Afrizal Ahmad F.

(03)

Dinni Hayyu F.

(10)

Fitri Nurdian
(14)
Izudin Afnani
(16)

Data yang didapat pada saat

praktikum :
Massa Daun Cengkeh

= 2.000 Gram = 2 Kg

Volume Solvent (Etanol)

= 30 L = 30.000 ml

etanol

= 0.789 gram/ml
=xV

Massa Etanol

= 0.789 gram/ml x 30.000 ml

= 23.670 gram = 23,67 Kg
T steam

= 64C

Laju alir steam

= 405 ml/min

Massa pikno kosong

= 34,54 gram

Massa pikno + air

= 58.86 gram

Volume pikno

= (massa pikno+air) (massa pikno kosong) / air

= (58.86 gram - 34,54 gram)/1 gram/ml

= 24,32 ml
kondensat

= (59,10 gram 34,54 gram) / 24,32 ml

= 1,00986 gram/ml

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Siklus

Massa Pikno + Isi (gram)

Campuran (gram/ml)

54,32

0,813

54,07

0,803

54,06

0,803

54,05

0,802

53,92

0,797

53,72

0,789

53,67

0,789

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Perhitungan :
Siklus 1
Campuran

= 0,813 gram/ml

Eugenol

= 1,06 gram/ml

Fraksi massa etanol dalam sampel (y 1)

y1 . etanol + x1. Eugenol
y1 . 0,789 + (1- y1) . 1,06
0,789 y1 + 1,06 1,06 y1

= Campuran
= 0,813
= 0,813

0,271 y1 = 0,247
y1

= 0,9114

Fraksi massa eugenol dalam sampel (x 1)

x1 = 1 - y 1
= 0,089
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 Siklus 2 dan 3 :
Campuran

= 0,803 gram/ml

Eugenol

= 1,06 gram/ml

Fraksi massa etanol dalam sampel (y2)

y2 . etanol + x2. Eugenol

= Campuran

y2 . 0,789 + (1- y2) . 1,06

0,789 y2 + 1,06 1,06 y2

= 0,803
= 0,803

0,271 y2 = 0,257
y2

= 0,9483

Fraksi massa eugenol dalam sampel (x2)

x2 = 1 - y2
= 0,0517
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 Siklus 4 :
Campuran

= 0,802 gram/ml

Eugenol

= 1,06 gram/ml

Fraksi massa etanol dalam sampel (y4)

y4 . etanol + x4 . Eugenol

= Campuran

y4 . 0,789 + (1- y4) . 1,06

0,789 y4 + 1,06 1,06 y4

= 0,802
= 0,802

0,271 y4 = 0,258
y4

= 0,952

Fraksi massa eugenol dalam sampel (x4)

x4 = 1 - y4
= 0,048
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 Siklus 5 :
Campuran

= 0,797 gram/ml

Eugenol

= 1,06 gram/ml

Fraksi massa etanol dalam sampel (y5)

y5. etanol + x5 . Eugenol

= Campuran

y5 . 0,789 + (1- y5) . 1,06

0,789 y5 + 1,06 1,06 y5

= 0,797
= 0,797

0,271 y5 = 0,269
y5

= 0,993

Fraksi massa eugenol dalam sampel (x5)

x5 = 1 - y5
= 0,007
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 Siklus 6 dan 7 :
Campuran

= 0,789 gram/ml

Eugenol

= 1,06 gram/ml

Fraksi massa etanol dalam sampel (y6)

y6. etanol + x6 . Eugenol

= Campuran

y6 . 0,789 + (1- y6) . 1,06

0,789 y6 + 1,06 1,06 y6

= 0,789
= 0,789

0,271 y6 = 0,271
y6

=1

Fraksi massa eugenol dalam sampel (x6)

x6 = 1 - y6
= 0,00
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X = Fraksi massa eugenol dalam sampel

Y = Fraksi massa etanol dalam sampel
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 Residu (Crude Oil)

Campuran

= 1,013 gram/ml

Eugenol

= 1,06 gram/ml

Fraksi massa etanol dalam residu (yr)

yr. etanol + xr . Eugenol
yr . 0,789 + (1- yr) . 1,06

= Campuran
= 1,013

0,789 yr + 1,06 1,06 yr

0,271 yr

= 0,047

yr

= 0,173

= 1,013

Fraksi massa eugenol dalam residu (xr)

xr = 1 - yr
= 0,827
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Data yang didapat pada praktikum :

Feed
Massa pikno kosong

= 34.61 gram

Massa Pikno + air

= 59 gram

Volume Pikno

= (59 34.61) gram/ (1 gram/ml)

= 24.4 ml

Massa Pikno + Feed

= 58.25 gram

Densitas Feed

= (58.25-34.61) gram/ 24.4 ml

= 0.969 g/ml

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Data yang didapat pada praktikum :

Distilat
LAJU ALIR FEED
(L/H)

KONSENTRASI
(%)

MASSA PIKNO+ AIR

(gram)

DENSITAS DESTILAT
(gram/ml)

80

79

55.93

0.874

85

80

55.4

0.854

90

86

55.39

0.852

95

86.5

55.39

0.852

LAJU ALIR FEED

(L/H)

KONSENTRASI
(%)

MASSA PIKNO+ AIR

(gram)

DENSITAS BOTTOM
(gram/ml)

80

10

58.49

0.979

85

10

58.56

0.982

90

10

58.63

0.985

95

10

58.65

0.998

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Perhitungan :

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KURVA SIKLUS VS XD

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