PCT40 Process Control Apparatus - Run 1 Results

Sample
Number

1
2
3

Elapsed
Time

00:00
00:30
01:00

Notes

Temperature

Temperature

Temperature

Flowrate

T1
[C]

T2
[C]

T3
[C]

F1
[ml/min]

[%]

41.4
41.4
43.8

23.2
23.2
24.2

23.6
23.6
24.4

1
1
1

0
0
0

Page 1

PSV
Position

PCT40 Process Control Apparatus - Run 1 Results

Hot
Pump
Setting
[%]

Thermostat
State

0
0
0

1
1
1

Heater
State

Off
Off
On

Proportional
Band
P
[%]

Integral
Time
I
[s]

Derivative
Time
D
[s]

Set
Point

Controller
Output

[C]

[%]

100
100
100

0
0
0

0
0
0

40
40
40

50
50
50

Page 2

PCT40 Process Control Apparatus - Run 2 Results

Sample
Number

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31

Elapsed
Time

00:00
00:05
00:10
00:15
00:20
00:25
00:30
00:35
00:40
00:45
00:50
00:55
01:00
01:05
01:10
01:15
01:21
01:25
01:30
01:35
01:40
01:45
01:50
01:55
02:00
02:05
02:10
02:15
02:20
02:25
02:30

Notes

Temperature

Temperature

Temperature

Flowrate

T1
[C]

T2
[C]

T3
[C]

F1
[ml/min]

[%]

34.1
41.7
44.8
41.8
47.0
43.3
48.2
45.2
48.1
46.2
47.8
48.4
49.4
49.9
50.2
51.3
51.9
53.8
52.8
55.0
53.0
56.3
54.9
57.5
55.2
59.2
56.8
60.2
57.4
62.2
59.5

25.0
24.8
24.6
24.7
24.7
24.6
24.6
24.8
25.9
25.8
25.8
25.7
26.4
26.6
26.6
27.4
27.3
27.1
28.4
28.9
28.9
28.7
29.1
28.9
29.2
29.4
29.6
29.8
30.0
30.3
29.9

27.6
27.7
27.8
27.7
27.7
27.6
27.6
28.1
28.3
28.7
29.7
29.5
29.1
29.8
30.4
29.7
29.6
30.2
30.5
31.3
30.9
30.9
31.2
30.8
31.4
31.5
31.5
31.9
32.5
32.6
32.8

1
1
3
1
1
2
1
1
1
1
1
2
2
1
2
1
1
1
2
2
1
1
2
1
2
1
2
2
1
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 3

PSV
Position

PCT40 Process Control Apparatus - Run 2 Results

32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67

02:36
02:40
02:45
02:50
02:55
03:00
03:05
03:10
03:15
03:20
03:25
03:30
03:35
03:40
03:45
03:50
03:55
04:00
04:05
04:10
04:16
04:20
04:25
04:30
04:35
04:40
04:46
04:50
04:55
05:00
05:05
05:10
05:15
05:20
05:25
05:30

62.4
60.0
64.8
61.6
65.0
62.5
66.4
63.4
68.3
65.0
68.7
66.1
69.5
67.5
70.2
68.3
71.4
70.0
72.8
70.4
73.6
72.3
73.9
72.8
75.4
74.6
76.3
75.7
77.3
77.4
78.5
77.1
77.0
76.9
76.8
76.6

31.8
31.0
30.4
30.9
31.3
31.1
31.1
31.5
32.4
32.1
33.1
32.1
33.0
32.2
33.4
34.2
33.5
34.2
34.3
35.1
34.7
34.3
35.2
35.8
34.6
37.3
36.6
36.4
37.3
36.7
38.5
37.6
38.0
38.0
38.3
37.7

Page 4

32.9
33.1
32.6
33.3
33.4
33.1
33.4
33.3
33.3
35.3
34.4
35.5
35.5
35.2
35.6
36.8
36.1
36.4
36.7
37.9
37.5
37.8
37.6
37.7
37.2
38.9
38.1
37.7
38.5
38.5
40.0
40.0
39.9
40.3
39.5
40.1

2
2
2
1
2
2
1
1
2
2
2
1
1
1
2
2
2
1
1
2
1
2
1
1
1
2
1
2
1
1
2
2
1
1
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 2 Results

68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103

05:35
05:40
05:45
05:50
05:55
06:00
06:05
06:10
06:15
06:20
06:25
06:30
06:35
06:40
06:45
06:50
06:55
07:00
07:05
07:11
07:15
07:20
07:25
07:30
07:35
07:40
07:45
07:50
07:55
08:00
08:05
08:10
08:15
08:20
08:25
08:30

