Excellent Testing Facilities for Automobile Materials

Metal Mechanical Testing Metallurgy Corrosion Testing Plastic/Polymer Testing Environment & Endurance Testing RoHS Failure Analysis

EXCELLENCE IN TESTING & INSPECTION

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Spectro is leading testing and inspection services provider having 12 branches in India and two in Middle East. Founded in the year 1995 as the first independent spectrometer laboratory in Delhi, It is now a well diversified setup analyzing a wide range of materials for more the 12000 customers in various sectors of Industry, Government and Inspection & nodal agencies.
SPECTRO has ISO 17025 accreditation in these fields i.e.

BIOLOGICAL

NDT

CHEMICAL

MECHANICAL

MECHANICAL CALIBRATION

THERMAL CALIBRATION

ELECTRO TECHNICAL CALIBRATION

ISO 9001:2008

ISO 14001:2004

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

One stop solution to your Testing needs.

Spectro Labs believes in establishing long-term, strategic relationships with our customers as opposed to short-term, opportunity-based engagements. We provide excellence in each aspect of Services, starting from accuracy to fast Delivery of Test Results. Customers are the ultimate promoters and ambassadors of goodwill. Our key customers are leaders in their respective fields. Spectro has a long standing track record of providing these services to the leading organizations of private & government sectors in the Construction, Oil and Gas, Refining, Chemicals, Electronics, Power Generation, Automotive, Defense, Mining, Process Industry.

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Clients in Auto Sector

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Metals & Alloys

Direct spectrometer techniques give very fast and accurate results provided standard samples are available in substantial quantities. Spectro Labs was the first lab to introduce direct Spectrometer (OES) techniques for metal analysis. It has the largest capability in the country to analyze any Metal- ferrous, non-ferrous or precious metals.Spectro has the largest range of certified reference materials (CRM) to cover the entire range of metals. Metals not possible to analyze by direct optical emission spectrometer are analyzed by XRF or by ICP Spectrometer. The XRF spectrometer has the capability to analyze elements from sodium to uranium in the periodic table, While the ICP can analyze many other elements not possible by above techniques. All precious and rare metals are now possible to be analyzed by these techniques. Hazardous elements and restricted substances like Pb, Cd, Hg and total Cr can also be analyzed in plastics and rubbers.

Major Equipments
hSpectrometer (OES) Spectro Max (2) hSpectrometer (XRF-WD) - Rigaku hSpectrometer (OES) - Metallab / GNR / Polyvac hSpectrometer (ICP) - Varian-VISTA-MRX hFTIR Spectrometer - Perkin Elmer hAtomic absorption spectrometer (GBC) hUV-VIS Spectrophotometer- Thermo Electron Corp hICP Simultaneous spectrometer. (Varian) hPortable Spectrometer XRF-X Met-OXFORD hPortable Spectrometer Arc Met-920-OXFORD
SPECTRO ANALYTICAL LABS LTD. www.spectrogroup.com

Mechanical Testing
The Mechanical Testing Department at spectro is well equipped to perform most standard mechanical testing, as well as specialized tests designed to the customer's requirements. A complete in-house machine shop supports the department with precise specimen preparation and fixture fabrication.

Capabilities:
hTensile Bar (Round, Flat, Tube) hRotating Beam Fatigue (RBF) hShear hWire/Spring Testing (Wrap, Coil, Bend) hCompression Testing hFlattening hTube Testing (Tensile, Hydrostatic Pressure, Flare) hTorsional and Axial Fatigue (200 lb) hFastener Testing hMicromechanical hBend Testing hBond-Pull Testing hAdhesion (Peel) Testing hIn-House Machine Shop, Specimen Preparation hHardness (Rockwell, Brinell, Knoop, Vickers) hHeat Treatment, Specimen Conditioning hCharpy Impact Testing hHydrogen Embrittlement (Static Load) hStrain Gaging hHi Temp Tensile

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Metallurgy
The metallurgical group is well equipped and staffed (9 full-time metallurgists and technicians) to evaluate materials ranging from cast iron to superalloys to composites. They are experienced in classical metallographic techniques, as well as the latest preparation methods. Advanced analytical tools such as image analysis and scanning electron microscopy (SEM) are used in their evaluations.

