UHT PLANT
A PROJECT REPORT B.Tech Electrical Submited by
BACHLORS IN Electrical Technology Year 2012 PROJECT SUPERVISOR Mr. Muhammad Naveed
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DECLARATION
We hereby declare that no portion of the work referred to in this project Thesis has been submitted in support of an application for another degree or qualification of this of any other university or other institute action of learning. If any act of plagiarism found, we are fully responsible for every disciplinary action taken against us depending upon seriousness of the proven offence, even the cancellation
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ACKNOWLEDGEMENT
We are thankful to ALLAH and many different people for helping us creating this project. Thanks to our families for their trust and understanding. Our friends (who have always been a source of inspiration) have helped to create a wonderful academic climate.
DEDICATED TO
Our dearest and most respected parents and teachers. Whose efforts and prayers are great source of strength to us in every noble venture? Theirs love inspired us to the higher idea of life.
ABSTRACT
The report is all about the research conducted by the group and the subsequent implementation of the project in the form of human tracking. The human tracking system offer the capability of searing a specific person in a multy story building without spending much time. Milk deposits from an ultra-high-temperature (UHT) plant were analysed for protein, fat and minerals. The physical appearance and composition of the deposits was found to vary with modifications of the plant. For each particular arrangement of the plant, a characteristic pattern of deposits occurred. Possible mechanisms involved in the formation of the deposits are discussed. Ultra-high temperature ceramics are the ideal materials for extreme conditions owing to their very high melting points and good thermo-mechanical properties at high temperatures. For these reasons, they are widely known as materials for aerospace applications. This paper presents a comparative spectral characterization of zirconium, hafnium, and tantalum carbides ultra-high temperature ceramics for concentrating solar power applications. Roomtemperature reflectance spectra have been measured from the ultraviolet wavelength region to the mid-infrared band. Using these spectral properties, the ceramics were evaluated as sunlight absorbers in receivers for high-temperature thermodynamic solar plants.
LIST OF CONTENTS
Chapter 1 The Heat Treatment Processes 1.1 1.2 1.3 1.4 1.4.1 1.5 1.6 1.7 1.8 1.9 1.10 1.11 1.12 1.13 Introduction Microbiology Bacteria Molds Yeast Bacteria Phages Toxicity Pasteurization Extended Shelf Life / Ultra Pasteurization UHT Treatment Sterilization EU Classification Process Evaluation The Logarithmic Reduction of spores and Sterilizing Efficiency 1.14 Terms & Expressions to Characterize Heat Treatment Processes 1.15 1.16 Residence Time Chemical & Bacteriological changes at High Temperature 31 28 29 27 15 17 17 20 20 20 21 21 22 23 24 25 27
Chapter 2 PT 100 2.1.Introduction 2.2.Features 2.3.Getting Started 2.4.Hardware Setup 2.5. 2.6. Software Setup Evaluation Board 33 33 34 35 36 37
2.6.1. The Constant Current Source 2.6.2. RTD Signal Chain 2.7. 2.8. 2.9. Types of PT 100 Technical Data Cabling
2.9.1. Line Resistance 2.9.2. Line Compensation 2.10. Measuring Junction Location 2.11. Wiring of PT 100 Sensors 2.11.1. Two Wire Connection 2.11.2. Three Wire Connection 2.11.3. Four Wire Connection
3.1.Introduction 3.2.Magnetic Field of an infinite solenoid inside 3.3.Outside 3.4.Quantitative Description 3.5.Magnetic Field and vector potential for finite continuous solenoid 3.6.Inductance of a solenoid 3.7.Electromechanical Solenoids 3.8. Rotary Solenoid 3.8.1. Rotary Voice Call 3.8.2. Pneumatic Solenoid Valves 3.8.3. Hydraulic Solenoid Valves 3.8.4. Automobile Starter Solenoid 3.9.Switching Functions & Symbols 3.9.1. Normally Closed (NC) 3.10. Latching or Bi-Stable 3.10.1. Number of Ways 3.11. Electric Position Indicator 3.11.1. Features
50 51 53 53
54 56 57 58 59 59 59 60 60 60 61 61 62 62
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63 63 63
Chapter 4 Line Heat System 4.1. Introduction 4.2. Milk Samples 4.3. Sample Preparation 4.3.1. Panelists 4.4. Descriptive Orientation Sessions 4.5. Line Separation 4.6. Determining Sensory Properties 4.7. Experimental Design and Statistical Analysis 65 66 67 67 67 67 69 69
Chapter 5 Temperature Controller 5.1. 5.2. 5.3. 5.4. 5.5. 5.6. 5.7. Basic of Temperature Control Practical Considerations Types of Control More about control Theory Power Control Outputs Solid State Relays 73 73 74 75 76 76 77 77 77 82
5.7.1. Thyrister Power Controllers 5.8. 5.9. Phase Angle Final Remarks
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6.1.Introduction 6.2. Tolerance Limits 6.3. Temperature Limiter 6.4. Applications 6.5. Brief Description 6.6. Functional Description 6.7. Binary Input 6.8. Analog Output 6.9. Instrument Description Transmitter 6.10. Schematic Arrangement of the Standard Cell
84 86 88 88 89 90 90 91 91 93
List of Figure
Figure 1.1: Temperature profiles for pasteurization processes Figure 1.2. Temperature profiles for direct infusion, high heat infusion & indirect UHT process. Figure 1.3. Temperature profiles for conventional in-container sterilization Figure. 1.4 Figure 1.5. Figure 2.1. Figure 2.2. Figure 2.3: Figure 2.4. Figure 2.5. Figure 2.6: Figure 2.7. Figure 3.1. Figure 3.2. Figure 3.3 Figure 3.4. Figure : 3.5. Figure 4.1 Figure 4.2. Holding Tube Deposit in UHT Plants PT 100 RTD Evaluation Board Simplified Block Diagram Simplified PT 100 RTD Evaluation Board Schematic Microsoft Excel-Based GUI Constant Current Source External RTD Connections Hardware Status Length of the wire Solenoid Coil Solenoid inside with 3 loops Solenoid outside Magnetic Field Continuous Solenoid Electric Indicator Line Separation Principal Component Analysis 25 30 31 34 35 36 37 38 39 47 50 51 52 54 62 68 71 23 22
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Figure 5.1. Figure 5.2. Figure 6.1. Figure 6.2. Figure 6.3. Figure 6.4. Figure 6.5. Figure 6.6
Phase Angle The response of a PI algorithm to a step in error Jomo Characteristics Torelance Band as a Function of the temperature TB/TW Block Diagram Brief Description Jumo Digital Meter. Measuring Cell.
78 81 85 87 88 89 91 93
List of Table
Table 1.1: A variety of dairy, food & beverage products and their suitability for treatment in thermal heat processing systems Table 1.2. for Dual Chemical Criteria 16 Present legislation according to EU directive 92/46 IDF & EU suggestions 26
List of Symbol
3.1. Normally Closed 61
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1.1.
