8188 Propafenone / Official Monographs
‘Table 3 (Cites)
SEI =
ium Husk isthe deaned, died seed coat (epidermis)
Separated by winnowing and thrashing from the seeds of
fi ote tak icone Bd
m, nda Paltu or spaghul, or ress Porogo.
arena Wai &'Ri (oes aha) Won
ommerce as Spanth or Heneh flan am
Pantaginoceoe), in whol on powdered form,
IDENTIFICATION
+ A. Mounted in esol, cells, viewed microscopically, are
composed of polygorial pramatc cells ang # -
Stfaight or Sighay wavy wall
* B_Mounted in alcohol and irrigated with water, viewed:
Iigroscopcaly, the mucage nthe outer pat ote
epidermal cells swells rapioy and goes ina solu0n.
impurtries. ;
* ARTICES Of BOTANICAL OmtciN, cidInsolible Ash (36M
NMT 10%Official Monographs / Ritonavir 8189
sree zi ual volumes of glycerin and alcohol: Add 35 mL of
see ae a solvent agi ve flask, me oer oe whe
7 atte itapoi vaste 15 bring the fqul level nto
[ee wetogel Mapping fash: Alow to sand for 13 min. Using
the neck oie os before, transfer the Wepped Ta-
the sine sopuate paper. Examine the papers at 30
rragneatio.
Acceptance criteria
Asa oyiur Husk: NME%OO insect fragments,
eg mes and psoeiss
Vue tam Huse MT 100 insect fragments, in-
Te Maing rites and psocids
TRAST perform ths test ina wel-ventlated hood « aetgBorameal Omar, Pesticide Residue Anais
erie 99cT01 g of Poylium Husk weighed to 0.1 9 AEG fees tne requemenis
accu
‘Transfer the Sample to 2 1000-mL. tall once
Mn nEn es tnbcmetinene prencuny 2d-— * BOTAMC CAMELS
Histology-—Husk: The epidermis is composed of large,
peer i a temperature of 24-26" and manta ts
tereeratore thoughout te test. Sr the husk or $5 tells having transparent wall iled with muclage, ahd
ePSjan it to sete while protecting the surface fom the cel swell apidly in aqueous mounts and appear
fans inthe hood. Remove the floating material wi a pobgoral to sightly rounded in a surface view when
Truce oF SOsmesh screen, and Wanster the mate Glewed from abave (rom below they appear clongated
Hee eran The sweling takes pace mainly ithe
ito a piece of titer paper in a dsh. Str the hu
Mla Bee Oe eases nove the fag tor Grestion. The muclage of the epidermal cals
rata aar and cone Hin re atrial Sains re wth ruthenium ean ead acetate TS
matt 26a eovedre nth no more motel 2P- seg Jonal stareh granules tha ae present in some
pape, Repeat ths reser he removed mata wth i oie epaermal cas id that may be ound ere
The paper na hod and then in an oven at 40" for 3 Sed in the muclage ae small and simple oF com-
in’cedlo room temperature. Wegh the fiter paper pounded nth four oF more components,
with the material Brush the material off the pape peace sym seed husk fis a pale to medium
Walgh the poper and then calculate te percentage of But colored powder having a sight pinkh tings and a
ore ccuacee etten bala marterste odor, Occasional single and 2- to
seer ce eritaras NM 596 seek cad starch granules, the individual grains be-
+ Oncanic InapuRITIES PROCEDURE 2: INSECT INFESTATION ing spheroidal plano to angular convex from 2-10 ym
Samples 25 1 Sn ter rt found embedded n the muclage. En-
Sample: 23-9 .- the Sample to a 250-ml beaker, add in darnscen eprermal cel ae filed with muclege
SufGent scent hexane to saturate, add an adeiional insurface view, the epidermal cells appear polygonal to
sufent slent exape 0 saturate add an eet) —_—_—sighty rounded. Muciag Hay ie elongated a
stghty Sa lead acetate TS, Some of te elongated and
‘min, string occasionally with a stirring rod, Wet 2
i peter Fectangular calls reptesenting the lower part of epider-
Trew’ of He paper with alcohol ana iter the mixture
sheet of tet paPecjum. Discard the filtrate. Transfer the ais and aso radlally swollen epidermal clls can
ise te the orginal beaker withthe ad of alcohol, found,
Tepaue tp the gia Boke wn es Bee, Meno amenaion TEs 1a abcd ee
jevel of the transferred residue. Boil for 10 min. Filter FED MICROORGANISMS (62): The total combined molds
‘rough alcohol wetted paper as above, Prepare ata aD Mets count does not exceed 1000 clue, and it
Ueeiaetng oe ab gata, nr me meg ecu ine for ver of Solem
‘conical flask into which is inserted a rubber disk sup nella species and Escherichia cof
pares gna nel od 2 gc « ReeB se perancal Ome, Total As (S61): NTL
sige tran the Height ofthe ask, the rod being 3.0% A
Kenge than the hight ofthe fas the tore and + GATE Derimmamion, Method (921): NMT. 12.0% |-~
ter to es the = in place, aie) che sk ‘being of | ° SWELL easy 5 lium Husk —
OF rape and size to prevent liquid in the body - of Ene
PP ram saliag when Its presed up against Sample arnser 250 ml of simulated intestinal fuid
ofthe fisk i Sealing Wher Pehe readue tothe saul enayes to giasestoppered S00-mL grad:
trap flask, completing the transfer with the aid of hot uated cylinder. Gradually, with shaking, add the Sample
water. Add sufficient hot water to bring the volume to until a uniform, smooth suspension is ‘obtained. Dilute
water, Add sufi ent not at enone aad Rake the ntl are uid to 900 mL Shake the cylinder for |
aoe ao tha the rubber dk shel vr aoe 5D rn for @ h. low the gel to settle for 16
above the liquid ep Rinse the rubber disk with hot niente Determine the volume of the gel
rater Spray the inside ofthe neck ofthe flask with a7 cep
antifoam /. Boil for 30 min, and cool to room tem- Powdered Psyllium Husk: NUT 40. ml/g —
yr S mB ‘Whole Psyllium Husk: NUT 35 tg"
ese a sol ove nag as oe
sure tng We fash and moving the td vetcaly ees ete
Lat Ua eae irs manages, — ‘ADOTIONE, :
wine cn, Awe ae leg AON Oe
dilow to stand for 20 min, Simultaneously rotate the fs, secured against insect attac
eres eee rom seed mater, nd tase fOr as
i Bae the neck of te task Prepare a sect of
fertraion by mortenng fh water and paca
Sa avacoum tunnel. Tarsfer the material trapped
fhe meek of the flask to the fiter with the aid of water.
the neck of tre ch'the paper with acohol to remove. DEFINITION, «
Hts, Pace the paper on a TOO-nm peti Renae Ort Soe
dish that has been wetted with a solution containing 110.0% of the labeled at
tains NUT 90.0% and NMT
of ritonavir (CorHaN.OsS:).