on
On Behalf Of
With compliments
Sample(s) submitted as
Description(s) on Label(s)
CWO-14064
Seals on Sample(s)
Sample(s) received on
May 2, 2006
The above sample(s) was/were examined as detailed below and the following results obtained:
Page 1
General:
The Al Shaheen Crude Oil samples were received from Intertek Caleb Brett Qatar Branch on May 02, 2006. The samples were in 3 x 20 Ltrs & 2 x 10 Ltrs IATA Cans. The labels indicated that the samples were drawn on 10th April 2006.
Please do not hesitate to contact us for any additional information or clarifications that you may require on this analysis.
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LABORATORY REPORT NO. - FUJ/FCA1025/06 Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006. CRUDE OIL - DETAILED ASSAY ALL CUTS OVERVIEW
CUT RANGE Whole Crude 1 LIGHT ENDS C42 3 65 - 150C 4 150 - 200C 5 200 - 250C 6 250 - 300C 7 300 - 350C 8 350 - 420C 9 420 - 560C 10
TEST
UNIT
METHOD
C5 - 65C
Distillation of Crude Oil (15 plate) Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Density @ 15C (dry) Specific Gravity @ 60/60 F (dry) API Gravity @ 60 F (dry) Water Content Light Ends methane ethane propane i-butane n-butane Total C1-C4 i-pentane n-pentane Sulphur Content Mercaptan Sulphur Mercaptan Sulphur Total Nitrogen Research Octane Number *** Motor Octane Number *** PIONA analysis Total paraffins Total olefins Total napthenes Total aromatics > 200 C & Unidentified Poly-N Aniline Point Smoke Point Naphthalene content Vanadium (V) Nickel (Ni) Iron (Fe) Nickel / Vanadium Ratio Freeze Point Cloud Point Pour Point (upper) Pour Point (lower) Kinematic Viscosity @ 20 C Kinematic Viscosity @ 40 C Kinematic Viscosity @ 50 C Kinematic Viscosity @ 80 C Kinematic Viscosity @ 100 C Kinematic Viscosity @ 150 C Distillation Cetane Index Refractive Index @ 20 C Refractive Index @ 70 C Micro Carbon Residue Asphaltene Total Acid Number Benzene Content Salt Content Salt Content as NaCl Salt Content Flash Point Sediment by Extraction Reid Vapour Pressure @ 100 F Hydrogen Sulphide Mercury Lead Wax Content prec. At -30 C
Note:
ASTM D 2892 & ASTM D 5236 ASTM D 2892 & ASTM D 5236 ASTM D 5002 / IP 365 / IP 190 Conversion Calculated 0.8868 0.8873 27.97 0.8865 0.8870 28.03 0.18 0.000 0.039 0.309 0.260 0.811 1.419 0.950 0.633
kg/L
% Vol.
ASTM D 4298
% mass
GC
ASTM D 4294 ASTM D 3227 UOP 163 ASTM D 5291 (Mod) ASTM D 2699 ASTM D 2700
0.043 235
0.066 314
0.180 225
0.356 103
1.88
2.41
2.86
5.00
< 0.05
0.08
0.15
0.37
57.0 55.0 61.63 < 0.01 36.24 2.13 < 0.01 < 0.01 33.72 < 0.01 23.61 18.23 24.44 5.97 55.2 27.0 0.17 112 38 15 0.34 58.4 21.0 60.4 68.6 73.0 84.6
% Vol
GC
C mm %Vol. mg/kg
C C C C
ASTM D 2386 ASTM D 2500 ASTM D 5853 / D97 ASTM D 5853 / D97 Below -45 Below -45 44.06 13.32
Below -70.0
1.670 1.443
mm2/S
ASTM D 445
10.21
See page 17
* *
43.3 1.4578
45.8 1.4771
46.8 1.4893
% mass % mass mgKOH/g % mass PTB mg/L mg/kg C % mass psi mg/kg mg/kg mg/kg % mass
ASTM D 4530 IP 143 ASTM D 664 GLC ASTM D 3230 IP 265 IP 265 ASTM D 93 (Mod.) ASTM D 473 ASTM D 323 UOP 163 Cold Vapor ASTM D 5863 / AAS UOP 46 1.70 0.329 < 0.01 46.3 145.8 149.0 Below -5 0.01 6.4 <1 <1 < 0.1 1.0
0.60
23.3 9.02
* Unable to perform test due to the heavy nature of the fraction. *** Samples were blended with ASTM grade Iso Octane, and results were caluclated from the blend's result. ## Unable to test due to the dark colour of the fraction. Page 3
560C +
METHOD
ASTM D 5002 Calculated Conversion
Whole Crude
0.8868 0.8873 27.97 0.8865 0.8870 28.03 0.18 0.000 0.039 0.309
kg/L
% Vol.