Introduction
As one of the most complete food products of all, dairy products are very important in human nutrition. But dairy products are also highly perishable and would easily lose their nutritional value, flavor and appearance if protective measures were not taken. Consequently, the dairy industry is one of the most advanced industries in the food processing area, taking care of the milk from when it leaves the udder of the cow through transportation to the dairy, processing, packaging, and distribution until it reaches the consumer. The technology of producing long-life products is today applied throughout the food and beverage industries, and in many cases, the processing plants are designed for multipurpose operation. When aseptic technology was introduced more than 35 years ago, it revolutionized the food industry by making it possible to distribute high quality food products over long distances in a cost-effective way. The heart of aseptic technology for production of long-life dairy products is aseptic processing. Since its introduction this concept has been developed and refined to a point where any need in respect of capacity, product viscosity, particulate content, acidity or sensitivity to heat treatment can be met while securing high quality, longlife products. APV was one of the pioneers in aseptic processing and over the years we have developed a wide range of processing concepts to satisfy all the needs of the industry. In this Technology Update, we will first discuss some of the micro-biological factors which must be considered in all aseptic processing, together with the heating processes most commonly used for reducing micro-organisms in dairy products: pasteurization, sterilization and ultra high temperature (UHT) treatment. So-called commercial sterility is the aim of all UHT processes, and the extent to which this is achieved in a particular process can be measured, notably by reference to the bacteriological effect (B*) and the chemical effect (C*) of such processes. These factors are explained in the section Process Evaluation. The main part of the Technology Update is devoted to an analysis of the processing systems of most interest to the dairy, food and beverage industries: Indirect Plate Sterilizer, Indirect Tubular Sterilizer, Steam Infusion Sterilizer, High Heat Infusion Sterilizer, Instant Infusion Pasteurizer, Steam Injection Sterilizer and Indirect Scraped Surface Heat Exchanger (SSHE) Sterilizer. In each case we describe the system, discuss its advantages and limitations, and list a number of
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products for which the system in question is particularly suitable The Pilot UHT Plant is able to combine most of the aseptic processes in one unit, which provides an efficient tool for pilot trials and product development. In aseptic processing, special consideration must be given to some of the auxiliary equipment required. Aseptic tanks are not
Table 1.1: A variety of dairy, food & beverage products and their suitability for treatment in thermal heat processing systems
A necessary requirement but often serves as a useful buffer for sterilized products. The area of extended shelf life products is becoming increasingly important. APV has developed concepts, offering the industry and consumers new solutions and exciting opportunities. With the large number of options available it becomes important to be able to choose the solution which provides the best quality product at a reasonable cost, giving safe and trouble free operation. A separate section has been made to cover this subject. The process control system
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is not only necessary, it must Incorporate up-to-date technology not least on the software side. Special attention must be given to the subsequent filling and packaging of aseptically processed products. Finally, we address the area of product development. APVs worldwide capabilities in respect to product testing makes it possible to work closely with customers in their efforts to upgrade production and launch new products. This Technology Update purely deals with the indirect and direct heat transfer processes. APV also manufactures various types of electrical or electro heat thermal processing equipment such as ohmic heating. This is dealt with in a separate Technology Update.
1.2.
Microbiology
The key to production of long-life products with aseptic technology is a detailed understanding of the microbiology of food. Using the example of the dairy industry, the milk in the udder of a healthy cow is free from bacteria, but as soon as the milk comes into contact with the air it becomes contaminated with micro-organisms. If the temperature is favorable, the micro-organisms multiply and very soon the milk will turn sour (or putrefy), developing an unpleasant flavor. To prevent this from happening, the raw milk is subjected to heat treatment. The term aseptic is usually defined as free from or keeping away diseaseproducing or putrefying micro-organisms. In the food industry the terms aseptic, sterile and commercially sterile are often used interchangeably. This is not strictly correct. Sterilization means 100% destruction of all living organisms, including their spores, and this is very difficult to achieve. Commercial sterility means that the product is free from microorganisms which grow and consequently contribute to the deterioration of the product. Micro-organisms are extremely small and can only be seen under a microscope. However, hundreds or thousands of individual cells or groups of cells can form colonies which are visible to the naked eye and some colonies have colors, shapes, textures or odors which make the organism identifiable.
1.3.
Bacteria
The term bacteria strictly means rod-shaped micro-organisms only, but is also used in a loose sense to include all microorganisms except yeast and molds. The individual bacterium varies in size from 0.5 to 3 micron. The groups of bacteria which are most important in the
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dairy industry are the lactic acid, coli form, butyric acid, and putrefaction bacteria. The bacterial count in milk coming from the farm varies from a few thousand bacteria/ml for high-quality milk; to several million if the standard of cleaning, disinfection and chilling is poor. For milk to be classified as top quality, the CFU (Colony Forming Units) should be less than 100,000/ml. Bacteria are single-celled organisms which normally multiply by binary fission, i.e. splitting in two. The simplest and most common way to classify bacteria is according to their appearance and shape. However, in order to be able to see bacteria, they must first be stained and then studied under a microscope at a magnification of approximately 1,000 X. Based on a method of staining, developed by the Danish Bacteriologist Gram, bacteria are divided into Gram negative (red) and Gram positive (blue). The three characteristic shapes of bacteria are spherical, rod shaped and spiral. Diplococcic arrange themselves in pairs; staphylococci form clusters, while streptococci form chains. Another way of classification is according to temperature preference: Psychotropic bacteria (cold tolerant) reproduce at temperatures of 45F or below. Psychrophilic bacteria (cold loving) have an optimum growth temperature below 68F. Mesophilic bacteria (loving the middle range) have optimum growth temperatures between 68F and 111F. Thermophilic bacteria (heat loving) have their optimum growth temperatures between 113F and 140F. Thermoduric bacteria (heat enduring) can tolerate high temperatures above 150F. They do not grow and reproduce at high temperatures, but can resist them without being killed. Bacteria can only develop within certain temperature limits, which vary from one species to another. Temperatures below the minimum cause growth to stop, but do not kill the bacteria. They are, however, damaged by repeated freezing and thawing. If the temperature is raised above the maximum, the bacteria are soon killed by heat. Most cells die within a few seconds of being exposed to 158F, but some bacteria can survive heating to 185F for 15 minutes, even though they do not form spores. A third way of classifying micro-organisms is by their oxygen requirement. The availability of oxygen is vital to the metabolism of all organisms.
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Some bacteria consume oxygen from the atmosphere; they are called aerobic bacteria. However, to some bacteria free oxygen is a poison; they are called anaerobic bacteria and obtain the oxygen they need from chemical compounds in their food supply. Some bacteria consume free oxygen if it is present, but they can also grow in the absence of oxygen; they are called facultative anaerobic. The acidity of the nutrient substrate for bacteria is also important. Sensitivity to pH changes varies from one species to another, but most bacteria prefer a growth environment with a pH around 7. Furthermore, the salt and/or sugar concentration of a substrate has an important influence on the growth of bacteria. The higher the concentration, the more growth is inhibited. This is caused by the high osmotic pressure which will draw water out from the cell, thereby dehydrating it. Osmotic pressure is used as a means of food preservation in sweetened condensed milk, salted fish and fruit preserves like jam and marmalade. Spores. The spore is a form of protection against adverse conditions, e.g. heat and cold, lack of moisture, lack of nutrients, or presence of disinfectants. Only a few bacteria are spore forming e.g. Bacillus and Clostridium. The spores germinate back into a vegetative cell and start reproduction when conditions become favorable again. The spores have no metabolism and can survive for years in dry air and are much more resistant to adverse conditions than bacteria. This includes heat treatment, and it takes typically 20 minutes at 248F to kill them with 100 percent certainty. The UHT time/temperature combination reduces the number of bacteria spores by a minimum of log 9, leaving very few bacteria spores in UHT treated products. Enzymes. When milk leaves the udder it contains enzymes, the so-called original enzymes. Enzymes are also produced by the bacteria in the milk, the so-called bacterial enzymes. Enzymes are not micro-organisms but are formed as a result of the metabolism of microorganisms. The ability of enzymes to trigger chemical reactions can be important when UHT products are produced. Some of the bacterial enzymes are able to cause sweet coagulation of milk products which destroys the product. The majority of these enzymes are produced by Gram negative Pseudomonas bacteria developing mainly in cold raw milk stored for excessive time in milk cooling tanks, road tankers or milk silos. This problem will be aggravated if the milk has been contaminated because of unhygienic conditions or lack of
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cleaning-in-place (CIP). The vast majority of enzymes will be destroyed by UHT treatment, but a few may still be active in the final product.
1.4.
Molds
Molds belong to the fungi group of micro-organisms which are widely distributed in nature among plants, animals and human beings. Molds normally grow anaerobically, and their optimum growth temperature is between 68F and 86F. Molds can grow in substrates with pH 2-8.5, but many species prefer an acid environment. The most common species in milk do not survive pasteurization conditions, and the presence of mold in pasteurized products is therefore a sign of re-infection. The penicillium family is one of the most common types of molds. Their powerful protein splitting properties make them the chief agent in ripening of, for instance, blue cheese.
1.4.1.