76.6
76.6
76.5
76.4
76.3
76.2
76.2
76.1
76.0
76.0
75.9
75.8
75.7
75.7
75.6
75.5
75.5
75.4
75.3
75.3
75.3
75.2
75.1
75.1
75.0
74.9
74.9
74.8
74.8
74.7
74.7
74.6
74.6
74.5
74.4
74.4

38.1
38.8
40.1
40.2
39.1
39.4
41.2
41.0
40.6
41.3
40.5
40.3
40.3
41.9
41.3
41.6
41.2
42.0
40.9
42.2
41.5
42.7
41.9
40.9
41.5
41.7
42.0
42.0
42.4
42.4
42.4
42.3
42.2
41.5
43.8
42.7

Page 5

40.2
40.2
40.8
41.5
40.8
40.9
41.4
41.4
41.6
41.1
42.4
42.5
41.4
41.5
42.2
41.9
42.8
42.2
41.6
42.9
42.4
41.7
42.0
41.7
41.9
43.6
43.5
43.3
44.8
43.2
44.2
43.6
44.1
44.5
44.2
44.4

1
1
1
1
1
2
1
8
1
2
1
2
1
1
1
2
1
1
2
1
2
1
2
1
1
1
1
1
2
2
1
2
1
1
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 2 Results

104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139

08:35
08:40
08:45
08:50
08:55
09:00
09:05
09:11
09:15
09:20
09:25
09:30
09:35
09:40
09:45
09:50
09:55
10:00
10:05
10:10
10:15
10:20
10:25
10:30
10:35
10:40
10:45
10:50
10:55
11:00
11:05
11:10
11:15
11:20
11:25
11:30

74.3
74.4
74.2
74.2
74.1
74.1
74.0
74.0
74.0
73.9
73.8
73.8
73.7
73.7
73.6
73.7
73.6
73.5
73.5
73.4
73.4
73.3
73.3
73.2
73.2
73.1
73.1
73.1
73.1
72.9
73.0
72.9
72.9
72.9
72.9
72.8

42.7
43.8
43.0
43.0
43.1
44.4
43.4
43.8
43.3
43.8
43.8
43.2
44.1
43.8
43.8
43.3
44.0
43.5
43.8
43.8
43.7
44.0
44.5
43.9
45.0
43.9
44.0
43.9
44.7
45.0
44.4
43.9
43.6
43.9
44.1
45.4

Page 6

44.9
44.1
44.5
45.3
44.3
44.3
45.1
45.2
44.6
44.7
43.8
44.6
44.8
45.4
44.6
43.9
44.5
44.4
44.9
45.0
45.4
45.4
44.3
45.1
45.0
46.5
45.5
46.0
45.4
45.1
46.2
46.3
45.6
45.5
46.7
45.5

1
1
1
2
2
1
2
1
1
1
1
2
1
2
1
1
1
1
1
1
2
2
1
1
1
2
1
1
1
1
1
2
1
2
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 2 Results

140
141
142
143
144
145
146
147
148
149
150
151
152
153
154
155
156
157
158
159
160
161
162
163
164
165
166
167
168
169
170
171
172
173
174
175

11:35
11:40
11:45
11:50
11:55
12:00
12:05
12:10
12:15
12:20
12:25
12:30
12:35
12:40
12:45
12:50
12:55
13:00
13:05
13:10
13:15
13:20
13:25
13:30
13:35
13:40
13:45
13:50
13:55
14:00
14:05
14:10
14:15
14:20
14:25
14:30

72.8
72.7
72.8
72.6
72.6
72.6
72.5
72.5
72.5
72.4
72.4
72.4
72.3
72.3
72.2
72.2
72.2
72.1
72.1
72.0
72.0
72.0
71.9
71.9
71.8
71.8
71.8
71.7
71.7
71.7
71.6
71.6
71.5
71.5
71.5
71.4

44.5
44.2
44.2
44.3
45.0
44.8
44.9
45.6
45.5
44.4
46.0
45.3
45.9
45.0
45.3
45.0
44.8
44.5
44.9
44.6
44.9
45.8
44.9
45.9
45.4
45.3
45.6
45.6
44.8
45.7
45.8
45.2
45.6
45.6
45.9
45.9

Page 7

46.9
46.5
46.8
45.5
45.3
45.6
47.0
46.6
46.1
46.8
46.4
46.2
47.2
46.4
45.6
46.6
46.8
46.2
46.8
45.2
47.1
46.4
46.1
46.7
46.2
45.9
45.8
47.2
45.2
46.8
46.9
47.2
45.8
47.0
46.5
45.8

