Vertex 70vs Manual

User Manual
1007253
VERTEX 70v
1
st
edition 2007, publication date November 2007
2007 BRUKER OPTIK GmbH, Rudolf Plank Str. 27, D-76275 Ettlingen, www.brukeroptics.com
All rights reserved. No part of this manual may be reproduced or transmitted in any form or by any
means including printing, photocopying, microfilm, electronic systems etc. without our prior written per-
mission. Brand names, registered trademarks etc. used in this manual, even if not explicitly marked as
such, are not to be considered unprotected by trademarks law. They are the property of their respective
owner.
The following publication has been worked out with utmost care. However, Bruker Optik GmbH does
not accept any liability for the correctness of the information. Bruker Optik GmbH reserves the right to
make changes to the products described in this manual without notice.
This manual is the original documentation for the VERTEX 70v spectrometer.
VERTEX 70v User Manual iii
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TABLE OF CONTENTS
1 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
General Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Warning Labels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Safety Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
2 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
3 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
General Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Delivery Scope. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Site Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Connecting VERTEX 70v to the Power Supply . . . . . . . . . . . . . . . . . . . 11
Connecting VERTEX 70v to a PC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Connecting VERTEX 70v to the Vacuum Pump . . . . . . . . . . . . . . . . . . 13
Connecting VERTEX 70v to the Purge Gas Line. . . . . . . . . . . . . . . . . . 15
4 Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
General Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
External Components. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Internal Components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Optical Path . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
5 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Switching VERTEX 70v On and Off . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
QuickLock. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
Automatic Accessory Recognition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Performing a Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Evacuating and Venting the Spectrometer. . . . . . . . . . . . . . . . . . . . . . . 36
Optimizing the Vacuum Operation of the Spectrometer. . . . . . . . . . . . . 40
Purging the Spectrometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
Exchanging the Beamsplitter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Exchanging the Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Cooling an MCT Detector. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
6 Maintenance and Repair . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
Evacuating the MCT Detector Dewar. . . . . . . . . . . . . . . . . . . . . . . . . . . 58
Replacing the Laser Module. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
Replacing a defective IR Source . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
Replacing the Fuses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
iv VERTEX 70v User Manual
Tabl e of Cont ent s
Replacing the Sample Compartment Windows . . . . . . . . . . . . . . . . . . . 69
Cleaning the Instrument . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
Maintaining the Vacuum Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
7 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Diagnostic Means. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
Problem - Possible Cause - Solution . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
A Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101
B Consumable Spares . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103
C Default Parameter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105
D Dimensional Drawings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 109
E Connecting VERTEX 70v to PC . . . . . . . . . . . . . . . . . . . . . . 115
General Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 115
Possible Connection Topologies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 116
Selecting Network Addresses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 119
Assigning Network Addresses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120
Checking the Connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 123
F Electronics and Power Supply . . . . . . . . . . . . . . . . . . . . . . . 125
Electronics Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 125
Power Supply Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 128
G Firmware Update . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 131
Updating the Firmware. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 132
Restoring a previous Firmware Version . . . . . . . . . . . . . . . . . . . . . . . . 134
Backing up the current Firmware Version . . . . . . . . . . . . . . . . . . . . . . 135
H Sample Preparation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 137
Sample Preparation Techniques . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139
I Service Addresses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 145
VERTEX 70v User Manual 1
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SAFETY 1
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GENERAL I NFORMATI ON
Read the following safety instructions carefully before putting the spectrometer into
operation. Keep this manual in a suitable place for future reference.
Always observe the instructions described in this manual to ensure user safety and to
avoid property damage. Improper use or failure to follow these safety instructions can
result in serious injuries and/or property damage. Any non-observance of the precau-
tions will infringe the intended use (i.e. performing spectroscopic measurements) of the
spectrometer. In this case Bruker Optik GmbH will not assume any liability.
It is the operators duty to plan and implement all necessary safety measures and to
supervise their observance. Moreover, the operator must ensure that the spectrometer
is in proper functioning condition. A safe and faultless operation can only be guaranteed
if the spectrometer is transported, stored, installed, operated and maintained properly
according to the procedures described in this manual.
Never remove or deactivate any supporting safety systems during spectrometer opera-
tion. Ensure that objects and/or material not required for the measurement is out of the
spectrometer operating area.
The spectrometer complies with the IEC/EN 61010-1 safety regulations.
Pr ot ect i ve Ear t hi ng
To avoid personal injuries and/or property damage caused by electrical power, the
spectrometer is equipped with a safety plug. Connect this plug only to a socket outlet
with earthing contact. Make sure that the socket complies with IEC (International Elec-
trotechnical Commission).