Yeast
Yeast also belong to the fungi group of micro-organisms. They vary greatly in size. Saccharomyces cerivisiae, used for brewing of beer, has a diameter of 2-8 micron, but other species may be as large as 100 micron. Yeast has the ability to grow both in the presence and absence of oxygen. The optimum temperature is between 68F and 86F. Optimum pH values are 4.5-5.0, but yeast will grow in the pH range of 3-7.5. From a dairy point of view, yeast are generally undesirable organisms. They ferment milk and cream, and cause defects in cheese and butter. In the brewing, baking and distillation industries, on the other hand, they are very valuable organisms.
1.5.
Bacteria Phages
Bacteria phages belong to the group of micro-organisms called viruses. Viruses have no metabolism of their own and therefore cannot grow on a nutrient substrate. Viruses infect living cells in plants and animals. Bacteria phages (also known as phages) infect bacteria and are consequently a problem in all dairy processes where bacteria cultures are used. They are very small in size 0.02-0.06 microns and can only be seen with an electron microscope. Bacteria phages grow at temperatures between 50F and 113F. They are killed by exposure to 145-190F for 30 minutes and tolerate pH values in the range of 3-11.
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1.6.
Toxicity
Micro-organisms which are harmful to man or animals are called pathogens. They can cause death or severe illness by the secretion of toxins either directly into contaminated foodstuffs, which are subsequently eaten, or by transfer to an animal host offering ideal conditions for reproduction and further generation of toxins. Some toxins are inactivated by heat treatment at 140F for one hour.
1.7.
Pasteurization
Most commercial liquid food products undergo some form of heat treatment and pasteurization is the most common. As it is usually bacterial growth that causes food to deteriorate, pasteurization preserves the freshness of the food product. There are basically two ranges of pasteurization: Low-temperature pasteurization. For milk, this is based on heating the product to 162169F and holding at that temperature for at least 15-20 seconds (or equivalent) The pasteurization may vary from country to country according to national legislation. A common requirement in all countries, however, is that the heat treatment must guarantee the destruction of unwanted micro-organisms and all pathogenic bacteria. The shelf life of pasteurized milk is limited (typically 5-7 days), and primarily depends on raw milk quality and storage temperature. During low-temperature pasteurization the phosphates enzyme is destroyed, while the peroxides enzyme is preserved. This serves as a measure to control the process and distinguish it from high temperature pasteurization. High-temperature pasteurization. This is based on heating the product to 185F or higher for a few seconds (or equivalent) (Fig. 1.1). The aim is to kill the entire population of bacteria which are pathogenic for both man and animals, and almost all other bacteria as well. By careful monitoring of the process parameters, a product with excellent quality can be obtained with minimum heat damage. The shelf life can be extended to several weeks in the cooling chain.
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During high-temperature pasteurization, both the phosphates and the peroxides enzymes are destroyed, and this serves as a measure to confirm that the process has actually taken places specified.
1.8.
The term extended shelf life, or ESL, is being applied more and more frequently. There is no single general definition of ESL. Basically, what it means is the capability to extend the shelf life of a product beyond its traditional well-known and generally accepted shelf life without causing any significant degradation in product quality. A typical temperature/time combination for high-temperature pasteurization of ESL milk is 257-266F for 2-4 seconds.
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1.9.
UHT Treatment
UHT or Ultra High Temperature treatment is based on the fact that higher temperatures permit a much shorter processing time. With proper time and temperature combination it is possible to achieve commercial sterility with only limited, undesirable, chemical changes in the product. In terms of nutritive value, flavor and appearance, the quality of the product is more vulnerable to the duration of the treatment than to the temperature applied. In the UHT process, the milk is typically heated to 279-302F and held at that temperature for just a few seconds before it is rapidly cooled down to room temperature (Fig. 1.2).
Fig1.2. Temperature profiles for direct infusion, high heat infusion & indirect UHT process.
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After the product has been cooled it is led to an aseptic filling machine in a closed piping system either directly or by way of an aseptic storage tank. The product obtained in this way has a shelf life at room temperature of several months. The quality of the final product depends on the raw material quality but also to a large extent, on the type of heat treatment system applied. This is the case for UHT milk and for a wide range of long-life food products like sauces, salad dressings, mayonnaise and soups, as well as for juices and soft drinks. In order to combat the Heat Resistant Spores (HRS) APV has developed the patented so-called High Heat Infusion system. It enables heat treatment temperatures as high as 302F without adversely affecting the product quality and still maintaining acceptable running times in the order of 24 hours between cleaning. Products with very high viscosity are more difficult to handle in a UHT system, and APV has developed a special patented version of the infusion system to handle high viscosity products. This so-called Instant Infusion system is based on very short but controllable and well defined retention time in the infusion chamber.
1.10.
Sterilization
Sterilization is another type of heating process used for products to increase keeping quality without refrigeration. The heat treatment takes place after the product is packed. The package, with its content, is heated to approx. 248F and held at that temperature for 10 to 20 minutes, after which it is cooled to room temperature. Because of the lengthy heat treatment at a relatively high temperature, this process reduces the nutritive value of the product, and it is also liable to change its color and flavor considerably.(Fig 1.3)
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1.11.
EU Classification
In Europe, the EU milk Hygiene Directive (92/46) suggests that limits and methods to enable a distinction to be made between different types of heat treated milk may be established (Article 20). The proposed parameters, limits and methods may be summarized as shown in Table 2. By this method the hygienic requirements concerning food safety can be satisfied taking into consideration the keeping qualities over varying length of time. This method also makes it possible to establish a new definition of different types of fluid milk products in a way that is independent of the technology of the heat treatment and the filling.
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It should be noted that the chemical criteria in Table 2 are the recommendation given by IDF and EU to the legislators, but the general perception is that this proposal will be followed.
Table 1.2. Present legislation according to EU directive 92/46 IDF & EU suggestions for Dual Chemical Criteria
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1.12.
Process Evaluation
All UHT processes are designed to achieve commercial sterility. This calls for application of heat to the product and a chemical sterility or other treatment that renders the equipment, final packaging containers and product free of viable micro-organisms able to reproduce in food under normal conditions of storage and distribution. In addition, it is necessary to inactivate toxins and enzymes present, and to limit chemical and physical changes in the product. In very general terms it is useful to have in mind that an increase in temperature of 50F increases the sterilizing effect 10-fold whereas the chemical effect only increases approximately 3-fold. In this section we will define some of the more commonly used terms and how they can be used for process evaluation.
1.13.
When micro-organisms and/or spores are exposed to heat treatment not all of them are killed at once. However, in a given period of time a certain number is killed while the remainder survives. If the surviving micro-organisms are once more exposed to the temperature treatment for the same period of time an equal proportion of them will be killed. On this basis the lethal effect of sterilization can be mathematically expressed as a logarithmic function: K t = log N/Nt where N = number of micro-organisms/spores originally present Nt = number of micro-organisms/ spores present after a given time of treatment (t) K = constant t = time of treatment A logarithmic function can never reach zero, which means that sterility defined as the absence of living bacterial spores in an unlimited volume of product is impossible to achieve. Therefore, the more workable concept of sterilizing effect or sterilizing efficiency is commonly used. The sterilizing effect is expressed as the number of decimal reductions achieved in a process. A sterilizing effect of 9 indicates that out of 109 bacterial spores fed into the process, only 1 (100) will survive. Spores of Bacillus subtitles or Bacillus
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stearo thermo philus are normally used as test organisms to determine the efficiency of UHT systems, because they form fairly heat resistant spores.
1.14.