2
2
1
1
1
2
2
2
82
2
1
1
1
1
1
1
1
2
1
2
1
2
1
1
2
1
2
1
2
1
1
2
1
1
2
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 2 Results

176
177
178
179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
198
199
200
201
202
203
204
205
206
207
208
209
210
211

14:35
14:40
14:45
14:50
14:55
15:00
15:05
15:10
15:15
15:20
15:26
15:30
15:35
15:40
15:45
15:50
15:55
16:00
16:05
16:10
16:15
16:20
16:25
16:30
16:35
16:40
16:45
16:50
16:55
17:00
17:05
17:10
17:15
17:20
17:25
17:30

71.4
71.4
71.3
71.3
71.3
71.2
71.2
71.2
71.0
71.0
71.0
71.0
70.9
70.9
70.9
70.8
70.8
70.7
70.7
70.7
70.6
70.5
70.6
70.5
70.5
70.5
70.4
70.4
70.3
70.3
70.4
73.1
72.1
73.6
72.7
75.9

45.4
45.4
45.0
45.5
44.8
45.6
45.0
46.2
45.2
45.7
45.8
46.1
45.9
45.5
45.7
45.3
45.6
44.9
45.7
46.3
45.9
45.2
45.2
45.5
44.5
44.5
45.8
45.0
45.0
45.1
44.8
45.0
45.5
45.4
45.9
45.7

Page 8

45.8
46.1
46.6
46.4
46.4
46.5
46.4
45.3
46.1
45.5
46.7
46.0
47.6
45.4
47.0
46.7
47.3
46.1
46.2
46.8
46.8
46.5
46.7
46.9
46.9
46.5
45.7
46.0
46.9
46.2
46.1
46.4
46.7
46.1
46.5
46.6

1
2
1
2
1
1
1
1
2
1
1
2
1
1
2
1
2
1
1
1
2
1
2
1
2
1
1
1
1
2
1
2
3
2
1
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 2 Results

212
213
214
215
216
217
218

17:35
17:40
17:45
17:50
17:55
18:00
18:05

73.9
76.8
74.5
77.9
75.9
78.5
76.6

45.4
45.2
45.3
44.8
45.4
45.3
45.1

Page 9

47.4
47.0
46.4
46.7
45.8
47.4
48.5

1
1
2
2
1
2
1

0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 2 Results

Hot
Pump
Setting
[%]

Thermostat
State

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0
0
0
0
0
0

Heater
State

Off
On
Off
On
Off
On
Off
Off
On
On
Off
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On

Proportional
Band
P
[%]

Integral
Time
I
[s]

Derivative
Time
D
[s]

Set
Point

Controller
Output

[C]

[%]

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

Page 10

PCT40 Process Control Apparatus - Run 2 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 11

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 2 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
On
Off
On
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 12

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 2 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
On
Off
On
Off
On
Off
On
Off
On

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 13

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 2 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 14

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 2 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
On
On
Off
On
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 15

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 2 Results

0
0
0
0
0
0
0

0
0
0
0
0
0
0

On
Off
On
Off
On
Off
On

100
100
100
100
100
100
100

0
0
0
0
0
0
0

0
0
0
0
0
0
0

Page 16

40
40
40
40
40
40
40

50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 3 Results

Sample
Number

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31

Elapsed
Time

00:00
00:05
00:10
00:15
00:20
00:25
00:30
00:35
00:40
00:45
00:50
00:55
01:00
01:05
01:11
01:15
01:20
01:25
01:30
01:35
01:41
01:45
01:50
01:55
02:00
02:06
02:10
02:15
02:20
02:25
02:30

Notes

Temperature

Temperature

Temperature

Flowrate

T1
[C]

T2
[C]

T3
[C]

F1
[ml/min]

[%]

72.5
70.7
68.8
67.3
65.8
64.6
63.5
62.3
61.1
60.2
59.3
58.3
57.4
56.6
56.0
55.3
54.6
54.0
53.4
52.6
52.1
51.7
51.2
50.6
50.1
49.5
49.1
48.6
48.2
47.9
47.5

25.6
25.6
25.5
25.3
25.3
25.5
25.7
26.0
26.2
26.4
26.7
26.8
27.0
27.1
27.1
27.2
27.3
27.4
27.4
27.4
27.5
27.6
27.6
27.6
27.6
27.6
27.6
27.7
27.7
27.7
27.8

