Atmos Lab's Eliquid Analysis 10/2012 GR

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ITANEITIL.THMIO KPHTHL.
TMHMA IATPIKHI:
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpciKAuo Kpirtq P.O.Box 2208 Heraklion Crete,
Greece
TO!UCOAOfiAt
Llu:uOuv-rl]<;: KaOTJYll-riJ<; ApLa-rEt6T)<; M. Taa-raaKT)<;
Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uoc.gr http://ctoxres.med.uoc.qr
nl.r1PooplE<; : 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 88
IHETOTIOIHTIKO ANAAY:EH:E* KAI TASINOMH:EH:E TOY AIAAYMATO:E
ANATIAHP!!:EH:E AGRINIO
ETAIPIA: ATMOS LAB
EMDOPIKH ONOMAI:IA YTPOY ANAIIAHP!!l:Hl:: AGRINIO
API@MOI: TIAPTIAAI:: 01/AGRINIO 112
TIOIOTIKOI: TIPOl:AIOPil:MOl: AIAA YMATOI: ANATIAHP!!l:Hl:
E<DAPMOZOMENH ANAAYTIKH TEXNIKH: Aptoc; XpcoJlaToypacpia-<DacrJlaTOJlcTpia Masac; (Gas
Chromatography -Mass Spectrometry) Kat vypi] XpcoJlawypacpia-<DacrJlUTOJlcTpia Masac; (Liquid
Chromatography-Mass Spectrometry)
TIOI:OTIKOI: TIPOI:AIOPII:MOI: MEXPI TIOI:Ol:TOY 99,9997%
ATIOTEAEI:MAT A
TiivaKac; 1.
Opw llo<JOTtKoiJ
0\l<Jl(l
llo<JO<JTO llpo<J()wpt<f!lOil
(%w/v) Mt9o()o1.l (LOQ)
( m)
propylene glycol 3,21
0,198
glycerol 83,59
I ,187
water 11,6997
nicotine 1,5 0,1
l:i>vol..o 99,9997
Acv mstVOJlf:lLClt
Acv mstVOJlf:lLat
Oscia wstKo
11
m 1
oscia wstKO'tTJm 3
Xp6vta LOStKOLTJTU 2 cr
opyavtcrJlOUS
To Epyacrn']pw q>EpEt mcrronoiT]<YTJ crU!lq>wva llE to ISO: 17025 yta nc; 8tabtKao-iEc;
8taxEiptcrT]c;, Kat apxEw9tTTJ<rTJc; twv bEtY!l6.twv Kat AEttoupyEi llE 8taKptPwlltvEc; crucrKEutc; Kat 6pyava.
H opyavoA.oyia LC-MS q>EpEt btaKpipwcr'l Kat&. ISO: 17025 llE nEbio tT]V aviXVEU<YTJ vapKwnKv oucrtffiv
crtTJV tpixa.
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TASINOMH!:H TOY YrPOY ANAITAHP!11:H1: AGRINIO
Ms trtv AXL 265/2002, <DEK 1214/B' /19.9.2002, trtv tcov !J.c!J.OVco!J.EVcov
auatanKffiv tou !J.dy!J.atO<; Kat tou Kavovtcr!J.OU 1272/2008 (EK) to AGRINIO (Apt81J.6<;
I1aptioa<;: 01/AGRINI0/12) IJ.c 99,9997% O"Ucrtacrrt nou ava<ptpstat crtov I1ivaKa 1,
co<; !lll smKivouvo yta trtv av8pffimvrt uyda, yta to Kat !J.c n<; <pUatKOXll!J.tKE<; tou
t8t6trtt<;. Emnp6a8sta, yta trt XPTt<Jrt tou avanA.ftpcocrrt<; an6 tO rtAKtpovtK6 tcrtyapo,
to !J.ctY!J.U tcrnvs61J.CVCOV at!J.WV nou ansA.su8spffivstat un'
6\j/rt trtv Katocrnaia aucrtacrrt tcov at!J.WV nou napayovtat !J.c trtV svspyonoirtcrrt tou !lllXUVta!J.OU
Ut!J.07tOtrt<Jll<; !J.EXPt 7tcptcKTIKOtrtta<; 0.1 o/o 0" IJ.c!J.OVCOIJ.EVO <JUO"taTIKO, Ka8ffi<; Kat t1l
auyKcKpt!J.EYll XPTt<Jll autffiv.
ANIXNEY!:H NITPOZAMINQN !:TO AIAA YMA ANAllAHP!11:H1:
EAPMOZOMENH ANAA YTIKH TEXNIKH : Yypf] XpcoJ.la'toypa<pia-<l>acrJ.lU'tOJ.lE'tpia Masac; (Liquid
Chromatography -Mass Spectrometry)
ANIXNEYOMENE!: OY!:IE!:
To OtaAUIJ.U avanA.ftpcocrrt<; AGRINIO (Apt81J.6<; I1aptioa<;:Ol/AGRINIO 112) yta trtv
avi:x;veucrrt -rcov napaKa-rco ITivaKa<; 2.
IIivaKaS 2.
4-(Methylnitrosamino )-1-(3-
pyridyl)-1-butanol
4'-(nitrosomethylarnino )-1-(3-
pyridyl)-1-butanone
N-nitrosoanatabine
N-nitrosoanabasine
AllOTEAE!:MATA
(ppm)
ND*
ND
ND
ND
'Opw lloO'O'TlKOU
llpoo-(hoptO'f.10U
ME06()ol) (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEY!:H llOA YKYKAIKQN AP!!MATIKQN Y APOrONAN0PAKQN !:TO
AIAA YMA ANAllAHP!11:H1:
EAPMOZOMENH ANAA YTIKH TEXNIKH : Apta XpffiJ.lU'toypa<pia- <l>acrJ.lU'tOJ.lE'tpia Masac; (Gas
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ANIXNEYOMENE1: OY1:IE1:
To 8u:iA.ufla avanA.i)procrT]<; AGRINIO (Apt8f.l6<; f1ap-ri8a<;:O 11 AGRINI0/12) yta 'tT]Y
aviX,VEUO"TJ -rrov napaKa-rro noA.uKUKAtKrov aprof.!anKrov u8poyovav8paKrov (PAHs), ITivaKa<; 3.
llivaKaS 3.
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
benzo(k)fluoranthene
benzo(b )fluoranthene
benzo(g,h,i)perylene
di benzo( a,h )anthracene
indeno( 1 ,2,3-CD)pyrene
AllOTEAE1:MATA
Opto lloao-rtKoil
1: uyKtv-r pro mt
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*NO: UVt:XVU811KUV 1tOAUKUKAtKOt apCOf..l.U'ttKOt u8poyovav8paK<; O"Uf..l.q>COVU f..l. TU ava<pp0f..1.VU 6pta
aviXVU<J11<;
laTfHKou TJ.lt}JlaToc;
Aum9uvn\<; Epya<rt"flpiou EnLGTlJJlrov
& Movaoac; To;tKol..oyia:;
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ITANEITIL.THMI 0 KPHTHL.
TMHMA IATPIKHL.
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpaKAuo Kpirtq P.O.Box 2208 Heraklion Crete,
Greece
EPI'AJ:TRPtO TO!lKOAOflAJ:
Llu:u0uvn1<;: ApuJTL6T)<; M. TaaTaUKT)<;
-.. Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uoc.gr http://ctoxres.med.uoc.qr
nl.f1pooplE<; : 2810 394687- 394681 - 394794, Fax: +30 281 0 39 46 88
IIIETOIIOIHTIKO ANAAYEHI:* KAI TASINOMHI:HI: TOY AIAAYMATOI:
ANAIIAHPQI:HI:APACHE
ETAIPIA: ATMOS LAB
EMTIOPIKH ONOMA!:IA YrPOY ANATIAHP!l!:H!:: APACHE
API0MO!: TIAPTIAA!:: 011 APACHE /12
TIOIOTIKO!: TIPO!:AIOPI!:MO!: AIAAYMATO!: ANATIAHP!l!:H!:
E<l>APMOZOMENH ANAA YTIKH TEXNIKH: Apta<; Xpcu)la:roypa.<pia-<l>a.cr)la.'toJ..I-rpia. Mat;;a.<; (Gas
Chromatography -Mass Spectrometry) Kat **Yypij Mat;;a.<; (Liquid
IIO!:OTIKO!: TIPO!:AIOPI!:MO!: MEXPI TIO!:O!:TOY 99,9944%
ATIOTEAE!:MAT A
IlivaKa<; 1.
'Opto Jioo-O'TlKOU
Ovo-ia
Iloo-oo-'TO Ilpoaatopto-Jlou
(%w/v) MtOoaov (LOQ)
( m)
0,198
glycerol 84,93
1,187
water 9,7144
nicotine 1,3 0,1
!:uvoJ.o 99,9944
'tUStVOf.1ha.t
'tUStVOJlChUt
Ostia. -rostK6'tlJm I
Ostia. wstK6-rlJm 3
Xp6vta. 'tOStKO'tTJ'tU 2 cr
opya.vtcr)lOUS
To <pl':pct mcrwnoi'l<Hl crUfl<pWva flc 10 ISO: 17025 yta nc; 8ta8tKacricc;
8ta;tcipta'lc;, Kat apxct08ET'lCJ'lc; 1wv 8ctyfllhwv Kat A.ctToupyci flc crucrKcuf:c; Kat 6pyava.
H opyavoA.oyia LC-MS <pf:pct KaTa ISO: 17025 flE 7tc8io T'lV avi;x:vcucr'l vapKwnKwv oucrtwv
cr1'lv 1pixa.
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TASINOMH:EH TOY YrPOY ANAllAHP!!:EH:E APACHE
ME pacrYJ TllY AXE 265/2002, <DEK 1214/B'/19.9.2002, TllY To.w J..LEJ..LovroJ..Ltvrov
crucrTanKmv Tou J.!EtYJ..lUToc; Kat pacrYJ wu KavovtcrJ..LOU 1272/2008 (EK) TO APACHE (Apt8J..L6c;
llapTi8ac;: 01/APACHE/12) J..l 99,9944% O"UO""CUO"TJ7WU avaq>EpETUl O"TOV llivaKa 1,
roc; J..lll EmKiv8uvo yta TTJY av8pmmv11 uyda, yta To 7tEptPaA.A.ov Kat J.!E pacrYJ Tt<; cpumKOXTJJ..ltKE<; Tou
t8t6TTJTE<;. Em7tp6cr8ETa, yta TTJ XPTJO"TJ Tou 8taAUJ..lUTO<; ava7tA.ijprocrYJc; a1t6 TO TJAEKTpovtK6 Tcrtyapo,
w J..lEtYJ..la Etcr1tYEOJ..lEVrov aTJ..lmv 1tou a7tEA.Eu8EpmvETm XPEtasETm A.aJ..lPavovmc; u1t'
0\j/TJ TllY EKUTOO"Ttaia crUO""CUO"TJ TCDV UTJ..lWV 1tOU 7tapayOVTUl J..l TllV EYEpyo7tOlTJO"TJ TOU J..lTJXUYlO"J..lOU
aTJ..lo1toiYJcrTJc; J..lEXPt 1tEptEKnK6TYJTac; 0.1% p;p crE J..LEJ..lovroJ..ltvo crucrTanK6, Ka8mc; Kat TTJ
<ruyKEKplJ..lEVTJ XPTJO"TJ UUTWV.
ANIXNEY:EH NITPOZAMIN!!N :ETO AIAA YMA ANAllAHP!!:EH:E
EAPMOZOMENH ANAAYTIKH TEXNIKH ** : Yyp'i) Xprof..t.a-toypacpia-<l>acrJlaTOJlt-rpia Masac; (Liquid
ANIXNEYOMENE:E OY:EIE1:
To 8taAUJ..lU ava7tA.ijprocrYJ<; APACHE (Apt8J..L6<; llapTi8ac;:Ol/APACHE/12) yta TTJV
avixvwcrYJ Trov 7tapaKaTro vnposaJ..ltvmv, llivaKac; 2.
TiivaKas 2.
AKpO>VUf.llO
pyridyl)-1-butanol
4'-(nitrosomethylamino )-1-(3-
pyridyl)-1-butanone
N -nitrosoanatabine
N -nitrosoanabasine
AllOTEAE1:MA T A
(ppm)
ND*
ND
ND
ND
'Opw lloO'O'TlKOU
llpoO"(hoptO'f.lOU
Mt96oou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEY1:H llOAYKYKAIK!!N AP!!MATIK!!N YAPOrONAN0PAK!!N 1:TO
AIAA YMA ANAllAHP!!1:H1:
EAPMOZOMENH ANAA YTIKH TEXNIKH : Apta XproJlawypacpia- <l>acrJlUWfltTpia Masac; (Gas
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ANIXNEYOMENKE OYEIKE
To 8uiAUJ.!a avanA.flprocrllc; APACHE (Apt8J.!6c; ITapri8ac;:01/APACHEI12) yta 't'llV
avi:x;vcucr11 -rrov napaK6.-rro noA.uKUKAtKffiv aproJ.!attKffiv u8poyovav8p6.Krov (PAHs ), ITivaKac; 3.
llivaKClS 3.
AKprovi>Jno
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
dibenzo( a,h )anthracene
AUOTEAEI:.MATA
Dpw UoaonKoi>
I:.uyKEVTpro<Jll UpoaowptaJ.loi> MEOooou
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: DoV ClVlXVU9TJKUV 7tOAUKUKAlKOt apffiJ..LU'tlKOt UOpoyovav9paKt; O'UJ..L<pffiVU J..LE '!U UVU<pEpOJ..LEVU 6pta
UVtXVEUO'TJt;.
/ AptoT1.0'1<;; M. TonToaKtls -- --
MSc (Org Chern), PhD (Chern), DSc (Bioi), ERT (Eur Registered Toxicologist)
KaO'I"f'ITtl<;; T ol;tKol.oyiac; laTplKou TJltlJUIToc;
daEU9-u\"t'i)<;; EpyaO'TT)piou laTpOOLKa<ntKcilv Ento't"'lf.lOlV
& Movaoac; Tol;tKol..oyiac;
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TMHMA IATPIKHZ:
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.9. 2208 HptiKA&to Kpq1:q P.O.Box 2208 Heraklion Crete,
Greece
EPtAt1'8PIQ TO!IKOAOfiAt
4u:u0uvu1<;: KaOT)YTlTTt<; ApLaTt:t6T)<; M. Taa-rartKT)<;
nAr)pocpoplE<; : 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 88
1111:TOIIOIHTIKO ANAA Y1:H1:* KAI T ASINOMH1:H1: TOY AIAA YMAT01:
ANAIIAHPQ1:H1:BARBARA
ETAIPIA: ATMOS LAB
EMDOPIKH ONOMAI:IA YrPOY ANAllAHP!li:HI:: BARBARA
API0MOI: llAPTIAAI:: 01/BARBARA /12
llOIOTIKOI: llPOI:AIOPII:MOI: AIAA YMA TO I: ANADAHPQI:HI:
E<DAPMOZOMENH ANAA YTIKH TEXNIKH: AEpto<; Xpw)lawypa<pia-<Dacr)laTO)lE-rpia Masas (Gas
Chromatography -Mass Spectrometry) Kat **Yypf] Masas (Liquid
DOI:OTIKOI: llPOI:AIOPII:MOI: MEXPI llOI:OI:TOY 99,9976%
AllOTEAEI:MA T A
1.
'Opto IIOGO'TlKOU
OuJia
IloJOGTO IlpoGcltoplGJ.lOU
(%w/v) MtOoclo\l (LOQ)
( m)
0,198
glycerol 80,19
1,187
water 15,0376
nicotine 1,1 0, 1
I:ilvolo 99,9976
DoEV 'tUSlVO)lEhat
DoEV 'tUSlVO)lEt'tal
OsEia -rostK6-rqm t
OsEia wstK6TIJm 3
Xp6vta -rostKOTTJTU 2 crE
opyavtcr)lOUS
*To Tol;tKoA.oyiw; c:rUJlq>wva JlE TO ISO: 17025 yta n<; iltailtmcriE<;
iltaxEiptcrTJ<;, Kat Twv Kat JlE crucrKEu<; Kat 6pyava.
** H opyavoA.oyia LC-MS q>pEt KaTa ISO: 17025 JlE TTJV vapKwnKcilV oucrt<Ov
O"TTJV Tpixa.
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T AEINOMH:EH TOY YrPOY ANAIIAHP!l:EH:E BARBARA
Me tT]Y AXI: 265/2002, EK 1214/B'/19.9.2002, 'tTJY tcov !J.c!J.OYCO!J.EVCOV
crucrtanKrov 'tOU !J.clY!J.UtOc; Kat 'tOU KavovtO"!J.OU 1272/2008 (EK) 'tO BARBARA (Apt8!J.6c;
I1apti8ac;: 01/BARBARA/12) !J.c 99,9976% crucrtaO"T] nou ava<pEpctat O"'tOV IlivaKa 1,
coc; llll cmKiv8uvo yta 'tT]V av8promvT] uyda, yta to Kat !J.c nc; qmcrtKOXT]!J.tKEc; wu
t8t6tT]tcc;. Emnp6cr8cta, yta 'tTJ XPllO"TJ tou avanA.ijpcocrT]c; an6 to T]AcKtpovtK6 tmyapo,
to !J.ctY!la nou ancA.cu8cprovcmt XPctasctat un'
0\j/T] 'tT]Y cKU'tOO"'ttaia O"UO"'tUO"T] 'tCOV U't!J.cDY 1tOU napayov'tat !J.c 'tT]V cVcpyonOiT]O"T] 'tOU !J.T]XUVlO"!J.OU
!J.EXPt ncptcKnK6'tT]tac; 0.1 % crc !J.c!J.OYCO!J.EVO crucrtanK6, Ka8roc; Kat 'tTJ
cruyKcKpt!J.EYT] XPllO"TJ autrov.
ANIXNEY:EH NITPOZAMIN!!N :ETO AIAA YMA ANAIIAHP!l:EH:E
EAPMOZOMENH ANAA YTIKH TEXNIKH ** : YypfJ XpmllaToypaq>ia-<l>acr!la'tO!lc'tpia Mat;ac; (Liquid
ANIXNEYOMENE:E OY:EIE:E
To 8taA.u!J.a avanA.ijpcocrT]c; BARBARA (Apt8!J.6c; I1apti8ac;:Ol/BARBARA/12) yta 'tT]Y
avixvcucrTJ tcov napaKatco IlivaKac; 2.
llivaKas 2.
pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N -ni trosoanabasine
AIIOTEAE:EMA T A
(ppm)
ND*
ND
ND
ND
Dpw IIo(JOTlKOU
llpo(JblOpt(Jf.lOU
Mt06()ou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEY:EH IIOA YKYKAIKQN AP!!MATIKQN YAPOrONAN0PAKQN :ETO
AIAA YMA ANAIIAHP!l:EH:E
EAPMOZOMENH ANAA YTIKH TEXNIKH : Apta Xpm11amypacpia- <l>acr!la'to!lc'tpia Mai:;ac; (Gas
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To 8ui:AuJla avan:Aflpcocrllc; BARBARA (Apt8J.16c; Ilap-ri8ac;:Ol/BARBARA/12) yta TllV
UVl:XVU0"11 TCOV napaKUTCO 7rOAUKUKAlKcOV apCOflUTlKcOV u8poyovav8paKCOV (PAHs), IlivaKac; 3.
IlivaKaS 3.
acenaphty1ene
fluorene
phenanthrene
anthracene
pyrene
benzo( a)anthracene
chrysene
benzo(g,h,i)pery1ene
indeno( 1 ,2,3-CD )pyrene
AIIOTEAE:EMA T A
'Opto IIOGO'tlKOV
I: 'UYKEVT piDGl} IlpoG(hoptGtto'6 Mt96oo'U
(LOQ)
(ppm)
(ppm)
ND* 0,005
NO 0,010
NO 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
NO 0,014
ND 0,021
ND 0,022
*ND: UVtXVEUEhjKUV 1tOAUKUKAtKOt apCO!lU'ttKOt u8poyovuv8paKEc; CJU!!<pffiVU !! "CU ava<pp0!1VU 6pta

