LESSON PLAN CBE682 SEPARATION PROCESSES II 1.

0 COURSE INFORMATION COURSE NAME : COURSE CODE : PROGRAM : SEMESTER : CREDIT HOURS : CONTACT HOURS : COURSE STATUS : PRE-REQUISITE : 2.0

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SEPARATION PROCESSES II CBE682 EH222 5 3 4 CORE NIL

SYNOPSIS This course is a continuation of Separation Processes I CBE582. The topics comprise of fluid-solid separation principles, membrane separation processes and mechanicalphysical separation principles. The students will be exposed to various unit operations related to the topics, and the basic principles and calculations will also be introduced. In addition, special topics on bioseparation and crystallization process are included. OBJECTIVES Upon completion of this course, students should be able to: 1. 2. 3. Explain the various types of unit operations based on mass transfer and fluid interactions principles. Perform chemical engineering calculations involving mass transfer in various unit operations. Describe and explain the concepts of fluid-solid separation processes, membrane separation principles, and mechanical separation processes.

3.0

4.0

METHODS OF INSTRUCTION Lectures and tutorials Lectures : 3 hours/week Tutorials : 1 hour/week

LESSON PLAN CBE682 SEPARATION PROCESSES II 5.0

WEEK

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LESSON PLAN
DURATION TOPICS & CONTENTS ACTIVITIES

(in weeks)
Chapter 1: Fluid-Solid Separation Process 1.1 Adsorption 1.1.1 Adsorption Equilibria Single Gases And Vapours Vapour and Gas Mixtures Liquids 1.1.2 Adsorption Operations Stagewise Operations Continuous Contact 1.2 Ion Exchange 1.2.1 Principles of Ion Exchange 1.2.2 Equilibrium Relations in Ion Exchanger 1.3 Leaching 1.3.1 Definition and Application 1.3.2 Principles of Continuous Countercurrent Leaching 1.3.3 Single Stage Calculation 1.3.4 Multistage Counter-current System 1.3.5 Leaching Equipment 1.4 Drying 1.4.1 Batch Drying 1.4.2 Continuous Drying 1.5 Evaporation 1.5.1 Types of evaporation equipment and operation methods 1.5.2 Calculation methods for single effect evaporators 1.5.3 Calculation methods for multiple effect evaporators 1.5.4 Condensers for evaporators 1.5.5 Evaporation of biological materials 1.5.6 Evaporation using vapour recompression Briefing on the course objectives and lesson plan.

Read the text book: Chapter 8, 9, 12

Tutorials

Assignment 1

1-5

Quiz 1

LESSON PLAN CBE682 SEPARATION PROCESSES II

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Read the text book: Chapter 13 Tutorials

6-8

Chapter 2: Membrane Separation Process 2.1 Separation of Gases 2.1.1 Type of membranes and membrane structure 2.1.2 Flow pattern in membrane separators 2.1.3 Product purity & yield 2.1.4 Applications 2.2 Separation of Liquids 2.2.1 Dialysis 2.2.2 Membranes for liquid-liquid extraction 2.2.3 Pervaporation 2.2.4 Reverse osmosis Chapter 3: Mechanical Physical Separation Processes 3.1 Filtration 3.1.1 Types of filtration equipment 3.1.2 Filter media and filter aid 3.1.3 Basic theory of filtration

Test 1 in Week 6: Topic: Chapter 1

Read the text book: Chapter 14 Tutorials Assignment 2 Quiz 2

9-11

3.2 Settling and Sedimentation 3.2.1 Equipment for settling and sedimentation 3.3 Centrifugal Settling 3.3.1 Cyclones & hydrocyclones 3.3.2 Centrifugal Decanters 3.3.3 Principles of Centrifugal sedimentation

12-14

Special Topics Crystallization Bioseparation

Read Reference Book

Presentation on Special Topics Test 2 in Week 12: Topic: Chapter 2 & 3

LESSON PLAN CBE682 SEPARATION PROCESSES II 6.0 ASSESSMENT Tests and Assignments Final Examination 7.0 TEXT BOOK USED

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: 40% : 60%

Geankoplis, C.J. (2003). Transport Processes and Separation Process Principles (4th ed.). New York: Prentice Hall. 8.0 REFERENCES 8.1 8.2 8.3 8.4 Coulson, M. and Richardson, J.F. (1993). Chemical Engineering: Unit Operations, Vol. 2 (4th ed.). Oxford: Pergamon Press. Seader, J.D. and Henley, E.J. (1998). Separation Process Principles. New York: Wiley & Sons. Treybal, E. (1990). Mass Transfer Operations (4th ed.). New York: McGraw Hill. McCabe, I., Smith, J.C. and Harriot, P. (2001). Unit Operations of Chemical Engineering (6th ed.). New York: McGraw Hill.