46.0
45.1
44.3
43.7
42.9
42.4
41.8
41.5
41.2
40.8
40.5
40.2
40.0
39.7
39.5
39.3
39.0
38.8
38.6
38.3
38.1
37.8
37.6
37.4
37.2
37.0
36.9
36.7
36.5
36.3
36.2

635
638
640
641
637
632
639
627
631
625
628
627
623
623
619
621
619
630
622
626
617
625
618
623
622
622
617
613
617
615
612

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

Page 17

PSV
Position

PCT40 Process Control Apparatus - Run 3 Results

32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67

02:35
02:40
02:45
02:50
02:55
03:00
03:05
03:10
03:15
03:20
03:25
03:30
03:35
03:40
03:45
03:50
03:55
04:00
04:05
04:10
04:15
04:20
04:25
04:30
04:35
04:40
04:45
04:50
04:55
05:00
05:05
05:10
05:15
05:20
05:25
05:30

47.0
46.6
46.2
45.8
45.6
45.2
44.8
44.5
44.3
43.9
43.7
43.5
43.1
42.9
42.6
42.3
42.0
41.8
41.5
41.3
41.0
40.8
40.6
40.4
40.2
40.0
39.8
39.6
39.5
39.3
39.1
38.9
38.8
38.6
38.5
38.2

27.8
27.7
27.7
27.7
27.7
27.7
27.8
27.8
27.8
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.8
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.7
27.6
27.7
27.7
27.7
27.6
27.7

Page 18

36.0
35.9
35.7
35.5
35.4
35.3
35.2
35.1
34.9
34.9
34.7
34.6
34.4
34.3
34.2
34.1
34.0
33.9
33.8
33.6
33.5
33.4
33.3
33.2
33.1
33.0
32.9
32.8
32.7
32.7
32.6
32.5
32.4
32.4
32.3
32.2

612
618
615
616
606
615
617
607
611
613
606
612
610
615
613
616
609
606
608
604
614
611
609
610
604
604
614
604
606
600
601
606
604
607
608
607

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 3 Results

68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103

05:35
05:40
05:45
05:50
05:55
06:00
06:05
06:10
06:15
06:20
06:25
06:30
06:35
06:40
06:45
06:50
06:55
07:00
07:05
07:10
07:15
07:20
07:25
07:30
07:35
07:40
07:45
07:50
07:55
08:00
08:05
08:10
08:15
08:20
08:25
08:30

38.1
37.9
37.8
37.6
37.4
37.3
37.2
37.0
36.8
36.7
36.5
36.4
36.3
36.2
36.0
35.9
35.8
35.7
35.6
35.5
35.4
35.3
35.3
35.2
35.1
35.0
34.9
34.8
34.7
34.6
34.5
34.4
34.3
34.2
34.2
34.1

27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.5
27.5
27.6
27.5
27.5
27.6
27.6
27.5
27.6
27.5
27.5
27.5
27.6
27.5
27.6
27.5
27.5
27.6
27.5

Page 19

32.2
32.1
32.0
31.9
31.9
31.8
31.7
31.6
31.5
31.5
31.4
31.3
31.3
31.3
31.3
31.2
31.1
31.1
31.1
31.0
31.0
30.9
30.8
30.8
30.7
30.7
30.7
30.6
30.5
30.5
30.5
30.4
30.4
30.4
30.3
30.2

609
603
602
606
605
610
598
598
608
607
601
600
607
601
597
599
598
604
607
597
598
595
602
604
602
598
600
604
595
598
596
594
600
600
598
593

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 3 Results

104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139

08:35
08:40
08:45
08:50
08:55
09:00
09:05
09:10
09:15
09:20
09:25
09:30
09:35
09:40
09:45
09:50
09:55
10:00
10:05
10:10
10:15
10:20
10:25
10:30
10:35
10:40
10:45
10:50
10:55
11:00
11:05
11:10
11:15
11:20
11:25
11:30

34.0
33.9
33.9
33.7
33.7
33.6
33.6
33.5
33.4
33.3
33.3
33.2
33.1
33.1
32.9
32.9
32.9
32.8
32.8
32.7
32.6
32.6
32.5
32.4
32.4
32.3
32.3
32.2
32.2
32.2
32.1
32.0
31.9
31.9
31.9
31.8

27.5
27.5
27.6
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.4
27.5
27.5
27.5
27.5
27.6
27.5
27.5
27.5

Page 20

30.2
30.2
30.1
30.1
30.1
30.0
30.0
30.0
29.9
29.9
29.9
29.8
29.8
29.7
29.7
29.7
29.7
29.6
29.6
29.6
29.5
29.5
29.5
29.4
29.4
29.4
29.4
29.3
29.3
29.2
29.3
29.2
29.2
29.2
29.2
29.1