Q10 value. The sterilizing effect of heat sterilization increases rapidly with the increase in temperature as described above. This also applies to chemical reactions which take place as a consequence of an increase in temperature. The Q10 value has been introduced as an expression of this increase in speed of reactions and specifies how many times the speed of a reaction increases when the temperature is raised by 50F. Q10 for flavor changes is in the order of 2 to 3, which means that a temperature increase of 50F doubles or triples the speed of the chemical reactions. A Q10 value calculated for killing bacterial spores would range from 8 to 30, depending on the sensitivity of a particular strain to the heat treatment. DValue. This is also called the decimal reduction time and is defined as the time required to reduce the number of microorganisms to one-tenth of the original value, i.e. corresponding to a reduction of 90%. Z-Value. This is defined as the temperature change which gives a 10-fold change in the D-value. F0 Value. This is defined as the total integrated lethal effect and is expressed in terms of minutes at a selected reference temperature of 250F. F0 can be calculated as follows: F0 = 10(T - 250.1) /z t/60, where T = processing temperature (F) z = Z-value (F) t = processing time (seconds) F0 = 1 after the product has been heated to 250F for one minute. To obtain commercially sterile milk from good quality raw milk, for example, an F0 value minimum of 5 to 6 is required. B* and C* Values. In the case of milk treatment, some countries are using the following terms: Bacteriological effect: B* (known as B star)
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B* is based on the assumption that commercial sterility is achieved at 275F for 10.1 seconds with a corresponding Z-value of 51F; this reference process is giving a B* value of 1.0, representing a reduction of thermo phallic spore count of 109 per unit (log 9 reduction). The B* value for a process is calculated similarly to the F0 value: B* = 10 ( T - 275 ) / 51 t/10.1, where: T = processing temperature (F) t = processing time (seconds) The C* value is based on the conditions for a 3 percent destruction of thiamine (vitamin B1); this is equivalent to 275F for 30.5 seconds with a Z-value of 89F. Consequently the C* value can be calculated as follows: C* = 10 ( T - 275 ) /89 t/30.5 Fig. 4 shows that a UHT process is deemed to be satisfactory with regard to keeping quality and organoleptic quality of the product when B* is > 1 and C* is < 1. The B* and C* calculations may be used for designing UHT plants for milk and other heat sensitive products. The B* and C* values also include the bacteriological and chemical effects of the heating up and cooling down times, and are therefore important in designing a plant with minimum chemical change and maximum sterilizing effect. The more severe the heat treatment is, the higher the C* value. For different UHT plants the C* value corresponding to a sterilizing effect of B* = 1 will vary greatly. A C* value of below 1 is generally accepted for an average design UHT plant. Improved designs will have C* values significantly lower than 1. The APV Steam Infusion Sterilizer has a C* value of 0.15.
1.15.
Residence Time
Particular attention must be paid to the residence time in a holding cell or tube and the actual dimensioning will depend on several factors such as turbulent versus laminar flow, foaming, air content and steam bubbles. Since there is a tendency to operate at reduced residence time in order to minimize the chemical degradation (C* value < 1), it becomes increasingly important to know the exact residence time. The APV infusion system has been designed with a special pump mounted directly below the infusion chamber, which ensures a sufficient
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over-pressure in the holding tube in order to have a single phase flow free from air and steam bubbles. This principle enables APV to define and monitor the holding time and temperature precisely and makes it the only direct steam heating system which allows true validation of flow and temperature at the point of heat transfer. The concept is illustrated in Fig. 1.4
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1.16.
Heating milk and other food products to high temperatures results in a range of complex chemical reactions causing changes in color (browning), development of off-flavors and formation of sediments. These unwanted reactions are largely avoided through heat treatment at a higher temperature for a very short time. It is important to seek the optimum time/temperature combination which provides sufficient kill effect on spores but at the same time, limits the heat damage in order to comply with market requirements for the final product. Even though the time/temperature combination is decisive for the final quality of the product attention also has to be paid to the actual heating profile since various reactions take place at different temperatures. This is illustrated in Fig. 1.5 in which type a deposit is a voluminous protein-rich deposit, whereas type B deposit is a mineral-rich deposit primarily developing at high temperatures. In particular type a deposit which originates from protein denaturation must be minimized since it is harmful to the product quality.
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CHAPTER # 2
PT 100
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PT 100
2.1. Introduction
The PT100 RTD Evaluation Board allows the user to evaluate Microchips solution to accurately measure temperature using RTD. When biasing RTDs to measure temperature, self-heat due to power dissipation has to be considered. RTD resistance availability typically ranges from 100 to 5,000. In order to measure the output voltage across the RTD over a wide temperature range, the biasing current has to be relatively high. This higher current causes more power dissipation through heat and skews the temperature reading. Microchps solution to this challenge is to use an MCP6S26 Programmable Gain Amplifier (PGA) to increase the sensor dynamic output range and increase measurement resolution while significantly reducing the biasing current magnitude. This board consists of a surface mount RTD to measure the PCB temperature. In addition, the user can connect and measure an external leaded RTD (2, 3 or 4-Wire) and configure the corresponding jumper to remotely measure temperature. The multiple input channel PGA adds gain programmability into the analog circuit. The multiple input channels are used to switch between RTDs and the gain is used to increase the sensor dynamic range. The PGA output is connected to a differential amplifier circuit which allows the user to scale the sensor output. The differential output is digitized using an MCP3301 12-bit differential analog-todigital converter. The data is transmitted to the PC using the USB interface. A Microsoft Excel-based Graphical User Interface (GUI) is used to obtain and display the data in realtime.
2.2. Features
The PT100 RTD Evaluation Board has the following features: A surface mount PT100 RTD External (2, 3 or 4-wire) RTD connector Gain and input channel programmability using MCP6S26 PGA MCP3301 12-Bit + sign ADC MCP41010 10 k Digital Potentiometer PIC18F2550 PICmicro Microcontroller
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PT 100
Figure 2.1.
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PT 100
Figure 2.2.
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PT 100
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PT 100
2. Select Enable/Disable for CH0 or CH1 (Channel 0 and Channel 1, respectively). 3. Select PGA gain, ADC sampling rate and sampling buffer size for the strip chart display. 4. Click start to start acquisition, stop to stop acquisition. Reset to Clear buffer. 5. Adjust the digital potentiometer positions to select the differential amplifier gain and trim the current sources for the local and external RTDs.
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PT 100
The amplifier maintains constant voltage at the transistor emitter terminal. Therefore, the emitter and collector currents are constant. The collector current biases the RTD. The biasing current can be fine tuned by adjusting the 10 k digital potentiometer using the GUI. A 100, 0.1% resistor is available for system calibration at 0C (RTD resistance at 0C is 100). This resistor can be jumped using JP1. When connecting an external PT100 RTD, connect JP2 to External Position.
Figure 2.5.
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The GUI uses a Microsoft Excel-based macro to open the USB port and communicate with the PIC18F2550. When the file is opened, the macro checks hardware status. The status display indicates hardware status as shown in Figure 2.6.
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PT 100
When start is clicked, the macro double checks hardware availability before starting the acquisition. All user options such as Sampling time, Strip chart buffer size, Digi. Pot Positions, or PGA Chn/Gain setup can be changed during acquisition.
1.TF101N
-50C...+550C Platinum resistance temperature sensor on ceramic substrate intended for installation into any housing depending to users requirements. Very small and quick sensor, only suitable for further treatment. Notice: do not cut the sensor leads. Thermal response time refer to manufacturer data: T0,9 in the air 10 s, in water <1 s
2. TF101K
-50C.. .+200C Platinum resistance temperature sensor on ceramic substrate protected by a heat-shrinkable sleeve and with PTFE isolated stranded wire. The TF101K version can be installed in motor or transformer windings. When build-in into windings do not pressure the sensor element. Precautions should be taken to protect sensor and extension leads against push and pull
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3. TF 101U2
-30C...+105C Sensors TF101U2 are encapsulated in a stainless-steel-shell V4A. They are suitable for measuring temperatures in fluids, under isolations, at surfaces or for inside or outside applications. The protection class is IP 66. The version with PVC-isolated cable (3 x 0,25 mm2 in one cable) can be easily wired. The maximum ambient temperature is 105 C.
-50C...+200C
4. TF101G3
-50C...+200C Platinum resistance temperature sensor on ceramic substrate built into a M6 brass threaded bush, especially suitable for being screwed into metal, e.g. for monitoring temperature of heat sinks or heating plates. Please note that there will be a measuring error due to the design,
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as the sensor can loose heat via the connection strand.Cable length: 2000 mm Weight: 21 g. (Dimensions see Dimension illustrations)
5. TF101ZG2
-50C...+200C Platinum resistance temperature sensor built into steel tube V4A, 1/2 inch, suitable for installation in pipes. Thermal response time T0,9 in the air 255 s, in water 45 s. Suitable for transmission in 2- or 3-wire technique. Weight 120 g (Dimensions see Dimension illustrations) Order numbers: 110 mm insertion depth T223137
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2.9. Cabling
ZIEHL thermostats of TR series are generally insensitive to interference in the sensor line. Occasionally, however, undesirable switching is unavoidable, especially when temperature is near the switching point. For this reason it is highly recommended that cables are not laid parallel to power current lines over long distances. When appropriate, cables should be screened or twisted together.