ASTM D 4298
% mass
GC
ASTM D 4294 UOP 163 ASTM D 5291 (Mod) ASTM D 5853 ASTM D 5853 ASTM D 445
2.37 339 0.15 Below -45 Below -45 44.06 13.32 10.21 1.5008 1.70 0.329 < 0.01 46.3 145.8 149.0 Below -5 0.01 6.4 <1 <1 < 0.1 1.0
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Sl. No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24
Vapour Temperature C Gas 15 - 40 40 - 65 65 - 100 100 - 125 125 - 150 150 - 175 175 - 200 200 - 225 225 - 250 250 - 275 275 - 300 300 - 325 325 - 350 350 - 375 375 - 400 400 - 420 420 - 450 450 - 475 475 - 500 500 - 520 520 - 540 540 - 560 560 + Residue
% Weight 1.28 1.35 1.35 2.57 2.19 2.47 3.16 3.23 3.64 4.01 4.49 4.78 4.63 4.74 4.74 4.56 2.73 3.65 5.37 4.15 2.71 2.53 2.69 22.98
Cumulative % Weight 1.28 2.63 3.98 6.55 8.74 11.21 14.37 17.60 21.24 25.25 29.74 34.52 39.15 43.89 48.63 53.19 55.92 59.57 64.94 69.09 71.80 74.33 77.02 100.00
% Volume 2.00 1.90 1.80 3.22 2.64 2.91 3.61 3.58 3.95 4.28 4.69 4.90 4.73 4.71 4.65 4.47 2.65 3.50 5.11 3.91 2.52 2.33 2.44 19.50
Cumulative % Volume 2.00 3.90 5.70 8.92 11.56 14.47 18.08 21.66 25.61 29.89 34.58 39.48 44.21 48.92 53.57 58.04 60.69 64.19 69.30 73.21 75.73 78.06 80.50 100.00
Page 5
Temperature C
Recovery %
50.0
60.0
70.0
80.0
90.0
% Weight
% Volume
Page 6
LABORATORY REPORT NO. - FUJ/FCA1025/06 SUMMARY OF PRODUCT / RESIDUE CUT POINTS AND YIELDS
Yield %
Cut Points
( C)
Weight %
Volume %
IBP - 65
2.70
3.70
65 - 150
7.23
8.77
150 - 200
6.39
7.19
200 - 250
7.65
8.23
250 - 300
9.27
9.59
300 - 350
9.37
9.44
350 - 420
12.03
11.77
420 - 560
21.10
19.81
560 +
22.98
19.50
Page 7
CUT RANGE TEST UNIT METHOD 2 C5 - 65C Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Mercaptan Sulphur Research Octane Number *** Motor Octane Number *** PIONA analysis Total Paraffins Olefins Napthenes Aromatics > 200 C & Unidentified Poly-Naphthenes
Note: *** Samples were blended with ASTM grade Iso Octane, and results were caluclated from the blend's result. Page 8
% Wt. ASTM D 2892 % Vol. % Wt. ASTM D 2892 % Vol. kg/L IP 365 Conversion Calculated % mass mg/kg ASTM D 4294 ASTM D 3227 ASTM D 2699 ASTM D 2700
2.70 3.70 3.98 5.70 0.6464 0.6465 87.37 0.043 235 74.2 71.0
95.32 < 0.01 % Vol GC 4.65 0.03 < 0.01 < 0.01
Note: *** Samples were blended with ASTM grade Iso Octane, and results were caluclated from the blend's result.
Page 9
CUT RANGE TEST UNIT METHOD 4 150 - 200C Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Mercaptan Sulphur PIONA analysis Total Paraffins Olefins Napthenes Aromatics > 200 C & Unidentified Poly-Naphthenes Aniline Point Smoke Point Naphthalene content Freeze Point C mm %Vol. C ASTM D 611 IP 57 ASTM D 1840 ASTM D 2386 % Vol GC 33.72 < 0.01 23.61 18.23 24.44 5.97 55.2 27.0 0.17 Below -70.0
Page 10
% Wt. ASTM D 2892 % Vol. % Wt. ASTM D 2892 % Vol. kg/L IP 365 Conversion Calculated % mass mg/kg ASTM D 4294 ASTM D 3227
CUT RANGE TEST UNIT METHOD 5 200 - 250C Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Mercaptan Sulphur Aniline Point Smoke Point Freeze Point Cloud Point Kinematic Viscosity @ 40 C mm2/S Kinematic Viscosity @ 50 C Distillation Cetane Index Refractive Index @ 20 C ASTM D 86 ASTM D 976 ASTM D 1218 ASTM D 445 1.443 See page 17 43.3 1.4578 % mass mg/kg C mm C C % Wt. ASTM D 2892 % Vol. % Wt. ASTM D 2892 % Vol. kg/L IP 365 Conversion Calculated ASTM D 4294 ASTM D 3227 ASTM D 611 IP 57 ASTM D 2386 ASTM D 2500 29.89 0.8250 0.8254 39.93 0.356 103 58.4 21.0 - 52.5 Below -42 1.670 8.23 25.25 7.65