601
599
598
593
601
599
589
594
590
593
595
593
591
595
595
590
593
590
589
589
592
587
590
591
590
594
595
594
596
595
592
597
593
590
586
589

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 3 Results

140
141
142
143
144
145
146
147
148
149
150
151
152
153

11:35
11:40
11:45
11:50
11:55
12:00
12:05
12:10
12:15
12:20
12:26
12:30
12:35
12:38

31.8
31.7
31.6
31.6
31.6
31.5
31.5
31.4
31.4
31.3
31.3
31.3
31.3
31.3

27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.6
27.6
27.5
27.5
27.5
27.5

Page 21

29.1
29.1
29.1
29.0
29.1
29.0
29.0
29.0
29.0
28.9
28.9
28.9
28.9
28.9

587
584
595
587
590
590
590
594
582
587
587
594
587
587

50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 3 Results

Hot
Pump
Setting
[%]

Thermostat
State

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Heater
State

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

Proportional
Band
P
[%]

Integral
Time
I
[s]

Derivative
Time
D
[s]

Set
Point

Controller
Output

[C]

[%]

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 22

PCT40 Process Control Apparatus - Run 3 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 23

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 3 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 24

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 3 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 25

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 3 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 26

40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 4 Results

Sample
Number

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31

Elapsed
Time

00:00
00:05
00:10
00:15
00:20
00:25
00:30
00:35
00:40
00:45
00:50
00:55
01:00
01:05
01:10
01:15
01:20
01:25
01:30
01:35
01:40
01:45
01:50
01:55
02:00
02:05
02:10
02:15
02:20
02:25
02:30

Notes

Temperature

Temperature

Temperature

Flowrate

T1
[C]

T2
[C]

T3
[C]

F1
[ml/min]

[%]

42.6
44.9
42.7
43.7
43.5
44.0
42.6
46.7
45.8
47.8
46.4
47.9
49.7
49.7
51.0
50.7
52.5
52.7
54.8
54.2
57.2
56.3
58.0
57.5
59.8
59.0
62.1
60.4
62.3
61.2
64.0

27.3
27.1
27.1
27.0
26.9
27.9
27.8
28.3
28.5
28.5
29.4
29.8
30.1
30.3
30.5
30.9
31.3
32.2
31.6
32.0
32.4
33.7
32.8
32.3
33.2
33.7
33.3
33.7
33.4
33.2
35.1

28.4
28.3
28.2
28.1
28.0
28.7
30.3
30.0
30.4
30.5
31.2
31.2
31.3
31.9
33.1
32.5
33.1
32.7
32.4
32.9
32.3
33.2
33.6
34.2
34.3
34.4
34.1
34.8
34.5
35.7
35.6

2
2
2
1
2
2
2
1
1
1
2
2
2
1
1
2
1
1
2
3
1
2
2
1
2
2
2
2
1
2
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 27

PSV
Position

PCT40 Process Control Apparatus - Run 4 Results

32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67

02:35
02:40
02:45
02:50
02:55
03:00
03:05
03:10
03:15
03:20
03:25
03:30
03:35
03:40
03:45
03:50
03:55
04:00
04:05
04:10
04:15
04:20
04:25
04:30
04:35
04:40
04:45
04:50
04:55
05:00
05:05
05:10
05:15
05:20
05:25
05:30

63.0
65.0
64.0
66.0
65.6
68.2
66.8
69.2
68.0
70.7
68.9
72.0
70.9
73.8
72.0
74.7
73.0
76.2
74.2
76.8
75.5
78.0
76.2
79.5
78.2
80.3
79.0
77.9
77.8
77.5
77.4
77.3
77.2
77.1
77.1
77.1

34.5
34.5
35.3
35.6
35.4
35.6
35.8
36.1
36.1
36.9
35.8
37.4
37.2
36.9
37.9
37.4
38.3
37.7
39.0
38.9
38.3
39.2
40.0
39.6
39.9
41.2
40.9
40.8
40.3
40.2
41.7
41.7
42.4
41.9
41.8
42.2

Page 28

35.0
35.4
35.9
35.7
35.5
36.2
35.8
35.8
36.5
37.0
36.2
37.2
37.2
38.7
37.5
38.1
38.5
39.3
39.5
38.3
39.5
38.8
38.4
39.2
39.7
39.6
39.6
39.6
40.4
39.6
39.1
40.1
39.9
40.2
41.1
40.8

