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KAPASITAS PRODUKSI

Kapasitas Produksi 150.000 ton/tahun


Operasi 300 hari/tahun
Basis produksi 1 jam operasi
Kapasitas Produksi pertahun
Kapasitas Produksi perjam
Data Fresh Feed
Methanol
Air(water)
Mol Methanol murni

=
=
=

150000
20833.33333
452.8985507

ton/tahun
kg/jam
kg/kmol

=
=
=

99.85%
0.15%
1041.965953

=
=
kmol

Bahan baku yang dibutuhkan sebanyak

Komponen
CH3OCH3
CH3OH
H20

BM
46
32
18

mol bahan baku


methanol
air

Kapasitas dan kemurnian dimetil eter


99.90%
0.10%

33342.9105
50.0895

kg/jam (PT .KALTIM METHANOL INDUSTRI)

mol bahan baku

=
=

=
=
=

33393

kg

1041.9660
2.7828
1044.7487
kmol

33342.9
50.0895
33393

kg
kg
kg

0.9985
0.0015

20831.2500
2.0833

99.99%

vaporizer-01 (VP-01)
Fungsi :

Keterangan :

Aliran 17

bottom produk SCB-01 sebagai input EV-01

Aliran 18

output EV-01 sebagai input R-01

Komponen

CH3OH

18.5875

3,626.5500

-34.2900

H2O

18.3036

3,816.4400

-46.1300

Pi =

exp (ANTA - (ANTB/(T+ ANTC)))

1 mmHg =

0.0013 atm

Komponen Masuk
komponen

Pi (mmHg)

K (mmHg)

Kmol (input)

CH3OH

2,284.3181

1.0019

1,041.9660

H2O

640.3427

0.2809

TOTAL

1,044.7487

95.2710

3.0000

atm

V/F

XFi
xi
((V / F ) K i ) (1 V / F )
Neraca Bahan di Evaporator (EV-01)

2.7828

2,924.6608

368.4210
2,280.0000
0.000

Input

Output

Komponen

mol input (kmol)

Input (kg)

CH3OH

1,041.9660

33,342.9105

H2O

2.7828

50.0895

Total

1,044.7487
33,393.0000
33,393.0000

vapor (kmol)
1,041.9660
2.7827
1,044.7487
33,393.0000

1044.7487

Xfi

Xi

Yi

BM

Kmol Yi liquid

0.9973

0.9973

0.9992

32.000

0.0027

0.0027

0.0007

18.000

0.0000
0.0000

1.0000

1.0000

1.0000

K
mmHg

72.981

44.186

Kmol Yi vapor

1,041.9660
2.7827
1,044.7487

Output
vapor (kg)

liquid (kmol)

liquid (kg)

33,342.9105

0.0000

0.00000

50.0895

0.0000

0.00000

33,393.0000
0.0000
33,393.0000

0.000

1044.7487

Neraca Panas
Panas Vaporizer - 01
Komponen

CH3OH
H2O
cp =

BM

32
18

21.1520
32.2430

0.0709
0.0019

0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Input :
Q .

Panas sensibel dari t-01


T =
Tref =
Komponen
CH3OH
H2O
Total

30.00
25

C
C

n (Kmol)
1041.9660
2.7827
1044.7487

303.15
298.15
CpdT
221.1775
168.4801

Ql (Kj)
230459.4754
468.8380
230928.3134

Output :
Panas laten keluar dari VP-01
T
95.27
Tref
25

C
C

368.42
298.15

Lvc = Lvb (((Tc-T)/(Tc-Tb))^0,38)

Komponen
CH3OH
H2O

Q .

Tc
512.6000
647.3000

Tb
337.7500
373.1500

Lvb
35278.0000
40683.0000

Panas sensible Vapor keluar dari EV-01

Uap

Liquid

komponen
CH3OH
H2O
CH3OH
H2O
Total

massa
33342.9105
50.0895
0.000
0.000
33393.0000

mol
1041.9660
50.0895
0.0000
0.0000
1092.0555

cpdT
3469.0771
2403.5925
3469.0771
2403.5925

Jumlah panas yang dibutuhkan


Q serap = Q masuk - Q keluar
=
39715947.2549
Pemanas yang digunakan adalah saturated steam pada 150oC
Hf =
632.1
kJ /kg
Hg =
2745.4
kJ/kg

Jumlah steam yag dibutuhkan


m = Q serap / (Hg - Hf)
=
18793.3314 kg
Panas steam yang masuk adalah :
Q Si =
51595212.0350

Qsi = Hg . m

Panas steam yang keluar:


Q So =
11879264.7801

Qso = Hf . m

Neraca Panas di vaporizer (VP-01)

Panas Masuk(Kj)
Q ... =
Q Si =

230928.3134
51595212.0350

Total

51826140.3484

Q ... =
QLc =
Q So =

Panas Keluar (Kj)


3735054.9813
36211820.5870
11879264.7801
51826140.3484

0.0000
0.0000

K
K

K
K

Lvc
32784.8935
40948.2593

Q
3614660.2384
120394.7426
0.0001
0.0002
3735054.9813

n
1041.9660
50.0895
1092.0555

Q
34160742.8162
2051077.7708
36211820.5870

Massa

Mol
33393.0000

1092.0555

Q
3735054.9810

0.0000

0.0000

0.0003

33393.0000

1092.0555

3735054.9813

Heat Exchanger
Komponen
CH3OCH3
CH3OH
H2O
cp =

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Input : Q1
Panas sensible yang masuk pada T =
T ref =
komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
0.0000
1041.9660
2.7827
1044.7487

CpdT
5325.7880
3469.0771
2403.5925

panas output keluar HE menuju Cooler ... : Q2


Panas sensibel yang masuk pada T =
Tref =
komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
453.2552
135.4556
456.0379
1044.7487

CpdT
15719.1373
10059.0462
6148.6773

panas output dari HE ke K-01 : Q3


Panas sensibel yang masuk pada T =
Tref =
komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
0.0000
1041.9660
2.7827
1044.7487

CpdT
11400.4677
7331.7422
4685.7352

Panas output reaktor ke HE : Q4


Panas sensibel yang masuk pada T =
Tref =

95.27 C
25 C
Q (kJ)
0.0000
3614660.2384
6688.5968
3621348.8352

200 oC
25 oC
Q (kJ)
7124780.5706
1362553.8725
2804030.1347
11291364.5777

159.79 oC
25 oC
Q (kJ)
0.0000
7639425.7702
13039.2293
7652464.9995

250 oC
25 oC

masuk dr evaporator

komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
453.2552
135.4556
456.0379
1044.7487

CpdT
21622.2456
13781.8544
8015.2470

Q (kJ)
9800395.0210
1866829.0000
3655256.7216
15322480.7426

neraca panas
Panas
Q1
Q2
Q3
Q4
Total

Panas Input (kJ)


Panas Output (kJ)
3621348.8352
11291364.5777
7652464.9995
15322480.7426
18943829.58
18943829.58
7652465.0001

7652465.0001

368.42 K
298.15 K
masuk dr evaporator

473.15 K
298.15 K

panas yang dtranfer Qduty

432.94 K
298.15 K

7652465.0001

7652465.0001

523.15 K
298.15 K

7670015.7425

Kompressor
Komponen
CH3OCH3
CH3OH
H2O

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

Panas masuk kompressor :


Tin

159.79

oC

432.94

Tref

25.0000

oC

298.1500

komponen

n (Kmol)

CpdT

Q(kJ)

CH3OCH3

0.0000

11,400.4677

0.0000

0.0000

CH3OH

1,041.9660

7,331.7422

7,639,425.7702

0.9973

H2O

2.7827

4,685.7352

13,039.2293

0.0027

Total

1,044.7487

7,652,464.9995

1.0000

Panas keluar kompressor :


Tout

180

oC

453.15

Tref

25

oC

298.1500

komponen

n (Kmol)

CpdT

Q(kJ)

