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DYAN HATINING AYU SUDARNI

2314201001

DISPERSI

t, min
Cpulse, gm/liter

10

15

20

25

Catatan : modelkan dengan Tangki seri dan Dispersi dan menentukan parameter denga
fitting dan grafik
Mencari waktu tinggal rata-rata ( )

15 min

47.5 min
Area ( C )
100 gm. min/liter
t, min
E, area
E, exp

0.00
0.00
0.00
0.00

5.00
0.03
0.45
0.33

10.00
0.05
0.75
0.67

15.00
0.05
0.75
1.00

20.00
0.04
0.60
1.33

25.00
0.02
0.30
1.67

A. Metoda Grafis
0.80
0.70
0.60
0.50
E

0.40

2(2 /)

0.30
0.20
0.10
0.00
-0.20 0.00

0.20

0.40

0.60

0.80

1.00

1.20

E max = 0,79
Point of Infection = 0,61 x E max = 0,4819
Pada saat 0,61 E max, = 0,38 dan 1,425
2(2 /)

1.045

0.1365031

1.40

1.60

1.80

2.00

2.2

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2314201001

DISPERSI

B. Metoda Fitting Parameter


t, min
Cpulse, gm/liter

10

15

20

25

10.000
0.050
0.750
0.667
0.636
0.114
0.013

15.000
0.050
0.750
1.000
0.791
-0.041
0.002

20.000
0.040
0.600
1.333
0.636
-0.036
0.001

25.000
0.020
0.300
1.667
0.330
-0.030
0.001

Mencari waktu tinggal rata-rata ( )

15 min

47.5 min
Area ( C )
100 gm. min/liter
Trail

0.1271125

t, min
E, area
E, exp

E, mdel
Error, E

0.000
0.000
0.000
0.000
0.111
-0.111
0.012

5.000
0.030
0.450
0.333
0.330
0.120
0.014

0.8
0.7
0.6
0.5
E

0.4

E, mdel

0.3

E, exp

0.2
0.1
0
0.2
-0.2

1
0.6

1.8
1.4

2.2

DYAN HATINING AYU SUDARNI


2314201001

DISPERSI

A R
t, min
C, (mol.L)
Area ( C )
E, area
35 E, exp

30
1

30.00
0.01
0.15
2.00

2.00

2.20

0
1
2.5
3
4
5
6
0
1.2
7
8.6
9.5
8
6.2
0
1.2
10.5
4.3
9.5
8
6.2
0 0.02388 0.1393 0.1711 0.1891 0.1592 0.1234
0 0.00514
0.03 0.0368 0.0407 0.0342 0.0265

arameter dengan metode

1.80

-ra = 0,05 Ca

35.00
0.00
0.00
2.33

2.40

Mencari waktu tinggal rata-rata (


C
47.80

4.65 min
t2 C
1245.28 min
26.05 min

Area tot
50.25 mol. min/liter

DYAN HATINING AYU SUDARNI


2314201001

30

35

30.000
0.010
0.150
2.000
0.111
0.039
0.002

35.000
0.000
0.000
2.333
0.024
-0.024
0.001
0.046

DISPERSI

DYAN HATINING AYU SUDARNI


2314201001

7.5
9
10
12
3.7
2
1.2
0.4
5.55
3
1.2
0.8
0.0736 0.0398 0.0239 0.008
0.0158 0.0086 0.0051 0.0017

DISPERSI

15
0
0
0
0

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2314201001

DISPERSI

DYAN HATINING AYU SUDARNI


2314201001

t, min
Cpulse, gm/liter

TANGKI SERI

10

15

20

25

Catatan : modelkan dengan Tangki seri dan Dispersi dan menentukan parameter dengan
metode fitting dan grafik
Mencari waktu tinggal rata-rata
( )