2
1
1
1
2
2
2
1
1
2
1
2
1
2
1
1
2
2
1
2
2
1
2
1
1
2
3
1
2
2
1
1
2
1
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 4 Results

68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103

05:35
05:40
05:45
05:50
05:55
06:00
06:05
06:10
06:15
06:20
06:25
06:30
06:35
06:40
06:45
06:50
06:55
07:00
07:05
07:10
07:15
07:20
07:25
07:30
07:35
07:40
07:45
07:50
07:55
08:00
08:05
08:10
08:15
08:20
08:25
08:30

77.0
76.9
76.8
76.8
76.7
76.6
76.6
76.4
76.4
76.3
76.3
76.2
76.1
76.1
76.0
75.9
75.9
75.8
75.8
75.7
75.6
75.6
75.5
75.5
75.4
75.3
75.3
75.2
75.2
75.1
75.1
75.0
74.9
74.9
74.9
74.8

42.8
42.3
42.6
42.2
42.9
42.6
42.7
42.6
41.9
42.5
43.7
44.5
43.3
43.4
43.6
44.2
44.6
44.0
43.7
42.8
42.8
44.4
43.6
43.3
44.5
44.0
45.0
43.8
44.0
44.7
44.4
44.8
44.8
46.2
45.7
44.7

Page 29

40.7
40.1
40.6
40.7
41.0
42.1
41.8
40.8
41.8
41.9
41.6
40.6
42.2
42.5
41.9
43.0
42.3
42.4
44.2
42.1
42.7
42.1
43.6
43.7
43.4
43.8
43.3
43.8
43.7
42.9
44.2
42.4
43.7
43.0
44.3
43.8

1
2
1
1
1
1
2
1
2
2
2
1
1
1
1
2
2
2
1
2
1
2
1
2
1
1
1
2
1
1
1
1
1
2
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 4 Results

104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139

08:35
08:40
08:45
08:50
08:55
09:00
09:05
09:10
09:15
09:20
09:25
09:30
09:35
09:40
09:45
09:50
09:55
10:00
10:05
10:10
10:15
10:20
10:25
10:30
10:35
10:41
10:45
10:50
10:55
11:00
11:05
11:10
11:15
11:20
11:25
11:30

74.8
74.7
74.6
74.6
74.6
74.5
74.5
74.4
74.4
74.4
74.3
74.2
74.2
74.2
74.1
74.1
74.0
73.9
74.0
73.9
73.8
73.8
73.8
73.7
73.7
73.6
73.6
73.6
73.5
73.5
73.4
73.4
73.3
73.3
73.3
73.2

44.8
45.2
45.2
44.7
45.8
45.6
44.9
45.2
45.0
45.8
46.4
45.9
46.1
45.4
45.4
45.8
45.5
44.8
46.2
45.2
46.7
46.2
46.3
46.4
46.5
45.9
46.9
45.5
46.1
46.3
46.4
47.3
47.4
46.7
46.6
46.8

Page 30

43.8
42.9
42.7
42.6
43.5
43.2
43.5
43.6
43.8
44.8
42.9
43.2
42.8
44.1
43.7
44.3
43.7
43.7
43.5
43.8
44.2
44.2
44.9
43.7
44.2
43.7
43.9
44.3
44.7
44.7
43.8
43.1
44.1
44.1
44.5
43.6

2
1
1
1
1
1
1
1
1
1
1
1
2
1
2
1
2
1
1
2
1
1
2
1
2
2
1
1
1
2
2
2
2
1
2
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 4 Results

140
141
142
143
144
145
146
147
148
149
150
151
152
153
154
155
156
157
158
159
160
161
162
163
164
165
166
167
168
169
170
171
172
173
174
175

11:35
11:40
11:45
11:50
11:55
12:00
12:05
12:10
12:15
12:20
12:25
12:30
12:35
12:40
12:45
12:50
12:55
13:00
13:05
13:10
13:15
13:20
13:25
13:30
13:35
13:40
13:45
13:50
13:55
14:00
14:05
14:10
14:15
14:20
14:25
14:30

73.2
73.2
73.2
73.0
73.0
73.0
72.9
72.9
72.9
72.9
72.9
72.9
72.8
72.8
72.8
72.7
72.7
72.6
72.6
72.6
72.5
72.5
72.4
72.4
72.4
72.4
72.3
72.3
72.2
72.2
72.1
72.1
72.1
72.0
72.0
72.0

46.5
47.2
47.2
46.7
45.7
45.8
46.2
47.2
46.4
47.2
46.4
47.2
46.7
46.5
46.6
47.0
47.4
47.8
47.1
47.0
47.6
47.6
46.8
46.4
47.4
46.9
47.4
47.4
47.3
47.3
47.8
46.9
47.5
46.8
47.5
47.1