CH3OCH3

0.0000

13,521.6415

0.0000

CH3OH

1,041.9660

8,672.1941

9,036,130.9711

H2O

2.7827

5,416.8734

15,073.8041

Total

1,044.7487

9,051,204.7751

Panas yang timbul karena kompressi :


Q'=Q2-Q1
Q' =

1,398,739.7756

Neraca Panas kompressor :


Q input (kJ)
Q in

7,652,464.9995

Q kompressi

1,398,739.7756

Q total

9,051,204.7751

Q Output (kJ)
Q out

9,051,204.7751

Q total

9,051,204.7751

0.0000
33,342.9105
50.0895
33,393.0000

Neraca Panas Heater - 01


Panas sensible yang keluar K-01 (Q) (INPUT) =

Panas sensible yang keluar Heater - 01


T output =
T ref =
Komponen
CH3OCH3
CH3OH
H2O
Total
panas yang disuplay steam
Q steam =

T=

453.1500
180.0000

250 C
25 C

523.15
298.15

kmol
0.0000
1041.9660
2.7827
1044.7487

Cp dT
21622.2456
13781.8544
8015.2470

Q...-Q

Q out
0.0000
14360223.0769
22304.4279
14382527.5047

5331322.7296

Dari tabel steam untuk saturated steam pada = 300 oC


Entalpi liquid jenuh HL =
1345.4 Kj/Kg
Entalpi liquid uap Hv =
2750.9 Kj/Kg
Panas laten.
1405.5 Kj/Kg
Jumlah steam yang dibutuhkan
m=Q steam/ L

3793.1859 kg/jam

Panas yang dibawa masuk oleh steam


Q s in
m x Hv =

10434674.9889 kj/jam

Panas yang dibawa keluar oleh steam


Q s out
m x Hl =

5103352.2593 kj/jam

Neraca panas heater - 02


Q
Q
Q s in
Q s uot
total

panas masuk (kj)


9051204.7751
10434674.9889
19485879.7640

panas keluar (kj)


14382527.5047
5103352.2593
19485879.7640

K
C

9051204.7751 kj

K
K
Komponen
CH3OCH3
CH3OH
H2O

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

Heat Exchanger
Komponen
CH3OCH3
CH3OH
H2O
cp =

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Input : Q1
Panas sensible yang masuk pada T =
T ref =
komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
0.0000
1041.9660
2.7827
1044.7487

CpdT
5325.7880
3469.0771
2403.5925

panas output keluar HE menuju Cooler ... : Q2


Panas sensibel yang masuk pada T =
Tref =
komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
453.2552
135.4556
456.0379
1044.7487

CpdT
16853.6396
10774.6364
6517.6997

panas output dari HE ke K-01 : Q3


Panas sensibel yang masuk pada T =
Tref =
komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
0.0000
1041.9660
2.7827
1044.7487

CpdT
10509.2631
6767.7454
4370.1162

Panas input dari reaktor ke HE : Q4


Panas sensibel yang masuk pada T =
Tref =

95.27 C
25 C
Q (kJ)
0.0000
3614660.2384
6688.5968
3621348.8352

210 oC
25 oC
Q (kJ)
7638999.5953
1459484.5590
2972318.3423
12070802.4965

151.00 oC
25 oC
Q (kJ)
0.0000
7051760.3045
12160.9406
7063921.2450

250 oC
25 oC

masuk dr evaporator

komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
453.2552
135.4556
456.0379
1044.7487

CpdT
21622.2456
13781.8544
8015.2470

Q (kJ)
9800395.0210
1866829.0000
3655256.7216
15322480.7426

neraca panas
Panas
Q1
Q2
Q3
Q4
Total

Panas Input (kJ)


Panas Output (kJ)
3621348.8352
12070802.4965
7063921.2450
15322480.7426
18943829.5779
19134723.7416
6873027.0813

6873027.0813

368.42 K
298.15 K
masuk dr evaporator

483.15 K
298.15 K

panas yang dtranfer Qduty

424.15 K
298.15 K

6873027.0813

6873027.0813

523.15 K
298.15 K

8449453.6613

REAKTOR-1 (R-0
Reaktor-01 (R-01)
berfungsi : Tempat berlangsungnya dehidrasi metahnol dengan katalis zeolit menjadi DME
Kondisi Operasi
Temperatur
Tekanan
Konversi CH3OH
Komposisi fresh feed

Kapasitas

Komponen

BM

CH3OCH3
CH3OH
H2O

Feed reaktor

46
32
18

Kmol

CH3OH
H2O

Kg
1041.9660
2.7827

33342.9105
50.08950

Reaksi :
2CH3OH
1041.9660
906.5104
135.4556

----------->

Neraca Massa Reaktor-01 (R-01)


Input
Komponen
Kmol
CH3OCH3
CH3OH
H2O

Kg
0.0000
1041.9660
2.7827

Total

1044.7487

0.0000
33342.9105
50.0895
33393.0000

Untuk word.
Komponen
CH3OCH3
CH3OH
H2O
Total

Input
Aliran 3
0.0000
33342.9105
50.0895
33393.0000

AKTOR-1 (R-01)

250
8
87

C
atm
0.87

BM
kg/mol
kg/mol
kg/mol

kemurnian CH3OCH3

CH3OCH3
CH3OH
H2O

16.8467
18.5875
18.3036

0.87
906.5103792

CH3OCH3
0.0000
453.2552
453.2552

H2O
0.0000
453.2552
453.2552

Output
20831.25
Kmol
453.2552
135.4556
456.0379
1044.7487

Kg
20849.7387
4334.5784
8208.6829
33393.0000

36212.5913
28.8180
36241.4093

Output
Aliran 5
20849.7387
4334.5784
8208.6829
33393.0000

99%

2361.44 -17.1000
3626.55 -34.2900
3816.44 -46.1300

Neraca Panas
Reaktor - 01 (R-01)
Komponen
CH3OCH3
CH3OH
H2O

cp =

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

D
0.0000
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Q in = aliran panas feed dari H-02


Q out = aliran panas produk ke HE-01

kondisi operasi :
T =
Tref =
Q in =
Q in =

C
-0.0001
0.0000
0.0000

19485879.7640 kJ

250
25

oC =
oC =

523.15
298.15

Q .
19485879.764

reaksi :
2CH3OH

----------------->

Panas Pembentukan pada T = 25 oC untuk reaktan


Reaksi :
Komponen
kg
n (Kmol)
CH3OH
33342.9105
1041.9660
Total
33342.9105
1041.9660
Panas Pembentukan pada T = 25 oC untuk produk
Reaksi :
Komponen
kg
n (Kmol)
CH3OCH3
20849.7387
453.2552
H2O
8208.6829
456.0379
Total
29058.4216
909.2931
H reaksi = H produk - H reaktan
H reaksi =
15906.0242

CH3OCH3

Hf (Kj/mol)

-201.3000

-209747.7464
-209747.7464

Hf (Kj/mol)

-184.1800
-242.0000

-83480.5408
-110361.1814
-193841.7222

Hr1 = Hr1 o + (n CpdT produk - n CpdT reaktan)


Hr1 =
-888665.3100

523.15
298.15

Panas sensibel Produk pada 250 oC:

Tref =
Komponen
CH3OCH3
CH3OH
H2O
Total

n (Kmol)
453.2552
135.4556
456.0379
1044.7487

CpdT

H (Kj)

21622.2456
13781.8544
8015.2470

9800395.0210
1866829.0000
3655256.7216
15322480.7426

K
K

13455651.7426

Karena reaksinya eksotermis sehingga memerlukan air pendingin


Massa air yang digunakan, m
Panas yang diserap air pendingin, Qc :
Qc = Q umpan - Q reaksi - Q produk

Qc =
Tref =
suhu air masuk =
suhu air keluar =

5052064.3315
25
30
50

oC =
oC =
oC =

m = Qc/Cp(Tout-Tin)

CpdT (air) =
m =

4.18 kJ/(kg.K)
60431.3915 kg

Panas yang dibawa air pendingin masuk, Q win


Q wi =
m . Cp . ( T in - T ref)

