Lampiran C2

C.
Hubungan Indeks Bias Campuran Terhadap Fraksi Mol Metanol

Tabel C.7 Hubungan indeks bias dengan fraksi mol metanol
Komposisi
Botol
ke1
2
3
4
5
6
7
8
9
10
11
Volume
aquadest
(ml)
10
9
8
7
6
5
4
3
2
1
0
Volume
metanol
(ml)
0
1
2
3
4
5
6
7
8
9
10
A
(gram)
6,447
6,434
6,153
6,479
6,451
6,073
6,419
6,449
6,329
6,47
6,357
B
(gram)
16,208
15,131
13,904
13,194
12,27
10,816
10,238
9,283
8,184
7,333
6,357
Massa
Aquadest
Mol
Aquadest
9,761
8,697
7,751
6,715
5,819
4,743
3,819
2,834
1,855
0,863
0
Keterangan : A= Massa botol kosong

B= Massa botol + aquadest
C= Massa botol + aquadest + metanol
Mr aquadest =18 g/mol
Mr metanol = 32 g/mol
0,5423
0,4832
0,4306
0,3731
0,3233
0,2635
0,2122
0,1574
0,1031
0,0479
0
C
(gram)
16,208
15,82
15,664
15,466
15,268
14,894
14,808
14,624
14,289
13,583
13,449
Massa
Metanol
0
0,689
1,760
2,272
2,998
4,078
4,570
5,341
6,105
6,250
7,092
Mol
Metanol
0
0,0215
0,0549
0,0709
0,0936
0,1273
0,1426
0,1667
0,1905
0,1951
0,2213
Fraksi
Mol
Metanol
0
0,04
0,11
0,16
0,22
0,33
0,40
0,51
0,65
0,80
1,00
Indeks Bias Campuran

1
1,3350
1,3365
1,3390
1,3406
1,3421
1,3426
1,3426
1,3411
1,3390
1,3340
1,3285
1,3350
1,3365
1,3390
1,3406
1,3421
1,3426
1,3421
1,3411
1,3385
1,3340
1,3285
1,3350
1,3365
1,3390
1,3405
1,3421
1,3426
1,3421
1,3411
1,3385
1,3340
1,3285
Indeks
Bias
Rata-rata
Indeks
Bias
Koreksi
1,3350
1,3365
1,3390
1,3405
1,3421
1,3426
1,3422
1,3411
1,3387
1,3340
1,3285
1,3300
1,3315
1,3340
1,3355
1,3370
1,3375
1,3371
1,3360
1,3336
1,3290
1,3236
(indeks bias)
0.0
0.1
0.2
0.3
0.4
0.5
Fraksi mol metanol
0.6
0.7
0.8
0.9
1.0
Gambar C.4 Kurva Hubungan Indeks Bias Campuran Terhadap Fraksi Mol Metanol
C.7
Penentuan Relative Volatility