2.9.1. Line-resistance
With RTD sensors the resistance of the connecting cable should be considered, otherwise
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there is an measuring error. The resistance must be compensated. The resistance of a connecting cable can be calculated as follows: R [] = 2 x l/(k x A), l = cable length [m], k = conductivity [S x m/mm2] e.g. Cu = 56, A = cross sectional area [mm2] For example copper-wire: I = 50 m, cross sectional area 1 mm2: R = 2 x 50/(56 x 1) = 1,79 , Resulting error = 1,79 /0,385 x K = 4,6 K.
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3-Wire Technique With 3-wire connection, a third wire (sense) connected to the sensor registers the drop in voltage in one line. For compensation of line resistance it is assumed that the voltage drop in the second line is identical (i.e. the same wire and same wire temperature). Compensation is then performed automatically. Possible changes of resistance in the line due to temperature changes are also compensated for.
4-wire technique With 4-wire connection, impressed current flows via two wires to the sensor. Via a two sensor line the drop in voltage is measured directly at the sensor. Possible differences in the sensor connection wiring can be disregarded. A disadvantage is the higher costs involved in running 4 wires.
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Combination of 2- and 3-wire technique When connecting 2-wire-sensors to units with 3-wire input, the line resistance can be compensated by connecting a compensation resistor (Rk) between ground and sense input. Rk must have the same value as the resistance of the line. The sensor then has to be connected to the + and the sense- input. Rk must be lower than the permitted resistance for 1 line of the 3-wire-input. Units requiring 3-wire configurations can also be operated by 2-wire sensors. The sensor input is simply shortened. The line resistance need not be compensated. 3-wire sensors can be used as 2-wire sensors, simply by omitting one wire. 2-wire sensors can be branched at any desired position in a 3 or 4-wire connection system. In this case though, the line resistance of the two wires from the branching point to the sensor is not compensated. ZIEHL thermostats, series TR are designed for use with 2 or 3-wire connection.
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Figure 2.7.
2.11.1.
Two-wire connection
Two-wire connections make life easy for the technician but at the expense of a much greater likelihood of measuring errors arising when long extension leads are used. The problem results from the resistance of the lead being added straight into the measured value. At 20C, the resistance of a 10-m, 2 x 0.25 mm2 copper lead is 1.4 ohms. In terms of temperature, this translates into a measuring error of 3.6 C. It is possible to eliminate the error through calibration, but every time the ambient temperature around the lead changes, the resistance
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will also change, producing a new error. A Pt1000 film detector would reduce the magnitude of the error to a tenth. If this is acceptable still there would then be a greater risk of self heating.
2.11.2.
Three-wire connection
A three-wire connection will eliminate most of the effect of the lead resistance on the measured value, although this is conditional on all three wires having the same resistance. This is almost impossible to achieve in practice. In fact only two wires have to have equal resistances but as two of them are colour coded red you cannot easily know which is the critical one. This is the reason we say all three wires should hav equal resistances.
Wires often come from different drawing mills and can therefore have a resistance that differs by 510%.
One or more strands may be missing in one of the leads. Pentronic has encountered leads in which two of the seven strands were missing - a difference of 28% in the lead resistance.
In extreme cases, there may be a combination of these factors at play. For example: a tenmeter length of three-wire lead that has a resistance difference across the wires of 10% will give a reading error of 0.18C. However, a three-wire lead will solve the problem of the effect of the temperature range on the wires.
2.11.3.
Four-wire connection
All instruments designed for optimum measuring accuracy have four-wire connections. The current and the signal are separated into two circuits, which render the unbalance in the resistances of the wires insignificant. This is true provided that the difference is not of an excessive magnitude - up to 100 ohms is often acceptable with modern instruments. The four-wire system was previously confined to laboratory use but is now used in process equipment, eg, indicators and controllers.
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CHAPTER # 3
SOLENOID VALVE
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Solenoid Valve
3.1. Introduction:
A solenoid is a coil wound into a tightly packed helix. In physics, the term solenoid refers to a long, thin loop of wire, often wrapped around a metallic core, which produces a magnetic field when an electric current is passed through it. Solenoids are important because they can create controlled magnetic fields and can be used as electromagnets. The term solenoid refers specifically to a coil designed to produce a uniform magnetic field in a volume of space (where some experiment might be carried out). In engineering, the term solenoid may also refer to a variety of transducer devices that convert energy into linear motion. The term is also often used to refer to a solenoid valve, which is an integrated device containing an electromechanical solenoid which actuates either a pneumatic or hydraulic valve, or a solenoid switch, which is a specific type of relay that internally uses an electromechanical solenoid to operate an electrical switch; for example, an automobile starter solenoid, or a linear solenoid, which is an electromechanical solenoid figure 3.1.
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A solenoid with 3 Amprian loops: a, b and c. In short: the magnetic field inside an infinitely long solenoid is homogeneous and its strength does not depend on the distance from the axis, nor on the solenoid cross-sectional area. This is a derivation of the magnetic flux density around a solenoid that is long enough so that fringe effects can be ignored. In the diagram to the right, we immediately know that the flux density vector points in the positive z direction inside the solenoid, and in the negative z direction outside the solenoid. We see this by applying the right hand grip rule for the field around a wire. If we wrap our right hand around a wire with the thumb pointing in the direction of the current, the curl of the fingers shows how the field behaves. Since we are dealing with a long solenoid, all of the components of the magnetic field not pointing upwards cancel out by symmetry. Outside, a similar cancellation occurs, and the field is only pointing downwards. Now consider the imaginary loop c that is located inside the solenoid. By Ampre's law, we know that the line integral of B (the magnetic flux density vector) around this loop is zero, since it encloses no electrical currents (it can be also assumed that the circuital electric field
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passing through the loop is constant under such conditions: a constant or constantly changing current through the solenoid). We have shown above that the field is pointing upwards inside the solenoid, so the horizontal portions of loop c do not contribute anything to the integral. Thus the integral of the up side 1 is equal to the integral of the down side 2. Since we can arbitrarily change the dimensions of the loop and get the same result, the only physical explanation is that the integrands are actually equal, that is, the magnetic field inside the solenoid is radially uniform. Note, though, that nothing prohibits it from varying longitudinally, which in fact it does.
3.3. Outside
Magnetic field created by a solenoid (cross-sectional view) described using field lines. A similar argument can be applied to the loop a to conclude that the field outside the solenoid is radially uniform or constant. This last result, which holds strictly true only near the centre of the solenoid where the field lines are parallel to its length, is important in as much as it shows that the flux density outside is practically zero since the radii of the field outside the solenoid will tend to infinity.
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An intuitive argument can also be used to show that the flux density outside the solenoid is actually zero. Magnetic field lines only exist as loops, they cannot diverge from or converge to a point like electric field lines can (see Gauss's law for magnetism). The magnetic field lines follow the longitudinal path of the solenoid inside, so they must go in the opposite direction outside of the solenoid so that the lines can form a loop. However, the volume outside the solenoid is much greater than the volume inside, so the density of magnetic field lines outside is greatly reduced. Now recall that the field outside is constant. In order for the total number of field lines to be conserved, the field outside must go to zero as the solenoid gets longer. Of course, if the solenoid is constructed as a wire spiral (as often done in practice), then it emanates an outside field the same way as a single wire, due to the current flowing overall down the length of the solenoid.
where
This equation is for a solenoid with no core. The inclusion of a ferromagnetic core, such as iron, increases the magnitude of the magnetic flux density in the solenoid. This is expressed
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by the formula
where eff is the effective or apparent permeability of the core, which is a function of the geometric properties of the core and its relative permeability. This equation is often used incorrectly due to the lack of understanding of the difference between relative and effective permeability, which can in fact differ by many orders of magnitude. For an open magnetic structure, the relationship between the effective permeability and relative permeability is given as follows:
3.5. Magnetic Field and Vector Potential For Finite Continuous Solenoid
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Solenoid Valve
Magnetic field line and density created by a solenoid with surface current density A finite solenoid is a solenoid with finite length. Continuous means that the solenoid is not formed by discrete coils but by a sheet of conductive material. We assume the current is uniformly distributed on the surface of it, and it has surface current density K. In cylindrical coordinates:
The magnetic field can be found by vector potential. The vector potential for a finite solenoid with radius a, length L in cylindrical coordinates is is[citation needed]:
where
The kind.