CpdT (air) =
Q wi =

4.18 ------------------- T = 30
1263016.0829 Kj

Panas yang dibawa air pendingin keluar, Qwo


Q wo = m.Cp.(Tout-Tref)
CpdT =
4.18 -------------------- T = 50
Q wo =
6315080.4143 Kj

Neraca Panas di Reaktor (R-01)


Panas Masuk

Q in =
Q win =

19485879.7640
1263016.0829

Qout =
Q wo =

Panas Keluar
15322480.7426
6315080.4143

298.15
303.15
323.15

Qr =
Total

20748895.8469

-888665.3100
20748895.8469

K
K

Data Hof 298 (Buku Coulson)


Hof 298
Komponen
KJ/Kmol
CH3OCH3
-184.18
CH3OH
-201.30
H2O
-242.00

BM
46
32
18

H2O

Panas sensibel reaktan pada 250 oC :


Reaksi :
Komponen
n (kmol)
CpdT
CH3OH
1041.9660
13781.8544
Total
Panas sensibel produk pada 250 oC :
Reaksi :
Komponen
n (kmol)
CpdT
CH3OCH3
453.2552
21622.2456
H2O
456.0379
8015.2470
Total
H reaksi = H produk - H reaktan
H reaksi =
-904571.3342

Q (Kj)

14360223.0769
14360223.0769

Q (Kj)

9800395.0210
3655256.7216
13455651.7426

oK
oK
oK

Cooler -01 (C-01)


Fungsi : untuk mendinginkan aliran produk keluar dari R-01
Input : panas sensibel keluar dari Reaktor-01
T ref =
T =
Komponen
CH3OCH3
CH3OH
H2O
Total

25
200

oC =
oC =

Kmol
453.2552
135.4556
456.0379

298.15
473.15

CpdT (Kj/kmol)
15719.1373
10059.0462
6148.6773

K
K

Qh (kj)
7124780.5706
1362553.8725
2804030.1347
11291364.5777

Output: Panas sensibel keluar dari Cooler

T ref =
T=
Komponen
CH3OCH3
CH3OH
H2O
Total

25
110

oC
oC

n (Kmol)
453.2552
135.4556
456.0379
1044.7487

298.15
383.15

CpdT (Kj/kmol)
6616.0207
4294.2134
2917.8249

K
K

Qout (kj)
2998745.7195
581675.1367
1330638.8582
4911059.7145

Panas kerja C-02 (Q duty C-01)


Q duty = Q sensible in - Q sensible out
Q duty =

6380304.8633 kJ

T air in =
T air out =
Tref =

30
50
25

oC =
oC =
oC =

303.15
323.15
298.15

oK
oK
oK

Cp air didapat dari tabel 2.355 ferry ^_^


CP air =

4.1799 kj/(kg.K)

maka kapasitas air yang dibutuhkan =


Panas air yang masuk =
Qw in
Komponen

76321.2620 kg
30

kg

CpdT (Kj/kmol)

oC =

303.15

Q (kj)

H2O

76321.2620

Qw out
Panas air yang keluar =
Komponen
H2O

4.1799

50
kg
76321.2620

CpdT (Kj/kmol)
4.1799

1595076.2158 Qw in

oC

323.15

Q (kj)
7975381.0791 Qw out

Neraca Panas pada Cooler-01 (C-01)

Panas masuk
Panas Keluar
Q sensibel in =
11291364.5777 Q sensibel out =
4911059.7145
Q air in =
1595076.2158 Q air out =
7975381.0791
Total
12886440.7936
12886440.7936

Komponen
CH3OCH3
CH3OH
H2O
cp =

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Condenser - 01

(CD-01)

Fungsi : Merubah fase dan menurunkan suhu produk keluaran C-02 menuju KD-01

CH3OCH3

17.0150

0.1791

-0.0001

CH3OH

21.1520

0.0709

0.0000

H2O

32.2430

0.0019

0.0000

Komponen

cp

cpVAPA

cpVAPB*T

cpVAPC*T^2

cpVAPD*T^3

Kondisi operasi :

Input

Tref

25.00

oC

298.15

Tin

110.00

oC

383.15

Tout

86.56

oC

359.71

12.57

atm

95,501.60

:
Panas sensibel vapor masuk CD-01 pada T

Output

110 oC

Tref

25

oC

298.15

Tin

110

oC

383.15

Komponen

n (Kmol)

CpdT

H (Kj)

CH3OCH3

453.2552

6,616.0207

2,998,745.7195

CH3OH

135.4556

4,294.2134

581,675.1367

H2O

456.0379

2,917.8249

1,330,638.8582

Total

1,044.7487

4,911,059.7145

:
Panas laten pengembunan keluar dari CD-01
Tout

86.5550

oC

359.7050

Tref

25.0000

oC

298.1500

Lvc = Lvb (((Tc-T)/(Tc-Tb))^0,38)

Komponen

Tc

Tb (K)

Lvb

Lvc

CH3OCH3

400.0000

248.2500

21,520.0000

13,001.9593

CH3OH

512.6000

337.7500

35,278.0000

33,524.3574

H2O

647.3000

373.1500

40,638.0000

41,384.1173

Total

Panas Sensibel kondensat keluar CD-01


komponen

massa

mol

cpdT

CH3OCH3

20,849.7387

453.2552

4,589.9871

2,080,435.4694

CH3OH

4,334.5784

135.4556

2,996.7200

405,922.4269

H2O

8,208.6829

456.0379

2,101.0768

958,170.7341

Total

33,393.0000

1,044.7487

9,687.7839

3,444,528.6303

Panas yg diserap oleh air pendingin :


Q duty

Q sensibel in - Q sensibel out

Q duty

Qin + Qlc -

Q duty

Qout

30,773,525.2761

kJ

T air in =

30.0000

oC

303.1500

T air out =

50.0000

oC

323.1500

Tref =

25.0000

oC

298.1500

368,113.1759

kg

30.0000

oC

303.1500

CpdT (Kj/kmol)

Q (kj)

4.1799

7,693,381.3190

Cp air didapat dari tabel 2.355 ferry ^_^

CP air =

4.1799

kj/(kg.K)

maka kapasitas air yang dibutuhkan =

Panas air yang masuk =

Komponen
air

kg
368,113.1759

Qw in

Panas air yang keluar

50.0000

oC

Komponen

kg

CpdT (Kj/kmol)

Q (kj)

air

368,113.1759

4.1799

38,466,906.5951

Neraca Panas pada Condenser - 02

(CD-02)

Panas masuk

Panas Keluar

Q in

4,911,059.7145

Q out

3,444,528.6303

Q Lc

29,306,994.1919

Qa out

38,466,906.5951

Qa in

7,693,381.3190

Total

41,911,435.2254

41,911,435.2254

323.1500

Qw out

(CD-01)

D
0.0000
0.0000
0.0000
BM :

K
K
K
mmHg

K
K

0.4338
0.1297
0.4365
Qin

1.0000

K
K

CH3OCH3

46.0000

CH3OH

32.0000

H2O

18.0000

n (kmol)

QLc

Tb (celcius)

453.2552

5,893,205.5235

-24.9000

135.4556

4,541,061.0674

64.6000

456.0379

18,872,727.6009

100.0000

1,044.7487

29,306,994.1919

xi
0.6244
0.1298
0.2458
Qout

1.0000

KOLOM DESTILASI-01 (KD-01)


Fungsi : Sebagai tempat memisahkan Methanol dengan DME

Komponen masuk
komponen
CH3OCH3
CH3OH
H2O
TOTAL

input (kmol/hr)
453.2552
135.4556
456.0379
1044.7487

Konstanta Tekanan Uap murni Komponen


(Data Physical Properties From: Coulson & Richardson's Chemical Engineering Vol 6, Appendix C)

Komponen
CH3OCH3
CH3OH
H2O

Konstanta Antoine
A
16.8467
18.5875
18.3036

Pi* = EXP (A-(B/(T+C)))


