STANDARD METHODS
FOR THE EXAMINATION OF
DAIRY PRODUCTS
17th Edition 2004
Edited by
H. Michael Wehr, PhD
Joseph F. Frank, PhD
Contents
Technical Committee . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . viii
Contributors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ix
Consensus Reviewers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . xi
Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . xiii
Chapter 1:
1.010
1.020
1.030
1.040
1.050
1.060
1.070
1.080
1.090
1.100
1.110
1.120
Chapter 2:
2.010
2.020
2.030
2.040
2.050
2.060
Chapter 3:
3.010
3.020
3.030
3.040
3.050
3.060
3.070
3.080
3.090
3.100
Chapter 4:
4.010
4.020
Standard Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Function of Standard Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Organization . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Changes in This Edition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Standard Methods for International Trade . . . . . . . . . . . . . . . . . . . . . . 3
Adopting New Methodology and Uniformity of Methods . . . . . . . . 6
Classification of Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Chapter and Method Formats Used in This Edition . . . . . . . . . . . . . . 8
Method Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Split-Sample Test Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Precision Parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Cited References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
4.030
4.040
4.050
4.060
4.070
4.080
4.090
4.100
4.110
Chapter 5:
5.010
5.020
5.030
5.040
5.050
5.060
5.070
5.080
5.090
5.100
5.110
5.120
Chapter 6:
6.010
6.020
6.030
6.040
6.050
6.060
6.070
6.080
Chapter 7:
7.010
7.020
7.030
7.040
7.050
7.060
7.070
7.080
7.090
7.100
7.110
Chapter 8:
8.010
8.020
8.030
8.040
8.050
8.060
8.070
8.080
8.090
8.100
8.110
8.120
Chapter 9:
9.010
9.020
9.030
9.040
9.050
9.060
9.070
9.080
9.090
9.100
9.110
Chapter 10:
10.010
10.020
10.030
10.040
Chapter 11:
11.010
11.020
11.030
11.040
11.050
11.060
Chapter 12:
12.010
12.020
12.030
12.040
12.050
12.060
12.070
12.080
12.090
12.100
12.110
Chapter 13:
13.010
13.020
13.030
13.040
13.050
Chapter 14:
14.010
14.020
14.030
14.040
14.050
14.060
14.070
14.080
Chapter 15:
15.010
15.020
15.030
15.040
15.050
15.060
15.070
15.080
15.090
15.100
15.110
15.120
15.130
15.140
15.150
15.160
15.170
15.180
Chapter 16:
16.010
16.020
16.030
16.040
16.050
16.060
. . . . . . . . . . . . . . .537
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 537
Nutrition and Labeling Requirements . . . . . . . . . . . . . . . . . . . . . . . . 537
Compositional Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 540
International Compositional Specifications . . . . . . . . . . . . . . . . . . . . 546
Microbiological Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 548
Cited References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 550
Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .551
DEDICATION
Carl H. Blank, PhD
March 16, 1927 May 4, 2002
Technical Committee
H. Michael Wehr, PhD, Chair
U.S. Food and Drug Administration
Washington, DC 20204
Edward A. Arnold, Jr.
Land O'Lakes/R. Tech Laboratories, Inc.
Arden Hills, MN 55126
Mary Bulthaus
Dairy Quality Control Institute
Moundsview, MN 551121400
John C. Bruhn, PhD
Department of Food Science and Technology
University of California
Davis, CA 956168598
James E. Fitts
Division of Milk Control
New York Department of Agriculture and Markets
Albany, NY 12235
Joseph F. Frank, PhD
Department of Food Science and Technology
University of Georgia
Athens, GA 306027610
Robert T. Marshall, PhD
Department of Food Science and Nutrition
University of Missouri
Columbia, MO 65211
Larry A. Maturin, PhD
U.S. Food and Drug Administration
Laboratory Quality Assurance Branch
Summit Argo, IL 605011957
APHA Committee on Laboratory Science and Practice (CLaSP) Liaison
Carl H. Blank, PhD
APHA Project Liaison
Ellen T. Meyer
Director of Publications