C.7.1 Penentuan Relative Volatility Distilat
Tabel C.8 Relative volatility distilat
t
(menit)
Suhu (C)
Massa
botol
kosong
(gram)
Massa
botol +
distilat
(gram)
Massa
distilat
(gram)
Jumlah
(gram)
67,609
72,569
4,96
391,95
9
Percobaa
n
Koreksi
Ratarata
10
64
65,961
57,410
5
20
61
62,82
67,609
76,987
9,378
30
63
64,914
67,609
73,689
6,08
40
61
62,82
67,609
75,358
7,749
50
62
63,867
67,609
78,27
10,661
60
49
50,256
67,609
75,612
8,003
70
60
61,773
67,609
89,928
22,319
80
60
61,773
67,609
73,118
90
52
53,397
67,609
100
50
51,303
110
54
55,491
Indeks bias
X metanol
Rata-rata
Koreksi
Kurva
1,331
1,33
1,331
1,33066
7
1,325699
0,92
1,330
5
1,329
5
1,328
5
1,330
5
1,329
5
1,3305
1,3305
1,325534
0,93
1,329
1,3285
1,329
1,33
1,329
1,328
5
1,328
5
1,328
5
1,328
5
5,509
1,33
1,331
1,3285
77,981
10,372
1,329
1,329
1,328
67,609
73,721
6,112
1,33
1,329
1,33
67,609
83,049
15,44
1,33
1,331
1,331
1,32966
7
1,32866
7
1,32933
3
1,324711
0,96
1,323723
0,995
1,324381
0,97
1,3285
1,3285
1,323558
0,998
1,3285
1,3285
1,323558
0,998
1,324875
0,955
1,323723
0,995
1,324711
0,96
1,325699
0,92
1,33
1,32983
3
1,32866
7
1,32966
7
1,33066
Y
metano
l
0,97
1,1326
Ratarata
0,9662
7
1,329
5
1,330
5
120
52
53,397
67,609
85,936
18,327
130
50
51,303
67,609
84,731
17,122
140
53
54,444
67,609
104,692
37,083
1,329
150
54
55,491
67,609
127,463
59,854
1,33
160
52
53,397
67,609
145,476
77,867
170
53
54,444
67,609
122,745
55,136
180
55
56,538
67,609
87,596
19,987
1,329
5
1,328
5
1,328
1,329
5
1,330
5
1,329
5
1,3295
1,3295
1,324546
0,965
1,3305
1,3305
1,325534
0,93
1,324217
0,975
1,324875
0,955
1,324217
0,975
1,323887
0,99
1,322735
0,999
8
1,329
1,331
1,3285
1,329
1,329
1,329
1,329
1,327
1,328
1,32916
7
1,32983
3
1,32916
7
1,32883
3
1,32766
7
Rata-rata
1,324455
C.7.2 Penentuan Relative Volatility Bottom

Tabel C.9 Relative volatility bottom
Massa
botol
kosong
(gram)
Suhu (C)
t
(menit
)
Percobaan
Koreks
i
10
75
77,478
20
75
30
76
Massa
botol +
distilat
(gram)
Massa
distilat
(gram)
Jumlah
(gram)
Ratarata
79,8628
83,444
Indeks bias
Rata-rata
1,34
1,341
1,34
1,340333
83,04
90,022
6,982
77,478
83,04
88,006
4,966
1,3416
1,3415
1,3415
1,341533
78,525
83,04
89,533
6,493
1,3426
1,3425
1,3426
1,342567
X metanol
Koreksi
1,33524
9
1,33643
5
1,33745
Kurva
0,155
0,19
0,31
Y
metano
l
0,64
5,5769
Ratarata
0,2417
40
78
80,619
83,04
88,3
5,26
1,3421
1,3422
1,3421
1,342133
50
78
80,619
83,04
86,375
3,335
1,3426
1,3425
1,3426
1,342567
60
70
72,243
83,04
88,857
5,817
1,3426
1,3426
1,3426
1,3426
70
77
79,572
83,04
88,146
5,106
1,3421
1,3423
1,342
1,342133
80
78
80,619
83,04
88,421
5,381
1,343
1,3428
1,343
1,342933
90
80
82,713
83,04
92,229
9,189
1,3421
1,342
1,3421
1,342067
100
79
81,666
83,04
86,955
3,915
1,3421
1,3429
1,3429
1,342633
110
80
82,713
83,04
87,509
4,469
1,34
1,342
1,34
1,340667
120
76
78,525
83,04
84,136
1,096
1,341
1,34
1,34
1,340333
130
77
79,572
83,04
84,121
1,081
1,339
1,3385
1,3385
1,338667
140
75
77,478
83,04
85,359
2,319
1,346
1,3445
1,3445
1,345
150
73
75,384
83,04
86,751
3,711
1,343
1,3428
1,343
1,342933
160
81
83,76
83,04
85,479
2,439
1,3421
1,342
1,3421
1,342067
170
82
84,807
83,04
88,432
5,392
1,3428
1,3428
1,3428
1,3428
180
81
83,76
83,04
89,533
6,493
1,342
1,342
1,341
1,341667
Rata-rata
6
1,33702
8
1,33745
6
1,33748
9
1,33702
8
1,33781
8
1,33696
2
1,33752
2
1,33557
9
1,33524
9
1,33360
3
1,33986
1,33781
8
1,33696
2
1,33768
6
1,33656
7
1,33687
6
0,22
0,31
0,33
0,22
0,29
0,22
0,33
0,163
0,15
0,12
0,333
0,29
0,22
0,3
0,2
C.7.3 Penentuan Relative Volatility Kolom 3