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.433841
0.129654
0.436505
1.000000

P =
T =

12.5660
86.5550

ditetapkan :
light key = CH3OH
heavy key = H2O
reference = H2O
komponen
CH3OCH3
CH3OH
H2O
TOTAL

Ki
2.2029
0.1789
0.0482

diinginkan distribusi komponen kunci


Komponen light key
LK(CH3OH) D =
LK (CH3OH) B =

135.3201
0.1355

LOG (CH3OH)D / (CH3OH)B =

2.9996

komponen heavy key


HK (H2O) D =
HK (H2O) B =

0.4560
455.5819

LOG (H2O)D / (H2O)B =

-2.9996

distribusi komponen lain


(. CH3OCH3/CH3OH) = (K CH3OCH3/K CH3OH) =
(. CH3OH/CH3OH) =
(. H2O/CH3OH) =

komponen
CH3OCH3
CH3OH
TOTAL

X = log ik
1.0905
0.0000
1.0905

dibuat persamaan garis lurus Y = aX + b


a (slope) =
b (intersept) =

5.5012
-2.9996
komponen
CH3OCH3
CH3OH
H2O
TOTAL

X = log ik
1.0905
0.0000
-0.5690
0.5215

kondisi top dew point KD - 02


komponen
CH3OCH3
CH3OH
H2O
Total

kmol

452.8019
0.1355
0.0003
452.9377

kondisi bottom bubble point KD - 02


komponen
CH3OCH3
CH3OH
H2O
TOTAL

kmol
0.4533
135.3201
456.0376
591.8110

komponen
CH3OCH3
CH3OH
H2O
Total

BM
46.0000
32.0000
18.0000

top distilation trial n error

P=
T=

11.0010
46.3680

bottom distilation trial n error


komponen
CH3OCH3
CH3OH
H2O
Total

BM
46.0000
32.0000
18.0000

P=
T=

15.0000
191.6000

Neraca massa KD-03


input
Komponen
CH3OCH3
CH3OH
H2O
Total

kmol
453.2552
135.4556
456.0379
1044.7487
33393.0000

M DESTILASI-01 (KD-01)

input (kg/hr)
fraksi mol, Xi
20849.7387
0.433841
4334.5784
0.129654
8208.6829
0.436505
33393.0000
1.000000

BM
46
32
18

emical Engineering Vol 6, Appendix C)

Konstanta Antoine
B
2,361.4400
3,626.5500
3,816.4400

Pi
21038.2551
1708.0628
460.7517

C
-17.1000
-34.2900
-46.1300

Ki (Pi/P)
2.2029
0.1789
0.0482

Titik Didih
-24.9000
64.6000
100.0000

Y = (Ki . Xi)
0.9557
0.0232
0.0211
1.0000

atm
oC

=
=

9550.1600
359.7050

Kref
0.1789
0.1789
0.1789

= (Ki/Kref)
12.3170
1.0000
0.2698

log
1.0905
0.0000
-0.5690

0.9990

0.9990
0.0010

Log ( CH3OCH3) = 1.0905

12.3170
1.0000
0.2698
Y = log iD/iB
2.9996
-2.9996
0.0000

mmHg
K

X.Y
3.2710
0.0000
3.2710

log ( CH3OH) =

0.0000

log ( H2O) =

-0.5690

X^2
1.1892
0.0000
1.1892

{(n x XY)-(X x Y)} /{n x X2)-(X)2}


{Y - (a x X)}/2
Y = log iD/iB
2.9996
-2.9996
-6.1300
-6.1300

iD/iB
999.0000
0.0010
0.0000
999.0010

B (kmol)
0.4533
135.3201
456.0376
591.8110

D (kmol)
452.8019
0.1355
0.0003
452.9377

Xi
0.9997
0.0003
0.0000
1.0000

Xi
0.0008
0.2287
0.7706
1.0000

kmol
452.8019
0.1355
0.0003
452.9377
atm
C

kmol
0.4533
135.3201
456.0376
591.8110
atm
C

kg
20828.8890
4.3346
0.0061
20833.2296

Yi
0.9997
0.0003
0.0000
1.0000

8360.7600
319.5180

kg
20.8497
4330.2438
8208.6768
12559.7704

Yi
0.0008
0.2287
0.7706
1.0000

11400.0000
464.7500

5.0000
21.8970

B
2361.4400
3626.5500
3816.4400

4.0000
15.3520

A
16.8467
18.5875
18.3036

B
2361.4400
3626.5500
3816.4400

bottom
kmol
0.4533
135.3201
456.0376
591.8110

kg
20.8497
4330.2438
8208.6768
12559.7704

mmHg
K

output

input
kg
20849.7387
4334.5784
8208.6829
33393.0000
33393.0000

mmHg
K

A
16.8467
18.5875
18.3036

top
kmol
452.8019
0.1355
0.0003
452.9377

kg
20828.8890
4.3346
0.0061
20833.2296
33393.0000

Pi* = EXP (A-(B/(T+C)))


C
Pi
Ki
-17.1000 8418.3581
1.0069
-34.2900
355.2902
0.0425
-46.1300
77.0001
0.0092

Pi* = EXP (A-(B/(T+C)))


C
Pi
Ki
-17.1000 106033.1783 9.3012
-34.2900 25917.5440
2.2735
-46.1300 9768.1578
0.8569

20833.33333
0.99979165

Xi = Yi/Ki
0.9929
0.0070
0.0001
1.0000

Xi = Yi/Ki
0.0001
0.1006
0.8993
1.0000

Kolom Destilasi - 01 (KD-01)

Tref =
Tin =
Ttop =
Tbottom =

Komponen
CH3OCH3
CH3OH
H2O
cp =

25
86.56
46.37
191.60

BM
46
32
18

C
C
C
C

298.15
359.71
319.52
464.75

A
17.0150
21.1520
32.2430

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Panas masuk KD-01, pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

n (kmol)
453.2552
135.4556
456.0379
1044.7487

359.71
CpdT
4589.9871
2996.7200
2101.0768

Panas masuk Kondenser, Qin CD-02 pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

B
0.1791
0.0709
0.0019

n (kmol)
482.0393
0.1442
0.0004
482.1839

CpdT
1470.6753
972.7628
722.6223

Panas Latent Condenser, QL CD-01 pada T =

Q
2080435.4694
405922.4269
958170.7341
3444528.6303
319.52
Q
708923.2748
140.2743
0.2601
709063.8091
319.52

Komponen
CH3OCH3
CH3OH
H2O

Tc (C)

Tc ( K)

126.8500
239.4500
374.1500

Tb (C)

400.0000
512.6000
647.3000

-24.9000
64.6000
100.0000

Lvc = Lvb (((Tc-T)/(Tc-Tb))^0,38)


Komponen
CH3OCH3
CH3OH
H2O

Tc
400.0000
512.6000
647.3000

Tb
248.2500
337.7500
373.1500
Total

Panas destilat, Qd CD-02 pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

n
452.8019
0.1355
0.0003
452.9377

319.52 K
Cp
1470.6753
972.7628
722.6223

Panas Refluks, Qr CD-02 pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

n
29.2374
0.0087
0.0000
29.2461

Lvb
21520.0000
35278.0000
40683.0000

Q
665924.6117
131.7661
0.2443
666056.6222

319.52 K
Cp
1470.6753
972.7628
722.6223

Q
42998.6630
8.5081
0.0158
43007.1869

Panas yang keluar dari bottom KD-01 pada T =


Komponen
CH3OCH3
CH3OH
H2O
total

n
0.4533
135.3201
456.0376
591.8110

Cp
14784.4768
9469.3352
5840.3149

464.75
Q
6701.1409
1281391.5542
2663403.2104
3951495.9055

Beban Panas CD-02, Q CD-02


Q CD-02 =
Q CD-02 =

Qin CD-02 + QL CD-02 - Qd CD-02- Qr CD-02


8157244.9409

Beban Panas reboiler, Q RB-01 :