/ M. ToaToaKTI.; --. -- ____:_..-'
Ka9lJY'lritc; To/;tKo#.oyiac; laTptKo\i TJLTII.laToc;;
l\u;u9l>\'Tl\c; Epya<J't'1lplol> la-rpolhKanlKrov EntoT1Wrov
& Movaoac; T o;tKoA.oyiac;
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TMHMA IATPIKHL.
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpciKAto Kpirtq P.O.Box 2208 Herak.lion Crete,
Greece
EPfAt'tlliPIO TO!IKOAOflAt
Llu:u0uvn1;: KaOlJYTinl; ApuJTL6T); M. Taa-raaKT);
Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uoc.ar http://ctoxres.med.uoc.qr
nXr1PooplE<; : 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 88
IIIETOIIOIHTIKO ANAA KAI T TOY AIAA

ET AlP lA: A TMOS LAB
EMTIOPIKH ONOMAl:IA YrPOY ANADAHP!!l:Hl:: BEBECA
API0MOl: IIAPTIAAl:: OI/BEBECNI2
llOIOTIKOl: IIPOl:AIOPil:MOl: AIAA YMATOl: ANADAHP!!l:Hl:
E<DAPMOZOMENH ANAA YTIKH TEXNIKH: Atptoc; Mal;a.c; (Gas
Chromatography -Mass Spectrometry) Kat **Yypi] XpcoJ..La.-roypa.cpia.-<Da.crJ..LUTOJ..LcTpia. Mal;a.c; (Liquid
llOl:OTIKOl: IIPOl:AIOPil:MOl: MEXPI llOl:Ol:TOY 99,9992%
1.
Ouaia
methyl cyclopentenolone
ethyl maltol
ethyl vanillin
propylene glycol
glycerol
water
nicotine
l:i>voA.o
AllOTEAEl:MAT A
Iloaoa-ro
(%w/v)
0,503
1, 130
0,004
9,35
85,86
1,6522
1,5
99,9992
'Opto IloaonKou
Ilpoaowptaf.lOU
Mt960o'U (LOQ)
( m)
0,121
0,135
0,032
0,198
l , 187
0,1
Acv -ra.stvoJ..LEha.t
ostia. -rostKOTIJTU a.n:a
cr-r6J..La.TOc;, Ka.TIJyopia. 4
ostia. -rostKOTIJTU a.n:o
cr-r6J..LaTO<;, Ka.TIJyopia. 4
Epc8tcrJ..LO<; bEpJ..LUTO<;,
Ka.TIJyopia. 2
Epc8tcrJ..L6c; ocp8a.A.J..Lffiv
Ka.TIJyopia. 2
Et8tKi] TOStKOTIJTU crta.
6pya.va.-cr-r6xouc; ccpan:a.s
EK8c<rrJ Ka.nwopia. 3
Acv ta.StVOJ..LEha.t
Acv ta.StVOJ..Lcha.t
ostia. TOStKOTIJTU 1
ostia. -rostKOTIJ'tU 3
Xp6vta. TOStKOTIJta. 2 cr
u8p6pwus opya.vtcrgous
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To q>EpEt mcrwn:oiTJOTJ <ril!J.q>mva IJ.E w ISO: 17025 yta
Kat Tmv OEtYflUTffiV Kat flE Kat 6pyava.
H opyavoA.oyia LC-MS 8taKpipmcrTJ KaTa ISO: 17025 IJ.E TTJV avixvrucrTJ vapKmnKffiv oucrtffiv
crTTJV Tpixa.
T AEINOMHl:H TOY YrPOY ANATIAHP!!l:Hl: BEBECA
ME TIJY AXL 265/2002, EK 1214/B'/19.9.2002, TIJV 't(J)V J.!EJ.!OV(J)J.!EvffiV
crucr-ranKffiv wu J.!El'YJ.ta-roc; Kat -rou KavovtcrJ.!OU 1272/2008 (EK) -ro BEBECA (Apt8J.t6c;
ITap-ri8ac;: 01/BEBECA/12) J.!E 99,9992% O'Ucr-mcrTJ nou ava<pEpE-rat cr-rov ITivaKa 1,
ffic; !lll Emriv8uvo yta TIJY av8pffimVTJ uyda, yta -ro Kat J.!E nc; <pumKOXTJJ.!tKEc; wu
t8t6-rTJ-rEc;. Emnp6cr8na, yta Til XPllO'TJ -rou 8taA.uJ.tawc; avanA.flpfficrTJc; an6 w TJA.EK-rpovtK6 wtyapo,
-ro J.!El'YJ.!a EtcrnvEOJ.!EVffiv a-rJ.tffiv nou anEA.Eu8EpffivE-mt un'
0\j/TJ TIJY EKa-rocrnaia crUO''taO'TJ 'tffiV U'tJ.!WV 7tOU napayov-rat J.!E TIJV EVEpyonOtTJO'TJ 'tOU J.!TJXUVtO'J.!OU
U'tJ.!07tOtTJO'TJc; J.!EXPt 7tEptEK'ttKOTIJ'tac; 0.1% O'E J.!EJ.!OVffiJ.!EVO O'UO''ta'ttKO, Ka8ffic; Kat 'tll
cruyKEKptJ.!EYTJ XPllO'TJ au-rffiv.
ANIXNEYl:H NITPOZAMIN!!N l:TO AIAA YMA ANATIAHP!!l:Hl:
EAPMOZOMENH ANAA YTIKH TEXNIKH ** : Yyp1l XpcoflaLOypa<pia-acrllaro!l'tpia Masa<; (Liquid
ANIXNEYOMENEl: OYl:IEl:
To 8taAUJla avanA.flpfficrTJc; BEBECA (Apt8J.!6c; ITap-ri8ac;:Ol/BEBECA/12) yta TIJY
aviXVEUO'TJ -rffiv napaKa-rffi ITivaKac; 2.
llivaKaS 2.
AKproVUfltO
pyridyl)-1-butanol
pyridyl)-1-butanone
N- ni trosoanatabine
N -nitrosoanabasine
AllOTEAEl:MATA
(ppm)
ND*
ND
ND
ND
'Opto llo<JOTlKOU

Mt9o&ou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
*ND: UVtXVU8rjKUV Vtrposa!ltV<; crUfl<j>COVU !l 'tU ava<pp0!-LVU 6pta UVtXVU<JT}<;.
ANIXNEYl:H llOAYKYKAIK!!N AP!!MATIK!!N YAPOrONAN0PAK!!N l:TO
AIAA YMA ANATIAHP!!l:Hl:
EAPMOZOMENH ANAA YTIKH TEXNIKH : Aepta Xpco!laLOypacpia- <l>acr!la'tO!l-rpia Masa<; (Gas
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To 8ui/..:uj.la avan/...i)proo-r1<; BEBECA (Apt8j.!6<; Tiap-ri8a<;:01/BEBECA/12) yta T'flV
avi:XVEU<J'fl TCDV napaKaTro 7tOAUKUKAlKWV aproj.!UTlKWV u8poyovav8paKroV (PAHs), TiivaKa<; 3.
llivaKUS 3.
AKpOOVVfllO
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
benzo(b )fl uoranthene
dibenzo(a,h)anthracene
AIIOTEAE:EMA T A
Opto IloaonKoi>
l: vyKEV'T proa11 Ilpoaowpt<YflOil ME90001>
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: i1EV UVtXVEU811KUV 7tOAUKUKAtKOt aproj.!U'ttKOt Ubpoyovav8pa.KES <JUf,Hprova. j.!E 'tU a.va.<pEpOj.!EVU 6pta.
a.VtXVEU<J'flS
0 , "
,/ / . , j.. ' "? \ !II\ -