Metallurgical Lab Capabilities:

hLight Microscopy hParticle Analysis (Identification, Size, Distribution) hMetallurgical Evaluation (Microstructure, Grain Size, Inclusion Rating, Heat Treat Analysis, Plating Thickness, Intergranular Attack, Porosity of Metals, Ceramics, & Composites) Coating Analysis hCircuit Boards/Microelectronics hScanning Electron Microscopy (SEM) hEnergy Dispersive X-Ray Spectroscopy (EDS) hPhysical Metallurgy Analysis hMacro/Micro/SEM Photography (Digital or Film) hMaterial Failure/Repairability Analysis hX-Ray Fluorescence (XRF) hQuantitative Image Analysis & Surface Topography hProduction Problems (Adhesive Bonding, Filter Residue, Surface Contamination) hFractography hMicrohardness (Knoop & Vickers)

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Corrosion Testing

Oxalic Acid Test, ASTM A 262, Practice A Ferric Sulfate - Sulfuric Acid, ASTM A262 - Practice B Nitric Acid, ASTM A262, Practice C, (Huey Test) Copper - Copper Sulfate - 16% sulfuric acid, ASTM A262 - Practice E (Straus Test) Copper - Copper Sulfate - 50% sulfuric acid, ASTM A262 - Practice F Salt Spray (Neutral / Fog), ASTM B117 Salt Spray Test (CASS) Pitting Corrosion Test, ASTM Gr 48 Crevice Corrosion Hydrogen-Induced Cracking (HIC) Test, NACE TMO284

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Plating And Coating Analysis

Spectro labs offers a complete line of services geared toward certifying platings, paints, and other coatings. The group relies on the extensive resources of the entire organization, utilizing advanced tools and techniques to inspect product quality and diagnose failures.

Capabilities:
hSalt spray hTaber abrasion/wear resistance hChip resistance (gravelometer) hPlating thickness / coating thickness hPlating composition / coating composition hCoefficient of friction hSolvent resistance SEM analysis hCure testing hThumbnail hardness hImpact testing hTape adhesion hCreep resistance hPlating/coating hardness hPlating/coating contamination analysis hPeel testing Coating weight hChemical analysis of plating solutions

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Plastic Testing
Polymers and rubbers are being regularly analyzed to check their composition and their toxic contents. Physical tests and Ageing tests are also being conducted. We are operating a Petroleum Testing Laboratory for a major Refinery. Tests routinely conducted for Polymers and Rubber materials in our Polymer Testing Laboratory are:

Properties
Ash content Bulk density Compression set under constant deflection Compression Properties Charpy Impact Carbon black in Olefin Plastic Coefficient of Friction Deflection Temperature under Load (DTUL or HDT) Density and Specific Gravity Durometer Hardness (Shore Hardness) Differential Scanning Calorimeter (DSC) Dielectric Constant and Dissipation Factor Flexural Properties Flammability FTIR (Fourier Transform Infrared Spectrometry) Impact Resistance of Plastic Film Izod Impact Melt Flow Index (MFI) Oxygen Concentration to Support Candle-like Combustion of Plastics Peel Tests QUV (Accelerated Weathering) Resistance of Plastics to Chemical Reagents Surface Resistivity and Volume Resistivity Shear Strength by Punch Tool Tear Resistance of Plastic Film by Pendulum Method (Elmendorf Tear) Tensile Teste of Plastics Tensile Tests of Rubber Thermo Gravimetric Analysis (TGA) Vicat Softening Temperature Viscosity of Polymers Water Absorption Xenon-Arc Exposure (Weather-Ometer)

Major Equipments
hGCMS hFTIR hHPLCGC With ECD FID hGas Chromotograph (Nucon)

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Polymer Testing
The Polymer Analysis Department is equipped with state-of-the-art equipment for polymer analysis and characterization. The equipment is housed in a room which is maintained at constant temperature and humidity. For information about our nonmetallics testing and polymer analysis capabilities,