Q RB-01 =
Q RB-01 =

Q bottom KD-01 + Qd CD-02 + Q CD-02 - Qin KD-02


9330268.8383

Neraca Panas :
Q input
Qin KD-02 =
Q RB-02 =
Total

Qoutput
3444528.6303 Qd CD-02 =
9330268.8383 Qbottom KD-02=
Q CD-02 =
12774797.4686
12774797.4686

K
K
K
K

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

Tb (K)
248.2500
337.7500
373.1500

Lvc
16911.3738
36633.0344
43541.1378

J/mol
J/mol
21520.0000
35278.0000
40683.0000

n (kmol)
482.0393
0.1442
0.0004
482.1839

-184180.0000
-201300.0000
-242000.0000

QLc
8151946.7157
5282.5540
15.6712
8157244.9409

Qoutput
666056.6222
3951495.9055
8157244.9409
12774797.4686

CONDENSOR -02 (CD-02)


Fungsi : Mengubah fase produk TOP KD-01 dari Vapor menjadi Liquid

Kondisi Operasi Feed =


P=
T=
komponen
CH3OCH3
CH3OH
H2O
TOTAL

9.6130
43.3500
Xf
0.4338
0.1297
0.4365
1.0000

0.6002

L/D + 1 =
L/D min =
L/D act = 1.25 x L/Dmin

1.0517
0.0517
0.0646

V=
R=
V=
=
V=
L=RxD

komposisi feed kondensor (V)


komponen
CH3OCH3
CH3OH
H2O
TOTAL

atm
C
XD
0.9997
0.0003
0.0000
1.0000

=
=

7305.8800
316.5000

12.3170
1.0000
0.2698

(-)/

0.9513
0.3998
-1.2249

trial n error

L+D
Lo / D
RxD+D
(R+1) x D

482.1839
29.2461

Xi
0.9997
0.0003
0.0000
1.0000

kmol
482.0393
0.1442
0.0004
482.1839

kg
22173.8076
4.6145
0.0065
22178.4285

BM
46
32
18

komposisi refluks (L)


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.9997
0.0003
0.0000
1.0000

kmol
29.2374
0.0087
0.0000
29.2461

kg
1344.9186
0.2799
0.0004
1345.1988

BM
46
32
18

komposisi distilat (D)


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.9997
0.0003
0.0000
1.0000

kmol
452.8019
0.1355
0.0003
452.9377

kg
20828.8890
4.3346
0.0061
20833.2296

BM
46
32
18

Neraca massa CD-03


komponen
CH3OCH3
CH3OH
H2O
Total

input
V
kmol
kg
482.0393 22173.8076
0.1442
4.6145
0.0004
0.0065
482.1839 22178.4285
22178.4285

output
L
kmol
29.2374
0.0087
0.0000
29.2461

kg
1344.9186
0.2799
0.0004
1345.1988
22178.4285

2)

mmHg
K
Xf/(-)/

XD/(-)/

0.4561
0.3243
-0.3563
0.4240

1.0509
0.0007
0.0000
1.0517

xf = 0
xd lbh bsr dr Xf

output
D
kmol
452.8019
0.1355
0.0003
452.9377
22178.4285

kg
20828.8890
4.3346
0.0061
20833.2296

Panas Condenser - 02
Tref =
T CD-02 =

25 oC =
46.37 oC =

298.15 K
319.52 K

Panas masuk Condensor, Qin CD-02 pada T =


Qin CD-02 =
709063.8091

319.52

Panas latent kondensor, QL CD-02 pada T =


QL CD-02 =
8157244.9409

319.52

Panas destilat, Qd CD-02 pada T =


Qd CD-02 =
666056.6222

319.52 K

Panas refluks, Qr CD-02 pada T =


Qr CD-02 =
43007.1869

319.52 K

Beban panas kondensor, Qc =


Qin CD + Ql CD - Qd CD - Qr CD
Q CD-02 =
8157244.9409
Kebutuhan air pendingin:
Tin
303.15
Tout
323.15
Cp
4.18
m=
97574.7003

K
K
kJ/kg.K
kg

30 oC
50 oC

Panas air pendingin masuk, Qwi pada T = 30 C


Qwi =
2039311.2352
Panas air pendingin keluar, Qwo pada T = 50 C
Qwo = 10196556.1761

Material Balance pada Condenser - 02 (CD-02)

Panas Masuk
Panas Keluar
Qin CD-02
709063.8091 Qd CD-02
666056.6222
QL CD-02
8157244.9409 Qr CD-02
43007.1869
Qwi
2039311.2352 Qwo
10196556.1761
Total
10905619.9853
10905619.9853

ACCUMULATOR-01 (ACC-01)
Fungsi : Menampung hasil kondensasi dari CD-02

20833.33333
Neraca Massa Accumulator-01 (ACC-01)
Input
Komponen
Aliran
Aliran
V(kmol)
V (kg)
CH3OCH3
482.0393 22173.8076
CH3OH
0.1442
4.6145
H2O
0.0004
0.0065
482.1839 22178.4285
Total
22178.4285

Aliran
Destilat (D) kmol
452.8019
0.1355
0.0003
452.9377

Output
Aliran
Destilat (D) kg
20828.8890
4.3346
0.0061
20833.2296
22178.4285

ACC-01)

Output
Aliran
Refluks (L) kmol
29.2374
0.0087
0.0000
29.2461
22178.4285

Aliran
Refluks (L) kg
1344.9186
0.2799
0.0004
1345.1988

x
0.999792 0.999792
0.000208 0.000208
2.92E-07 2.92E-07
1.0000

REBOILER-01 (RB-01)
Fungsi : Untuk menguapkan kembali liquid yang masuk dari kD-01

Kondisi Operasi feed :


P=
T=

L* = F + L
V* = V + (q - 1) F
B* = L* - V*

15.0000
191.6000

atm
C

1073.9948
482.1839
591.8110

=
=
107.3995
48.2184
59.1811

11400.0000
464.7500
966.5953

komposisi feed reboiler


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.0008
0.2287
0.7706
1.0000

kmol
0.8225
245.5735
827.5988
1073.9948

kg
37.8373
7858.3528
14896.7776
22792.9677

BM
46
32
18

komposisi refluks reboiler


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.0008
0.2287
0.7706
1.0000

kmol
0.3693
110.2534
371.5612
482.1839

kg
16.9875
3528.1090
6688.1008
10233.1974

BM
46
32
18

komposisi bottom produk reboiler


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.0008
0.2287
0.7706
1.0000

kmol
0.4533
135.3201
456.0376
591.8110

kg
20.8497
4330.2438
8208.6768
12559.7704

BM
46
32
18

Neraca massa RB-01

mmHg
K

output

input (L*)
komponen
CH3OCH3
CH3OH
H2O
TOTAL

kmol

kg

0.8225
37.8373
245.5735
7858.3528
827.5988
14896.7776
1073.9948 22792.9677
22792.9677

V*
kmol
0.3693
110.2534
371.5612
482.1839

B*
kg
kmol
16.9875
0.4533
3528.1090 135.3201
6688.1008 456.0376
10233.1974 591.8110
22792.9677

ut

677

kg
20.8497
4330.2438
8208.6768
12559.7704

REBOILER -01
T =
P =

191.60 oC =
15.00 atm

464.75 K
11400 mmHg

Panas keluar dari bottom Rb-01, Qout RB1


Qout RB1 =

3951495.9055

Panas Sensibel Vapor yang keluar, Q


Komponen

CH3OCH3
CH3OH
H2O
Total

n
0.3693
110.2534
371.5612
482.1839

Cp
14784.4768
9469.3352
5840.3149

Q
5459.8209
1044026.4671
2170034.1594
3219520.4473

Panas Laten Vapor yang keluar, QLv


Lvc = Lvb*(((Tc-T)/(Tc-Tb))^0,38)

Komponen
CH3OCH3
CH3OH
H2O

Tc
400.0000
512.6000
647.3000

Tb
248.2500
337.7500
373.1500
Total

Lvb
21520.0000
35278.0000
40683.0000

Cp
14784.4768
9469.3352
5840.3149

Q
12160.9618
2325418.0213
4833437.3698
7171016.3529

Panas masuk Rb-01,Q.


