DAFTAR ISI

Halaman
Halaman Judul..................................................................................................
i
Halaman Pengesahan
ii
Kata Pengantar.................................................................................................. iii
Abstrak/Abstract
v
Daftar isi ........................................................................................................... vi
Daftar Tabel...................................................................................................... viii
Daftar Gambar..................................................................................................
ix
Lampiran
x
BAB I PENDAHULUAN
1.1 Latar Belakang......................................................................................
1.2 Rumusan Masalah ................................................................................
1.3 Tujuan Penelitian..................................................................................
1.4 Manfaat Penelitian ...............................................................................
BAB II
2.1
2.2
2.3
2.4
2.5
2.6
2.7
2.8
2.9
2.10

TINJAUAN KEPUSTAKAAN
Biodisel..............................................................................................
Syarat Mutu Biodisel.........................................................................
Metode Pemurnian Biodisel ..............................................................
Membran............................................................................................
Membran Adsorpsi ............................................................................
Adsorpsi.............................................................................................
Adsorben............................................................................................
Purolit.................................................................................................
Khitosan.............................................................................................
Titrasi.................................................................................................

BAB III METODELOGI PERCOBAAN

3.1. Tempat Dan Waktu Penelitian ...........................................................
3.2. Alat Dan Bahan..................................................................................
3.3. Prosedur Kerja ...................................................................................
3.3.1. Pembuatan Larutan...................................................................
3.3.2. Standarisasi Larutan.................................................................
3.3.3. Pembuatan Membran Khitosan Murni.....................................
3.3.4. Pembuatan Membran Adsorpsi ...............................................
3.3.5. Karakterisasi Membran.............................................................
3.3.6. Pemurnian Biodiesel dengan Metode Batch.............................
3.4. Analisis Kadar Gliserol Total (FBI-A02-03)......................................
BAB IV

1
3
3
4
5
5
7
8
9
10
11
12
13
14
15
15
15
15
16
17
17
18
19
20

HASIL DAN PEMBAHASAN

4.1. Pembuatan Membran Adsorpsi Purolit........................................ 22
vi

4.2. Adsorpsi Gliserol Total Dalam Biodiesel.....................................25

4.3. Regenerasi Membran Khitosan Murni dan Membran Adsorpsi
Purolit.......................................................................................... 27
BAB V

PENUTUP
5.1. Kesimpulan ...............................................................................30
5.2. Saran ........................................................................................30

DAFTAR PUSTAKA
LAMPIRAN

vii

DAFTAR TABEL

Halaman
Tabel
Tabel
Tabel
Tabel

2.1
2.2
2.3
4.1

Persyaratan kualitas biodiesel menurut SNI-04-7182-2006. ......

6
Fitur Dasar Purolit ...................................................................... 13
Sifat Fisik dan Kimia Purolit ...................................................... 13
Hasil karakterisasi porositas, derajat pengembangan dan ketebalan
membran adsorpsi purolit dan membran murni........................... 25

viii

DAFTAR GAMBAR

Halaman
Gambar 2.1
Gambar 2.2
Gambar 2.3
Gambar 2.4
Gambar 4.1
Gambar 4.2
Gambar 4.3
Gambar 4.4
Gambar 4.5
Gambar 4.6

Membran Adsorpsi.................................................................... 10
Proses Adsorpsi......................................................................... 11
Struktur Purolit.......................................................................... 12
Struktur khitosan....................................................................... 14
Membran adsorpsi purolit......................................................... 23
Morfologi partikel purolit yang dikarakterisasi dengan
menggunakan SEM (A). Komposisi partikel purolit yang
dikarakterisasi dengan menggunakan SEM-EDX (B).............. 24
Morfologi membran adsorpsi purolit yang dikarakterisasi dengan
menggunakan SEM. Morfologi penampang melintang membran
purolit (A). Morfologi permukaan atas membran purolit (B)..
24
Grafik pengaruh waktu kontak terhadap adsorpsi gliserol total. 26
Perbedaan gliserol total pada biodiesel dengan menggunakan
membran adsorpsi purolit yang sebelum dan sesudah
diregenerasi..............................................................................
28
Perbedaan gliserol pada biodiesel dengan menggunakan membran
murni khitosan yang sebelum dan sesudah diregenerasi.........
29

ix

DAFTAR LAMPIRAN

Halaman
Lampiran 1 Skema Kerja. ..............................................................................

34

Lampiran 2 Jadwal Pelaksanaan Penelitian....................................................

39

Lampiran 3 Rincian Dana Penelitian..............................................................

40

Lampiran 4 Perhitungan..................................................................................

41

Lampiran 5 Foto Kegiatan..............................................................................

50