Capabilities:
hFailure analysis and custom testing hGardner impact hIzod impact hTaber abrasion hAsh content hUV exposure hDSC/TGA/ analysis hReverse engineering hContamination ID hOils hDegree of crystallinity hMelting point and glass transition hDegree of cure hGC/MS hCompression set hMaterial identification Accelerated aging (heat, fluids) hFiller/additive analysis (EDS and TGA) hDensity/specific gravity hTensile, flexural, & compressive properties hFlexural modulus hWater absorption hHardness (shore, rockwell, durometer) hFTIR (Fourier Transform Infrared Spectroscopy) and MicroFTIR hCreep & fatigue hCoefficient of friction hCoefficient of thermal expansion hElectrical properties (dielectric, resistivity) hFlammability (UL94, FMVSS 302) hMelt flow rate & viscosity SEFA-8 testing of laboratory furniture

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Role Of Thermal Technique In Polymer Studies

A complete thermal analysis system comprises different techniques. Each technique characterizes the sample in a particular way. The combination of all the results simplifies interpretation. TGA measures the weight curve, DSC the heat flow. All these measurement quantities change as a function of temperature or time.TGA is a technique that measures the change in weight of a sample as it is heated, cooled or held at constant temperature. Its main use is to characterize material with regard to their composition. Application areas include plastics, elastomers and thermosets, mineral compounds and ceramics as well as wide range of analyses in the chemical and the pharmaceutical testing. Differential scanning calorimetry (DSC) is the most frequently used thermal analysis technique.DSC measures enthalpy changes in samples due to changes in their physical andchemical properties as a function of temperature or time.

Exremely Wide Application Range:

Thermogravimetry provides quantitative information on the composition and thermal stability of many different types of materials. The method is fast and can even be used with very small samples. Control in numerous fields such as plastic, building material as plastic, building material minerals, pharmaceuticals and Foodstuffs. Thermogravimetry provides quantitative information on the composition and thermal stability of many different types of materials. The method is fast and can even be used with very small samples. The DSC signal can also be quantitatively evaluated,allowing transition and reaction enthalpies to bedetermined.The TGA/DSC is an exceptionally versatile tool for the characterization tool for the physical & chemical material properties under precisely controlled atmospheric conditions. it yields valuable information for research, development and quality.

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Role Of Thermal Technique In Polymer Studies

Examples of Thermal Events and Processes that can be determined by TGA/DSC TGA
h Analysis of polymer blends and copolymer h Determine cure temperature for thermally cured polymer h Reaction rate and temperature evaluation h Inorganic filler content h Transformation temperature h Polymer thermal degradation profiles h Polymer thermal & oxidative ability h For Polymer synthesis h For vulcanization and curing h For heterogeneous materials h In polymer solutions h For insulting materials h Polymer may be used in harsh conditions

DSC
h Melting Temperature h Heat of Melting h Percent crystallinity h Tg of softening h Crystallization h Presence of recyclates/regrinds h Plasticizers content h Polymer blends (presence, composition and compatibility h Evaluate drug and polymer purities h Moisture or volatile compounds

FTIR
hQuantitative scan hQualitative scan hSolids, Films, Liquids hOrganic Samples hInorganic samples hPlastics hPolymers hContamination identification hImpurities Screening hFormulations, deformulations hToys hConsumer goods hHousehold products hMedical device hCoating, adhesives hComparative analysis hFTIR can identify chemical agents

Rubber analysis of SBR:

In rubber analysis, the sample is first heated to 600C under inert condition. The volatile components (plasticizers, often oils) vaporize and pyrolysis of the polymer being shortly afterward of about 400C at 600C, the atmosphere is then switched from inert to oxidative, resulting in the combustion of the carbon black additive. Inorganic components remain behind as a residue.

Identification of plastics:
Plastics can be identified by measuring their glass transition temperatures and melting temperatures. The figure shows the melting peaks of different polymers. The peaks clearly differ in size and their position on the temperature axis. The example of PP and POM shows that identification depends both on the melting temperature and on the enthalpy of fusion. If the type of polymer is known, the degree of crystallinity can be determined from the melting peak.