Komponen

CH3OCH3
CH3OH
H2O
Total

n
0.8225
245.5735
827.5988
1073.9948

Beban Panas Reboiler, QRb :


QRb=Qd+Ql+Qb-Qin KD
QRb =
Qrb=

Q bottom KD-01 + Qd CD-03 + Q CD-03 - Qin KD-01


9330268.8383

Fluida panas yang digunakan adalah saturated steam pada T = 150 oC


Hg =
Hliq =

2745.4 KJ/Kg
632.1 KJ/Kg

Lvc
15569.8517
21559.8707
34858.0055

Jumlah steam yang diperlukan :


m = Q serap / (Hg - H liq)
kg
m=
4415.0233

245.2791 mol

Panas steam yang masuk adalah :


Qsi = Hg . m
Qsi =
12121005.0957 kJ
Panas steam yang keluar:
Qso = H liq . m
Qso =
2790736.2574 Kj
Neraca Panas pada Reboiler-01

Q
Qsi

Total

Panas Masuk
7171016.3529 Qv
12121005.0957 QLv
QB
Qso
19292021.4486

Panas Keluar
3219520.4473
9330268.8383
3951495.9055
2790736.2574
19292021.4486

n (kmol)
0.3693
110.2534
371.5612
482.1839

QLc
5749.8552
2377049.2078
12951880.7743
15334679.8374

12121005.0957

Cooler -02 (C-02)


Fungsi : untuk mendinginkan aliran produk keluar dari RB-01
Input : panas sensibel keluar dari RB-02
T ref =
T =
Komponen
CH3OCH3
CH3OH
H2O
Total

25
192

oC =
oC =

Kmol
0.8225
245.5735
827.5988
1073.9948

298.15
464.75

CpdT (Kj/kmol)
14784.4768
9469.3352
5840.3149

K
K

Qh (kj)
12160.9618
2325418.0213
4833437.3698
7171016.3529

Output: Panas sensibel keluar dari Cooler

T ref =
T=
Komponen
CH3OCH3
CH3OH
H2O
Total

25
87

oC
oC

n (Kmol)
0.8225
245.5735
827.5988
1073.9948

298.15
359.71
CpdT (Kj/kmol)
4589.9871
2996.7200
2101.0768

K
K

Qout (kj)
3775.4909
735915.0950
1738848.5457
2478539.1317

Panas kerja C-02 (Q duty C-01)


Q duty = Q sensible in - Q sensible out
Q duty =

4692477.2212 kJ

T air in =
T air out =
Tref =

30
50
25

oC =
oC =
oC =

303.15
323.15
298.15

oK
oK
oK

Cp air didapat dari tabel 2.355 ferry ^_^


CP air =

4.1799 kj/(kg.K)

maka kapasitas air yang dibutuhkan =


Panas air yang masuk =
Qw in
Komponen

56131.4532 kg
30

kg

CpdT (Kj/kmol)

oC =

303.15

Q (kj)

H2O

56131.4532

Qw out
Panas air yang keluar =
Komponen
H2O

kg
56131.4532

4.1799

50
CpdT (Kj/kmol)
4.1799

1173119.3053 Qw in

oC

323.15

Q (kj)
5865596.5265 Qw out

Neraca Panas pada Cooler-03 (C-03)

Panas masuk
Panas Keluar
Q sensibel in =
7171016.3529 Q sensibel out =
2478539.1317
Q air in =
1173119.3053 Q air out =
5865596.5265
Total
8344135.6582
8344135.6582

Komponen
CH3OCH3
CH3OH
H2O
cp =

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Kolom Destilasi - 02 (KD-02)

Tref =
Tin =
Ttop =
Tbottom =

25
95.17
64.70
111.76

Komponen
CH3OCH3
CH3OH
H2O

A
17.0150
21.1520
32.2430

cp =

C
C
C
C

298.15
368.32
337.85
384.91

B
0.1791
0.0709
0.0019

n (kmol)
0.4533
135.3201
456.0376
591.8110

368.32 K
CpdT
5317.1863
3463.5634
2400.0971

Panas masuk Kondenser, Qin CD-03 pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

C
-0.0001
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

Panas masuk KD-02, pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

K
K
K
K

n (kmol)
0.9559
285.0978
0.9618
287.0154

Panas Latent Condenser, QL CD-03 pada T =

CpdT
2837.1057
1864.4982
1348.1194

Q
2410.0423
468689.8056
1094534.5128
1565634.3607
337.85 K
Q
2711.9662
531564.2815
1296.5670
535572.8147
337.8484 K

D
0.0000
0.0000
0.0000

Komponen
CH3OCH3
CH3OH
H2O

Tc (C)

Tc ( K)

126.8500
239.4500
374.1500

Tb (C)

400.0000
512.6000
647.3000

-24.9000
64.6000
100.0000

Tb (K)
248.2500
337.7500
373.1500

Lvc = Lvb (((Tc-T)/(Tc-Tb))^0,38)


Komponen
CH3OCH3
CH3OH
H2O

Tc
400.0000
512.6000
647.3000

Tb
248.2500
337.7500
373.1500
Total

Panas destilat, Qd CD-03 pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

n
0.4533
135.1848
0.4560
136.0941

337.8484 K
Cp
2837.1057
1864.4982
1348.1194

Panas Refluks, Qr CD-03 pada T =


Komponen
CH3OCH3
CH3OH
H2O
Total

n
0.5026
149.9130
0.5057
150.9213

n
0.0000
0.1353
455.5816
455.7169

Cp
2837.1057
1864.4982
1348.1194

Cp
6773.7289
4394.8370
2979.3899

Beban Panas CD-03, Q CD-03


Q CD-03 =
Q CD-03 =

Qin CD-03 + QL CD-03 - Qd CD-03- Qr CD-03


10111151.6184

Beban Panas reboiler, Q RB-03 :

Q
1285.9329
252051.8165
614.7931
253952.5426

337.8484 K

Panas yang keluar dari bottom KD-02 pada T =


Komponen
CH3OCH3
CH3OH
H2O
total

Lvb
21520.0000
35278.0000
40683.0000

Q
1426.0333
279512.4649
681.7739
281620.2721
384.9060 K
Q
0.0000
594.7099
1357355.1076
1357949.8174

Lvc
15329.4040
35270.4553
42599.3213

Q RB-02 =
Q RB-02 =

Q bottom KD-02 + Qd CD-03 + Q CD-03 - Qin KD-02


10157419.6177

Neraca Panas :
Q input
Qin KD-03 =
Q RB-03 =
Total

Qoutput
1565634.3607 Qd CD-02 =
253952.5426
10157419.6177 Qbottom KD-02=
1357949.8174
Q CD-02 =
10111151.6184
11723053.9784
11723053.9784

J/mol
J/mol
21520.0000
35278.0000
40683.0000

n (kmol)
0.9559
285.0978
0.9618
287.0154

-184180.0000
-201300.0000
-242000.0000

QLc
14653.2519
10055528.0525
40970.3139
10111151.6184

CONDENSOR-03
Fungsi : Mengubah fase TOP KD-02 dari Vapor menjadi Liquid

Kondisi Operasi Feed :