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CUT RANGE TEST UNIT METHOD 7 300 - 350C Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Total Nitrogen Aniline Point Cloud Point Pour Point (upper) Kinematic Viscosity @ 40 C Kinematic Viscosity @ 50 C Kinematic Viscosity @ 80 C Distillation Cetane Index Refractive Index @ 20 C ASTM D 86 ASTM D 976 ASTM D 1218 mm2/S ASTM D 445 % mass % mass C C C % Wt. ASTM D 2892 % Vol. % Wt. ASTM D 2892 % Vol. kg/L IP 365 Conversion Calculated ASTM D 4294 ASTM D 5291 (Mod) ASTM D 611 ASTM D 2500 ASTM D 97 48.92 0.8803 0.8808 29.15 1.88 < 0.05 68.6 -4 -6 6.438 4.977 2.640 See page 17 46.8 1.4893 9.44 43.89 9.37
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CUT RANGE TEST UNIT METHOD 8 350 - 420C Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Total Nitrogen Aniline Point Cloud Point Pour Point (upper) Kinematic Viscosity @ 40 C Kinematic Viscosity @ 50 C Kinematic Viscosity @ 80 C Distillation Cetane Index ASTM D 86 ASTM D 976 mm2/S ASTM D 445 % mass % mass C C C % Wt. ASTM D 5236 % Vol. % Wt. % Vol. kg/L 11.77 55.92 60.69 0.9052 0.9057 24.73 2.41 0.08 73.0 + 18 + 15 16.23 11.46 5.068 * * 12.03
IP 365 Conversion Calculated ASTM D 4294 ASTM D 5291 (Mod) ASTM D 611 ASTM D 2500 ASTM D 97
Note:
Page 14
CUT RANGE TEST UNIT METHOD 9 420 - 560C Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Total Nitrogen Aniline Point Cloud Point Pour Point (upper) Kinematic Viscosity @ 50 C Kinematic Viscosity @ 80 C Kinematic Viscosity @ 100 C Micro Carbon Residue % mass ASTM D 4530 mm2/S ASTM D 445 % mass % mass C C C % Wt. ASTM D 5236 % Vol. % Wt. % Vol. kg/L 19.81 77.02 80.50 0.9449 0.9455 18.16 2.86 0.15 84.6 ## + 42 74.55 21.06 11.53 0.60 21.10
IP 365 Conversion Calculated ASTM D 4294 ASTM D 5291 (Mod) ASTM D 611 ASTM D 2500 ASTM D 97
Note:
CUT RANGE TEST UNIT METHOD 10 560 C + Distillation of Crude Oil Yield Yield Cum. Yield Cum. Yield Density @ 15C Specific Gravity @ 60/60 F API Gravity @ 60 F Sulphur Content Total Nitrogen Vanadium (V) Nickel (Ni) Iron (Fe) Nickel / Vanadium Ratio Pour Point (upper) Kinematic Viscosity @ 100 C mm /S Kinematic Viscosity @ 150 C Micro Carbon Residue Asphaltene % mass % mass ASTM D 4530 IP 143
2
22.98 19.50 100.00 100.00 1.0250 1.0257 6.45 5.00 0.37 112
% mass % mass
mg/kg
IP 470 ( AAS )
38 15
Calculated C ASTM D 97
0.34 + 51 3013
Page 16
Boiling range Yield on whole crude Initial boiling point 10% recovered 20% recovered 30% recovered 40% recovered 50% recovered 60% recovered 70% recovered 80% recovered 90% recovered Final Boiling Point Volume recovered Residue Loss
200 - 250 7.65 8.23 213.0 216.0 217.5 219.0 220.0 222.0 224.0 226.5 230.0 235.0 243.0 97.0 1.3 1.7
250 - 300 9.27 9.59 264.0 266.5 267.5 269.0 270.0 272.0 274.0 275.5 278.5 284.0 290.5 97.5 1.3 1.2
300 - 350 9.37 9.44 310.0 314.0 315.5 317.0 319.0 321.0 324.0 326.0 329.5 337.5 345.1 98.5 1.0 0.5
Note: ** Unable to perform ASTM Distillation due to the heavy nature of the fraction.
Page 17
LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006
1.0500
1.0000
0.9500
0.9000
Density - (kg/L)
0.8500
0.8000
0.7500
0.7000
0.6500
0.6000
0.5500
Density @ 15 C
C5 - 65C 0.7316
65 - 150C 0.7897
Fraction
Page 18
LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006
5.000
4.000
Sulphur % mass
3.000
2.000
1.000
0.000
Sulphur
C5 - 65C 0.043
65 - 150C 0.066
560+C 5.00
Fraction
Page 19
LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006
0.500
0.450
0.400
0.300
0.250
0.200
0.150
0.100
0.050
0.000
Nitrogen
560+C 0.370
Fraction
Page 20
LABORATORY REPORT NO. FCA/1025/06 Sample ID - Al Shaheen Crude Oil Ex Qatar sampled on 10th April 2006
90.6
80.6
70.6
50.6
40.6
30.6
20.6
10.6
0.6
Aniline Point
Fraction
Page 21