, ,'.; ;;.r,
- / - . '\-\
,. /
. \
. \,
. ,_-.
/
'"-"-f!.!
M. ToaTn<iKT).;
Ka91JY'1nl<; luTplKOU TJLiiJ.laToc;
EnLOTTJJHilv
& Movaoac; To!;tKoA.oyiac;
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ITANEITIL:THMI 0 KPHTHL:
TMHMA IATPIKHL.
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 Hpcuuuo Kpirtll P.O.Box 2208 Heraklion Crete,
Greece
.IPrAtTHPIO TO!lKOAOr tAt
Llu:u0uvn1<;: KaOT)YTITTJ<; ApuJTt:L6T)<; M. TaaT<JUKT)<;
nXr)po<j>oplE<;: 2810 394687 - 394681- 394794, Fax: +30 281 0 39 46 SlSl
IllETOIIOIHTIKO ANAA Yl:Hl:* KAI TASINOMHl:Hl: TOY AIAA
ANAIIAHPfil:Hl:BEBECA18mg
ETAIPIA: ATMOS LAB
EMTIOPIKH ONOMAEIA YrPOY ANAITAHP!!EHE: BEBECA 18mg
API0MOE IIAPTIAAI:: 01/ BEBECA 18mg/12
IIOIOTIKOE IIPOEAIOPII:MOE AIAA YMATOI: ANAIIAHPQI:HI:
EAPMOZOMENH ANAA YTIKH TEXNIKH: Aptoc; Xpmllaroypaq>ia-acrllao!l'tpia Masac; (Gas
Chromatography -Mass Spectrometry) Kat **YypfJ Xpmllawypaq>ia-acrllao!lpia Masac; (Liquid
IIOEOTIKOI: IIPOEAIOPIEMOI: MEXPI IIOI:OI:TOY 99,9999%
IltVIlKil 1.
0\l(Jl(l
propylene glycol
glycerol
ethyl vanillin
nicotine
Methyl cyclopentonolone
Ethyl maltol
water
EuvoA.o
AIIOTEAEI:MA T A
no(JO(JTO (o/ow/v)
2,73
93,15
0,006
1,6
0,525
1,152
0,8369
99,9999
OplO no(JOTLKOU
npo(JOlOpt(Jf!OU
Mseooou (LOQ)
( m)
0,198
1 '187
0,032
0,1
0,121
0,135
L'lV
L'lV
an:o
cr611aoc;, Kanwopia 4
EpEltcr!l6c; 'tOU 8p!lU'tO<;
(Kanwopia 2)
EpEltcr!l6c; 'tffiV oq>ElaA.11ciw
(Kanwopia 2)
EtOtKTj am
6pyava
KElcrT) (Kanwopia 3)
1
3
Xp6vta 2 cr
uop6Ptous opyavtcr11ous
an:o
cr611aoc;, Kanwopia 4
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To <ppst maronoirJO"ll mJflq>Wva flE ro ISO: 17025 yta nc; 8ta8tmaisc;
8taXEipwllc;, Kat apxsto8ET110"1lt; TWV 8EtyflCLTWV Kat AEtroupyd flE 8taKptPWJlEVEt; <JU<JKEUEt; Kat 6pyava.
H opyavoA.oyia LC-MS <ppst 8taKpipwall Kara ISO: 17025 flE ns8io r11v avixvrua11 vapKWnK<iw ouatv
ar11v rpixa.
TASINOMH:EH TOY YrPOY ANAIIAHPQ:EH:E BEBECA 18mg
'tllV AXI 265/2002, <DEK 1214/B'/19.9.2002, 'tllV 'trov
crucr'tanKrov 'tOU J..lEtYJ..lU'toc; Kat 'tou KavovtcrJ..lOU 1272/2008 (EK) 'tO BEBECA 18mg
(Apt8f..l6c; Tiapn8ac;: 011 BEBECA 18mg/12) J..lE 99,9999% cri>cr'tacr11nou ava<ppE'tat cr'tov TiivaKa
1, roc; J..lll yta 'tllV av8promv11 yta 'to Kat J..lE nc;
qmcrtKOXllf..ltKc; 'tOU t8t6'tll'tEc;. yta 'tll XPTJ<Jll wu 8taAUJ..lU'toc; avanA.iJprocrllc; an6 'tO
TlAEK'tpOVtKO 'tcrtyapo, 'tO J..lElYJ..lU Et<J1tVEOJ..lEVffiV U'tJ..lcDV 7t0U U7tEAEU8EpcDVE'tat XPEtaSE'tat
un' O\j/11 'tllV EKa'tocrnaia cri>crmcr11 'trov U'tf..lcDV nou napayovmt J..lE 'tllV
EVEpyonOlll<Jll 'tOU J..lllXUVt<Jf..lOU U'tf..l01t0tll<Jllc; J..lEXPt 1tEptEK'ttKO'tll'tUc; 0.1% crE J..lEJ..lOVffiJ..lEVO
<JU<J'tUTIKO, Ka8roc; Kat 'tll cruyKEKptf..lEVll XPTJ<Jll UU'tcDV.
ANIXNEY:EH NITPOZAMINQN :ETO AIAA YMA ANAIIAHPQ:EH:E
E<l>APMOZOMENH ANAA YTIKH TEXNIKH : Yypij Mat;ac; (Liquid
To 8taAUJ..la avanA.iJprocrllc; BEBECA 18mg (Apt8f..l6c; Tiap'ti8ac;:Oll BEBECA 18mg/12)
yta 'tllV avixvwcr11 'trov napaKa'tro vt-rposaJ..ltvrov, TiivaKac; 2.
llivaKUS 2.
AKpCOVUJllO
pyridyl)-1-butanol
pyridyl)-1-butanone
N-nitrosoanatabine
N-nitrosoanabasine
AIIOTEAE:EMA T A
(ppm)
ND*
ND
ND
ND
Opw Iloao-rtKou
Ilpoa&toplGJlOU
ME06&ou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEY:EH IIOA YKYKAIKQN APQMATIKQN YAPOrONAN0PAKQN :ETO
AIAA YMA ANAIIAHPQ:EH:E
2
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EAPMOZOMENH ANAA YTIKH TEXNIKH : Aptu Xprof..tmoypu<piu- <l>ucrf..LU'Wf..I.Tpiu Masuc; (Gas
ANIXNEYOMENEI: OYI:IEI:
I
To 8uiA.uf..La avanA.T)pwcr11c; BEBECA 18mg(Apt8f.l6c; I1apTi8ac;:Oll BEBECA 18mg/12)
yta TllV UVtXVEUO"ll TWV napaKUTW 7tOAUKUKAtKWV apWf.lUTtKWV u8poyovav8paKWV
(PAHs), I1i.vaKac; 3.
TiivaKas 3.
AKprovilt.tw
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
AllOTEAEI:MATA
'Opw lloaonKoiJ
I:uyKtv-rproo-11 llpoaowptat.toil MdMoou
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
NO 0,021
ND 0,022
*NO: f..ev UVtXVU9l]KUV 1tOAUKUKAtKOt UpUlf..I.UTtKOt UOpoyovav9pUKc; CJUf..l.<j>UlVU f.! TU UVU<pp0f..1.VU 6ptU
uvixveucrl]c;.
3
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TMHMA IATPIKHL.
T.e. 2208 HpaKAuo Kpirtq
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
P.O.Box 2208 Heraklion Crete,
Greece
DI:I:TODOIHTIKO ANAA Y:I:H:I: META ADO :I:YMDYKNQ:I:H* KAI
T AEINOMH:I:H:I: EI:I:DNEOMENOY ATMOY DOY DPOKYDTEI ADO THN
ATMODOIH:I:H YrPOY ANADAHP!!:I:H:I:
BEBECA 18mg
ETAIPIA: ATMOS LAB
EMTIOPIKH YrPOY BEBECA 18mg
01/ BEBECA 18mg /12
ATMOY MET A AllO
E<DAPMOZOMENH ANAA YTIKH TEXNIKH: Aptoc; Xpco)lamypa<pia-<Dacr)laTO)l-rpia Mul;ac; (Gas
Chromatography -Mass Spectrometry) Kat vypij Xpco)lamypa<pia-<Dacr)laTO)lTpia Mul;ac; (Liquid
MEXPI 99,97%
llivaKaS 1.
Ouo-ia
propylene glycol
glycerol
nicotine
Methyl cyclopentanolone
Ethyl vanillin
Ethyl maltol
water

A
noo-OO"TO (%w/v)
9,89
75,94
1,6
0,801
0,008
1,785
9,95
99,97
Opw noO"OTlKOU
n
Me961>ou (LOQ)
( m)
0,198
1,187
0,1
0,121
0,032
0,135

I ,
8aVIlTTJq>OpO <JE 1W<pTJ f.lE TO
8f:pf.11l
o
1tEpt1tTWO"TJ KllT<l1tOOTJ<;
Xp6vta 2 o
u8p6PtOus opyavtof.1ous
an6
oT6f.1aTO<;, Kanwopia 4
Eps9tof.16<; TOU bEpf.1aro<;
(Kantyopia 2)
Epe9tof.16<; TWV o<p9aA.f.1WV
(Ka<TJyopia 2)
EtiltKTJ om 6pyava
EK9EoTJ
(KaTTJyopia 3)-MnopEi va
1tpOKilAE<JEl Ep9t<Jf.10 O"TTJV
avanvo
an6
o<6f.1a<os, Kanwopia 4
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To q>f:pEtm<norroiT]<HJ <ril!lq>wva 1-LE to ISO: 17025 yta nc; 8ta8tKacric;
btaXEiptcrT]c;, Kat 1wv blY!lCL1WV Kat Anoupyi !l crucrKuc; Kat 6pyava.
T ASINOMHI:.H TOY EII:.DNEOMENOY ATMOY
M -rT)V 265/2002, <DEK 1214/B'/19.9.2002 Kat 'CT)V -ccov f.!f.!OVCOf.!8vcov
crDcrmnKrov -roD f.!ElYf.!a-coc; -coD Kavovtcrf.!OD 1272/2008 (EK), -co f.!ElYf.!U tcrnv6f.!VOD a-rf.!OD
1WD nporimt an6 TTJV a-rJ.!onoi.T)<JT) -roD Dypou avanA.T]pcocrT)c; BEBECA 18mg (Apt8f.!6c;
ITap-ci.8ac;: 011 BEBECA 18mg/12) f.! crucr-cacr11 99,97% 6ncoc; avaq>p-rat cr-cov ITi.vaKa 1,
coc; noA.u (T + )cr nEpi.n-ccocrT) EITA<D'Hc; ME TO .6.'EPMA KAI nc; EITIBAAB'Ec;
(Xn) <J 7tpt7t'CCO<JT) KU'CUJtO<JT)c; Ka-canOcrT)c; .
ANIXNEYI:.H NITPOZAMINQN I:.TON EII:.DNEOMENO ATMO MET A ADO
I:.YMDYKN!!I:.H
E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH : Yypf] XpcoJlaLOypa<pia-<l>acrJlaTOJlETpia (Liquid
ANIXNEYOMENEI:. OYI:.IEI:.
0 t<J7tV0f.!VOc; U'rf.!Oc; JtOD npoKDmt an6 'CT)V U'Cf.!07tOtT)<JT) 'COD 8taAUf.!U'rOc; avanA_TjpcocrT)c;
BEBECA 18mg (Apt8f.!6c; ITap-ci.8ac;:Oll BEBECA 18mg /12) yta 'CT)V avi.xvwcr11 -ccov
napaKa-rco ITi.vaKac; 2.
llivaKas 2.
pyridy1)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N -nitrosoanabasine
ADOTEAEI:.MA T A
(ppm)
ND*
ND
ND
ND
'Opto DoGO'TlKOU
DpoGblOplGJlOU
ME9obou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEYI:.H DOA YKYKAIKQN AP!!MA TIKQN Y APOrONAN0PAK!!N I:.TON
EII:.DNEOMENO ATMO META ADO I:.YMDYKNQI:.H
E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH : Apta XpcoJlaToypa<pia- <l>acrJlUTOJlC:Tpia (Gas
2
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ANIXNEYOMENKE OV:EIEI:
0 Etmrw:6jlEVOt; Utjl6t; nou npOKU7rtEt an6 TT]V Utjl07r0tr]CH] 'LOU DtaA:UjlUtOt; avanA.ijprocrT]t;
BEBECA 18mg (Apt8jl6t; ITapti8at;:O 11 BEBECA 18mg I 12) yta "CT]V avixvwcrT] trov
napaKatro noA.uKUKAtKffiv aprojlanKci:>v u8poyovav8p6.Krov (PAHs ), ITivaKa<; 3.
llivaKaS 3.
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
AIIOTEAEI:MA T A
Opto IloooTtKou
I:uyKEV'Tp<Ooll Ilpoo(hoptoJlOU ME96()ou
(LOQ)
(ppm)
(ppm)
ND* 0,005
NO 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
NO 0,003
ND 0,060
ND 0,006
NO 0,014
ND 0,021
ND 0,022
*ND: llVtXVEU8TJKUV 1tOAUKUKAtKOt u8poyovav8pa.KE<; O"Ujl<pffiVU jlE TU a.va.<pcpOjlcVU 6pta.
a.vixvcucrTJ<;.
,.,.,,..... "' .; i' .
_ _ / ,/ . J