P=
1
T=
64.69839

atm
C

=
=

760
337.8483886

mmHg
K

komponen
CH3OCH3
CH3OH
H2O
TOTAL

XD
0.0033
0.9933
0.0034
1.0000

39.1543
3.5711
1.0000

(-)/

Xf/(-)/

XD/(-)/

0.9568
0.5260
-0.6928

0.0194
0.9600
-0.6878
0.2916

0.0035
1.8885
-0.0048
1.8872

Xf
0.0185
0.5050
0.4765
1.0000
1.6928

L/D + 1 =
L/D min =
L/D act = 1.25 x L/Dmin
V=
R=
V=
=

trial n error
1.8872
0.8872
1.1089

L+D
Lo / D
RxD+D
(R+1) x D

V=
L=RxD

komposisi feed kondensor (V)


komponen
Xi
CH3OCH3 0.0033

287.0154
150.9213

kmol
0.9559

kg
43.9710

BM
46

CH3OH
H2O
TOTAL

0.9933
0.0034
1.0000

285.0978
0.9618
287.0154

9123.1286
17.3117
9184.4113

32
18

Komposisi refluks (L)


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.0033
0.9933
0.0034
1.0000

kmol
0.5026
149.9130
0.5057
150.9213

kg
23.1213
4797.2150
9.1030
4829.4393

BM
46
32
18

komposisi distilat (D)


komponen
CH3OCH3
CH3OH
H2O
TOTAL

Xi
0.0033
0.9933
0.0034
1.0000

kmol
0.4533
135.1848
0.4560
136.0941

kg
20.8497
4325.9135
8.2087
4354.9720

BM
46
32
18

Neraca massa CD-04


input (V)
komponen

kmol

output
kg

CH3OCH3 0.9559
43.9710
CH3OH 285.0978
9123.1286
H2O
0.9618
17.3117
287.0154
9184.4113
Total
9184.4113

L
kmol
0.5026
149.9130
0.5057
150.9213

D
kg
kmol
23.1213
0.4533
4797.2150 135.1848
9.1030
0.4560
4829.4393 136.0941
9184.4113

kg
20.8497
4325.9135
8.2087
4354.9720

xf = 0
xd lbh bsr dr Xf

Panas Condenser - 03
Tref =
T CD-03 =

25 oC =
64.70 oC =

298.15 K
337.85 K

Panas masuk Condensor, Qin CD-03 pada T =


Qin CD-03 =
535572.8147

337.85

Panas latent kondensor, QL CD-03 pada T =


QL CD-03 =
10111151.6184

337.85

Panas destilat, Qd CD-03 pada T =


Qd CD-03 =
253952.5426

337.85 K

Panas refluks, Qr CD-03 pada T =


Qr CD-03 =
281620.2721

337.85 K

Beban panas kondensor, Qc =


Qin CD + Ql CD - Qd CD - Qr CD
Q CD-03 =
10111151.6184
Kebutuhan air pendingin:
Tin
303.15
Tout
323.15
Cp
4.18
m=
120946.7897

K
K
kJ/kg.K
kg

30 oC
50 oC

Panas air pendingin masuk, Qwi pada T = 30 C


Qwi =
2527787.9046
Panas air pendingin keluar, Qwo pada T = 50 C
Qwo =
12638939.5230

Material Balance pada Condenser - 03 (CD-03)

Qin CD-03
QL CD-03
Qwi
Total

Panas Masuk
Panas Keluar
535572.8147 Qd CD-03
253952.5426
10111151.6184 Qr CD-03
281620.2721
2527787.9046 Qwo
12638939.5230
13174512.3376
13174512.3376

ACCUMULATOR - 02 (ACC-02)
Fungsi : Menampung hasil kondensasi dari CD-03

Neraca massa ACC-02


Komponen
CH3OCH3
CH3OH
H2O
Total

Input
Aliran
Aliran
V(kmol)
V (kg)
0.9559
43.9710
285.0978
9123.1286
0.9618
17.3117
287.0154
9184.4113
9184.4113

Aliran
Destilat (D) kmol
0.4533
135.1848
0.4560
136.0941

Output
Aliran
Aliran
Destilat (D) kgRefluks (L) kmol
20.8497
0.5026
4325.9135
149.9130
8.2087
0.5057
4354.9720
150.9213
9184.4113

Aliran
Refluks (L) kg
23.1213
4797.2150
9.1030
4829.4393

x
0.004788 0.004788
0.993328 0.993328
0.001885 0.001885
1.0000

Reboiler - 02 RB-02
Fungsi :Untuk menguapkan kembali liquid yang masuk KD-02

Kondisi Operasi Feed :


P=
T=

1.5004 atm
111.76 C

1140.304 mmHg
384.9060124 K
742.7323
287.0154
455.7169

L* = F + L
V* = V + (q - 1) F
B* = L* - V*
komposisi feed reboiler
komponen
CH3OCH3
CH3OH
H2O
TOTAL

=
=

Xi
0.0000
0.0003
0.9997
1.0000

kmol
0.0000
0.2205
742.5118
742.7323

kg
0.0000
7.0575
13365.2116
13372.2691

BM
46
32
18

komposisi refluks reboiler


komponen
Xi
CH3OCH3 0.0000
CH3OH
0.0003
H2O
0.9997
TOTAL
1.0000

kmol
0.0000
0.0852
286.9302
287.0154

kg
0.0000
2.7272
5164.7435
5167.4707

BM
46
32
18

komposisi bottom produk reboiler


komponen
Xi
CH3OCH3 0.0000
CH3OH
0.0003
H2O
0.9997
TOTAL
1.0000

kmol
0.0000
0.1353
455.5816
455.7169

kg
0.0000
4.3302
8200.4681
8204.7984

BM
46
32
18

Neraca massa RB-03

input (L*)
komponen

kmol

kg

CH3OCH3 0.0000
0.0000
CH3OH
0.2205
7.0575
H2O
742.5118 13365.2116
742.7323 13372.2691
total
13372.2691

output
V*
kmol
0.0000
0.0852
286.9302
287.0154

B*
kg
kmol
kg
0.0000
0.0000
0.0000
2.7272
0.1353
4.3302
5164.7435 455.5816 8200.4681
5167.4707 455.7169
8204.7984
13372.2691

REBOILER -02
T =
P =

111.76 oC =
1.50 atm

384.91 K
1140.304 mmHg

Panas keluar dari bottom Rb-02, Qout RB2


Qout RB2 =

1357949.8174

Panas Sensibel Vapor yang keluar, Q


Komponen

CH3OCH3
CH3OH
H2O
Total

n
0.0000
0.0852
286.9302
287.0154

Cp
6773.7289
4394.8370
2979.3899

Q
0.0000
374.5547
854876.9169
855251.4716

Panas Laten Vapor yang keluar, QLv


Lvc = Lvb*(((Tc-T)/(Tc-Tb))^0,38)

Komponen
CH3OCH3
CH3OH
H2O

Tc
400.0000
512.6000
647.3000

Tb
248.2500
337.7500
373.1500
Total

Lvb
21520.0000
35278.0000
40683.0000

Cp
6773.7289
4394.8370
2979.3899

Q
0.0000
969.2646
2212232.0245
2213201.2890

Panas masuk Rb-02,Q.


Komponen

CH3OCH3
CH3OH
H2O
Total

n
0.0000
0.2205
742.5118
742.7323

Beban Panas Reboiler, QRb :


QRb=Qd+Ql+Qb-Qin KD
QRb =
Qrb=

Q bottom KD-02 + Qd CD-03 + Q CD-03 - Qin KD-02


10157419.6177

Fluida panas yang digunakan adalah saturated steam pada T = 150 oC


Hg =
Hliq =

2745.4 KJ/Kg
632.1 KJ/Kg

Lvc
8952.7999
31306.5914
40011.0464

Jumlah steam yang diperlukan :


m = Q serap / (Hg - H liq)
kg
m=
4806.4258

267.0237 mol

Panas steam yang masuk adalah :


Qsi = Hg . m
Qsi =
13195561.3583 kJ
Panas steam yang keluar:
Qso = H liq . m
Qso =
3038141.7406 Kj
Neraca Panas pada Reboiler-03

Q
Qsi

Total

Panas Masuk
2213201.2890 Qv
13195561.3583 QLv
QB
Qso
15408762.6473

Panas Keluar
855251.4716
10157419.6177
1357949.8174
3038141.7406
15408762.6473

n (kmol)
0.0000
0.0852
286.9302
287.0154

QLc
0.0000
2668.1378
11480377.2651
11483045.4030

Cooler -03 (C-03)