9.0

ADDITIONAL INFORMATION Attendance is compulsory. Students who fail to comply 80% of the attendance will be barred from taking the final examination. Absence from lecture, tutorial, test or presentation must be supported by relevant document. Late submission of assignment will be penalized with deduction of marks. No plagiarism is allowed in any aspect. Students will be penalized due to non compliance of this matter. APPROVED BY: SIGNATURE: ------------------------------------------------------NAME: Dr Noor Fitrah Abu Bakar POSITION: Ketua Pusat Pengajian, Bioprocess Engineering DATE: 9 Sept 2011

PREPARED BY: SIGNATURE: ----------------------------------------------------NAME: Nurul Asyikin Md Zaki POSITION: Lecturer DATE: 8 Sept 2011

LESSON PLAN CBE682 SEPARATION PROCESSES II

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LESSON PLAN CBE682 SEPARATION PROCESSES II

WEEK 15 CHAPTER/TOPIC Fluid-Solid Separation Process

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COURSE OUTCOME CO1 Ability to explain the various types of unit operations based on mass transfer and fluid interactions principles. CO2 Ability to perform chemical engineering calculations involving mass transfer in various unit operations. CO3 Ability to describe and explain the concepts of fluid-solid separation processes, membrane separation principles, and mechanical separation processes. COURSE LEARNING OUTCOMES Students should be able to: Define and explain the concept of adsorption. Define and calculate the adsorption isotherm. Define and explain the principles of ion exchange. Define and calculate the equilibrium relations of ion exchange. Define and explain the concept and application of leaching process. Perform and evaluate related calculations involved in single stage and multistage leaching processes. Determine and discuss on the leaching equipment. Define and explain the concept and principles of drying process. Determine and explain the various equipment for drying. Calculate the humidity from vapour-pressure data and humidity chart. Define and explain the equilibrium moisture content of DELIVERY METHODS lecture, tutorials ASSESSMENT

Assignment, quiz, test and/or exam.

LESSON PLAN CBE682 SEPARATION PROCESSES II

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dried materials and rate of drying curves. Solve drying process calculation for constant-rate and falling-rate drying period. Discuss the latest trend in drying process, especially for biological materials: Freeze Drying, Unsteady-State Thermal Processing, Sterilization, Pasteurization. Define and explain the operation principles and equipment for evaporation process. Solve problems using calculation methods for single and multiple effect evaporators. Define and explain the principles of evaporation for biological materials and vapour compression. lecture, tutorials Assignment, quiz, test and/or exam.

68

Membrane Separation Process Students should be able to: Define and explain various type of membranes and membrane structures, and flow pattern in membrane separators for separation of gases. Define and calculate the product purity and yield for separation of gases.

LESSON PLAN CBE682 SEPARATION PROCESSES II

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Discuss the application of membrane separation of gases.

Define and explain the concept of dialysis. Define and explain the membrane for liquid-liquid extraction. Define, discuss and explain the pervaporation process and reverse osmosis. 9 11 Mechanical Physical Separation Processes CO1 Ability to explain the various types of unit operations based on mass transfer and fluid interactions principles. CO2 Ability to perform chemical engineering calculations involving mass transfer in various unit operations. CO3 Ability to describe and explain the concepts of fluid-solid separation processes, membrane separation principles, and mechanical separation processes. Students should be able to: Define and explain the fundamental filtration process. Discuss the choice of packed and tray absorption columns. Explain the basic requirements for filtration equipment, filter media and filter aid. Define and explain the concept of settling and sedimentation. Define and explain the principles of centrifugal settling including cyclones & hydrocyclones and centrifugal decanters. Define and explain the concept of centrifugal sedimentation. Perform related calculations for lecture, tutorials Assignment, quiz, test and/or exam.

LESSON PLAN CBE682 SEPARATION PROCESSES II

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filtration, settling and sedimentation processes: determine critical particle diameter, flow rate, terminal settling velocity and mechanical size reduction. Students should be able to: Acquire fundamental concepts of bioseparation and crystallization. Explain the cases for using bioseparation and crystallization. Discuss the application and advantages of bioseparation and crystallization. lecture, tutorials Assignment, presentationz, test and/or exam.

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Special Topics: Bioseparation & Crystallization

LESSON PLAN CBE682 SEPARATION PROCESSES II

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COURSE CODE COURSE NAME CREDIT HOURS

CBE682 SEPARATION PROCESSES II 3

PROGRAM PREPARED BY DATE

EH222 NURUL ASYIKIN MD ZAKI 10 AUG 2011

Program Outcomes Ability to acquire and apply knowledge of mathematics, basic and applied sciences including microbiology and molecular genetics. Ability to undertake problem identification, formulation and solution in engineering. Ability to perform research, design and conduct experiments, as well as to analyse and interpret data. Ability to utilise modern science and engineering tools and systems. Ability to utilise a systems approach to design and evaluate operational performance. Ability to acquire in-depth technical knowledge in chemical and bioprocess engineering principles. Ability to communicate effectively not only with engineers but also with the community at large, particularly with life scientists and chemists 8 Ability to observe the principles of health, safety and environment (HSE) in chemical and bioprocess industries. 9 Ability to function effectively as an individual and in a group with the capacity to be a leader or manager as well as an effective team member. 10 Ability to incorporate entrepreneurship in chemical, food/ pharmaceutical/other biotechnology related business. 11 Recognise the importance of professional ethics in engineering practice.
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LESSON PLAN CBE682 SEPARATION PROCESSES II

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Recognising the need to undertake lifelong learning, and possess/acquire the capacity to do so.

PROGRAMME OUTCOMES COURSE OUTCOMES PO 1 PO 2 PO 3 PO 4 PO 5 PO 6 PO 7 PO 8 PO 9 PO 10 PO 11 PO 12

INSTRUCTIONAL METHODS

ASSESSMENT

CO1 Ability to explain the concept of distillation, gas absorption and liquid-liquid extraction. CO2 Ability to perform chemical engineering calculations involving mass transfer in various unit operations. CO3 Ability to describe and explain the mechanism

Lectures and tutorials

Assignments, quiz, test and/or exam

Lectures and tutorials

Assignments, quiz, test and/or exam

Lectures and tutorials

Assignments, quiz, test and/or exam

LESSON PLAN CBE682 SEPARATION PROCESSES II

of operation for each unit operation and to explain their applications.

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