THE DETERMINATION OF PHYSICAL ORGANIC COMPOUND ABSTRACT A experiment has been done to determine the melting and boiling

point of a substance . On experiment to determine the big of boiling point a substance, while the determine of melting point to identity a crystal compound and to get a purity of the compound. A melting point apparatus was used to determine the melting point of which is the sample X show the range of the substance start to it begin to melt until it is all melted is 121-122
0

. A ben!oic acid was suspected as sample X , because the melting point of them was same,the ben!oic acid ha"e the range melting point is 121-122,# 0 the determination technics. $he conclusion is a sample X has a big "anance was suspected as A compound ha"e been %nown, so in experiment should same, but in there is any different it meants the both compound is not same , and if the different only a few degrees & less than 1 substance is same. $he resisitance in experiment is uncomplete of the appliance, so that difficult to get the maximal result. $he suggestion, laboratory wor%er to completed the material and appliance to get maximal result. APPLIANCE AND MATERIAL A. Appliance (elting )oint Apparatus & ()A ' apiler &one the tip of it is close ' *. (aterial +ample X & representing a crystal ' PROCEDURE $he sample X should be in powder,than insert into capiler which the tip of it is close.$han insert it into melting point apparatus and the temperature in celcius is noted, when it begin to melt until it is all melt.
0

. $he difference can cause because of

' it meants the both

INTRODUCTION ondensation ,is- homogeneous mixture ,among.between- two /ihat "itamin of ayau more. 0omogeneous burden that components in condensation cannot dibedalan one with is other. Ability each1e"ery dissol"e /ihat "itamin type to ,be- dissol"e in a,n pelarut different each other. +olubility a,n /ihat "itamin ,is- also influenced by pressure. solid +olubility /ihat "itamin and hydrogen ,donot baya% affect by pressure, and gas solubility will increase e"er greaterly ,his.its- ,of- pressure. $his matter ,of- ditun2u%ana by solid /ihat "itamin solubility will increase gone up it,him- gas solubility and temperature will decrease gone up it,him- temperature. ondensation a,n /ihat "itamin in pelarut ,is- maximum concentration of the /ihat "itamin able to be dissol"e in its its,his-. ompound with incessant tonic bona generally better in pelarut of polar, while /ihat "itamin which ,do- not dissol"e easier polar in pelarut ,do- not polar. /on compound generally will be incessant better if.when its reaction ,of- him of e%soterm. 3unction bunch of polar will predominate the nature of condensation a,n small molecule, but for big molecule ,of- bunch polarity becoming not mean to be compared to part of other molecule which the non polar. 4tanol much more dissol"e in water compared to he%sanol a,n compound reacting with certain perea%si can change the nature of its condensation. /ts it,him- insoluble amine al%yl in water will react with acid solution of yielding salt of al%il dissol"e ammonium in water. Alcohol condensation in water caused by both earning each other hidorgen. 0owe"er by increasing long ,him. it- enchain its its,his-, condensation in water also on the wane. )art of hydrocarbon a,n

alcohol ha"e the character of hidrofob namely ha"e the character of to refuse water molecules. 5ong (%in part of hydrocarbon will more and more to growing low ,is- condensation of alcohol in water. condensation of Alcohol also go up denagn increase of bunchs amount O0 him. +aturated condensation ,is- a,n situation when a,n condensation ha"e contained a,n /ihat "itamin with maximum concentration. maximum oncentration "alue able to reach by a,n such this /ihat "itamin with condensation and gi"en ,by- + lambing& +olubility'. ondensation which enter can dissol"e referred ,as- ,by- dissol"e /ihat "itamin ,of- condensation less saturated. ondensation which cannot again dissol"e dissol"e /ihat "itamin ,is- so that formed ,by- sediment referred ,as,by- condensation pass saturatedly. 6esult of condensation times1rill a,n /ihat "itamin & 7sp' ,is- result of ions concentration times1rill in saturated condensation which ,is- ha"e ran% ,to- counted coefficient according to e8uation of ioni!ation. )rice of 7sp ,is- remain to ,at- temperature which remain to, if.when temperature boosted up ,by- price of 7sp more and more big because condensation more and more big ,at- high temperature. Of price of 7sp and multiplication of ions can %now ,by- what is a,n condensation ha"e is saturated, not yet saturated or pass saturated pursuant to following 9 a. /f.:hen price of 7sp bigger than result of its ions concentration times1rill hence latutan not yet is saturated & ,do- not happened sediment ' b. /f.:hen price of 7sp smaller than result of its ions concentration times1rill hence condensation pass saturatedly is & happened ,of- precipitation' c. /f.:hen price of 7sp ,is- e8ual to result of its ion concentration times1rill hence condensation earn saturatedly & will tuang' APPLIANCE AND MATERIALS. A. Appliance - appliance.

