par
\pard\sl-135 \li1679 \ri318 \fi2141 \expndtw2 \b \f10 \fs18 \cf1 from (ppm)/
\plain\tx5640 \tab \expndtw0 \b \f10 \fs18 \cf1 Water Added
\plain\tx8912 \tab \expndtw-4 \b \f10 \fs18 \cf1 Volume
\plain\par
\pard\sl-134 \li1634 \ri1571 \fi45 \expndtw1 \b \f10 \fs18 \cf1 Standard (ppm)
\plain\tx7464 \tab \expndtw1 \b \f10 \fs18 \cf1 (mol/L)
\plain\par
\pard\sl-135 \li1634 \ri399 \fi1960 \expndtw0 \b \f10 \fs18 \cf1 volume used (mL
)
\plain\tx6030 \tab \expndtw-2 \b \f10 \fs18 \cf1 (mL)
\plain\tx9037 \tab \expndtw-2 \b \f10 \fs18 \cf1 (mL)
\par
\plain\sl-125\fs12\par\sl-240\fs24\par\pard\pard\sl-214 \li962
\f10 \fs18 \cf1 1
\plain\par
\sl-174\fs17\par\pard\pard\sl-214 \li962 \ri503 \expndtw0 \f10
\plain\par
\plain\par
\plain\par
\plain\par
\ri503 \expndtw0
\fs18 \cf1 2
\fs18 \cf1 3
\fs18 \cf1 4
\fs18 \cf1 5
\fs18 \cf1 6
\plain\tx3941
\plain\tx5007
\plain\tx6146
\plain\tx7785
\plain\tx9153
\tab
\tab
\tab
\tab
\tab
\expndtw0 \f10 \fs18 \cf1 0

\expndtw-12 \f10 \fs18 \cf1 25
\expndtw-12 \f10 \fs18 \cf1 25
\par
3.
\plain\tx896 \tab \expndtw2 \f20 \fs18 \cf1 Use the following table of standard
concentrations and absorbance for the phosphate ion. Create a calibration
\plain\par
\pard\sl-260 \li900 \ri36 \expndtw2 \f20 \fs18 \cf1 graph and determine the phos
phate concentration of an unknown water sample whose absorbance is 0.44.
\plain\par
\pard\sl-260 \li900 \ri6585 \expndtw2 \f20 \fs18 \cf1 (Path length 1.0 cm)
\par
\plain\sl-260\fs26\par\pard\pard\sl-260 \li900 \ri0 \expndtw1 \b \f10 \fs18 \cf1
Concentration (ppm)
\plain\par
\pard\sl-260 \li900 \ri1663 \expndtw0 \f10 \fs18 \cf1 0
\plain\par
\pard\sl-260 \li900 \ri1570 \expndtw-12 \f10 \fs18 \cf1 10
\par
\column
\plain\sl-260\fs26\par\pard\pard\sl-260 \li0 \ri4250 \expndtw-3 \b \f10 \fs18 \c
f1 Absorbance
\plain\par
\pard\sl-260 \li0 \ri5127 \expndtw0 \f10 \fs18 \cf1 0
\plain\par
\pard\sl-260 \li0 \ri4894 \expndtw-11 \f10 \fs18 \cf1 0.15
\plain\expndtw-11 \f10 \fs18 \cf1 0.32
\par
\sect\sectd\sbknone\plain\sl-283\fs28\par\sl-240\fs24\par\par\par\par\par\par\pa
r\par\par\par\par\par\par\par\par\par\par\par\par\par\par\par\pard\pard\sl-257 \
li0 \ri8585 \expndtw-6 \f20 \fs26 \cf1 {\f63 \u57454\'3f}\f10 \fs16 22
\par
}

Solutions and Colloids in The Purification of Water

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Solutions and Colloids in The Purification of Water

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{\rtf \ansi\ansicpg1252\deff0

{\fonttbl{\f11\fswiss\fcharset0 Arial Narrow;}{\f10\fswiss\fcharset0 Arial;}{\f1

\plain\expndtw0 \f20 \fs18 \cf1 polarity.

{\sp{\sn fAllowOverlap}{\sv 1}}

\fs18 \cf1 Wash the cell carefully

2 \f20 \fs18 \cf1 3.

{\sp{\sn pib}{\sv {\pict\jpegblip\picw612 \pich792

{\sp{\sn txflTextFlow}{\sv 3}}}{\shptxt \f20 \fs6 \cf1 yden }}

\plain\sl-217\fs22\par\sl-240\fs24\par\par\par\pard\pard\sl-215 \li0 \ri718 \exp

\fs14 SO\dn3 \fs9 4

{\sp{\sn posrelh}{\sv 1}}

sk. (See diagram)

\expndtw0 \f10 \fs18 \cf1 0

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