Tabel C.10 Relative volatility kolom 3
t
(menit
)
Suhu (C)
Ratarata
Massa
botol
koson
g
(gram)
6,409
6,409
6,409
Massa
botol +
distilat
(gram)
Massa
distila
t
(gram)
9,733
11,237
8,434
3,324
4,828
2,025
Percobaa
n
Koreksi
10
20
30
74
65
65
76,431
67,008
67,008
40
64
65,961
6,409
8,011
50
65
67,008
6,409
60
61
62,82
70
67
80
Jumla
h
(gram)
Indeks bias
X metanol
Rata-rata
Koreksi
Kurva
1,33
1,33
1,33
1,33
1,33
1,33
1,33
1,33
1,33
1,32504
1,32504
1,32504
0,945
0,945
0,945
1,602
1,3295
1,3295
1,33
1,324711
0,96
8,555
2,146
1,33
1,33
1,33
7,703
1,294
1,3365
1,337
1,3365
69,102
6,409
8,933
2,524
1,332
1,332
1,331
65
67,008
6,409
8,248
1,839
1,334
1,333
1,334
90
67
69,102
6,409
8,524
2,115
1,3340
1
1,334
1,334
100
68
70,149
6,409
8,152
1,743
1,339
1,339
1,339
110
68
70,149
6,409
8,078
1,669
1,337
1,337
1,3369
120
61
62,82
6,409
8,021
1,612
1,338
1,3375
1,3375
130
64
65,961
6,409
8,213
1,804
1,33
1,335
1,335
140
60
61,773
6,409
8,413
2,004
1,34
1,339
1,339
1,32504
1,33162
7
1,32668
7
1,32866
3
1,32899
5
1,33393
2
1,33192
3
1,33261
5
1,32833
3
1,33426
0,945
6,409
1,33
1,33
1,33
1,32966
7
1,33
1,33666
7
1,33166
7
1,33366
7
1,33400
3
67,298
8
38,959
1,339
1,33696
7
1,33766
7
1,33333
3
1,33933
0,72
0,84
0,818
0,8
0,638
0,718
0,69
0,838
0,66
Y
metanol
0,93
2,6635
Ratarata
0,833
150
61
62,82
6,409
8,529
2,12
1,334
1,333
1,334
160
66
68,055
6,409
8,971
2,562
1,33
1,33
1,331
170
67
69,102
6,409
8,023
1,614
1,332
1,331
1,331
180
67
69,102
6,409
8,543
2,134
1,333
1,333
1,333
3
1,33366
7
1,33033
3
1,33133
3
1,333
Rata-rata
1
1,32866
3
1,32536
9
1,32635
7
1,32800
4
1,32835
0,818
0,94
0,955
0,819

Massa
botol
koson
g
(gram)
Suhu (C)
t
(menit
)
Percobaa
n
Koreksi
10
68
70,149
20
64
30
Ratarata
64,797
7
Massa
botol +
distilat
(gram)
Massa
distila
t
(gram)
Jumla
h
(gram)
44,403
Indeks bias
1,3341
1,334
1,334
6,395
8,812
2,417
65,961
6,395
9,952
3,557
1,3355
63
64,914
6,395
7,994
1,599
1,3285
40
63
64,914
6,395
8,318
1,923
1,328
50
63
64,914
6,395
8,292
1,897
1,3285
1,338
7
1,328
5
1,328
5
1,328
1,3355
1,329
1,328
1,3285
Rata-rata
1,33403
3
1,33656
7
1,32866
7
1,32816
7
1,32833
X metanol
Koreksi
Kurva
1,329025
0,8
1,331528
0,722
1,323723
0,995
1,323229
1,323393
0,999
8
0,999
Ratarata
0,8974
Y
metano
l
0,95
2,1732
3
60
58
59,679
6,395
7,288
0,893
1,3295
70
63
64,914
6,395
7,712
1,317
1,33
1,329
5
1,33
80
64
65,961
6,395
9,143
2,748
1,331
1,331
1,333
90
64
65,961
6,395
10,015
3,62
1,332
1,331
1,332
100
64
65,961
6,395
9,736
3,341
1,3325
110
64
65,961
6,395
9,609
3,214
1,3325
120
60
61,773
6,395
9,127
2,732
1,3325
130
62
63,867
6,395
9,111
2,716
1,3325
140
60
61,773
6,395
9,581
3,186
1,3325
150
59
60,726
6,395
8,987
2,592
1,3325
1,334
5
1,331
160
64
65,961
6,395
8,544
2,149
1,3325
1,329
1,3295
170
65
67,008
6,395
8,459
2,064
1,3325
1,33
1,33
180
64
65,961
6,395
8,833
2,438
1,3325
1,333
1,333
1,332
5
1,330
5
1,330
5
1,321
1,3295
1,3295
1,324546
0,965
1,33
1,33
1,33166
7
1,33166
7
1,33243
3
1,32504
0,954
1,326687
0,84
1,326687
0,818
1,327444
0,86
1,326127
0,91
1,331167 1,326193
0,89
1,3323
1,3303
1,3305
1,32
1,3345
1,331
1,3311
1,3245
1,33383
3
1,3315
1,33033
3
1,33083
3
1,33283
3
Rata-rata

