Materials & Streams Report

April 1, 2014

for lab 2
1. OVERALL PROCESS DATA
Annual Operating Time
Recipe Batch Time
Recipe Cycle Time
Number of Batches per Year
MP = Undefined

7,886.72h
43.06h
33.81h
233.00

- Page 1 -

2.1 STARTING MATERIAL REQUIREMENTS (per Section)

Section

Starting Material Active Product

Amount
Needed
(kg
Sin/kg
MP)

Main Section

(none)

Unknown Unknown Unknown Unknown

(none)

Molar
Yield
(%)

Mass
Yield
(%)

Gross
Mass
Yield
(%)

Sin = Section Starting Material, Aout = Section Active Product

2.2 BULK MATERIALS (Entire Process)

Material
Biomass
Media
Water
Air
Acetone
TOTAL

kg/yr

kg/batch

11,650
104,850
2,330,000
2,258,877
133,550
4,838,926

50.000
450.000
10,000.000
9,694.750
573.174
20,767.924

kg/yr

kg/batch

11,650
104,850
2,330,000
2,258,877
133,550
4,838,926

50.000
450.000
10,000.000
9,694.750
573.174
20,767.924

kg/kg MP

2.3 BULK MATERIALS (per Section)

SECTIONS IN: Main Branch
Main Section
Material
Biomass
Media
Water
Air
Acetone
TOTAL

kg/kg MP

- Page 2 -

2.4 BULK MATERIALS (per Material)

Biomass
Procedure
Main Section (Main Branch)
P-1
TOTAL

Media
Procedure
Main Section (Main Branch)
P-1
TOTAL

Water
Procedure
Main Section (Main Branch)
P-1
TOTAL

Air
Procedure
Main Section (Main Branch)
P-1
TOTAL

Acetone
Procedure
Main Section (Main Branch)
P-2
TOTAL

% Total

kg/yr

kg/batch

100.00
100.00

11,650
11,650

50.000
50.000

% Total

kg/yr

kg/batch

100.00
100.00

104,850
104,850

450.000
450.000

% Total

kg/yr

kg/batch

100.00
100.00

2,330,000
2,330,000

10,000.000
10,000.000

% Total

kg/yr

kg/batch

100.00
100.00

2,258,877
2,258,877

9,694.750
9,694.750

% Total

kg/yr

kg/batch

100.00
100.00

133,550
133,550

573.174
573.174

kg/kg MP

kg/kg MP

kg/kg MP

kg/kg MP

kg/kg MP

2.5 BULK MATERIALS: SECTION TOTALS (kg/batch)

Raw Material
Biomass
Media
Water
Air
Acetone
TOTAL

Main Section
50.000
450.000
10,000.000
9,694.750
573.174
20,767.924

- Page 3 -

2.6 BULK MATERIALS: SECTION TOTALS (kg/yr)

Raw Material
Biomass
Media
Water
Air
Acetone
TOTAL

Main Section
11,650
104,850
2,330,000
2,258,877
133,550
4,838,926

- Page 4 -

3. STREAM DETAILS
Stream Name
Source
Destination
Stream Properties

Feed
INPUT
P-1

water
INPUT
P-1

Air
INPUT
P-1

Vent
P-1
OUTPUT

Activity (U/ml)
Temperature (C)
Pressure (bar)
Density (g/L)
Total Enthalpy (kW-h)
Specific Enthalpy (kcal/kg)
Heat Capacity (kcal/kg-C)

