Universidad Nacional de Colombia. Departamento de Qumica.

Laboratorio de Qumica Orgnica I (1000035)

I-2011
Profesor: Eliseo Avella Moreno

UNIVERSIDAD NACIONAL DE COLOMBIA

FACULTAD DE CIENCIAS.
DEPARTAMENTO DE QUMICA
LABORATORIO DE QUMICA ORGNICA I (1000035)
FO RMAT O

GUA

DE

INFO RME

DE

L A PR CT ICA

DE

L ABO RAT O RIO

PURIFICA CIN D E SLID OS

CRISTALIZACIN
ALUMNOS: __________________________________________

CDIGOS: ____________

__________________________________________

____________

__________________________________________

____________

FECHA:

______________________

GRUPO No.

OBJETIVO: Purificar un compuesto orgnico slido mediante recristalizacin en virtud a solubilidad en

funcin de temperatura.
Tomar el punto de fusin del compuesto y usarlo como criterio de pureza.
Sustancia:

_________________________________

Estructura:

Apariencia: ________________________
___________________________________
___________________________________
___________________________________
___________________________________
___________________________________
p. f. _________ C (Dato de la literatura)

SOLUBILIDAD (Datos de la literatura)

Disolvente

Cristalizado obtenido.

Peso inicial: __________ g

t: C

S: g/100 mL

Peso: ___________ g,

ENSAYOS DE SOLUBILIDAD
Disolvente

fro

caliente

t: temperatura, S: solubilidad
Apariencia: _________________________________

Universidad Nacional de Colombia. Departamento de Qumica.

Laboratorio de Qumica Orgnica I (1000035)
I-2011
Profesor: Eliseo Avella Moreno

_____________________________________________________________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
_______________________________________________________ Fue necesario decolorar? _____
Rendimiento: ______ %

p. f. _____________ C (Dato experimental sin corregir)

p. f. _____________ C (Dato experimental corregido)

Haga aqu un diagrama de flujo que muestre el procedimiento que us en la recristalizacin.

ANLISIS DE RESULTADOS Y CONCLUSIONES

Universidad Nacional de Colombia. Departamento de Qumica.

Laboratorio de Qumica Orgnica I (1000035)
I-2011
Profesor: Eliseo Avella Moreno

------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------REFERENCIAS:
-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------

Universidad Nacional de Colombia. Departamento de Qumica.

Laboratorio de Qumica Orgnica I (1000035)
I-2011
Profesor: Eliseo Avella Moreno

UNIVERSIDAD NACIONAL DE COLOMBIA

FACULTAD DE CIENCIAS.
DEPARTAMENTO DE QUMICA
LABORATORIO DE QUMICA ORGNICA I (1000035)
FO RMAT O

GUA

DE

INFO RME

DE

L A PR CT ICA

DE

L ABO RAT O RIO

PURIFICA CIN D E SLID OS

SUBLIMACIN
ALUMNOS: __________________________________________

CDIGOS: ____________

__________________________________________

____________

__________________________________________

____________

FECHA:

______________________

GRUPO No.

OBJETIVO: Purificar un compuesto orgnico slido mediante sublimacin.

Tomar el punto de fusin del compuesto y usarlo como criterio de pureza.
Sustancia:

_________________________________

Estructura:

Peso inicial: __________ g

Aspecto: ____________________________
____________________________________
____________________________________
____________________________________
____________________________________
p. f.
______ C (Datos de la literatura)
p. sublim. ______C
Presin ______ mm Hg

SUSTANCIA PROBLEMA No. ______ Nombre: ______________________ Peso inicial: _______ g

Estructura:

Aspecto: ____________________________
____________________________________
____________________________________
____________________________________
____________________________________
p. f.
______ C (Datos de la literatura)
p. sublim. ______C P.________ mm Hg

SUBLIMADO OBTENIDO: Peso: ____________ g,

Aspecto: ____________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
Rendimiento: ______ %

p. f. _________ C

p. sublim. ____________C (____ mm Hg)

Universidad Nacional de Colombia. Departamento de Qumica.

Laboratorio de Qumica Orgnica I (1000035)
I-2011
Profesor: Eliseo Avella Moreno

Dibuje aqu el (los) montaje (s) que us en la sublimacin

Sustancia problema No. ______

Peso inicial sometido a RECRISTALIZACIN: _______ g

Cristalizado obtenido. Peso: ___________ g, Apariencia: _________________________________

_____________________________________________________________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
_______________________________________________________ Fue necesario decolorar? _____
Rendimiento: ______ %

p. f. _____________ C (Dato experimental corregido)

Sustancia problema No. ______

Peso inicial sometido a SUBLIMACIN: _______ g

Sublimado obtenido: Peso: _____________ g.

Aspecto: __________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
_____________________________________________________________________________________
Rendimiento: ______ %

p. f. _________ C
p. sublim. ____________C (____ mm Hg)
(Datos experimentales corregidos)

Universidad Nacional de Colombia. Departamento de Qumica.

Laboratorio de Qumica Orgnica I (1000035)
I-2011
Profesor: Eliseo Avella Moreno

ANLISIS DE RESULTADOS Y CONCLUSIONES

------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------REFERENCIAS:
-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------