Methanol Solution
Product Number Lot Number CAS Number Concentration Molecular Formula Molecular Weight DEA Class B 7150 61K88041 [94-09-7] 1.02 mg Benzocaine/mL GC grade methanol (conc. verified by UV) C9H11NO2 165.2 Preparation of a non-controlled substance Expiration Date Storage Stability Synonyms Ethyl p-aminobenzoate; 4-Aminobenzoic acid ethyl ester If stored at 2-8C in an air tight container, protected from light, decomposition of the product is less than 1% in 36 months. Af ter opening, concentration may change due to loss of solvent. June 2008 2-8C
15000
10000 165 92 5000 41 0 40 50 60 70 80 90 100 m/z 110 120 130 140 150 160 52 65 74 81 108 137 150
Hewlett-Packard 5890 Series II Gas Chromatograph Hewlett-Packard 5971 Mass Selective Detector Hewlett-Packard G1034C MS ChemStation (HP-DOS series)
FT-IR
100 % 80 T r a n s m i t t a n c e
60
40
20
KBr
4000 3600 3200 2800 2400 2000 1600 1200 800 400
Wavenumbers (cm-1 )
BENZOCAINE
Methanol Solution
Product Number B 7150 Lot Number 61K88041
O H N 2 C OC H C H 2 3
Ultraviolet Spectrum Peak Absorbance Solvent Dilution 291.4 nm 0.645 Methanol 1 : 199 (v/v)
Capillary Gas Chromatography Column Supelco SPB-1 (Cat. No. 2-4162) I.D. 0.20 mm Length 15 m Film Thickness 0.20 m Oven Temperature 50C (2 min.), then 15/min. to 300C, hold 11 min. Injector Temperature 250C, Split Detector Hewlett-Packard 5971 Mass Selective Detector (70 eV, 40-500 m/z)
1.0 0.9 0.8 A b s o r b a n c e 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 200 220 240 260 Wavelength (nm) 280 300 320
5.00 10.00 15.00 Time (min) 20.00 25.00
Hewlett-Packard 5890
B 7150/61K88041/09/16/041
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