/ i . ' '\\ \-
.,.,,... / .. -
" / ,. / \ ,
/ ._ .. z:(j J
/ '
/ Apto'Td011S M. TonTniKTJ.; --
Kn9l)YlJnlS T hnptKoi> T JlltJlToc:;
Epya<J"t'11piou la'Tpo()tKMLKrov E7ttGT1)Jlrov
& Movuoac:; To;tKoA.oyiac;
3
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TIANETIIl:THMIO KPHTHl:
TMHMA IATPIKHL:
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.9. 2208 Hpiuuo.&\0 Kpi)"tl) P.O.Box 2208 Heraklion Crete,
Greece
EPfAli:THPIO TO!IKOAOfiAli:
L\u:u9uv-ri)<;: Ka9T)YTJ-ri)<; ApLaTt:t6T)<; M. Taa-raaKT)<;
Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uoc.ar http://ctoxres.med.uoc.qr
nt .. r]po<j>oplE<; : 2810 394687- 394681 - 394794, Fax: +30 281 0 39 46 88
lllETOllOIHTIKO ANAA YEHE* KAI TASINOMHEHE TOY AIAA YMATOE
ANAllAHP!!EHE CAMILA
ETAIPIA: ATMOS LAB
EMTIOPIKH ONOMAI:IA YrPOY ANATIAIIP.QI:HI: : CAMILA
API0MOI: TIAPTIAAI:: 011 CAMILA /I2
TIOIOTIKOI: TIPOI:AIOPII:MOI: AIAA YMATOI: ANATIAIIP.QI:HI:
E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH: Atptos; Xpffi!la:roypacpia-<l>acrlla.To!l-rpia Masas; (Gas
Chromatography -Mass Spectrometry) Kat **Yypl) Xpffi!la-roypacpia-<l>acr!la.LO!lf:Tpia Masas; (Liquid
TIOI:OTIKOI: TIPOI:AIOPII:MOI: MEXPI TIOI:OI:TOY 99,9983%
TiivaKa<; 1.
ethyl vanillin
propylene glycol
glycerol
water
nicotine
I:l>voA.o
ATIOTEAEI:MA TA
llO(JO(J'TO
(%w/v)
0,001
15,52
80,70
2,2773
1,5
99 9983
'Opto llO(JO'TlKOU
llpo(J(hopt(JflOU
Mt96aov (LOQ)
( m)
0,032
0,198
I, I87
0, I
an6
crT6!la.TOs;, Ka.TT]yopia 4
Epc8tcr!l6s; Mp!la.Tos;,
Ka.TT]yopia 2
Epc8tcr!l6s; ocp8a.A.!lciw
Ka.TT]yopia 2
Et8tK1) crm
6pyava-cr-r6xous;
tK8c(JT] Kanwopia 3
.t.cv
.t.cV
I
3
Xp6vta 2 crc
u8p6pwus; opyavtcr!lous;
To q>EpEt rrt<JT07tOtT)<JT) <JlJf.lq>rova f.lE TO ISO: 17025 yta nc;
8taxEiptoT)c;, Kat Trov Kat f.lE ouoKEDc; Kat 6pyava.
H opyavoA.oyia LC-MS KaTa ISO: 17025 f.lE TTJV avixvEDoTJ vapKronKffiv oumffiv
on1v tpixa.
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T AEINOMH:EH TOY YrPOY ANATIAHPU:EH:E CAMILA
TT]V 265/2002, <DEK 1214/B'/19.9.2002, TT]V TffiV j..lf:j..lOVffij..lEVffiV
crucr-rauKmv Tou f.!ctYf.!UTOS Kat TOU Kavovtcrf.!OU 1272/2008 (EK) TO CAMILA (Apt8f.!6S
ITapn8ac;: 011 CAMILA 112) f.!l:': 99,9983% crU<JTa<JT] nou crTov ITivaKa 1,
roc; f.!T] yta TT]V av8pcD1ttVT] uycia, yta TO Kat j..lf: TtS <pUcrtKOXT]f.!lKES TOU
t8t6TT]Tf:t;. yta TTJ XPTJ<JT] Tou 8taA.uf.!UTOS avanA.i]pmcrTJs an6 TO T]Af:KTpovtK6 Tcrtyapo,
TO j..lctyj..la f:t(J1tVf:Oj..lf:VffiV UTj..lcDV 1tOU XPI::tasf:Tat un'
0\j/Tj TT]V f:KUTO<JTtata crU<JTa<JT] TffiV UTj..lcDV 1tOU napayOVTat j..lf: TT]V GVI::pyo7tOtTj<JTj TOU f.!TJXUVt<Jj..lOU
UTj..l01tOtTj<JT]S f.!EXPl 1tl::pti::KTtKOTT]TaS 0.1% <Jf: j..lf:j..lOVffij..lEVO <JU<JTaTtKO, Ka8roc; Kat TT]
XPTJ<JT] auTmv.
ANIXNEY:EH NITPOZAMINQN :ETO AIAA YMA ANATIAHPU:EH:E
E<l>APMOZOMENH ANAA YTIKH TEXNIKH **: Yypi] Xpffif.!a:roypa<pia-<l>aof.!UTOf.!cTpia Masac; (Liquid
To 8taAUf.!U avanA.i]pmcrT]c; CAMILA (Apt8f.!6S ITapTi8ac;:Oll CAMILA /12) yta TTJV
avixvcucr11 Trov napaKaTm vnposaJ..ttvrov, ITivaKac; 2.
IlivaKas 2.
AKprov'UfllO
4-(Methy1nitrosamino )-1-(3-
pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N -nitrosoanabasine
ATIOTEAE:EMAT A
(ppm)
ND*
ND
ND
ND
'OptO llO(JOTlKO'U
llpo(J&10pt(Jf.10'U
Mt9o&ol) (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEY:EH TIOAYKYKAIKUN APUMATIKQN YAPOrONAN0PAK!1N :ETO
AIAA YMA ANATIAHPU:EH:E
E<l>APMOZOMENH ANAAYTIKH TEXNIKH: Apta <l>aof.!UTOf.!cTpia Masac; (Gas
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To 8ui/..u11a avarr/..ijprocr11c; CAMILA (Apt9!l6c; ITapri8ac;:O 11 CAMILA I 12) yta "ClJV
avixvcucr11 -crov rrapaKa-cro rrof..uKUKAtKcOV apro!lanKmv u8poyovav9paKrov (PAHs), ITivaKac; 3.
TiivaKas 3.
acenaphty1ene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
AIIOTEAEI:MAT A
'Opto IloaonKo-6
I:uyKEVTpOOO"TJ Ilpoa&wptof.10'6 ME96&ou
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: avtxv'U8TJKUV noA.uKUKAtKoi apcof..LanKoi u8poyovav8paKE<; <n)f..L<pcova f..L m ava<pp6p.tva 6pta
UVLXVUGTJ<;.
0 .:1tcu9uvri)<; wu Epyg. piou,
/
,r''
-'
/
/ Aptcndb1J<; M. ToaToaKtJc;., , --
Ka91JYTJn1c; To;tKoJ..oyiac; laTptKou TJ.LiltJaToc;
EpyaOT1Jpioll laTpOOtKaOTtKrov EmoTTJfJWV
& Movaow; T o;tKol..oyia;
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TMHMA IATPIKHL:
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpciKAEto Kpi)"tl) P.O.Box 2208 Heraklion Crete,
Greece

Llu:uOuvTT]<;: KaOT)YTITtl<; ApuJTL6T)<; M. TaaT<JUKT)<;
Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uac.qr http://ctoxres.med.uoc.qr
m .. l'jpooplc:c;: 2810 394687 - 394681- 394794, Fax: +30 281 0 39 46 SUl
llii:TOllOIHTIKO ANAA YI:HI:* KAI TASINOMHI:HI: TOY AIAA
ANADAHP!!I:HI: GINA 18mg
ETAIPIA: ATMOS LAB
EMIIOPIKH ONOMAEIA YrPOY ANAITAHP!ll:Hl:: GINA 18mg
API0MOI: IIAPTIAAI:: 02/ GINA 18mg/12
TIOIOTIKOI: TIPOI:AIOPII:MOI: AIAA YMA TO I: ANATIAHP!ll:Hl:
EAPMOZOMENH ANAA YTIKH TEXNIKH: Aptat; Xpffif..Lawypa<pia-<l>acrf..LaTofJ-rpia M6.1;at; (Gas
Chromatography -Mass Spectrometry) Kat **Yypl) Mal;a<; (Liquid
TIOI:OTIKOI: TIPOI:AIOPII:MOI: MEXPI TIOI:Ol:TOY 99,9999%
IlivaKa 1.
Ouaia
propylene glycol
glycerol
ethyl vanillin
nicotine
water
l:uvow
ATIOTEAEI:MA T A
llOCJOCJTO (%w/v)
53,36
38,90
0,006
0,001
1,6
6,1329
99,9999
OpLO noaOTlKOU
llpoaowptCJf.lOU
(LOQ)
( m)
0,198
1,187
0,032
0,121
0,1

ano
cr-r6f..La-rot;, KaTTJyopia 4
Epe8tcrf..L6t; -rou 8pf..LU"CCt;
(Ka-rTJyOpia 2)
Epe8tcrf..L6t; -rffiv o<p8aA.f..LOW
(KaTTJyopia 2)
Et8tK1l cr-ra
6pyava
K8ECJTJ (KaTTJyopia 3)
1
3
Xp6vta 2 cr
u8p6pwus opyavtcrf..Lous
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*To Epyacrri]pto q>pt mcrrorroiT]cr'l mJ!lq>cova !1 ro ISO: 17025 yta
Kat TCOV 0tYilUTCOV Kat Attoupyi !1 Kat 6pyava.
** H opyavoA.oyia LC-MS q>f:pst otaKpipcocrT] Kara ISO: 17025 !1 rrsoio TT]V avixvsucr'l vapKconKwv oucrtwv
crrTJV rpixa.
T AEINOMHI:H TOY YrPOY ANAIIAHPQI:HI: GINA 18mg
M TYJV AXL 265/2002, <DEK 1214/B'/19.9.2002, TI)V TOW Jlf:J..I.OV(J)J..t.EV(J)V
crucr-ranKffiv -rou J..t.iYJ..t.aTO<; Kat TOU KavovtcrJ..t.OU 1272/2008 (EK) TO GINA 18mg
(Apt8J..t.6<; ITapTiba<;: 02/ GINA 18mg/12) J..t. 99,9999% <JUcr-racrYJ nou avac:ppTat cr-rov ITivaKa 1,
ro<; J..I.YJ ntKivbuvo yta TYJV av8pffimVYJ uyia, yta TO Kat Jlf: n<;
c:pucrtKOXYJJltK<; -rou tbtOTI)T<;. Emnp6cr8Ta, yta YJ XPTJ<JYJ Tou btaAUJlaTo<; avanA.i]procrYJ<; an6 w
YJAEKLpOVtKO Tcrtyapo, TO J..t.iYJ..t.a tcr1tV0J..t.VffiV a1:J..t.WV 7tOU a7tAU8pffiV1:at
un' O\j/YJ TYJV KaTocrnaia crucrTacrYJ Trov aT)lffiv nou napayov-rat J..I.E TI)V
VpyonOtYj<JTj TOU JlYJXaVt<JJ..t.OU aTJ..t.07tOtYj<JYJ<; JlEXPt 7tptKTtKOTYJTa<; 0.1% <J Jlf:J..I.OVWJ..t.EVO
crucrTanK6, Ka8ffi<; Kat TTJ cruyKKptJ..t.EVYJ XPTJ<JYJ auTffiv.
ANIXNEYI:H NITPOZAMINQN I:TO AIAA YMA ANAIIAHPQI:HI:
E<l>APMOZOMENH ANAA YTIKH TEXNIKH ** : Yypl) Mal;w; (Liquid
To btaAUJla avanA.i]procrYJ<; GINA 18mg (Apt8J..t.6<; I1apTiba<;:02/ GINA 18mg/12) yta
TTJV avixvwcrYJ Trov napaKaTro ITivaKa<; 2.
IlivaKas 2.
AKproVUJltO
4-(Methy1nitrosamino )-1-(3-
pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N -nitrosoanabasine
AIIOTEAEI:MA T A
(ppm)
ND*
ND
ND
ND
Opw IloaoTtKou
IlpoaowptO'JlOU
Mt96oou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEYI:H IIOA YKYKAIKQN APQMATIKQN Y APOrONAN0PAKQN I:TO
AIAA YMA ANAIIAHPQI:HI:
E<l>APMOZOMENH ANAA YTTKH TEXNIKH : Apta Xpffillawypac:pia- <l>acr!laTO!l-rpia Mal;w; (Gas
2
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ANIXNEYOMENEI:. OYI:.IEI:.
To 8uiA.u11a avanA.i)pcocrrv; GINA 18mg(Apt8!l6t; ITap-ri8at;:02/ GINA 18mgll2) yta
-rT)V avixvcucrT) -rcov napaKa-rco noA.uKUKAtKffiv apco!lanKffiv u8poyovav8paKcov (PAHs), ITivaKat; 3.
IlivllKilS 3.
AKprovilt.tto
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
benzo(k)fl uoranthene
AIIOTEAEI:.MA T A
'Opto Ilo(JO'TlKoil
l:'UyKEVTpW(Jl} Ilpo(JOlOpt(JflOil Ms9oOo'U
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: Llev UVtXVU8TJKUV 1tOAUKUKAtKOt a.pCOIJ.UHKOt u8poyovuv8pa.KS <JUj..lq>ffiVU j..l La. 6pta.
a.vixveumlS
3
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ITANEITIL.THMI 0 KPHTHL.
TMHMA IATPIKHL:
T.9. 2208 Kpip:q
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
Greece
*
ANAA MET A AllO KAI
T ATMOY llOY llPOKYllTEI AllO THN
YrPOY
GINA 18mg
ETAIPIA: ATMOS LAB
EMllOPIKH ONOMA.EIA YrPOY ANAIIAHPQ.EH.E: GINA 18mg
API0MO.E IIAPTIAA.E: 01/ GINA 18mg 112
TIOIOTIKO.E TIPO.EAIOPI.EMO.E EI.ETINEOMENOY ATMOY MET A ATIO .EYMTIYKNQ.EH
E<DAPMOZOMENH ANA/\ YTIKH TEXNIKH: Xpw!lawypa<pia-<Dacr!la'W!-LETpia (Gas
Chromatography -Mass Spectrometry) Kat **Yyp1) (Liquid
TIO.EOTIKO.E TIPO.EAIOPI.EMO.E MEXPI TIO.EO.ETOY 99,98%
TiivaKa 1.
Ouaia
propylene glycol
Glycerol
Nicotine
Ethyl vanillin
Water
.Ei>vol..o
ATIOTEAE.EMA TA
noaoaT6 (%w/v)
68,70
28,25
1,6
0,027
0,007
1,4
99,98
Opw noaOTlKOU
npoaOlOptGflOU
Mt96oou (LOQ)
( m)
0,198
1,187
0,1
0,121
0,032

