Concentration [wt%]

10
20
30
40
50

Empty test tube [g]

U
B
U
B
U
M
B
U
M
B
U
M
B

12.756
12.797
14.282
14.176
14.299
14.208
13.975
14.112
14.106
14.14
12.806
12.857
12.842

Concentration [wt%]

After extraction [g]

17.993
21.816
17.514
16.762
14.983
19.888
16.775
14.741
22.028
16.36
17.162
22.556
17.162

Acetic acid recovered [%]

U
B
U
B
U
M
B
U
M
B
U
M
B

10.4587
11.7826
10.7521
11.9604
12.8984
12.2192
10.4646
13.2418
12.9719
9.2135

U
B
U
B
U
M
B
U
M
B
U
M
9.0451 B

10
20
30
40
50

37
56
7
6
24

0
0
62
74
53

Total [g]
5.237
9.019
3.232
2.586
0.684
5.68
2.8
0.629
7.922
2.22
4.356
9.699
4.32

14.256
5.818
9.164

10.771

18.375

Mass [wt %]
37%
63%
56%
44%
7%
62%
31%
6%
74%
21%
24%
53%
24%

10.458
3700%
6300%
5600%
44%
7%
62%
31%
6%
74%
21%
24%
53%
24%
63
44
31
21
24

120

Phase separation (wt %)

Mass [g]

100
80
60
40
20
0
10

20

30

aqueous(NH

1.05

Concentration of acetic
massacid
10.4587
11.7826
10.7521
11.9604
12.8984
12.2192
10.4646
13.2418
12.9719
9.2135
9.0451

mass original
yield

upper phase
middle phase
bottom phase

40

50

aqueous(NH4)2 SO4 (w/v %)