DAFTAR ISI

HALAMAN JUDUL....................................................................... i
LEMBAR PENGESAHAN SKRIPSI ......................................... iii
LEMBAR PERNYATAAN ......................................................... iv
ABSTRAK...................................................................................... v
ABSTRACT .................................................................................. vi
KATA PENGANTAR ................................................................. vii
DAFTAR ISI ................................................................................. ix
DAFTAR GAMBAR ................................................................... xii
DAFTAR LAMPIRAN .............................................................. xiii
BAB I PENDAHULUAN .............................................................. 1
1.1 Latar Belakang .......................................................................... 1
1.2 Rumusan Masalah ..................................................................... 3
1.3 Batasan Masalah ....................................................................... 3
1.4 Tujuan Penelitian ...................................................................... 4
1.5 Manfaat Penelitian .................................................................... 4
BAB II TINJAUAN PUSTAKA ................................................... 5
2.1 Kitosan ...................................................................................... 5
2.2 Kitosan Makropori .................................................................... 5 .
2.3 Porogen...................................................................................... 6
2.4 Cross-linking agent.................................................................... 7
2.5 Methyl Orange........................................................................... 8
2.6 Metode Pengukuran Methyl orange dengan Menggunakan
Spektrofotometry UV-Vis ............................................................... 9
2.7 Scanning Electron Microscopy (SEM) .................................... 10
2.8 Hipotesa ................................................................................... 11
BAB III METODE PENELITIAN ............................................ 12
3.1 Tempat dan Waktu Penelitian ................................................. 12
3.2 Bahan dan Alat Penelitian ....................................................... 12
3.2.1 Bahan Penelitian ................................................................... 12
3.2.2 Alat Penelitian ...................................................................... 12
3.3 Tahapan Penelitian .................................................................. 12
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3.4 Prosedur Kerja ......................................................................... 13

3.4.1 Pembuatan Kitosan Makropori ............................................. 13
3.4.2 Pembuatan Kitosan Tanpa Porogen ...................................... 13
3.4.3 Prosedur Penentuan Konsentrasi methyl orange dalam Larutan
....................................................................................................... 14 .
3.4.3.1 Preparasi Larutan Induk Methyl orange 1000 ppm ........... 14
3.4.3.2 Preparasi Larutan Stok Methyl orange 20 ppm ................. 14
3.4.3.3 Penentuan Panjang Gelombang Maksimum Methyl orange ..
....................................................................................................... 14
3.4.4 Penentuan Pengaruh pH Sampel terhadap Adsorpsi Methyl
orange oleh Kitosan Makropori ..................................................... 15
3.4.4.1 Penentuan Kosnentrasi Methyl orange Sebelum Adsorpsi ..
....................................................................................................... 15
3.4.4.2 Penentuan Kosnentrasi Methyl orange Sesudah Adsorpsi ...
....................................................................................................... 15
3.4.5 Penentuan Waktu Kontak Optimum terhadap Adsorpsi Methyl
orange oleh Kitosan Makropori ..................................................... 15
3.4.6 Penentuan Pengaruh Komposisi Perbandingan
Kitosan:Epichlorohydrin terhadap Adsorpsi Methyl orange oleh
Kitosan Makropori......................................................................... 16
3.4.6.1 Penentuan Kosnentrasi Methyl orange Sebelum Adsorpsi ....
....................................................................................................... 16
3.4.6.2 Penentuan Kosnentrasi Methyl orange Sesudah Adsorpsi ....
....................................................................................................... 16
3.4.7 Karakterisasi Kitosan ........................................................... 16
BAB IV PEMBAHASAN ............................................................ 18
4.1 Hasil Karakterisasi Kitosan ..................................................... 18
4.2 Penentuan Pengaruh pH Sampel terhadap Adsorpsi Methyl
orange oleh Kitosan Makropori ..................................................... 20
4.3 Penentuan Waktu Kontak Optimum terhadap Adsorpsi Methyl
orange oleh Kitosan Makropori ..................................................... 22

4.4 Penentuan Pengaruh Komposisi Perbandingan

Kitosan:Epichlorohydrin terhadap Adsorpsi Methyl orange oleh
Kitosan Makropori ........................................................................ 24
BAB V PENUTUP ....................................................................... 27
5.1 Kesimpulan.............................................................................. 27
5.2 Saran ........................................................................................ 27
DAFTAR PUSTAKA .................................................................. 28
LAMPIRAN ................................................................................. 32

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