I ,
@UVIlTT]q>OpO O"E flE TO
i>f:pfla
3, aE
7rEpt7rTffiO"T]
Xp6vta 2 O"E
opyavtO"flOUS
arr6 TOU
KaTT]yopia 4
TOU
(KaTT]yopia 2)
Tmv oq>9aA.fl<llV
(KaTT]yopia 2)
am 6pyava
K9EO"TJ,
Mrropci va rrpoKaA.aEt
EpE9tO"flO
OOOU (KaTT]yOpia 3)
To q>EpEt maTorroiT]O"TJ aUf.Lq>mva f.LE TO ISO: 17025 yta
Kat Tmv OEtYflUTmv Kat A.t:tmupyci f.LE Kat 6pyava.
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TASINOMHI:H TOY EII:IINEOMENOY ATMOY
'tTJV AXL: 265/2002, <DEK 1214/B'/19.9.2002 KaJ 'tTJV -rwv JlEJ.lOVWJ.lEvwv
crucrwnKrov -rou JlclYJ.law<; -rou KavovtcrJ.lOU 1272/2008 (EK), -ro JlclYJ.la a-rJ.lou
n:ou an:6 'tTJV a'tJ.lOn:OiTJcrTJ uypou avan:A.ftpwcrTJ<; GINA 18mg (Apt8fl6<; flapri8ac;: 01/
GINA 18mg/ 12), JlE crucrwcrTJ 99,98% 6n:w<; ava<ppcwt cr-rov ITivaKa 1, roc; n:oA.u
(T +) CJE 1tcpin:-rwcrTJ En:a<pf}<; Jlc 'tO bEpJ.la Kat w<; (Xn) CJE 1tcpimwcrTJ KU'tU1tOCJTJ<;.
ANIXNEYI:H NITPOZAMIN.QN I:TON EII:IINEOMENO ATMO MET A AIIO
I:YMIIYKN .QI:H
E<l>APMOZOMENH ANAA YTIKH TEXNIKH ** : Yypij Masac; (Liquid
0 Etcrn:vc6JlEVO<; a-rJ.l6<; n:ou n:porin:-rEt an:6 'tTJV a-rJ.lon:oiTJCJTJ uypou avan:A.ftpwcrTJc; GINA 18mg
(Apt8Jl6<; flap-ri8ac;:Oll GINA 18mg /12) yta 'tTJV avixvcucrTJ -rrov n:apaKa-rro
ITivaKa<; 2.
IlivaKas 2.
pyridyl)-1-butanol
pyrid yl)-1-butanone
N -nitrosoanatabine
N-nitrosoanabasine
AIIOTEAEI:MA TA
(ppm)
ND*
ND
ND
ND
'Opw Iloao'TlKO'U
IlpoaowptaJ!Oll
(LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEYI:H IIOA YKYKAIK.QN AP.QMATIK.QN Y APOrONAN0PAK.QN I:TON
EII:IINEOMENO ATMO META AIIO I:YMIIYKN!!I:H
E<l>APMOZOMENH ANAA YTIKH TEXNIKH : Apta Xpwf.!awypaq>ia- <l>acrJ.lU'Wf.lE'tpia Masac; (Gas
0 EtcrnvE6JlEVO<; a-rJ.l6c; n:ou n:porin:-rct an:6 LTJV a-rJ.lon:oiTJCJTJ uypou avan:A.ftpwcrTJ<; GINA 18mg
(Apt8Jl6c; flap-ri8ac;:Oll GINA 18mg /12) yta 'tTJV -rwv n:apaKa-rw
n:oA.uKUKAtKffiv apwJ.lanKmv u8poyovav8paKwv (PARs), ITivaKac; 3.
2
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llivaKas 3.
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
AIIOTEAEI:.MA T A
Opw IloaoTtKoi>
1:,1)yKEVT proa11 Ilpoac)wptaJLOU Mt06()o1)
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: avtxvcu811Kav noA.uKUKAtKoi apco).la:nKoi u8poyovav8paK<; cru).l<pcova )1 -ra ava<pt:p6)1va 6pta
avixvcucr11c;.
0 Tou tP"{g. piou
/ .
/ // ... ... ...; -
.,. / \ ""
/ \ ' 'l " ''
. i':.-, \:) "--
' '-. ctJ ":" --
/ AptoTEiBra; M. ToaTaaKtJc;.
Ka9ttYTtnl<; laTptKoi> TJ.LftJUITo<;
\um9'U\'Ttl<; EpyaG't'llpio1) la'tpoBtKOTtKrov E7ttO't11J1WV
& Movaoa.c;
3
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TMHMA IATPIKHL.
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.9. 2208 HpaKAuo Kpirtll P.O.Box 2208 Heraklion Crete,
Greece
EPrAl:TRPlO TO!IKOAOriAl:
L\u:uOuvTi);: KaOT)YTITTJ; Apl<JTL6T); M. TaaT<JrtKT);
nArJPo>oplEc;: 2810 394687- 394681 - 394794, Fax: +30 281 0 39 46
lllETOllOIHTIKO ANAA Yl:Hl:* KAI T AEINOMHI:Hl: TOY AIAA
ANAIIAHP!!l:Hl: HABANA 18mg
ET AIPIA: A TMOS LAB
EMllOPIKH ONOMAI:IA YrPOY ANAITAHP.Qr.Hr.: HABANA 18mg
API0MOr. IIAPTIAAr.: 02/ HABANA 18mg/12
IIOIOTIKOr. IIPOr.AIOPir.MOr. AIAA YMA TOr. ANAIIAHP.Qr.Hr.
E<l>APMOZOMENH ANAA YTIKH TEXNIKH: Aptoc; XpCD!!CL'Wypuq>iu-<l>uof..Ul'tO!!ETpiu (Gas
Chromatography -Mass Spectrometry) Kat **Yypft XpCDf..tmoypuq>iu-<l>uo!!CL'W!!E'rpiu (Liquid
IIOr.OTIKOr. IIPOr.AIOPir.MOr. MEXPI IIOr.Or.TOY 99,9999%
IlivaKUS 1.
propylene glycol
glycerol
ethyl vanillin
nicotine
Ethyl alcohol
water
r.uvoJ...o
AllOTEAEr.MA T A
flOO'OO'TO (%w/v)
69,72
27,49
0,007
1,6
0,002
0,92
0,2609
99,9999
OplO flOO'OTlKOU
llpoaowptO'I.lOU
Meeooou (LOQ)
( m)
0,198
l, 187
0,032
0, l
0,121
l gr/Lt

uno
OTO!!U'Wc;, KuTllyopiu 4
Epe8to116c; ou op!luwc;
(KuTllyopiu 2)
Epe8to116c; TCDv oq>8uA.wbv
(Kunwopiu 2)
EtotKft om
6pyuvu o-r6xouc;
K8<n] (Kunwopiu 3)
1
3
Xp6vtu 2 o
uop6ptouc; opyuvtO!!OUc;
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*To Epyacrn'jpto q>EpEt mcnonoill<HJ <J1Jflq>wva flE to ISO: 17025 yta nc; l'itabtKacriEc;
l'itaxEiptcrllc;, Kat apxEto8tllcrllc; twv l'iEtyfl<'nwv Kat A.EttoupyEi flE l'itaKptPWflEvEc; crucrKwc; Kat 6pyava.
H opyavoA.oyia LC-MS q>pEt l'itaKpipwcrll Kata ISO: 17025 flE nEI'iio tllv avixvwcr11 vapKwttKffiv oumwv
crt11v tpixa.
T ASINOMHI:H TOY YrPOY ANAllAHP!!l:Hl: HABANA 18mg
Me TllY AXL 265/2002, <DEK 1214/B'/19.9.2002, TllY TO)V )lcflOYmJ.lEYmv
crucrmnKffiY Tou JlclYJ.lUTO<; Kat TOU KaYOYt0JlOU 1272/2008 (EK) TO HABANA 18mg
(Apt8)l6<; I1apTi8ac;: 02/ HABANA 18mg/12) Jlc 99,9999% 0UcrTU0111tOU aYa<ppcTat crTOY
IliYaKa 1, me; llll cmKiY8uYo yta TllY aY8pffimY11 uycia, yta TO Kat Jlc
n<; <pUcrtKOXllfllKE<; Tou t8t6Tl1Tc<;. Em7tp6cr8cTa, yta Tll XPTJ011 Tou 8taAu)laTo<; aYa1tAijpmcr11<; a1t6 TO
llAcKTpOYtKO Tcrtyapo, TO JlclYJ.lU cl01tVcO)lcYffiY UT)lcOY 1tOU U1tcAcU8cpffiYcTat XPctascmt
U1t' 0\jfll TllY cKUTOcrnaia crU0TU01l TillY UT)lcOY 1tOU 1tapayOYTat )lc TllY
CVcpy07t0l11011 TOU llllXUYl0)lOU UT)l01t0t11011<; JlEXPt 1tcptcKHKOTllTU<; 0.1% 0c )lc)lOYffi)lEVO
crucrTanK6, Ka8ffi<; Kat Tll cruyKcKpt)lEYll XPTJ01l auTffiY.
ANIXNEYI:H NITPOZAMIN!!N l:TO AIAA YMA ANAllAHP!!l:Hl:
E<DAPMOZOMENH ANA!\ YTIKH TEXNIKH ** : Yypij Xpffi)latoypa<pia-<Daa)laTOJ.IEtpia Masac; (Liquid
To 8taAUJ.la aYa1tA.ijpmcr11<; HABANA 18mg (Apt8)l6<; I1apTi8ac;:02/HABANA 18mg/12)
yta TllY UVlX)'cU011 TillY 1tapaKaTm YtTPOSU)llYWY, IliYaKa<; 2.
llivaKas 2.
AKpO>VUJUO
4-(Methylnitrosarnino )-1-(3-
pyridyl)-1-butanol
pyridyl)-1-butanone
N-nitrosoanatabine
N-ni trosoanabasine
AllOTEAEI:MAT A
(ppm)
ND*
ND
ND
ND
'OplO llOGOTlKOU

(LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEYI:H llOA YKYKAIK!!N AP!!MA TIK!!N Y APOrONAN0PAK!!N l:TO
AIAA YMA ANAllAHP!!l:Hl:
2
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E<DAPMOZOMENH ANAAYTIKH TEXNIKH: Apta Xpcof..La-roypa<pia- <Dacrf..LUTOflTpia Masac; (Gas
ANIXNEYOMENE'E OY'EIE'E
To 8uiA.u11a HABANA HABANA 18mg/12)
cSc'r<icr811Kc yta TllV avi:X,VcUO"ll TCOV 1tapaKIXTCO 1tOAUKUKAtKcDV apCO!lUTtKcDV u8poyovav8paKCOV
(PAHs), 3 ..
IlivaKas3.
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
benzo(g,h,i )perylene
AllOTEAE'EMAT A
Opw llo<JoTtKoi>
'I:uyKtVTpO>Gll llpoG(hoptGf.lOU M965ou
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: aVt:X,VC:U8TJKUV n:OAUKDKAtKOi apCDf..LUTtKOt ubpoyovav8paKC:S CJUf..Lij>CDVa f..LC: Ta ava!pC:pOflVU 6pta
avi:x,vc:ucr11c;.
3
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TMHMA IATPIKH2:
T.e. 2208 HpciKAuo KpirtrJ
UNIVERSI'IY OF CRETE
MEDICAL SCHOOL
Greece
IIIETOIIOIHTIKO ANAA Yl:H:E META ADO l:YMDYKN.Ql:H * KAI
T AEINOMHI:Hl: Ell:IINEOMENOY A TMOY IIOY IIPOKYIITEI ADO THN
ATMODOIHI:H YrPOY ANADAHP!!l:Hl:
HAVANA 18mg
EMIIOPIKH ONOMAI:IA YrPOY ANAIIAHP!li:HI:: HAVANA 18mg
API0MOI: IIAPTIAAI:: 011 HAVANA 18mg /12
IIOIOTIKOI: IIPOI:AIOPII:MOI: l:TON Ell:DNEOMENO A TMO META ADO
l:YMDYKN.Ql:H
E<DAPMOZOMENH ANAAYTIKH TEXNIKH: Aptoc; Masac; (Gas
Chromatography -Mass Spectrometry) Kat **Yypll Xpffillawypa<pia-<DacrllULOflE'Lpia Masac; (Liquid
IIOI:OTIKOI: IIPOI:AIOPII:MOI: MEXPI IIOI:OI:TOY 99,97%
IlivaKa 1.
Ouuia
propylene glycol
Glycerol
Nicotine
Ethyl vanillin
Water
I:uvolo
AIIOTEAEI:MA TA
nouOCJTO (o/ow/v)
65,96
32,00
I, I
0,002
0,006
0,90
99,97
Opto nouOTLKOU
n poulhoptuf.10U
Mt96oou (LOQ)
( m)
0,198
1' 187
0,1
0,121
0,032
LlEV
LlEV
I, 8avatT]<p6po
cre ma<pi] flt 1:0 8pfla
3, crE

Xp6vta 2 crE
arr6 wu
KaTT]yopia 4
TOU
(KatT]yopia 2)
nov o<p9aAflWV
{KatT]yopia 2)
Et8tKij crm 6pyava
K8EcrTJ , Mrropci
va rrpOKUAEcrEt Epc8tCJflO CJTT(V
oM (Kanwopia 3)
*To Epyacrti]pto <ppEt mcrwrroiTJGTJ CJUfl<prova flE TO ISO: 17025 yta
Kat trov OEtyfl<ltrov Kat flE Kat 6pyava.
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TASINOMHI:H TOY EII:IINEOMENOY ATMOY
Me tl)V AXL 265/2002, <DEK 1214/B'/19.9.2002 Kal "Cl)V tcov f.lcf.lOVCOf.lEVcov
crucrmnKffiv tou f.lclYf.lUtoc; tou KuvovtO"f.lOU 1272/2008 (EK), w f.lclYf.lU tmrvOf.lVou Utf.lOU
nou nporuntt uno"Cl)v Utf.!Onoil)O"ll uypou uvunA.ijpcocrl)c; HAVANA 18mg (Apt8f.loc; I1upti8uc;:
011 HAVANA 18mg/12) f.l O"Ucrmcr11 99,97% oncoc; uvuq>Epcmt crtov ITivuKu 1, coc;
nolcu (T +) a npimcocrl) nu<pijc; f.l to 8Epf.lU Kat coc; (Xn) a npintCOO"l)
KUtUnOO"l)c;.
ANIXNEYI:H NITPOZAMIN.QN I:TON EII:IINEOMENO ATMO META AIIO
I:YMIIYKN.QI:H
E<DAPMOZOMENH ANAAYTIKH TEXNIKH ** : Yyp1l Xprof.laToypa<pia-<Dacrf.!a:rof.!cTpia Masa<; (Liquid
0 tcrnvOf.lVoc; Utf.loc; nou nporimt uno "Cl)V Utf.!Onoil)O"ll uypou uvunA.ijpcocrl)c; HAVANA 18mg
(Apt8f.loc; I1upti8uc;:Ol/ HAVANA 18mg /12) ytu "Cl)V uvixvcuO"l) tcov nupuK<itco
vnposuf.ltvffiv, ITivuKuc; 2.
ll(vaKas 2.
pyridyl)-1-butanol
pyridyl)-1-butanone
N-nitrosoanatabine
N -nitrosoanabasine
AIIOTEAEI:MAT A
(ppm)
ND*
ND
ND
ND
'OplO IIOGOTlKOU

(LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEYI:H IIOA YKYKAIK.QN AP.QMATIK.QN Y APOrONAN0PAK.QN I:TON
EII:IINEOMENO A TMO MET A AIIO I:YMIIYKN.QI:H
E<DAPMOZOMENH ANAA YTIKH TEXNIKH: AEpta Xprof.!awypa<pia- <Dacrf.!UTOf.lETpia Masa<; (Gas
0 mnvOf.lVoc; Utf.loc; nou nporuntt uno tl)V Utf.lonoil)O"ll uypou uvunA.Tjpcocrl)c; HAVANA 18mg
(Apt8f.loc; I1upti8uc;:Ol/ HAVANA 18mg /12) ytu tl)V uviXVUO"l) -rcov nupuK<itco
noAUKUKAtKffiv upcof.lUTIKffiv u8poyovuv8p<iKcov (PAHs), ITivuKuc; 3.
2
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TiivaKas 3.
Acenaphtylene
Fluorene
Phenanthrene
Anthracene
Pyrene
benzo(a)anthracene
Chrysene
AllOTEAEI:MA T A
'Opto llo<JO'TlKOU
1: U"{KEVT pro <Jfl llpo<J(hopt<JJ.wi> MEOooou
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*NO: llV aVtXVU811KUV 1tOAUKUKAtKOt u8poyovav8paK<; <JU).Hj>COVa La opta
avixvcucr11s-
0 lltEU8uvni<; -rou Epyg. piou,
/
/
/'
_,/

/ \ '-..'c:tJ
/ ' "-.,
/ Aplo'tLo
11
c; M. TCJaT<JaKTJ.:; --- --
Ka9l)Y1Jnl<; IrnplKoi> Tf.Li}J!Toc;
.iu:u9'Uvn1c; EpyafJ't'Tipiou la-rpOOlKUO'ttKrov EnlOTlJJ!WV
& Movaoac; To;LKol.oyias;
3
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ITANEITIL:THMIO KPHTHL:
TMHMA
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpciKAuo KpQl:IJ P.O.Box 2208 Heraklion Crete,
Greece
TO!IItOAOflAt
L\u:uOuvTI)<;: KaOTJYTJTTt<; ApLaTL6TJ<; M. Taa-raaKTJ<;
"' Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uoc.gr http://ctoxres.med.uoc.qr
m .. l']po<!>oplE<; : 2810 394687- 394681- 394794, Fax: +30 281 0 39 46 88
III.ETOIIOIHTIKO ANAA Y.EH.E* KAI TAEINOMH.EH.E TOY AIAA YMATO.E
ANAIIAHPQ.EH.EKAPNOS
ETAIPIA: ATMOS LAB
EMIIOPIKH ONOMAI:IA YTPOY ANAIIAHPQI:HI:: KAPNOS
API0MOI: IIAPTIAAI:: 01/KAPNOS/12
IIOIOTIKOI: IIPOI:AIOPII:MOI: AIAA YMATOI: ANAIIAHPQI:HI:
E<DAPMOZOMENH ANAAYTlKH TEXNIKH: XpwJ..La-roypa<pia-<DacrJ..LU'toJ.!ETpia (Gas
Chromatography -Mass Spectrometry) Kat **Yypi] XpwJ.!aTOypa<pia-<DacrJ..LUTOJ.!ETpia (Liquid
AIIOTEAEI:MATA
IlivaKac; 1.
'Opw IIO<JOTlKOU
Ouaia
Iloaoa-r6 Ilpoa<hopt<J!lOU
(%w/v) Mt06oou (LOQ)
( m)
0,198
glycerol 89,61
1,187
water 5,6996
nicotine 1,4 0,1
I:uvol.o 99,9896
f1V
AEV
1
3
Xp6vta 2 cr
u8p6Pwus opyavtcrJ..Lous
* To <ptpEt rctowrcoiT]OTJ OU!l<pffiva llE TO ISO: 17025 yta nc; 8ta8tKaoicc;
8taxciptcrT]c;, Kat apxcw8ETTJcrTJc; Tffiv OEtYilUTffiV Kat A.ctToupyci llE 8taKptPffillEYEc; crucrKwtc; Kat 6pyava.
** H opyavoA.oyia LC-MS <ptpct 8taKpipfficrTJ KaTa ISO: 17025 llE rc8io TTJV aviXVEDOTJ vapKffinK6:JV oucrtffiv
O"TTJV Tpixa.
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TASINOMHl:H TOY YrPOY ANAIIAHP!ll:Hl: KAPNOS
ME TTJV AXL 265/2002, EK 1214/B'/19.9.2002, TTJV nov J..I.EJ..I.OVo:>J..I.Evo:>V
crucrTanKrov Tou J..I.ElYJ..I.UTOc; Kat wu KavovtcrflOU 1272/2008 (EK) TO KAPNOS (Apt8J..1.6c;
TiapTi8ac;: 01/KAPNOS/12) J..I.E 99,9896% crucrTacrTj 1tOU ava<pEpEmt crTOV TiivaKa 1,
o:>c; J..I.Tj E1tlKtV8UVO yta TT]V av8pro1tlVT] uyda, yta TO Kat J..I.E nc; <j)UcrlKOXTJJ..llKEc; TOU
t8t6TT]TEc;. Emnp6cr8Em, yta TTJ :xpftcrTJ TOU 8taAUJ..laTOc; avan'Aftpo:>crT]c; an6 TO TJAEKTpovtK6 Tcrtycipo,
To J..I.EtYJ..la EtcrnvE6J..1.Evo:>v aTJ..lcOV nou anE'AEu8EprovETat un'
0\j/Tj TT]V EKUTOcrnaia crucrTacrTj To:>V UTJ..lcOV 1tOU 7tapciyOVTat J..I.E TT]V EVEpyo7tOtTjcrTj TOU J..I.TJXUVtcrJ..I.OU
UTJ..l01tOtTjcrT]c; J..I.E:xpt 1tEptEK'!lKOTT]Tac; 0.1 % crE J..I.EJ..I.OVo:>J..I.EVO crucrmnK6, Ka8roc; Kat TTj
cruyKEKptJ..I.EVTJ :xpftcrTJ auTrov.
ANIXNEYl:H NITPOZAMIN!!N l:TO AIAA YMA ANAIIAHP!ll:Hl:
E<DAPMOZOMENH ANAA YTIKH TEXNIKH .. : Yypl'l Xpwf.!atoypa<pia-<Dacrf.!atOflt:tpia Mal;ac; (Liquid
ANIXNEYOMENEl: OYl:IEl:
To otci'AuJ..la avan'Aftpo:>crT]c; KAPNOS (Apt8J..1.6c; TiapTi8ac;:Ol/KAPNOS/12) yta TTJV
aviXVEUcrTJ -rwv napaKci-rw TiivaKac; 2.
IlivaKas 2.
pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N-nitrosoanabasine
AIIOTEAEl:MA T A
(ppm)
ND*
ND
NO
ND
'Opto IIO(JO'TlKOU
Ilpo(J<>topt(Jf.10U
MdM<>ou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEYl:H IIOA YKYKAIK!!N AP!!MATIK!!N Y APOrONAN0PAK!!N l:TO
AIAA YMA ANAIIAHP!ll:Hl:
E<DAPMOZOMENH ANAA YTIKH TEXNIKH : Apta Xpwf.!atoypa<pia- <Dacrf.!atof.!Ctpia Mal;ac; (Gas
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To 8uiAUJ.!U avanA.iJpwoTJ<; KAPNOS (Apt8J.!6<; I1ap-ri.8ac;:Oll KAPNOS 112) yta 'tTJV
UVtXVEU<JTj 'tWV napaKU't(l) 1tOAUKUKAtKWV apWJ.!U'ttKWV u8poyovav8paKWV (PAHs), Tii.vaKa<; 3.
llivaKUS 3.
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo( a)anthracene
chrysene
AllOTEAEI:MATA
Opto lloGonKou
l:l)yKEVTpiDGT) llpoG&toptGJlOU Mc06&o1)
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: avtxvd>811Kav noA.uKUKA.tKoi apcoJlanKoi uopoyovav8paK<; cn)Jl<pcova !l -ra avacpcp6!1va 6pta
avixvcu<>ll<;-
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TMHMA IATPIKHL,
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.9. 2208 HpciKAuo KpquJ P.O.Box 2208 Heraklion Crete,
Greece
EPfA.tTHPIO TO!IKOAOflAt
Llu:uOuvTi);: KaOTIYTITTJ; ApuJTt:L6ll; M. TaaTaaKll;
m .. l')po>oplEc;: 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46
IIII:TOIIOIHTIKO ANAA YI:HI:* KAI TASINOMHI:HI: TOY AIAA
ANAIIAHP!!I:HI: MAXXX 18mg
ETAIPIA: ATMOS LAB
EMDOPIKH ONOMA.EIA YrPOY ANADAHP!l..EH.E: MAXXX 18mg
API0MO.E DAPTIAA.E: 02/ MAXXX 18mg/l2
DOIOTIKO.E DPO.EAIOPI.EMO.E AIAA YMA TO.E ANADAHP!l..EH.E
E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH: AEpto<; Xpffijlamypa<pia-<l>acrjla'tOjle'tpia Masas (Gas
Chromatography -Mass Spectrometry) Kat **Yypi] Xpffijla-roypa<pia-<l>acrjla'tOjle-rpia Masas (Liquid
DO.EOTIKO.E DPO.EAIOPI.EMO.E MEXPI DO.EO.ETOY 99,9999%
llivaKa 1.
Ouaia
propylene glycol
glycerol
ethyl vanillin
nicotine
Ethyl maltol
water
.Ei>vol.o
ADOTEAE.EMA T A
noaoaT6 (o/ow/v)
68,77
28,91
0,004
1,6
0,214
0,010
0,4919
99,9999
Opto noaOTlKOU
n poaO lOp lGJlOU
ME96oou (LOQ)
( m)
0,198
1,187
0,032
0,1
0,121
0,135

ano
cr-r6jla-ros, Ka-r1nopia 4
Epe8tcrjl6<; -rou bEpjlUTOS
(Ka-r1nopia 2)
Epe8tcrjl6<; 'tffiV o<p8aAjlWV
(Ka'tllyopia 2)
Et8t!d] <J'tU
6pyava
EK8ecr11 (Kannopia 3)
1
3
Xp6vta 2 cre
opyavtcrjlOUS
ano
cr-r611a-ros, Kannopia 4
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To EpyaoTijpto q>EpEt moTorroiT]<JT] <JlJjlq>WVCL jl TO ISO: 17025 ym nc; 8m8tKCL<Jic; rrapaA.api]c;,
8mxEipwTJc;, Kamypaq>i]c; Kill Twv Kill AEtToupyEi llE 8taKptPwllEvEc; Kill 6pyava.
** H opyavoA.oyia LC-MS q>EpEt btCLKpipwoT] KCLTU ISO: 17025 jl rr8io Eq>CLpjloyi]c; TTJV avixvcuoT] vapKWnKv oucrtffiv
<JTT]V TPlXCL.
T ASINOMHI:H TOY YrPOY ANAllAHPQI:HI: MAXXX 18mg
M TllY AX.L 265/2002, <l>EK 1214/B'/19.9.2002, LllY TWY
crucrmnKffiY TOU Kat TOU 1272/2008 (EK) TO MAXXX 18mg
ITapTiOa<;: 02/ MAXXX 18mg/12) 1-L 99,9999% cri>crTacrll7tOU aYa<pptat crroY ITiYaKa
1, m<; mKiYOUYO yta TllY aY8pffimYll uyda, yta TO Kat Tt<;
rou t8t6tllt<;. Emnp6cr8ta, yta Tll XPTJGll rou aYanA.i)pmcrll<; an6 ro
llAKrpoYtK6 rmyapo, ro ar11ffiY nou anA.cu8cpffiYmt XPt<isTat
U1t' 0\(/ll 'IllY f:KaTocrnaia cri>crracrll TWY UTI!WY 1tOU napayOYLat l!f: TllY
f:YcpyonoillGll 'IOU 1-LllXUYtGI!OD U'I1!01t0lllGll<; 1tptKLtKO'Illta<; 0.1% G
crucrTattK6, Ka8ffi<; Kat tll XPTJGll aurffiY.
ANIXNEYI:H NITPOZAMINQN I:TO AIAA YMA ANAllAHPQI:HI:
E<DAPMOZOMENH ANAA YTIKH TEXNIKH ** : Yypij XpcoJ.l.a'tOypaq>ia-<DacrJ.l.UTOJ.l.ETpia Mal;ac.; (Liquid
To 8taA.u11a aYanA.i)pwcrll<; MAXXX 18mg I1apri8a<;:02/ MAXXX 18mg/12)
yta 'IllY aYixvcucrll rmY napaKarm ITiYaKa<; 2.
IlivaKUS 2.
AKpmVUf.UO
pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N- ni trosoanabasine
ATIOTEAEI:MATA
'Opw llOO'OTlKOU
l;l)yKEVTpffiO'll Tipoaowptaf.lOU
ME0000l) (LOQ)
(ppm)
(ppm)
ND* 0,01
ND 0,01
ND 0,05
ND 0,01
*NO: UVtXVU8rjKUV vnpoi;UJ.l.LVc; crUJ.l.(j>COVU J.l.E Til avaq>p6p..cva 6pta UVLXVUO"ll'.;
ANIXNEYI:H TIOA YKYKAIKQN APQMATIKQN Y APOrONAN0PAKQN I:TO
AIAA YMA ANAllAHPQI:HI:
2
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E<l>APMOZOMENH ANAA YTIKH TEXNIKH : Apta XproJ..Lawypa<pia- <l>aoJ..LU'tOJ..L-rpia Mai;m; (Gas
To 8taA.u/-la avanA.iJpro011c; MAXXX 18mg(Apt8!-l6c; Ilapri8ac;:02/ MAXXX 18mg/12)
yta 't11V aviX,VED0"11 rrov napaKatro noA.uKUKA.tKrov apro/-lanKrov u8poyovav8paKrov (PAHs ), fHvaKac;
3.
IIivaKilS 3.
acenaphty1ene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
benzo(g,h ,i )pery lene
AIIOTEAE:EMAT A
'Opto IIOGO'TlKOU
!: UYKEVT pro Gfl IIpoGotoptGflOU MEOooou
(LOQ)
(ppm)
(ppm)
ND* 0,005
NO 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
NO 0,021
ND 0,022
*NO: ClVtXVU811K!lV 7tOAUKUKAtKOl aproJ..L!l-rLKOt ubpoyovav8paK<; f..L -ra ava<pp0f..LV!l 6pta
aviXVU011S