$ube reaction of.,;rip pipette.,*ea%er glass. *. (aterialss. :ater 6efine.,4ther,<aoh =>,<ahco? =>,0 5 =>, ondensed 02+O#,0?)o# @=>,)aper 5itmus, ompound X. . :or%ing procedure $his attempt ,is- ,done.conducted- to %now faction from a compound X. 3irst of all compound of X enhanced ,by- water, percei"e what is compound of x the dissol"e insoluble or. /f compound of X the dissol"e in water hence ta%ing again compound of X new and later1then enhance with ether, dissol"e otherwise hence compound of X that ,is- including faction of +2 but if dissol"e hence compound of X that ,is- tested with litmus paper, red litmus paper designate faction of +A, blue litmus ,of- faction of +*, unad2usted litmus ,of- faction of +1. /f compound of X the insoluble if enhanced ,by- water hence ta%ing compound of X new and enhance <aoh =>, if dissol"e hence enhancing with <ahco? =>., dissol"e result designate faction of A1 and do not be dissol"e designate faction of A2. :here at the &time' of addition of <aO0=> if the compound do not be dissol"e hence ta%ing compound of X new and 0 5 =>, dissol"e result designate faction of *, if.when do not be dissol"e, compound of X which is 2ust is enhanced ,by- ,of- 02+o# @A>. 6esult do not be dissol"e designate faction of / while dissol"e result hence compound of X which is 2ust is enhanced ,by- ,of- 0?)o# B= >, if dissol"e designate faction of <1 and do not be dissol"e designate faction of <2.

RESULT OF PERCEPTION AND SOLUTION. X1 & white serbu%'

/f X1 sample enhanced with water will be dissol"e. :hile X1 sample added ,by- insoluble ether and there are white sediment. 0ence condensation class of sample X1 ,is- Clucose representing faction condensation class of +2. X2 & white serbu%' /f X1 sample enhanced with insoluble water. :hile X2 sample if.when enhanced ,by- <aoh => will be dissol"e, ,is- later1then enhanced ,by- <ahco? = is> dissol"e. 0ence condensation class of sample X2 ,is- Acid of ben!oate representing condensation class of A1 X? & transparent condensation' /f X? sample enhanced with water will be dissol"e. :hile X? sample if.when enhanced with ether will be dissol"e, ,is- later1then tested with litmus paper ,there- no change. 0ence condensation class of sample X? ,is- $ertiary ,of- *utanol representing faction condensation class of +1 X# & brown condensation ,of- %ehitaman' /f X# sample enhanced with insoluble water, :hile X# sample enhanced with <aoh => nor is dissol"e, ,is- later1then enhanced ,by- 0 5 = is> dissol"e. 0ence condensation class of sample X# ,is- aniline representing faction condensation class *. SOLUTION. +ampel X1 which in form of white chromatic serbu% ,is- Clucose & A012OA'. ;issol"e Clucose in water representing pelarut of polar but insoluble Clucose in ether and form white sediment. *ecome glucose condensation class ,is- +2. :hich included in condensation class of +2 among others ,is- salt of acid of organic & 6 O2<A, 6 O?<A', Amine of 0idro%lorida & 6<0? 5', +our ,of- Amino. +ampel X2 which in form of white chromatic serbu% ,is- acid of ben!oate & A0= ooh'. +our ,ofinsoluble ben!oate in water. $his matter as according to literature that Acid of *en!oat ha"e small condensation in water and to heighten its condensation hence turned into sour form ,of- its salt form. /n conse8uence when acid of ben!oate enhanced ,by- <aoh => causing dissol"e ben!oate

asan and form <atrium *en!oat & its salt'. acid of *en!oate dissol"e also in <ahco? =>. *ecoming class of,is acid solution of ben!oate ,is- A1. +ampel X? which in the form of transparent condensation ,is- tert-butanol. ;issol"e $ert-butanol in water. $his matter as according to literature that dissol"e tert-butanol in water because less its it,him- bunch of tert-butanol. ;issol"e $ert-butanol also in ether and tested with litmus paper got ,by- result of that unad2usted litmus paper. $his matter pro"e that tert-butanol ,is- acid wea%. $his matter as according to literature that acidity of alcohol progressi"ely ,is- downhill the than se%under primer,alcohol alcohol and of alcohol feeblest tertiary ,of- its acidity. ondensation class of tert-butanol ,is- +1 +ampel X# which in the form of tan condensation ,of- %ehitaman ,isinsoluble aniline.Anilin in water. dissol"e nor Aniline in <aoh => *ut aniline earn dissol"e in 0 5 =>. *ecoming Aniline condensation class ,is- *. CONCLUSION. ;issol"e glucose in water but insoluble in ether. its ondensation class ,is- +2.Acid of *en!ote dissol"e tidal in water but dissol"e in <aoh => and <ahco? =>. its ondensation class ,is- A1. ;issol"e $ert-butanol in ether and water. $ert-*utanol ,is- acid wea%. its ondensation class ,is+1./nsoluble Aniline in and water of <aoh =>. *ut dissol"e in 0 5 =>. its ondensation class ,is*.