, and
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By using
coil. Ignoring end effects, the total magnetic flux through the coil is obtained by multiplying by the cross-section area :
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Solenoid Valve
A table of inductance for short solenoids of various diameter to length ratios has been calculated by Dellinger, Whitmore, and Ould.[3] This, and the inductance of more complicated shapes, can be derived from Maxwell's equations. For rigid air-core coils, inductance is a function of coil geometry and number of turns, and is independent of current. Similar analysis applies to a solenoid with a magnetic core, but only if the length of the coil is much greater than the product of the relative permeability of the magnetic core and the diameter. That limits the simple analysis to low-permeability cores, or extremely long thin solenoids. The presence of a core can be taken into account in the above equations by replacing the magnetic constant 0 with or 0r, where represents permeability and r relative permeability. Note that since the permeability of ferromagnetic materials changes with applied magnetic flux, the inductance of a coil with a ferromagnetic core will generally vary with current.
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The force applied to the armature is proportional to the change in inductance of the coil with respect to the change in position of the armature, and the current flowing through the coil (see Faraday's law of induction). The force applied to the armature will always move the armature in a direction that increases the coil's inductance. Electromechanical solenoids are commonly seen in electronic paintball markers, pinball machines, dot matrix printers and fuel injectors.
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found in a B-29 aircraft fuselage on display at the National Museum of the USAF in Dayton, Ohio. Solenoids of this variety continue to be used in countless modern applications, and are still manufactured under Leland's original brand "Ledex", now owned by Johnson Electric.
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Solenoid Valve
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Solenoid Valve
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Solenoid Valve
3.11.1 . Features
- Reproducible switching point accuracy - Long mechanical and electrical service life - Readily retrofitted - Simple, accurate adjustment of switching point - With LED indicator
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Solenoid Valve
3.12.1. Features
- Higher peak pressures produced by radial flow - Spacing from 75 mm (between pipe centres) - No welding or adjustment necessary - Simple, economical connection of valve to irregularly shaped tanks - Available pipe lengths: 70 to 200 mm - High-grade aluminium tube
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CHAPTER # 4
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4.1. Introduction
The growth of UHT milk has been remarkable, increasing worldwide in the past 20 years especially in Europe, Asia, and South America. Surprisingly, shelf-stable milk consumption in the U.S. is very low compared to other regions in the world (Burton 1988; Kissell 2004). UHT-processed fluid milk is very popular in other parts of the world; however, the U.S. population has been slow to accept it because of the "cooked" flavor in the UHT milk, their familiarity with fresh milk (Dairy Biz Archive 2000), and the higher cost of UHT milk (Kissell 2004). A number of studies have determined sensory properties of various milk samples including plain milk (Claassen and Lawless 1992; Frost et al. 2001; Francis et al. 2005), chocolate milk (Thompson et al. 2004), powdered milk (Kamath et al. 1999; Drake et al. 2003) and processed milks that are not specific to UHT milk (Chapman et al. 2001; Fromm and Boor 2004; Clare et al. 2005). In addition, lexicons for milk alternatives, such as soymilk, have been published (Torres-Penaranda and Reitmeier 2001; Day N' Kouka et al. 2004; Chambers et al. 2006; Keast and Lau 2006). Descriptive sensory terms for ultra-pasteurized milk were developed by Chapman et al. ( 2001) and were primarily described as "cooked aroma" and "cooked flavor". Clare et al. (2005) used cooked/ caramelized, sweet aromatic/cake mix, fatty/ stale, sweet taste, bitter taste, astringent, and color intensity to differentiate UHT from microwave-treated milks. Fromm and Boor (2004) characterized sensory shelf-life attributes for pasteurized fluid milk. Attributes related to milk flavor defects describing as hay/grain, sour/fermented, baby
formula, nutty, rancid, and metallic were key sensory attributes associated with pasteurized fluid milk throughout shelf-life. These results showed that excluding bacterial contaminants from milk is essential to extend shelf-life of milk products. Processing variables have been shown to affect sensory properties of preserved milk. Clare et al. (2005) found that UHT milk had more caramelized and fatty/stale flavor, more brown color, and more astringency than microwave processed milk probably because of the higher heat treatment. Keast and Lau (2006) found regional differences in sensory quality of soymilk with those from Asia (Hong Kong, Malaysia and Singapore) being sweeter, less salty, darker in color, and stronger in beany flavor than soymilks. Although previous
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researchers have investigated the sensory properties of processed milks, none have shown complete information for explaining the sensory characteristics of UHT milk or have
considered the differences of UHT milk properties based on country of origin. Although there are many potential reasons that UHT milk is more accepted in countries other than the U.S., it is possible that differences in regional milk source or processing requirements from country to country could result in sensory differences that would have an impact on
acceptance. If the sensory properties of UHT milk from different countries can be grouped and differentiated from those in the U.S., it may be possible to determine sensory properties of UHT milk that can be modified to improve U.S. UHT milk. The objectives of this study were to 1) determine the sensory properties of a wide range of commercial UHT milk samples from various countries representing different regions of the world, to 2) compare flavor and texture differences among samples from various countries to determine if regional differences are a major influence on sensory properties of UHT milk, and to 3) compare UHT to control pasteurized and sterilized milk samples.
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refrigerator, True Manufacturing Co, St Louis, MO, USA) for storage at 1C.
4.3.1 Panelists
Five highly trained panelists from the Sensory Analysis Center, Kansas State University (Manhattan, KS) participated in the study. Each panelist had completed 120 h of training in sensory evaluation of foods; had a minimum of 2000 h of testing experience on a variety of food products including fresh milk, UHT milk, soy milk, yogurt, ice cream, and cheese. Other researchers have used trained panelists to describe the flavor (TalaveraBianchi, Chambers, and Chambers, 2008) and texture characteristics of dairy products (Yates and Drake, 2007; Karagul-Yuceer, Isleten, and Uysal-Pala, 2007).
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provided for start and shutdown operations of the separator allow the continuous operation of the separator during the UHT process. By use of the buffer tank, the UHT heating can be maintained without interruption during the automated solids discharge of the separator. The In-Line Separation is integrated in the automatic process control of the UHT Plant so that the process steps in a thermal heating plant such as sterilization, cooling, production, production stop and CIP are completely automated.
Fig 4.1 Line Separation for UHT milk, and to rate the intensities of the control milk samples. Because of the limited amount of international samples, panelists were initially given six locally purchased UHT and ultra-pasteurized milk samples to begin the lexicon development. During orientation sessions, the procedures for attribute determination and vocabulary description were adapted from flavor profile analysis (Caul 1957; Keane 1992) and other studies for developing flavor and texture lexicons (Drake et al., 2007; Lee and Chambers 2007; Talavera-Bianchi, Chambers, and Chambers, 2008; Hongsoongnern and Chambers, 2008a,b). A discussion of milk samples was held until the panel came to agreement on attribute description of UHT milk. The panel changed some attribute definitions and references after orientation sessions. They deleted attributes that they did not find in UHT, pasteurized or sterilized milk samples and added new attribute terms they found in samples they had not previously tasted. The final
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attributes, definitions, and references used to describe sensory properties of UHT, pasteurized.