/ AptoniOllS M. ToanHiKTJ.:; - - -
Ka911Yllnl<; To;tKol.oyiac; ITfHKou TfllJflllTO<;
L\u;o9uvn't.:; EpyaG't'Tipiou laTpOOtK<rTlKrov EnlOT1JJlWV
& Movaoac; To;tKoA.oyias;
3
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TMHMA IATPIKHL:
T.e. 2208 HpciKAuo KpirtiJ
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
Greece
IHETOIIOIHTIKO ANAA YEH:E META AIIO :EYMIIYKNQ:EH * KAI
TAEINOMH:EH:E EI:EIINEOMENOY ATMOY IIOY IIPOKYIITEI AIIO THN
ATMOIIOIH:EH YrPOY ANAIIAHPQ:EH:E
MAXXX18mg
ETAIPIA: ATMOS LAB
EMDOPIKH YrPOY MAXXX 18mg
01/ MAXXX 18mg /12
ATMOY META ADO
E<DAPMOZOMENH ANAA YTIKH TEXNIKH: Aptoc; Masac; (Gas
Chromatography -Mass Spectrometry) KaL vypll Xpffi!lawypaq>ia-<Dacr!laTo!lETpia Masac; (Liquid
MEXPI 99,97%
llivaKa 1.
propylene glycol
glycerol
nicotine
Ethyl vanillin
Ethyl maltol
water

A
fioGOGT6 (%w/v)
66,58
24,96
1,6
0,265
0,005
0,014
6,55
99,97
Opto fiO!JO'TlKOU
fipomStoplGf.lOU
ME86&ou (LOQ)
( m)
0,198
I, 187
0,1
0,121
0,032
0,135
L'lEV
f..EV
0/;Eia to/;tKOtl]Ta I ,
0aVUll]q>OpO O"E J..LE tO
opJ..La
OI;Eia to/;tKOtl]ta 3, Tol;tK6 crE
1IEpi1ItWO"l] KUtU7IOOT]c;
Xp6vta tol;tKOtl]Ta 2 crE
uopopwus opyavtcrflOUc;
OI;Eia ol;tKOtl]Ta an6 tou
crt6J..Latoc;, Katl]yopia 4
EpE8tcrJ..L6c; tou opJ..Lawc;
(Katl]yopia 2)
EpE8tcrJ..L6c; twv oq>8UAJ..LWV
(Katl]yopia 2)
tol;tKOtl]ta crta 6pyava
crtoxouc; -Eq>anas K8EcrlJ
(Kat yo ia 3)
0/;Eia to/;tKOtl]tU an6 tOU
crt6J..Latos. Katl]yopia 4
To Tol;tKoA.oyiac; q>pEt mcrwnoil]crl] crUJ..Lq>wva J..LE to ISO: 17025 yta nc; otaOtKacriEc;
otaxEiptcrl]c;, Kat apxEto8tl]crl]c; twv OEtyJ..Latwv Kat AEttoupyEi J..LE OtaKptPwJ..LtvEc; crucrKEuc; Kat 6pyava.
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TOY ATMOY
ME 'tTJV AXL 265/2002, <l>EK 1214/B'/19.9.2002 KOI 'tTJV -rrov !lE!lOYro!lvrov
crucr-ranKffiv -rou !lEiY!la-roc; -rou Kavovtcr!lOU 1272/2008 (EK), -ro !lEiY!la Et0"1tEO!lEVOU a-r!lOU
nou npoKl>n-rEt an6 'tTJY a-r!l07tOtTJO"TJ uypou avanA.i)procrT]c; MAXXX 18mg (Apt8116c; I1apri8ac;: 01/
MAXXX 18mg/ 12), !lE crl>cr-racr11 99,97% 6nroc; ava<ppE-rat cr-rov IlivaKa 1, roc; noA.u
(T +) O"E 1tEpimrocrTj EJta<pi)c; !lE 'tO 8p11a Kat roc; (Xn) O"E 1tEpin-rrocrTj Ka'tU1tOO"T]c;.
NITPOZAMIN!!N ATMO META AIIO

E<l>APMOZOMENH ANAA YTIKH TEXNIKH ** : YypiJ (Liquid

0 Etcr1tVEO!lEvoc; a-r116c; nou npoKl>mEt an6 1TJV a-rllonoiT]crTJ uypou avanA.i)procrTJc; MAXXX 18mg
(Apt8!l6c; I1ap-ri8ac;:Ol/ MAXXX 18mg 112) yta 1TJV aviX,VEUO"TJ -rrov napaKa-rw
vnposa!ltvffiv, IlivaKac; 2.
IHvaKas 2.
AKpffiVllJllO
4-(Meth ylnitrosamino )-1-(3-
pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N -nitrosoanabasine

(ppm)
ND*
ND
ND
ND
'Opto IloJOTlKOll
Ilpom)toptJJlOll
Mc06()ou (LOQ)
(ppm)
0,01
0,01
0,05
0,01
IIOA YKYKAIK!!N AP!!MA TIK!!N Y APOrONAN0PAK!!N
ATMO MET A AIIO
E<l>APMOZOMENH ANAA YTIKH TEXNIKH : Apta <l>acrf.!atoflc'tpta (Gas
2
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0 ctcr7tVc6J..LcVoc; a-rJ..L6c; 1tou 1tp01c6mct a1t6 TTJV aTJ..l01tOillcr11 uypou ava1tA.ijprocrlls MAXXX 18mg
(Apt8J..L6c; ITap-ri8ac;:Oll MAXXX 18mg 112) yta TTJV avixvcucr11 -rrov 7tapaKa-rro
1tOAUKUKAtKffiv aproJ..LanKffiv u8poyovav8paKrov (PAHs ), ITivaKac; 3.
llivaKUS 3.
AKpOOVUJUO
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
AIIOTEAE:EMA T A
OplO IIOO'OTlKOU
:EuyKEV'TpOOO'll IIpoO"owptO"Jloil MEOooou
(LOQ)
(ppm)
{ppm)
ND* 0,005
NO 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
NO 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*NO: LlV UVtXVU811KUV 7tOAUKUtcAtKOt a.pCO)..lUTtKOt uopoyovav8pa.Kt; <JU)..l<j>COVU TU 6pta.
UVtXVU<J11S
IUTfHKou TJ..LiiJ.laToc:;
Epya<J'Tl"'piou laTpOOlKO"TtKrov E7tlO'TllflWV
& To;tKoA.oyiac:;
3
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TMHMA IATPIKHL.
UNIVERS11Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpciKA&to Kpirtq P.O.Box 2208 Heraklion Crete,
Greece
EPfAiTRPlO TO!lKOA.OflAi
Llu:u0uvn1<;: KaOrrYTJTTJ<; ApuJTL6T)<; M. TaaTaaKT)<;
,. Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris@med.uoc.gr http://ctoxres.med.uoc.qr
nf..rlPooplE<;: 2810 394687 394681 394794, Fax: +30 281 0 39 46 SHl
lliETOllOIHTIKO ANAA Yl:H:E* KAI TASINOMHl:Hl: TOY AIAA
ANAIIAHP!l:EHl: RY69 18mg
EMDOPIKH ONOMAEIA YrPOY ANAllAHPQEHE: RY69 18mg
API0MOE 011 RY69 18mg/12
IIOIOTIKOE YMA TOE ANAIIAHPQEHI:
E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH: Apta<; XpCDJla'toypa<pia-<l>acrJla'tOJle'tpia Masa<; (Gas
Chromatography -Mass Spectrometry) Kat **YypfJ XpCDJla'toypa<pia-<l>acrJla'toJ.!Epia Masas (Liquid
IIOI:OTIKOI: MEXPI IIOI:OI:TOY 99,9999%
IlivaKas 1.
OuGia
propylene glycol
glycerol
ethyl vanillin
Ethyl maltol
nicotine
water
I:uvolo
AIIOTEAEI:MAT A
00GOGTO (o/ow/v)
64,86
29,94
0,006
0,585
0,425
1,7
2,4839
99,9999
Upto floGonKou
flpoGotoplGI.lOU
Mt96ooll (LOQ)
( m)
0,198
1,187
0,032
0,135
0,121
0,1
!lev
fleV
ano
cr'tOJla'tO<;, Ka'tT)yopia 4
Epe8tcrJ.!OS 'tOU bEpJlU'tO<;
(KanJYopia 2)
Epe8tcrJlOS 'tCDV o<p8aAJlcOV
(Ka'tT)yopia 2)
Et8tKTj O""CU
6pyava
K8e<Yl] (Kanwopia 3)
ano
cr't6Jla't0s, Kanwopia 4
!lev
I
3
Xp6vta 2 cre
u8p6pwus opyavtcrJlous
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To Epyacrn)pto <ppt mcrT07WtTJ<J'l ISO: 17025 yta nc; 8ta8tKacric;
8taxiptc:rTJc;, Kat apxto9TTJ<JTJc; rwv Kat Atmupyi crucrKUtc; Kat 6pyava.
H opyavoA.oyia LC-MS q>EpEt 8taKpipwcr'l Kara ISO: 17025 n8io TTJV avixvU<JTJ vapKwnKwv oucrtwv
<JTTJV Tpixa.
TASINOMH1:H TOY YrPOY ANAIIAHP.Q1:H1: RY69 18mg
Me TT)V AXL 265/2002, <DEK 1214/B'/19.9.2002, TT)V Tcov !!E!!OVCO!!Evcov
<rucrTanKrov TOU !!ctY!!UToc; Kat TOU Kavovtcr!!OD 1272/2008 (EK) TO RY69 18mg
(Apt8!!6c; ITapTi8ac;: 01/ RY69 18mg/12) !!E 99,9999% crDcrTacrT) 1rou avacppETat crTOV ITivaKa 1,
coc; !!11 E1tlKtVbUVO yta TT)V av8pffimVT) uycia, yta TO Kat !!E nc;
q>UcrtKOXT)!!lKEc; TOU tbtOTT)Tcc;. Em1tp6cr8ETa, yta TT) XPTJ<JT) TOU 8taAD!!UToc; ava1tATJpCOcrT)c; a1t6 TO
T)AEKTpOVlKO Tcrtyapo, TO !!clY!!U El<J1tVEO!!EVCOV UT!!WV 1tOU U1tEAEU8cpcOVELal XPEtasE-rat
U1t' 0\j/T) TT)V EKUTO<JTtata <JU<JLU<JT) TCOV UT!!WV 1tOU 1tapayOVTat !!E TT)V
EVEpyo1tOtT)<JT) TOU !!T)XUVtcr!!OD UT1!01tOtT)<JT)c; !!EXPl1tcplEKTtKOTT)TUc; 0.1 o/o <JE !!E!!OVCO!!EYO
crucrTanK6, Ka8roc; Kat TT) ouyKEKPt!!EVT) XPiJcrTt auTv.
ANIXNEY1:H NITPOZAMIN.QN 1:TO L\IAA YMA ANAIIAHP.Q1:H1:
EAPMOZOMENH ANAAYTIKH TEXNIKH ** : Yyp11 XpcoJ.La:roypacpia-<l>acrJ.La-roJ.LTpia Masac; (Liquid
ANIXNEYOMENE1: OY1:IE1:
To 8taA.u!!a ava7tA.ijpcocrT)c; RY69 18mg (Apt8!!6c; ITapTi8ac;:Oll RY69 18mg/12) yta
TT)V avixvcucrT) Tcov 7tapaKaTco vtTposa!!tvrov, ITivaKac; 2.
llivaKClS 2.

pyridyl)-1-butanol
pyridyl)-1-butanone
N -nitrosoanatabine
N -nitrosoanabasine
AIIOTEAE1:MAT A
(ppm)
ND*
ND
ND
ND
'Opw IloaOTlKOU

Mc96()ol) (LOQ)
(ppm)
0,01
0,01
0,05
0,01
ANIXNEY1:H IIOA YKYKAIK.QN AP.QMA TIK.QN Y L\POrONAN0P AK.QN 1:TO
L\IAA YMA ANAIIAHP.Q1:H1:
2
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E<l>APMOZOMENH ANAAYTIKH TEXNIKH: Af:pta Xpwf..Lawypa<pia- <l>acrJ..LaTOJ..LE-rpia Masac; (Gas
ANIXNEYOMENE:E OYEIE'E
To 8taAU!la avanA.flprocrT]<; RY69 18mg(Apt8!l6<; I1apTi8a<;:Ol/ RY69 18mg!l2) yta
TT]V avixvcucr11 Trov napaKaTro noA.uKUKAtKmv apro!laTtKmv u8poyovav8paKrov (PAHs), ITivaKa<; 3.
llivaKUS 3.
AKprovi>t.uo
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
ATIOTEAE:EMA T A
Opw TioaonKoi>
l:uyKEVTpOO<Jfl
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
NO 0,003
ND 0,060
NO 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: UVtXVEU8TJKUV 7tOAUKUKAtKOt apWf..LU'ttKOi uopoyovav8paKE<; GUJ..L<pffiVU f..LE -ra ava<pEpOJ..LEVU 6pta
aviXVEUcrTJc;.
0 "COU .Epy. piou,
/
----