Page 31

44.3
44.0
43.6
43.8
44.1
44.9
43.8
44.8
45.0
44.0
44.6
44.4
43.6
44.8
44.8
45.2
45.0
45.2
43.8
44.0
43.9
44.3
44.5
44.2
45.2
44.6
45.0
44.4
44.7
43.9
44.5
44.8
44.5
45.1
45.5
44.9

2
1
2
2
2
1
2
1
2
1
1
2
2
1
3
1
1
1
2
1
1
2
1
1
2
1
1
2
1
2
1
1
1
2
1
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 4 Results

176
177
178
179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
198
199
200
201
202

14:35
14:40
14:45
14:50
14:55
15:00
15:05
15:10
15:15
15:20
15:25
15:30
15:35
15:40
15:45
15:50
15:55
16:01
16:05
16:10
16:15
16:20
16:25
16:30
16:35
16:40
16:45

72.0
71.9
71.9
71.9
71.8
71.8
71.8
71.7
71.7
71.6
71.6
71.6
71.5
71.5
71.4
71.5
71.4
71.3
71.3
71.3
71.2
71.2
71.7
72.4
74.3
73.6
75.7

47.4
46.7
47.5
47.0
47.7
46.5
47.4
47.1
47.0
46.9
47.2
46.9
47.7
47.1
47.2
47.1
46.9
46.7
47.2
46.4
47.0
46.5
47.1
47.3
47.8
46.6
47.4

Page 32

44.7
44.1
44.5
44.3
45.0
44.6
44.5
45.0
44.4
45.1
44.9
44.4
44.3
44.5
44.4
44.3
43.8
44.3
44.4
44.1
44.0
43.8
43.8
44.2
44.8
44.2
44.2

2
1
1
2
1
1
1
1
2
2
2
2
2
1
1
2
1
2
1
1
2
2
1
1
1
2
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 4 Results

Hot
Pump
Setting
[%]

Thermostat
State

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Heater
State

On
Off
On
Off
On
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off

Proportional
Band
P
[%]

Integral
Time
I
[s]

Derivative
Time
D
[s]

Set
Point

Controller
Output

[C]

[%]

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

Page 33

PCT40 Process Control Apparatus - Run 4 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
Off
On

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 34

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 4 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 35

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 4 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
On
Off
On
Off
On
Off
On
Off
On
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 36

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 4 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 37

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 4 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off
On
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 38

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

PCT40 Process Control Apparatus - Run 5 Results

Sample
Number

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31

Elapsed
Time

00:00
00:05
00:10
00:15
00:20
00:25
00:30
00:35
00:40
00:45
00:50
00:55
01:00
01:05
01:10
01:15
01:20
01:25
01:30
01:35
01:40
01:45
01:50
01:55
02:00
02:05
02:10
02:15
02:20
02:25
02:30

Notes

Temperature

Temperature

Temperature

Flowrate

T1
[C]

T2
[C]

T3
[C]

F1
[ml/min]

[%]

74.5
72.4
70.0
67.9
65.9
64.1
62.3
61.0
59.7
58.5
57.4
56.3
55.3
54.3
53.5
52.7
52.0
51.2
50.5
49.9
49.2
48.6
48.0
47.6
47.1
46.6
46.1
45.6
45.1
44.6
44.2

25.9
25.9
25.7
25.5
25.8
26.3
26.6
26.9
27.1
27.2
27.3
27.3
27.4
27.4
27.4
27.5
27.5
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6

43.3
40.9
40.0
39.2
38.5
38.1
37.8
37.5
37.2
36.8
36.5
36.3
36.0
35.7
35.4
35.2
35.0
34.8
34.6
34.3
34.1
34.0
33.7
33.5
33.4
33.2
33.1
32.9
32.7
32.6
32.4

1089
1090
1082
1083
1085
1083
1080
1078
1085
1083
1083
1075
1083
1085
1088
1085
1083
1083
1088
1075
1080
1083
1081
1080
1086
1080
1085
1079
1085
1076
1075

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

Page 39

PSV
Position

PCT40 Process Control Apparatus - Run 5 Results

32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67

02:35
02:40
02:45
02:50
02:55
03:00
03:05
03:10
03:15
03:20
03:25
03:30
03:35
03:40
03:45
03:50
03:55
04:00
04:05
04:10
04:15
04:20
04:25
04:30
04:35
04:40
04:45
04:50
04:55
05:00
05:05
05:10
05:15
05:20
05:25
05:30