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Environment & Endurance Testing

SPECTRO offer a variety of shock and vibration testing services for testing a wide range of products across many industries. Automotive components are tested to simulate the effect of road condition. Other components may be exposed to vibration during transportation until they reach their final destination. Aerospace/Defense products are also exposed to vibration conditions thus requiring vibration testing to ensure product quality and safety. The Environmental Simulation Department performs a variety of tests designed to simulate the effects of various environmental conditions on components and finished products. Some of the more common environments simulated in our chambers include, salt fog (ASTM B117), ultra-violet (UV, QUV), cyclic corrosion (GM 9540P), and CASS (ASTM B368) testing. We can also perform temperature and humidity cycling in chambers that range from 2 cubic feet. We specialize in evaluating products that are exposed to these environments before, during, and after exposure. This can include operating components in complete power up mode during the exposure cycle and acquiring real time data using our 8 channel data acquisition system.
Capabilities and Testing Process:

Humidity / Temp. Cycle Test:

Environmental temperature testing will expose the unit under test to constant high or low temperatures or cycle temperature during testing. Humidity testing can be added concurrently to a temperature test.
Specification: Bump Test:

mI E C 6 8 - 2 - 3 8

Vibration & Shock Testing: Vibration and shock testing is an important part of product performance and evaluation. Vibration and shock testing may be used to evaluate products and packaging for their predicted and to determine influence of packaging techniques and modes of transportation.
Specification:
mIS-9000 mJSSS-55555

The purpose of the Bump test is to verify the product's ability to withstand repeated force stress during transportation.
Specification: mJISD 1601 Dust & Sand:

DropTest:

The purpose of the drop test is to simulate two situations: one is improper handling of packages during shipping and transportation, and the other is accidental dropping of unpackaged hand held products.
Specification: mASTM D 775-80

Dust creates a harsh environment for chassis, underhood, and exterior mounted devices; and can be a long term problem in interior locations (such as under the dash and seats in automobiles). Exposure to fine dust causes problems with moving parts, forms conductive bridges and acts as an absorbent material for the collection of water vapor. Some electromechanical components may be able to tolerate fine dust, but larger particles affect or totally inhibit mechanical action.
Specification: mI P :

55

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Benefit of Vibration Testing

> Ensure a reliable product. > Reduce the new product development time. > Ensure that the designed product is fit for designated use. > Reduces damages during transit. > Reduces non performance. > Fast launch of new product > Optimization of product design. > Maintain consistency in quality standards. > Ensure products survive the effects of transportation rejection during warranty.
Test Parameter

Frequency Acceleration Displacement No. Of Bumps Pulse Duration Direction Types of Vibrations Sweep mode Sweep Waveform Sweep Rate

5 to 5000 Hz Up to 50g 50mm (Peak Peak) Up to 9999 Up to 15 m Sec X, Y, Z Sine Linear / Log Triangular / Forward / Reverse 1 to 999 Hz/min. For

Applications :Auto Industry Electronic Industry

mTV mMonitor mRefrigerator mAir Conditioner mLaptops mMicrowave mWashing Machine

mVehicle Seats mHeadlights mSteering mGear mBreaks mEngine

Corrosion Testing Services

mSalt Spray Test mSalt Spray (Neutral/Fog), ASTM B117 mHydrogen Induced Cracking (HIC) Test, NACE TM 0284 mSulfide Stress Corrosion Cracking (SSCC), NACE TM 0177

mAmmonia Vapour test mChloride Stress Corrosion Test as per ASTM Gr 35 mNitric Acid, ASTM A262 Practice C (Huey Test) mCorrosion Test as per ASTM A 761

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

RoHS
RoHS (Restriction of Hazardous Substances) EU Directive 2002/95/EC New European RoHS directives now severely restrict the presence of Pb, Hg, Cd, Cr6+, PBB & PBDE (Br) in all electrotechnical products. In the electronics industry this is the driving force behind Lead-free (Pb-Free) manufacturing.