15 min

47.5 min
Area ( C )
100 gm. min/liter
t, min
E, area
E, exp

0.00
0.00
0.00
0.00

5.00
0.03
0.45
0.33

10.00
0.05
0.75
0.67

15.00
0.05
0.75
1.00

20.00
0.04
0.60
1.33

25.00
0.02
0.30
1.67

A. Metoda Grafis
0.80
0.70
0.60
0.50
E

0.40
0.30

/_ = 2/( 1)

0.20
0.10
0.00
-0.20 0.00

0.20

0.40

0.60

0.80

1.00

1.20

E max = 0,78
Point of Infection = 0,55 x E max = 0,429 (Asumsi N=4)
Pada saat 0,61 E max, = 0,29 dan 1,56
/_ = 2/( 1)
=
N

1.27
3.480005

1.40

1.60

1.80

2.00

2.20

2.4

DYAN HATINING AYU SUDARNI


2314201001

TANGKI SERI

B. Metoda Fitting Parameter


t, min
Cpulse, gm/liter

10

15

20

25

Mencari waktu tinggal rata-rata


( )

15 min

47.5 min
Area ( C )
100 gm. min/liter
Trail N

( N ) N 1
E ( N t i ) * E N
exp( N )
( N 1)!

3.03138

t, min
E, area
E, exp

E, mdel
Error, E

0.000
0.000
0.000
0.000
0.000
0.000
0.000

5.000
0.030
0.450
0.333
0.564
-0.114
0.013

10.000
0.050
0.750
0.667
0.839
-0.089
0.008

15.000
0.050
0.750
1.000
0.696
0.054
0.003

E, mdel

20.000
0.040
0.600
1.333
0.454
0.146
0.021

25.000
0.020
0.300
1.667
0.260
0.040
0.002

E, exp

0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
0.2
-0.2

1.8

0.6

1.4

2.2

DYAN HATINING AYU SUDARNI


2314201001

30

35

n parameter dengan

30.00
0.01
0.15
2.00

1.80

2.00

2.20

35.00
0.00
0.00
2.33

2.40

TANGKI SERI

DYAN HATINING AYU SUDARNI


2314201001

30

35

=/

30.000
0.010
0.150
2.000
0.137
0.013
0.000

2.2

35.000
0.000
0.000
2.333
0.068
-0.068
0.005
0.051

TANGKI SERI

DYAN HATINING AYU SUDARNI


2314 201 001

EXAMPLE 14.2 (F)

Example 14.4 CSTR with Dead Space and Bypass


The elementary reaction
A+B
C+D

is to be carried out in the CSTR shown schematically in Figure 14-15. There is both bypassing and a st
region in this reactor. The tracer output for this reactor is shown in Table E14-4.1. The measured react

is 1.0 m3 and the flow rate to the reactor is 0.1 m3/min. The reactions rate constant is 0.28 m3/kmol.m
The feed is equimolar is A nad B with an entering concentration of A equal to 2.0 kmol/m3. Calculate t
conversion that can be expected in this reactor (Figure E.14-4.1)
Table E.14-4.1. Tracer Data
CT(mg/dm )
3

t (min)

1000
4

1333
8

1500
10

1666
14

1750
16

1800
18

the effluent trecer concentration is :

Diketahui

k
Cto
t (min)
CT exp
CT model
Error

Jadi

0.2036229
0.6908655

Trial

1 m3
0.1 m3/min
0.28 m3/kmol.min
2000 mol/m3
4
1000

8
1333

10
1500

14
1666

0.2036229
0.6908655
10

16
1750

18
1800

995.61525 1366.6388 1497.0473 1682.8399 1748.1429


1800
0.0043848 0.0252354 0.0019685 0.010108 0.0010612 2.33E-008
error
0.0427578

DYAN HATINING AYU SUDARNI


2314 201 001

bypassing and a stagnant


he measured reactor volume

is 0.28 m3/kmol.min.
mol/m3. Calculate the-

EXAMPLE 14.2 (F)