1,319606
0,999
9
1,328827
0,818
1,326522
0,89
1,325369
0,93
1,325863
0,918
1,327839
0,843
1,32598
t
(menit
)
Suhu (C)
Ratarata
63,169
Massa
botol
kosong
(gram)
Massa
botol +
distilat
(gram)
Massa
distila
t
(gram
)
6,38
7,708
1,328
Percobaan
Koreksi
10
64
65,961
20
62
63,867
6,38
7,367
30
63
64,914
6,38
40
62
63,867
50
62
60
Jumla
h
(gram)
Indeks bias
X metanol
Rata-rata
1,329
1,329
1,329
1,329
0,987
1,329
1,33
1,329
1,329333
7,712
1,332
1,3273
1,3275
1,327433
6,38
8,491
2,111
1,328
1,328
1,327967
63,867
6,38
7,394
1,014
1,3275
1,3275
1,327533
55
56,538
6,38
8,838
2,458
1,3280
1,3281
1,328067
70
61
62,82
6,38
6,758
0,378
1,329
1,3292
1,3289
80
63
64,914
6,38
7,586
1,206
1,339
1,339
1,339
1,339
90
63
64,914
6,38
7,256
0,876
1,329
1,329
1,329
1,329
100
62
63,867
6,38
6,826
0,446
1,33
1,33
1,329667
110
62
63,867
6,38
9,177
2,797
1,3285
1,3285
1,3285
120
59
60,726
6,38
8,513
2,133
1,329
1,3295
1,329333
130
61
62,82
6,38
8,436
2,056
1,33
1,329
1,328
5
1,329
5
1,33
1,33
1,33
140
58
59,679
6,38
9,712
3,332
1,331
1,331
1,331
1,331
150
57
58,632
6,38
8,132
1,752
1,329
1,329
1,329
1,329
160
63
64,914
6,38
7,359
0,979
1,327
1,327
1,3272
1,327133
27,029
1,327
5
1,327
9
1,327
6
1,328
1
1,328
5
Koreksi
Kurva
1,32405
2
1,32438
1
1,32250
4
1,32303
1
1,32260
3
0,9999
1,32313
0,9999
0,98
0,983
0,9998
0,9998
1,32395
0,985
3
1,33393
0,64
2
1,32405
0,98
2
1,324711 0,96
1,32355
0,998
8
1,32438
0,97
1
1,32504 0,955
1,32602
0,91
8
1,32405
0,98
2
1,32220 0,9998
Ratarata
0,962
2
Y
metano
l
0,98
1,9238
2
170
64
65,961
6,38
7,288
0,908
1,329
1,329
1,329
1,329
180
63
64,914
6,38
7,316
0,936
1,328
1,328
1,3285
1,328167
Rata-rata
8
1,32405
2
1,32322
9
1,32438
3
0,98
0,9998

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C.

Hubungan Indeks Bias Campuran Terhadap Fraksi Mol Metanol

Keterangan : A= Massa botol kosong

Indeks Bias Campuran

Fraksi mol metanol

Penentuan Relative Volatility

C.7.2 Penentuan Relative Volatility Bottom

C.7.3 Penentuan Relative Volatility Kolom 3

C.7.4 Penentuan Relative Volatility Kolom 5

C.7.5 Penentuan Relative Volatility Kolom 8

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