(Version 10.2, 2005, SYSTAT Software, Inc, San Jose, CA). The covariance matrix was used for extraction and the varimax procedure was used for rotation. Attributes where all scores were the same for all samples and attributes present in 5 or fewer samples were removed before the analysis. PCA plots of the major principal components were made to show differences and similarities among UHT, pasteurized, and sterilized milks. Hierarchical cluster trees based on sensory properties were obtained from hierarchical cluster analysis (Ward's method) using the SYSTAT program version 10.2(2005, SYSTAT Software, Inc,
San Jose, CA). Attributes added to previous lexicons to better describe the texture and flavor of in some samples. Dairy notes (overall dairy, dairy fat and dairy sweet) and fat feel were negatively correlated with chalky texture and processed flavor. Overall dairy showed little linear or curvilinear
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relationship to cooked and brown flavors when examined either by correlation or plots. That indicates that brown and cooked notes may be modified independently of dairy impact. Malty flavor appeared in only a few samples, but when it did it seemed to have some positive relationships to brown, cooked, fat feel, and dairy fat. Three major clusters of UHT, pasteurized, and sterilized milk samples were found, but they did not group on the basis of either country or fat content. There were more similarities of milks from the same manufacturer than milks from the same country or milks with the same fat content. This suggests that manufacturing process may have affected the sensory properties of UHT milks much more than did country of origin or fat content, disproving our theory that the base milk may be a major factor in U.S. consumers dislike of UHT milk, while consumers in other countries find it acceptable. Cluster 1 consisted of milk samples from most countries included in this study, except for Peru and the U.S., with the different manufacturers. The milks in this cluster were highest in dairy fat, dairy sweet, overall dairy flavor, and fat feel and had little or no chalky or processed flavor. The two pasteurized control milk samples also appeared in this cluster. Although other clusters contained whole milk samples, this cluster consisted only of whole milk, which may indicate that in order to have the highest dairy notes and fat feel with little or no processing effect, the UHT milk should be made from whole milk. Cluster 2 consisted of samples from six of the seven countries included in this study, all the various fat levels, and various manufacturers. These samples typically were moderate to high in dairy notes (dairy fat, dairy sweet, and overall dairy) and fat feel, and had low levels of chalky and processed notes. This cluster included most of the samples from Parmalat and most of the U.S. samples. A subcluster in that group contained samples that generally were highest in cooked, but without the processed note found in some other samples. All the products in that subcluster were malty; something unique to that group. Products in that subcluster came from Italy, Thailand, and Peru, including 2 samples (a whole and a low-fat) from the same manufacturer in Thailand. One of the sub-clusters included most of the U.S. milk samples (four out of seven) and half of the Parmalat samples, including Parmalat samples from both Italy and the U.S. This group of milk had higher processed notes and scored in the middle of all samples for cooked and brown. Those products had moderate to higher levels of dairy notes and no maltiness was found in them. The third subcluster in that group was comprised of samples from Italy,
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France, Korea, and Peru. Sensory properties in that subcluster fell in the midrange of most products. Cluster 3 consisted of about one-third of the Thai samples (including 2 pairs of products from the same brands in Thailand), two Italian samples, and 1 U.S. sample from the same manufacturer as one of the Italian samples. These products had the highest levels of processed, cooked, brown and some of the highest chalky scores of all products tested. This groups contained samples with the lowest levels of dairy sweet and dairy fat. The two sterilized milk samples from Thailand were in this cluster which should not be surprising given their high level of processing. The attributes in this cluster and the fact that the sterilized milks are in this cluster suggest processing, rather than country or fat content, related issues associated with the milks in this group.
Figure 4.2.
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CHAPTER # 5
TEMPERATURE CONTROLLER
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Temperature Controller
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Temperature Controller
A) Thermal Lag the time delay for a temperature change in one part of the system to show up in other parts of the system; this varies considerably with the operating temperature, ambient conditions, mass & conductivity of the load etc. B) Temperature the variations in temperature between different physical Gradients parts of the system at any given instant. C) Sensor placement of the sensor in relation to the heat source and Location the load. D) Controller these contribute to the inherent accuracy of the controller Sensitivity & and determine its suitability for any application. E) Heat Balance for temperature control to be possible, there must be more heat available from the heat source than is actually required to maintain the desired temperature and replace losses.
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Temperature Controller
parameters can usually be adjusted (or tuned) by the user to give the optimum control for the particular conditions of their system. C) Auto-Tune in this type of control, the controller has onboard logic which will enable it to automatically select the optimum values for the Proportioning, Integral and Derivative parameters; it does this by monitoring the rate of temperature rise of the system and the subsequent response to heat input. The operator doesnt normally need to alter any settings on the controller. D) Fuzzy Logic the controller automatically and gradually decreases or increases the internal set-point until the process stabilizes at the desired operating temperature; this results in the elimination of overshoot/ undershoot.
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An offset in the control temperature can be compensated by incorporating an Integral parameter, which positions the proportional band for the correct power output to achieve equilibrium at set-point. (PI control). A further addition of the Derivative function (to give PID control) can provide anticipatory control and a fast reaction to disturbances. This is a derivative of the error between actual temperature and set point temperature with respect to time; it is typically set to a value approx. 15% of the I value.
5.6. Outputs
The controller output has to be interfaced to the heat source (or other actuating device) and this is done by various methods, the choice of which depends on the type of process and equipment being used; A) Relay O/P used in on/off or time proportioning modes to switch contactors etc.; electromechanical relays are inexpensive, small, usually housed within the controller, but can have limited life if cycled rapidly - where more rapid switching is needed a solid state relay is recommended.
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Temperature Controller
B) SSR O/P this is a switching device which contains 2 SCRs (silicon (Solid State Relay) controlled rectifiers) or a single triac complete with a zero voltage crossover or synchronizing drive circuit; it usually takes the form of a potted assembly having no moving parts to wear out, and can be either ac or dc input type. C) Analogue where continuously variable control is needed, a OUTPUT linear DC voltage or current output can be used; 4- 20mA, 0-5V, 0-10V, 1-5V are all standard outputs and are used for e.g. control valve actuators, thyristor drives etc. which vary the power to the load. The output relays of temperature controllers are capable of switching currents typically 8, 16 or 20 Amps depending on the model of controller. Most heater loads however, are typically more than the controller's relay can handle. For these applications solid state relays or Thyristor power controllers depending on the type of load and the type of control required, need to be incorporated within the control system.
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portion of the AC cycle, similarly if half power is required the device is not triggered to conduct until it is 50% of the way through half of a mains cycle. This type of triggering is ideal for low inertia heaters such as lamps and air heater show in figure 5.1.
Wt= Total power R = heater resistance VP = phase voltage IP = phase current VL = line voltage IL = line current Single Phase, Line And Neutral Or Line And Line
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Temperature Controller
Wt= 1.73VL x IL or 3 x VL 2/R Where VL = 1.73 x VP Three Phase, Four Wire, STAR Configuration
Wt = 3 x VL x IL or 3 x VL 2/R Where VL = VP and IL = IP The Proportional-Integral-Derivative (PID) algorithm As the name suggests, the PID algorithm consists of three basic modes, the Proportional mode, the Integral and the
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Temperature Controller
Derivative modes. When utilizing this algorithm it is necessary to decide which modes are to be used (P, I or D?) and then specify the parameters (or settings) for each mode used. Generally, three basic algorithms are used P, PI or PID. A Proportional algorithm the mathematical representation is,
The proportional mode adjusts the output signal in direct proportion to the controller input (which is the error signal, e). The adjustable parameter to be specified is the controller gain, kc. This is not to be confused with the process gain, kp. The larger kc the more the controller output will change for a given error. For instance, with a gain of 1 an error of 10% of scale will change the controller output by 10% of scale. Many instrument manufacturers use Proportional Band (PB) instead of kc.1 The time domain expression also indicates that the controller requires calibration around the steady-state operating point. This is indicated by the constant term mvss. This represents the 'steady-state' signal for the mv and is used to ensure that at zero error the cv is at set point. In the Laplace domain this term disappears, because of the deviation variable representation. A proportional controller reduces error but does not eliminate it (unless the process has naturally integrating properties), i.e. an offset between the actual and desired value will normally exist. A proportional integral algorithm the mathematical representation is,
The additional integral mode (often referred to as reset) corrects for any offset (error) that may occur between the desired value (set point) and the process output automatically over time2. The adjustable parameter to be specified is the integral time (Ti) of the controller. Reset is often used to describe the integral mode. Reset is the time it takes for the integral action to produce the same change in mv as the P modes initial (static) change. Consider the following figure,
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Temperature Controller
The output immediately steps due to the P mode. The magnitude of the step up is Kce . The integral mode then causes the mv to ramp. Over the period 'time 0 to time TI' the mv again increases by Kce. Integral wind-up When a controller that possesses integral action receives an error signal for significant periods of time the integral term of the controller will increase at a rate governed by the integral time of the controller. This will eventually cause the manipulated variable to reach 100 % (or 0 %) of its scale, i.e. its maximum or minimum limits. This is known as integral wind-up. A sustained error can occur due to a number of scenarios, one of the more common being control system override. Override occurs when another controller takes over control of a particular loop, e.g. because of safety reasons. The original controller is not switched off, so it still receives an error signal, which through time, winds-up the integral component unless something is done to stop this occurring. There are many techniques that may be used to stop this happening. One method is known as external reset feedback (Luyben, 1990). Here, the signal of the control valve is also sent to the controller. The controller possess logic that enables it to integrate the error when its signal is going to the control value, but breaks the loop if the override controller is manipulating the
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Derivative action (also called rate or pre-act) anticipates where the process is heading by looking at the time rate of change of the controlled variable (its derivative). TD is the rate time and this characterizes the derivative action (with units of minutes). In theory derivative action should always improve dynamic response and it does in many loops. In others, however, the problem of noisy signals makes the use of derivative action undesirable (differentiating noisy signals can translate into excessive mv movement). Derivative action depends on the slope of the error, unlike P and I. If the error is constant derivative action has no effect. Use Matlab / Simulink to explore the effect a step change in error has on the various modes of an ideal PID control algorithm. Assume that kc = 1, Ti = 10 mins and TD = 5mins. PID algorithms can be different Not all manufactures produce PIDs that conform to the ideal 'textbook' structure. So before commencing tuning it is important to know the configuration of the PID algorithm! The majority of text-book tuning rules are only valid for the ideal architecture. If the algorithm is different then the controller parameters suggested by a particular tuning methodology will have to be altered.