0.00
25.00
1.01
999.97
0.00
0.00
1.00

0.00
25.00
1.01
994.70
0.00
0.00
1.00

0.00
25.00
1.01
1.18
0.00
0.00
0.24

0.00
37.00
1.01
1.14
43.14
3.82
0.24

50.000
0.000
450.000
0.000
0.000
0.000
500.000
500.015

0.000
0.000
0.000
0.000
0.000
10,000.000
10,000.000
10,053.239

0.000
0.000
0.000
7,437.016
2,257.734
0.000
9,694.750
8,221,312.821

0.000
314.902
0.000
7,446.672
1,945.764
0.000
9,707.338
8,494,958.001

Broth
P-1
P-2

Acetone
INPUT
P-2

Biomass
P-2
OUTPUT

Filltrate
P-2
P-3

0.00
5.00
0.87
1,002.76
- 243.64
- 19.96
1.00

0.00
25.00
1.01
786.58
0.00
0.00
0.52

0.00
7.95
0.98
975.65
- 4.10
- 14.98
0.88

0.00
5.36
0.87
990.66
- 241.38
- 19.16
0.98

0.000
176.000
45.000
9.000
10,270.000
10,500.000
10,471.071

573.174
0.000
0.000
0.000
0.000
573.174
728.693

59.212
176.000
0.000
0.000
0.000
235.212
241.083

513.962
0.000
45.000
9.000
10,270.000
10,837.962
10,940.118

Component Flowrates (kg/batch)

Biomass
Carb. Dioxide
Media
Nitrogen
Oxygen
Water
TOTAL (kg/batch)
TOTAL (L/batch)

Stream Name
Source
Destination
Stream Properties
Activity (U/ml)
Temperature (C)
Pressure (bar)
Density (g/L)
Total Enthalpy (kW-h)
Specific Enthalpy (kcal/kg)
Heat Capacity (kcal/kg-C)

Component Flowrates (kg/batch)

Acetone
Biomass
Impurity
MAB
Water
TOTAL (kg/batch)
TOTAL (L/batch)

- Page 5 -

Stream Name
Source
Destination
Stream Properties
Activity (U/ml)
Temperature (C)
Pressure (bar)
Density (g/L)
Total Enthalpy (kW-h)
Specific Enthalpy (kcal/kg)
Heat Capacity (kcal/kg-C)

Distillate
P-3
OUTPUT

Bottom
P-3
OUTPUT

0.00
45.00
1.01
974.01
245.53
19.51
0.98

0.00
76.89
0.87
975.79
0.54
51.80
1.00

508.919
45.007
0.000
10,271.557
10,825.483
11,114.373

0.000
0.000
9.000
0.000
9.000
9.223

Component Flowrates (kg/batch)

Acetone
Impurity
MAB
Water
TOTAL (kg/batch)
TOTAL (L/batch)

- Page 6 -

4. OVERALL COMPONENT BALANCE (kg/batch)

COMPONENT
Acetone
Biomass
Carb. Dioxide
Impurity
MAB
Media
Nitrogen
Oxygen
Water
TOTAL

INITIAL

INPUT

OUTPUT

FINAL

IN-OUT

0.000
0.000
0.000
0.000
0.000
0.000
30.571
9.281
0.000
39.852

573.174
50.000
0.000
0.000
0.000
450.000
7,437.016
2,257.734
10,000.000
20,767.924

568.132
176.000
314.902
45.007
9.000
0.000
7,446.672
1,945.764
10,271.557
20,777.033

5.042
0.000
0.098
0.000
0.000
0.000
20.915
6.251
0.000
32.307

0.000
- 126.000
- 315.000
- 45.007
- 9.000
450.000
0.000
315.000
- 271.557
1.564

- Page 7 -

5. EQUIPMENT CONTENTS
FR-101
Procedure

Operation

P-1
P-1
P-1
P-1
P-1
P-1
P-1

START
CHARGE-1 (Charge)
CHARGE-2 (Charge)
HEAT-1 (Batch Heating)
FERMENT-1 (Batch Kinetic Fermentation)
COOL-1 (Batch Cooling)
TRANSFER-OUT-1 (Transfer Out)

BCF-101
Procedure

Operation

P-2
P-2
P-2
P-2

START
AFTER AUTO-INIT
FILTER-1 (Cloth Filtration)
CAKE-WASH-1 (Cake Wash)
END

V-101
Procedure

Operation

P-3
P-3
P-3

START
AFTER AUTO-INIT
DISTILL-1 (Batch Distillation)
END

Time (in h)

Volume (in L)

0.000
1.167
2.926
3.409
27.409
28.559
33.809

0.000
500.015
10,553.253
10,599.654
10,592.424
10,471.071
0.000

Time (in h)

Volume (in L)

33.809
33.809
36.809
37.059
37.059

0.000
10,471.088
242.898
241.083
0.000

Time (in h)

Volume (in L)

37.059
37.059
43.059
43.059

0.000
10,940.148
9.223
0.000

- Page 8 -