/ ' \ <_:<13
/ ApLoTdO'IS M. ToaT<f(iKflc;;, '--,
Ka911Y'InlS laTplKou Tf.LTJJlflToc;;
EpyaOTflp{ol) laTpOOLKCIOTlKcilv EnlOTflf!IDV
& Movaoac; To;tKoJ.oyia;
3
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ITANEITII:THMIO KPHTHI:
TMHMA IATPIKHL.
T.9. 2208 HpciKAEto KpiJul
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
Greece
DII:TODOIHTIKO ANAA YI:HI: MET A ADO I:YMDYKN!!I:H * KAI
T ASINOMHI:HI: EII:DNEOMENOY ATMOY DOY DPOKYDTEI ADO THN
ATMODOIHI:H YrPOY ANADAHP!!I:HI:
RY6918mg
ETAIPIA: ATMOS LAB
EMllOPIKH ONOMAI:IA YrPOY ANATIAHPQI:HI:: RY69 18mg
API0MOI: llAPTIAAI:: 01/ RY69 18mg /12
llOIOTIKOI: llPOI:AIOPII:MOI: EII:llNEOMENOY A TMOY MET A AllO I:YMllYKNQI:H
E<DAPMOZOMENH ANA/\. YTIKH TEXNIKH: Apwc; XpcoJ.la'tOypa<pia-<DacrJ.lU'tof.lETpia Masac; (Gas
Chromatography -Mass Spectrometry) Kat ''Yypi] Masac; (Liquid
llOI:OTIKOI: llPOI:AIOPII:MOI: MEXPI llOI:OI:TOY 99,97%
llivaKa 1.
Oua(a
propylene glycol
glycerol
nicotine
Ethyl vanillin
Ethyl maltol
Water
I:uvol..o
AllOTEAEI:MA TA
noaO<JTO (o/ow/v)
66,66
28,08
1,4
0,387
0,006
0,499
2,94
99,97
OplO noaOTlKOU
n poaowptaflOU
Me86oou (LOQ)
( m)
0,198
1,187
0,1
0,121
0,032
0,135
Ac:v
Ac:v
OI;Eia tol;tK6tT]TU I , 8avatT]<p6po
<JE f.LE tO Of:pf.La
Ol;c:ia tol;tK6tT]TU 3, Tol;tK6 crc:
7rEpi7rtW<JT] KUtU7rO<JT]<;
Xp6vta tO/;tKOtT]tU 2 ()f: uop6pwuc;
OI;Eia tol;tK6tT]TU an6 tou
crt6f.Latoc;, KatT]yopia 4
Epc:9tcrf16c; tou oEpf.Latoc;
(KatT]yopia 2)
Epc:9tcrf16c; twv o<p9aA.wi>v
(KatT]yopia 2)
to/;tKOtT]tU crm 6pyava
crt6xouc;-c:<panas EK9E<JT] , MnopEi
VU 7rpOKUAE<JEl EpE9t<Jf10 <JtT]V
UVU7rV01 (Katl)yopia 3)
Ol;c:ia to/;tK6tT]tU an6 tou
crt6f!UtOS, KatT]yopia 4
' To Tol;tKoA.oyiac; <ptpc:t mcrtonoiT]<JTJ crUf.L<pwva f.LE to ISO: 17025 yta nc; otaotKacric:c;
otaxEiptmlc;, Kat apxc:to9EtT]<JT]<; tWV OElYf!UtWV Kat AEttoupyEi f.LE OlUKptPWf!EvE<; <JU<JKEUE<; Kat 6pyava.
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TASINOMH:EH TOY EI:ETINEOMENOY ATMOY
ME TllV AXL 265/2002, <l>EK 1214/B'/19.9.2002 KOI TllV TroY f.!Ef.!OVrof.!EVrov
OU<JTUTtKWV TOU f.!ElYflUTOc; TOU Kavovt<Jf.!OU 1272/2008 (EK), TO f.!Etyfla Et<J1tVEOf.!EVOU UTflOU
nou np01c6n-rEt an6 T'llV UTfl07tOtll<Jll uypou avanA.iJprocrllc; RY 69 18mg (Apt8f.!6c; I1ap-ri8ac;: 011
RY69 18mg/12), f.!E crucrmcr11 99,97% 6nroc; ava<ppETat cr-rov ITivaKa 1, roc; no/..u
(T +) <JE 7tEpt7tTro<Jll Ena<.pftc; f.!E TO 8pfla Kat roc; (Xn) <JE 1tEpin-rrocr11 KUTU7t0<Jllc;.
ANIXNEY:EH NITPOZAMIN!!N :ETON EI:ETINEOMENO ATMO META ATIO
:EYMTIYKN!!:EH
E<l>APMOZOMENH ANAA YTIKH TEXNIKH : Yyp1) XpwJlaTOypa<pia-<l>acrJlaTOflETpia Mal;;a<; (Liquid
0 Et<J1tVEOf.!Evoc; a-rf.!6c; nou nporimEt an6 TllV aTf.!07tOtll<Jll uypou avanA.iJprocrllc; RY69 18mg
(Apt8f.!6c; I1apd8ac;:Ol/ RY69 18mg /12) yta TllV avixvwcr11 -rrov napaKa-rro
vnposaf.!tvffiv, ITivaKac; 2.
IltVClKClS 2.
pyridyl)-1-butanol
pyridyl)-1-butanone
N-ni trosoanatabine
N -nitrosoanabasine
ATIOTEAE:EMAT A
(ppm)
ND*
ND
ND
ND
'OplO floGO'tlKOU
UpoG()wptGJ.lOU
ME9o()ol) (LOQ)
(ppm)
0,01
0,01
0,05
0,01
*ND: avtxveu8l]Kav vt-rpo/;;af.liV<; crUJl<pCDva -ra ava<pep6flVa 6pta avix;veuml<;
ANIXNEY:EH UOA YKYKAIK!!N AP!!MATIK!!N Y APOrONAN0PAK!!N :ETON
EI:EUNEOMENO ATMO MET A ADO :EYMUYKN!!:EH
E<l>APMOZOMENH ANAA YTIKH TEXNIKH : Apta XpCDJla-roypa<pia- <l>acrJlUTOflETpia Ma/;;a<; (Gas
0 EtcrnvEOf.!EVoc; a-rf.!6c; nou nporinTEt an6 TllV aTf.!07tOtll<Jll uypou avanA.iJprocrllc; RY69 18mg
(Apt8f.!6c; I1ap-ri8ac;:O 11 RY69 18mg I 12) yta TllV avixvwcr11 -rrov napaKa-rro
noA.uKUKAtKffiv aprof.!anKffiv u8poyovav8paKrov (PAHs), ITivaKac; 3.
2
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TiivaKaS 3.
AKpO>VVf.llO
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
ATIOTEAEI:MAT A
'OplO llO<JO'TlKOV
l:lY'fKEV'tpO><JT) Tipo<J&wpt<Jf.lOil MtOo&ou
(LOQ)
(ppm)
(ppm)
ND* 0,005
ND 0,010
ND 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
ND 0,021
ND 0,022
*ND: UVlXVEU811KUV 1tOAUICU1CAlKOi apCOI!UTlKOi OUI!<f>COVU 1-LE La avacpEp011VU 6pta

.- / . 1- ,
/ '. '-...'0':]
/ Apto't'l01}<; M. TociToaK1}.; ___;__.--'
Ka01)Y1}n\<; laTplKOU TJ..Lt\J..LaTo<;
t:\u:1)9'U\'Tit<; EpyO't'T)piou laTpOOLKO't'tKrov E1tlOT1)J1WV
& Movaow; To;ucoA.oyiac;
3
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IIANEIIIl:THMI 0 KPHTHl:
TMHMA
UNIVERSI1Y OF CRETE
MEDICAL SCHOOL
T.e. 2208 HpaKAuo Kpircq P.O.Box 2208 Heraklion Crete,
Greece

Llu:uOuvTft<;: Ka01JYTITTt<; AptaTEL6T)<; M. TaaTaUKT)<;
Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris(Q)med.uoc.ar http://ctoxres.med.uoc.qr
nXr)po<(>oplE<;: 2810 394687 - 394681- 394794, Fax: +30 281 0 39 46 RR
TilETOTIOIHTIKO ANAA Y:EH:E* KAI TAEINOMH:EH:E TOY AIAA
ANATIAHPQ:EH:E MINT 18mg
ETAIPIA: ATMOS LAB
EMTIOPIKH ONOMAI:IA YrPOY ANAIIAHPQI:HI:: MINT18mg
API0MOI: IIAPTIL\AI:: 01/ MINT 18mgll2
IIOIOTIKOI: IIPOI:I\IOPII:MOI: 1\IAA YMA TO I: ANAIIAHPQI:HI:
E<l>APMOZOMENH ANA/\ YTlKH TEXNIKH: Apto<; XpwJ..lawypa<pia-<l>aoJ..laWJ..lETpia Masa<; (Gas
Chromatography -Mass Spectrometry) Kat .. YypiJ Masa<; (Liquid
IlivaKas 1.
Ouaia
propylene glycol
glycerol
nicotine
water
I:uvoA.o
AIIOTEAEI:MA T A
Ooao1no (%w/v)
47,66
49,78
1,8
0,759
99,999
Upto noaOTtKOU
npoaowptaJ.tOil
ME96oou (LOQ)
( m)
0,198
1 '187
0,1

1
3
Xp6vta 2 o
opyavtoJ..lous
To Tol;tKoA.oyiac; q>i:pEtnt<nonoiT]<HJ <JD!lq>mva !-IE ro ISO: 17025 yw nc; 8ta8tKacriEc;
8taxEiptcrT]c;, Kat apxEw8i:rT]crT]c; rcov 8Ety!larmv Kat A.EtroupyEi !!E crucrKrni:c; Kat 6pyava.
H opyavoA.oyia LC-MS q>i:pEt Kara ISO: 17025 !!E nE8io TT]V avi;zyrncrl] vapKmnKwv oucrtwv
crr11v rpixa.
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TOY YrPOY MINT 18mg
ME pacrYJ -rYJv AXI: 265/2002, <DEK 1214/B'/19.9.2002, -rYJv -row 1-LEI!OVffii!EVffiv
crucr-ranKrov mu I!ElYI!amc; Kat pacrYJ mu Kavovtcr11ou 1272/2008 (EK) m MINT 18mg
ITap-rioac;: 011 MINT 18mg /12) 1-LE 99,999% <JUcr-racrYJ 1tou avacppE-rat crmv ITivaKa 1,
ffi<; 1-LTJ E7tlKlVOUVO yta 'tT]V av9pc07ttVYJ uyEia, yta 'tO 7tEptpaAAOV Kat 1-LE pacrYj n<;
cpucrtKOXYJI!lKE<; -rou tot6'tT]-rE<;. Em7tp6cr9E-ra, yta 'tTJ XPll<JT] mu otaAUI!a-ro<; ava7tAllPffi<JT]<; a1t6 -ro
YJAEK'tpOVlKO -rmyapo, 'tO El<J7tVE01!EVffiV U'tl!cOV 7tOU U7tEAEU9EpcOVE'tal XPElUSE'tat
Aai!P<ivov-rac; u1t' O\j/TJ 'tTJV EKamcrnaia crucr-racrYJ -rffiv a-r11rov 1tou 7tapayov-rat 1-LE 'tTJV
EVEpyo7tOtT]<JT] mu a-ri!07tOtT]<JT]<; 1-LEXPt 7tEptEKnK6-rYJ-ra<; 0.1% PIP <JE 1-LEI!OVffii!EVO
crucr-ranK6, Ka9roc; Kat TJ XPllO"TJ au-rrov.
NITPOZAMIN!lN AIAA YMA
E<DAPMOZOMENH ANAAYTIKH TEXNIKH ** : YypfJ (Liquid

To otaAulla ava7tAllPffi<JT]<; MINT 18mg ITap-rioac;:Ol/ MINT18mg /12) yta
TTJV aviXVED<JTJ -rffiv 7tapaKa-rffi vnposalltvrov, ITivaKa<; 2.
lltVUKUS 2.
4-(Meth ylnitrosamino )-1-(3-
pyridyl)-1-butanol
pyridyl)-1-butanone
N-nitrosoanatabine
N-nitrosoanabasine

(ppm)
ND*
ND
ND
ND
Dpw IloGOTlK01)

(LOQ)
(ppm)
0,01
0,01
0,05
0,01
IIOA YKYKAIK!lN AP!lMATIK!lN Y APOrONAN0PAK!lN
AIAA YMA
E<DAPMOZOMENH ANAA YTIKH TEXNIKH: Apta XpffiJ..tmoypacpia- (Gas
2
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To ouiA.ufla avanA.ftpwcrrJ<; MINT 18mg (Apt8fl6<; ITap-rioac;:Ol/ MINT 18mgl12) yta
'rl]V aviXVEDGT] 'r(J)V napaKU'r(J) TCOAUKUKAtKWV apWflUTtKWV uopoyovavepaKWV (PAHs), ITivaKa<; 3.
llivaKas 3.
acenaphtylene
fluorene
phenanthrene
anthracene
pyrene
benzo(a)anthracene
chrysene
AIIOTEAEI:MA T A
'Opto IloaO'TlKOU
l;l)yKEV'TpOOGll Ilpoa(hoptGf.lOU Mt960o1)
(LOQ)
(ppm)
(ppm)
ND* 0,005
NO 0,010
NO 0,005
ND 0,006
ND 0,003
ND 0,003
ND 0,003
ND 0,060
ND 0,006
ND 0,014
NO 0,021
ND 0,022
*ND: avtxveu811Kav noA.uKUKAtKoi u8poyovav8paK<; m 6pta
avixvwcr11<;.
3
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Atmos Lab's Eliquid Analysis 10/2012 GR

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