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Failure Analysis

Failure analysis is the process of collecting and analyzing all the data to identify the cause of a failure and how to prevent it from recurring. It is an important discipline in many industries, such as the electronics industry, petrochemicals industry where it is a vital tool used in the development of new methods & products and for the improvement of existing methods & products. The main principle of failure analysis is a forensic inquiry into the method or product upon the failure. Such inquiry can be conducted using scientific analytical methods such as Mechanical, Non-Destructive and Electrical Testing measurements, or through speculative approach when the data is not available but an action has to be taken. Failure Analysis and prevention are important functions to all of the engineering disciplines. The materials engineer often plays an important role in the analysis of failures, whether failure occurs during manufacturing or production processing or component/product fails in service. Features of root cause failure analysis capabilities include: ~Evaluation of field failures ~Evaluation of Life Cycle Test Failure ~Identification of Failure mode ~Contamination Analysis ~Corrosion and Environmental effects ~Photographic Documentation ~Broad Failure Analysis experience Fracture Evaluations ~Identification of product defects Spectros Failure Analysis reports provide a clear picture of the root cause, and include recommendations to avoid future failures - from component design, through material selection and processing. Over the last few years many such types of evaluations have been performed.

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

OTHER SERVICES
Engineering Consulting Inspection

Several senior consultants with many years' experience are available on our panel to help and advise on corrosion or materials selection queries. Our team can also advise on your welding engineering and heat treatment problems.

Supplier Assessment & Process Audit Social Audit In Process Quality Inspection Third Party Inspection Textile Inspection NDT Inspection Radiation Monitoring Metal Scrap Inspection
Material and Product Sourcing

Contract Research and Laboratory Outsourcing We can effectively operate and manage an inhouse laboratory for a corporation while retaining our innovative, professional and superior quality service. We bring to these engagements, our strong process, management expertise as well as results reporting method based on integrity and reliability. We are currently doing the laboratory outsourcing activity of major petrochemical industries.

Spectro covers the entire sourcing process from locating suppliers to transferring design specifications. Spectro will setup the supply chain and logistics control to ensure that shipments meet all export guidelines. Spectro can also source ferrous and non-ferrous metals, casting & forging, engineering goods, nonmetallic materials such as polymer, ceramic, glass, as per buyer specifications. Our strength and expertise in material testing and inspection services helps maintain quality control on all shipments.
www.spectrogroup.com

SPECTRO ANALYTICAL LABS LTD.

Trusted Partner in progress

Always Committed.

Organizations need trusted partners who can help them progress through ever - changing requirements. Spectro not only provides constant support in the growth of its clients but also remained true to its customers and helped them in developing specialized testing facilities in their development programs

Trust is at the core of all ethical business dealings. Spectro will live up to its commitments. One key to building trust is being transparent in the way we communicate with others, and by providing timely and accurate information. Our diverse and experienced professionals work together toward a common goal of excellence in every aspect of our business. We live up to our commitments.

SPECTRO ANALYTICAL LABS LTD.

www.spectrogroup.com

Branch Laboratories
Kanpur (Uttar Pradesh) Jaipur (Rajasthan) Patiala (Punjab) Jammu (J & K) Mumbai (Maharashtra) Bhubaneswar (Orissa) Cochin (Kerala)

Representative Offices
Roorkee Calcutta Bangalore Kandla Hyderabad Paradip Bangalore Pata

International Branch Laboratories

Muscat (Oman) Doha (Qatar)

Associate Companies
Spectro Lab Equipments (P) Ltd.
Manufacturing and Agencies for Laboratory Test Equipments

Spectro Corporate Trainers (P) Ltd

Instrument & Corporate Systems Training

Spectro Weld Institute (P) Ltd.

Training Institute for Welding, NDT, etc

Spectro Inspection. Services (P) Ltd.

Third Inspection Services for Mineral, Coal & Other Material

Spectro Labcare (P) Ltd

Equipment Validation Maintenance & Reconditioning

Spectro Bharti Automation (P) Ltd

Development of Automation system in Auto & other Industries

For any queries please contact Mr. Kuldeep Dhingra

Managing Director care@spectro.in 91-11-40522000

Mr. Kamal K Mehta Vice President

kkm@spectro.in 91-11-40503721, 0-9818377989

Head Office & Central Laboratory

E-41, Okhla Industrial Area, Phase-II New Delhi-110020 (India) Ph:- 91-11-41611000, 40522000 Fax:- 91-11-40503150/51 www.spectro.in
SPECTRO ANALYTICAL LABS LTD. www.spectrogroup.com