Fungsi : untuk mendinginkan aliran produk keluar dari ACC-02
Input : panas sensibel keluar dari ACC-02
T ref =
T =
Komponen
CH3OCH3
CH3OH
H2O
Total

25
65

oC =
oC =

Kmol
0.4533
135.1848
0.4560
136.0941

298.15
337.85

CpdT (Kj/kmol)
2837.1057
1864.4982
1348.1194

K
K

Qh (kj)
1285.9329
252051.8165
614.7931
253952.5426

Output: Panas sensibel keluar dari Cooler

T ref =
T=
Komponen
CH3OCH3
CH3OH
H2O
Total

25
30

oC
oC

n (Kmol)
0.4533
135.1848
0.4560
136.0941

298.15
303.15
CpdT (Kj/kmol)
332.1876
221.1775
168.4801

K
K

Qout (kj)
150.5657
29899.8423
76.8333
30127.2413

Panas kerja C-02 (Q duty C-01)


Q duty = Q sensible in - Q sensible out
Q duty =
T air in =
T air out =
Tref =

223825.3013 kJ
30
50
25

oC =
oC =
oC =

303.15
323.15
298.15

oK
oK
oK

Cp air didapat dari tabel 2.355 ferry ^_^


CP air =

4.1799 kj/(kg.K)

maka kapasitas air yang dibutuhkan =


Panas air yang masuk =
Qw in
Komponen

kg

2677.4002 kg
30

CpdT (Kj/kmol)

oC =

303.15

Q (kj)

H2O

2677.4002

Qw out
Panas air yang keluar =
Komponen
H2O

kg
2677.4002

4.1799

50
CpdT (Kj/kmol)
4.1799

55956.3253

oC

Qw in

323.15
Q (kj)
279781.6266 Qw out

Neraca Panas pada Cooler-03 (C-03)

Panas masuk
Panas Keluar
Q sensibel in =253952.5426 Q sensibel out =
30127.2413
Q air in =
55956.3253 Q air out =
279781.6266
Total
309908.8679
309908.8679

Komponen
CH3OCH3
CH3OH
H2O
cp =

A
17.0150
21.1520
32.2430

B
0.1791
0.0709
0.0019

C
-0.0001
0.0000
0.0000

D
0.0000
0.0000
0.0000

cpVAPA + cpVAPB*T + cpVAPC*T^2 + cpVAPD*T^3

KOLOM DESTILASI-02 (KD-02)


Fungsi : Tempat untuk memisahkan Methanol dengan Air

Komposisi Feed KD-02


Komponen
CH3OCH3
CH3OH
H2O
TOTAL

kmol
0.4533
135.3201
456.0376
591.8110

kg
20.8497
4330.2438
8208.6768
12559.7704

Fraksi mol, Xi
0.0008
0.2287
0.7706
1.0000

Konstanta Tekanan Uap murni Komponen


(Data Physical Properties From: Coulson & Richardson's Chemical Engineering Vol 6, Appendix C)

Komponen
CH3OCH3
CH3OH
H2O
Pi* = EXP (A-(B/(T+C)))
komponen
CH3OCH3
CH3OH
H2O
TOTAL
P =
T =

A
16.8467
18.5875
18.3036

Konstanta Antoine
B
C
2361.4400
-17.1000
3626.5500
-34.2900
3816.4400
-46.1300

Titik Didih
-24.9000
64.6000
100.000

Xi
0.0008
0.2287
0.7706
1.0000

Pi (mmHg)
24842.2687
2265.7926
634.4717

Ki (Pi/P)
24.2127
2.2084
0.6184

Yi = (Ki . Xi)
0.0185
0.5050
0.4765
1.0000

1.3500
95.1705

atm
oC

=
=

1026.0000
368.1705

ditetapkan
light key = CH3OH
heavy key = H2O
reference = H2O
komponen
CH3OCH3
CH3OH
H2O

Ki
24.2127
2.2084
0.6184

diinginkan distribusi komponen kunci

= (Ki/Kref)
39.1543
3.5711
1.0000

99,9% =

komponen light key


LK(CH3OH) D =
LK (CH3OH) B =

log
1.5928
0.5528
0.0000
0.999
0.001

135.1848
0.1353

LOG (CH3OH)D / (CH3OH)B =


komponen heavy key
HK (H2O) D =
HK (H2O) B =

2.9996

0.4560
455.5816

LOG (CH3OH)D / (CH3OH)B =


komponen
CH3OH
H2O
TOTAL

Kref
0.6184
0.6184
0.6184

X = log ik
0.5528
0.0000
0.5528

-2.9996
Y = log iD/iB
2.9996
-2.9996
0.0000

X.Y
1.6582
0.0000
1.6582

X^2
0.3056
0.0000
0.3056

dibuat persamaan garis lurus Y = aX + b


a (slope) =
b (intersept) =

10.8521
-2.9996

{(n x XY)-(X x Y)} /{n x X2)-(X)2}


{Y - (a x X)}/2

maka untuk setiap komponen


komponen
CH3OCH3
CH3OH
H2O

X = log ik
1.5928
0.5528
0.0000

Y = log iD/iB
14.2854
2.9996
-2.9996

kondisi top dew point KD - 03


komponen
CH3OCH3
CH3OH
H2O
Total

kmol

0.4533
135.1848
0.4560
136.0941

Xi
0.0033
0.9933
0.0034
1.0000

kondisi bottom bubble point KD - 03

iD/iB
192949714321756.0000
999.0000
0.0010

B (kmol)
0.0000
0.1353
455.5816

komponen
CH3OCH3
CH3OH
H2O
Total

kmol
0.0000
0.1353
455.5816
455.7169

Xi
0.0000
0.0003
0.9997
1.0000

top distilation trial n error


komponen
CH3OCH3
CH3OH
H2O
Total

BM
46.0000
32.0000
18.0000

kmol
0.4533
135.1848
0.4560
136.0941

kg
20.8497
4325.9135
8.2087
4354.9720

Yi
0.0033
0.9933
0.0034
1.0000

1.0000
64.698

atm
C

760.0000
337.8484

mmHg
K

BM
46.0000
32.0000
18.0000

kmol
0.0000
0.1353
455.5816
455.7169

kg
0.0000
4.3302
8200.4681
8204.7984

Xi
0.0000
0.0003
0.9997
1.0000

1.5004
111.7560

atm
C

1140.3040
384.9060

mmHg
K

P=
T=
bottom distillation trial n error
komponen
CH3OCH3
CH3OH
H2O
Total
P=
T=

Neraca massa KD-02


input
Komponen
CH3OCH3
CH3OH
H2O
Total

kmol

output
kg

0.4533
20.8497
135.3201
4330.2438
456.0376
8208.6768
591.8110
12559.7704
12559.7704

top
kmol
0.4533
135.1848
0.4560
136.0941

kg
20.8497
4325.9135
8.2087
4354.9720
12559.7704

D-02)

mmHg
K

D (kmol)
0.4533
135.1848
0.4560

A
16.8467
18.5875
18.3036

B
2361.4400
3626.5500
3816.4400

C
-17.1000
-34.2900
-46.1300

A
16.8467
18.5875
18.3036

B
2361.4400
3626.5500
3816.4400

C
-17.1000
-34.2900
-46.1300

Pi* = EXP (A-(B/(T+C)))


Pi
Ki
13153.1727
17.3068
765.6342
1.0074
185.1160
0.2436

Pi
33737.2908
3805.2359
1139.3595

output
bottom
kmol
kg
0.0000
0.0000
0.1353
4.3302
455.5816 8200.4681
455.7169 8204.7984
12559.7704

0.004787571
0.993327531
0.653569022

Ki
29.5862
3.3370
0.9992

Xi = Yi/Ki
0.0002
0.9860
0.0138
1.000

Yi=Xi.Ki
0.0000
0.0010
0.9989
0.99987

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