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6.1. Introduction
As long as 130 years ago, Sir William Siemens made the suggestion that the change of electrical resistance of metals as a result of changes in temperature could be utilized for the measurement of temperature itself. The material to be used should be a noble metal: platinum, since platinum shows characteristics that are not shared by other metals. In 1886 Siemens continued to develop the platinum resistance thermometer, and, by taking appropriate precautions, constructed a precision resistance thermometer that was suitable for measuring high temperatures. Since then, platinum resistance thermometers have been used as indispensable devices for measuring temperature as a physical variable. These days, specially adapted designs make it possible to cover a multitude of applications over the temperature range from 200 to +850 C. Platinum thermometers can thus be used not only in industrial measurement technology, but in sectors such as HVAC engineering, household equipment, medical and electrical engineering, as well as in automobile technology. Wire wound platinum temperature sensors on a glass or ceramic core as well as platinum chip sensors made in thin-film technology are incorporated as the temperature-sensitive heart of the resistance thermometer. Temperature-dependent resistance Platinum temperature sensors use the effect of the temperature-dependence of the electrical resistance of the noble metal platinum. Since the electrical resistance increases with rising temperature, we speak of a positive temperature coefficient (often abbreviated to PTC) for such temperature sensors. In order to use this effect for measuring temperature, the metal must vary its electrical resistance with temperature in a reproducible manner. The characteristic properties of the metal must not change during operation, as this would result in measurement errors. The temperature coefficient should, as far as possible, be independent of temperature, pressure and chemical influences. Standardized platinum temperature sensors For more than 130 years, platinum has been the basic material of choice for temperature- dependent sensors. It has the advantage that it is highly resistant to corrosion, is relatively easy to work (especially in wire manufacture), is available in a very pure state and exhibits good reproducibility of its electrical properties. In order to maintain the features noted above and to ensure
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interchangeability, these characteristics are defined in the internationally valid standard IEC 751 (translated in Germany as the DIN EN 60 751). This standard specifies the electrical resistance as a function of temperature (table of reference values), permissible tolerances (as tolerance classes), the characteristic curves and usable temperature range. The characteristic curves are calculated using certain coefficients, whereby the calculation distinguishes between the temperature ranges from 200 to 0 C and from 0 to 850 C. The range 200 to 0 C is covered by a third-order polynomial: R(t) = R0 (1+ A x t + B x t2+Cx(t100C) x t3) A second-order polynomial is applied for the range 0 to 850 C R(t) = R0 (1+Axt+Bxt2) with the coefficients A = 3.9083x103C1 B = 5.775x107C2 C = 4.183x1012C4 The term R0 is referred to as the nominal value, and represents the resistance at 0 C. According to EN 60 751, the nominal value is 100.000_ at 0 C. It is therefore referred to as a Pt 100 temperature sensor. Temperature sensors with higher nominal values are also available on the market, such as Pt 500 and Pt 1000. They have greater sensitivity, since the slope of the characteristic is directly proportional to R0, the nominal value. Their advantage thus lies in the fact that their resistance has a larger change with temperature show in figure 6.1.
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The resistance change in the temperature range up to 100 C is approximately: 0,4_/ C for Pt 100 temperature sensors 2,0_/ C for Pt 500 temperature sensors and 4,0_/ C for Pt 1000 temperature sensors. As an additional parameter, the standard defines a mean temperature coefficient between 0 C and 100 C. It represents the average change in resistance, referred to the nominal value at 0 C:
R0 and R100 are the resistance values for the temperatures 0 C and 100 C respectively. Calculating the temperature from the resistance For the use as a thermometer, the resistance of the temperature sensor is used to calculate the corresponding temperature. The formulae cited above define the variation in electrical resistance as a function of temperature. For temperatures above 0 C, a closed form of the representation of the characteristic according to EN 60 751 can be derived to determine the temperature.
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Tolerance Class B applies for the entire defined range from 200 to +850 C. Extended tolerance classes the two tolerance classes specified in the standard are frequently inadequate for certain applications. JUMO has defined a further division of the tolerance classes, based on the standardized tolerances, in order to cover the widest possible range of applications throughout the market. In addition to the definition equations for the temperature-dependent deviations, the range of validity has also been defined. Because of the inexactly linear relationship between the resistance and temperature, measurements must be made at various temperatures to determine the deviations from the standard curve 3 (for t >0 C) or 4 (for t < 0 C) respectively. For series manufacture of temperature sensors, tests are generally made only at 0 C and 100 C. So it is not possible to make a precise determination of the individual characteristic of a temperature sensor. Since, on the one hand, it is not possible to make the measurement uncertainty endlessly small and, on the other hand, the characteristic curve is subject to variations caused by production tolerances, the range of validity of the narrower tolerance classes must be restricted compared with the measuring range of the temperature sensor. Another conclusion from this situation is that the temperature classes cannot be narrowed without limit.
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6.4. Applications
Monitoring and limiting temperatures, pressure and other process variables, e.g. Protection of burner control systems. Monitoring of heating elements. Protection of thermal oil systems. Protection of boiler plants.
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The standard signals can be processed by suitable indicator/ control units or directly on a PLC. Temperature compensation (TC) Depending on the instrument version which was ordered, the instrument can be operated without, with single or 4-fold temperature compensation. The strong dependency of the conductivity on the temperature of the medium usually necessitates a compensation of the temperature dependent variation. The version without TC can be used for measurements with stable temperature conditions in which measurement inaccuracies can be tolerated. In addition, instruments without TC can be connected to evaluation units in which TC is performed in the software, for example (PLC or similar) is also included in versions without TC. For most applications the version with a single TC is sufficient. A scaled potentiometer enables the adjustment of the temperature coefficient in the range 0 3%/C. The version with a 4-fold TC permits a very comfortable process control. Depending on the medium or the medium temperature up to 4 preset temperature coefficients can be selected (selection e.g. via PLC, depending on process development, medium or temperature). The temperature coefficients can also be set via 4 scaled potentiometers in the range 0 3 %/C. Measuring cell The cell consists of a hermetically sealed PVDF body inside which the two measurement coils are arranged. Holes in the measuring cell enable the measurement medium to flow through. The cell is temperature and pressure-stable to a high degree. For temperature measurement and compensation, the cell is fitted with a fast-response temperature sensor (Pt100). For applications which have to comply with the highest standards of hygiene, connection type Varivent is available which also features a cell with a special style (see detailed diagram of process connection -90). The measurement principle means that there is an inevitable isolation between the measurement medium and the current output show in figure 6.6 measuring cell.
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