43.9
43.6
43.1
42.7
42.4
42.0
41.8
41.4
41.1
40.8
40.6
40.3
40.0
39.7
39.5
39.3
39.0
38.8
38.6
38.4
38.2
38.0
37.8
37.5
37.3
37.1
37.0
36.8
36.6
36.4
36.3
36.1
36.0
35.8
35.7
35.5

27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.6
27.5
27.6
27.5
27.5
27.6
27.6
27.5
27.5
27.6
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.6
27.6
27.6
27.5
27.5
27.5
27.6
27.5

Page 40

32.3
32.2
32.1
31.9
31.8
31.7
31.6
31.5
31.4
31.3
31.3
31.2
31.1
31.0
31.0
30.9
30.8
30.7
30.6
30.5
30.5
30.4
30.3
30.3
30.2
30.1
30.1
30.0
30.0
29.9
29.9
29.8
29.8
29.7
29.7
29.6

1077
1083
1075
1085
1074
1077
1080
1072
1077
1075
1074
1083
1085
1080
1084
1076
1073
1075
1085
1074
1083
1078
1072
1081
1074
1084
1085
1078
1073
1080
1077
1073
1074
1072
1084
1072

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

PCT40 Process Control Apparatus - Run 5 Results

68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103

05:35
05:40
05:45
05:50
05:55
06:00
06:05
06:10
06:15
06:20
06:25
06:30
06:35
06:40
06:45
06:50
06:55
07:00
07:05
07:10
07:15
07:20
07:26
07:30
07:35
07:40
07:45
07:50
07:55
08:00
08:05
08:11
08:15
08:20
08:25
08:30

35.4
35.2
35.1
35.0
34.9
34.7
34.6
34.5
34.4
34.3
34.2
34.1
33.9
33.9
33.8
33.7
33.6
33.4
33.4
33.3
33.2
33.1
33.0
32.9
32.8
32.8
32.7
32.6
32.5
32.5
32.4
32.3
32.3
32.2
32.1
32.1

27.5
27.5
27.5
27.5
27.4
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.5
27.4
27.5
27.5
27.5
27.5
27.4
27.5
27.4
27.5
27.5
27.4
27.4
27.5
27.5
27.4
27.4
27.4
27.5
27.5
27.4

Page 41

29.6
29.5
29.5
29.4
29.4
29.3
29.3
29.2
29.2
29.2
29.2
29.1
29.1
29.0
29.0
29.0
28.9
28.8
28.8
28.8
28.8
28.8
28.8
28.7
28.7
28.7
28.6
28.6
28.6
28.5
28.6
28.5
28.5
28.5
28.4
28.4

1079
1070
1076
1074
1072
1077
1080
1077
1081
1081
1072
1080
1078
1079
1072
1080
1068
1074
1080
1074
1075
1072
1080
1077
1077
1077
1074
1077
1080
1072
1080
1069
1081
1069
1071
1079

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

PCT40 Process Control Apparatus - Run 5 Results

104
105
106
107
108
109
110
111
112
113
114
115
116
117

08:35
08:40
08:45
08:50
08:55
09:00
09:05
09:10
09:15
09:20
09:25
09:30
09:35
09:40

32.0
32.0
31.8
31.8
31.7
31.7
31.6
31.5
31.4
31.4
31.3
31.3
31.3
31.3

27.5
27.4
27.5
27.4
27.5
27.4
27.5
27.5
27.4
27.4
27.4
27.4
27.4
27.5

Page 42

28.5
28.4
28.4
28.4
28.4
28.3
28.2
28.2
28.2
28.2
28.2
28.2
28.2
28.1

1072
1075
1083
1074
1074
1074
1072
1083
1073
1072
1070
1075
1069
1072

100
100
100
100
100
100
100
100
100
100
100
100
100
100

PCT40 Process Control Apparatus - Run 5 Results

Hot
Pump
Setting
[%]

Thermostat
State

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Heater
State

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

Proportional
Band
P
[%]

Integral
Time
I
[s]

Derivative
Time
D
[s]

Set
Point

Controller
Output

[C]

[%]

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 43

PCT40 Process Control Apparatus - Run 5 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 44

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 5 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 45

40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

PCT40 Process Control Apparatus - Run 5 Results

0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0

Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off
Off

100
100
100
100
100
100
100
100
100
100
100
100
100
100

0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0

Page 46

40
40
40
40
40
40
40
40
40
40
40
40
40
40

0
0
0
0
0
0
0
0
0
0
0
0
0
0