1.1 Introduction
The advanced instrumentation is a course offered to MS/M.Phill students to get them a better understanding of the laboratories and the equipments used in them. This practice helps students to familiarize themselves with the working knowledge of the instruments so it can help them in future research work. The various laboratories at the NCEG include i. ii. iii. iv. v. vi. vii. viii. Geotechnical laboratory Geochemistry laboratory Geophysics laboratory Thin section cutting and polishing laboratory GIS laboratory Paleoclimatology laboratory Petroleum Geology laboratory Geodesy laboratory
1. 2. 3. 4. 5.
Equipment Sieves, a bottom pan, and a cover. Usually Sieve numbers 4, 10, 20, 40, 60, 140, and 200 are generally used for most standard sieve analysis work. A balance sensitive up to 0.1 g. Mortar and rubber-tipped pestle. Oven. Mechanical sieve shaker
Procedure 1. First of all I collected a representative oven dry soil sample. Samples having largest particles of the size of No. 4 sieve openings (4.75 mm) was about 500 grams. For soils having largest particles of size greater than 4.75 mm, larger weights are needed. 2. Then I broke the soil sample into individual particles using a mortar and a rubber-tipped pestle. The idea was to break up the soil into individual particles, not to break the particles themselves. 3. After that I determined the mass of the sample accurately to 0.1 g (W). 4. I prepared a stack of sieves. A sieve with larger openings is placed above a sieve with smaller openings. The sieve at the bottom should be No. 200. A bottom pan was placed under sieve No. 200. The sieves that are generally used in a stack are Nos. 4, 10,20,40,60, 140, and 200; however, more sieves can be placed in between. 5. Then we I poured the soil prepared in step 2 into the stack of sieves from the top. 6. I placed the cover on the top of the stack of sieves. 7. I ran the stack of sieves through a sieve shaker for about 10 to 15 minutes. 8. Then I stopped the sieve shaker and removed the stack of sieves. 9. I weighed the amount of soil retained on each sieve and the bottom pan. 10. If a considerable amount of soil with silty and clayey fractions is retained on the No. 200 sieve, it has to be washed. Washing is done by taking the No. 200 sieve with the soil retained on it and pouring water through the sieve from a tap in the laboratory. Calculation 1. First calculate the percent of soil retained on the nth sieve (counting from the top)
Equipment 1. Moisture can(s). 2. Oven with temperature control. For drying, the temperature of oven is generally kept between 105C to 110C. 3. Balance. The balance has a readability of 0.01 g for specimens having amass of 200 g or less. Procedure 1. First of all I determined the mass (g) of the empty moisture can plus its cap (W1), and also recorded the number. 2. Then I placed a sample of representative moist soil in the can. I closed the can with its cap to avoid loss of moisture. 3. After wards I determine the combined mass (g) of the closed can and moist soil (W2). 4. I removed the cap from the top of the can and placed it on the bottom of the can. 5. Then I put the can (in step 4) in the oven to dry the soil to a constant weight. In most cases, 24 hours of drying is enough. 6. 7. In the end, I determined the combined mass (g) of the dry soil sample plus the can and its cap (W3). Calculation 1. Calculate the mass of moisture = W2 - W3 2. Calculate the mass of dry soil = W3 W1 3. Calculate the water content