Qual i f i ed Per sonnel
Primary installation and all maintenance and repair works not described in this manual
should only be performed by Bruker service personnel. Only authorized operating per-
sonnel that have been briefed about the spectrometer operation and all relevant safety
aspects should operate and maintain (i.e. only maintenance works that are described in
this manual) the spectrometer.
All repairs, adjustments and alignments on any spectrometer component must be per-
formed in accordance with the safety regulations and standards applied in the country in
which the instrument is installed.
2 VERTEX 70v User Manual
1
SAFETY
Warning Labels
Cor r ect Usage
The spectrometer and its components should only be used according to the instructions
described in the manual or advised by a Bruker engineer. In case of accessories or
components made by other manufacturers and used in connection with the spectrome-
ter, Bruker does not assume any liability for safe operation and proper functioning.
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WARNI NG LABELS
When operating the spectrometer you have to observe a number of safety instructions
which are highlighted by various warning labels. This section describes the warning
labels and explains their meaning. All warning labels on the spectrometer must always
be kept legible. Immediately replace a worn or damaged label.
The following warning labels indicate different dangerous situations which may be
caused by improper use of the spectrometer.
Caut i on - Gener al Hazar d
This warning symbol indicates general hazard. Observe the safety
instructions and follow the precautions described to avoid personal injury
and/or property damage.
Caut i on - El ect r i cal Shock
This warning symbol indicates electrical hazard. The symbol is located near
live parts or on enclosures behind which are live parts that represent an
accidental contact hazard. Never touch these parts. Before removing the
corresponding compartment covers and beginning any maintenance or
repair work, first turn off the mains switch and unplug the main power cable.
Ensure that all live parts do not come into contact with a conductive sub-
stance or liquid. Non-observance of these safety instructions can cause
severe personal injury and/or property damage.
Caut i on - Hot Sur f ace
This warning symbol indicates components and surfaces which can
become very hot during spectrometer operation. Do not touch these com-
ponents and surfaces. Risk of skin burn! Be careful when operating near
hot components and/or surfaces.
Caut i on - Laser Radi at i on
This warning symbol indicates the existence of laser radiation. Never look
directly into the laser beam or use any kind of optical instruments to do so.
Otherwise permanent eye damage can be the result.
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SAFETY
Warning Labels
Besides the dangers described above, there can also be hazardous situations caused
by the sample material. Depending on the type of hazardous substances you work with,
you have to observe specific substance-relevant safety instructions. Put on the corre-
sponding warning label on the appropriate spectrometer position. The label must be
legible and permanently discernible. The following list contains some examples of haz-
ardous substances:
Caut i on - Fr ost bi t e
This warning symbol indicates cryogenic materials (e.g. liquid nitrogen)
required to operate the spectrometer (e.g. cooling detector). Skin contact
with these liquids or cooled components causes severe frostbite. Always
handle the liquids with utmost care. Observe the safety instructions for
handling of cryogenic liquids.
Caut i on - Har mf ul Mat er i al
This warning symbol indicates the existence of harmful or irritant material
(e.g. the window material BaF
2
). Observe the safety instructions on the
packaging, and the safety data sheets attached. Non-observance may
cause personal injury.
Caut i on - Toxi c Mat er i al
This warning symbol indicates the existence of toxic material (e.g. the win-
dow material KRS-5). Observe the safety instructions on the packaging,
and the safety data sheets attached. Non-observance may cause severe
personal injury or even death.
Caut i on - I nf ect i ous Mat er i al
This warning symbol indicates the possible presence of bio-hazardous and
infectious material. When working with this kind of material always, observe
the prevailing laboratory safety regulations and take all necessary precau-
tions and disinfection measures (e.g. wearing protective clothing, masks,
gloves etc.). Failure to do so may cause severe personal injury or even
death. (For information on how to use, dilute and efficiently apply disinfec-
tants, refer to the Laboratory Biosafety Manual: 1993 by WHO - World
Health Organization.)
Caut i on - Radi oact i ve Mat er i al
This warning symbol indicates the possible presence of radioactivity. When
working with radioactive material, always observe the safety regulations
and take all necessary protective measures (e.g. wearing protective cloth-
ing, masks gloves etc.). Failure to do so may cause severe personal injury
or even death.
1
SAFETY
Safety Instructions
Wast e Di sposal
Dispose all waste produced (chemicals, infectious and radioactively contaminated sub-
stances etc.) according to the prevailing laboratory regulations. Detergents and clean-
ing agents must be disposed according to the local waste regulations.
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SAFETY I NSTRUCTI ONS
The following chapters describe all relevant safety aspects of the spectrometer opera-
tion. Depending on the degree of hazard the safety instructions are classified as fol-
lows:
Danger indicates that death, severe personal injury or substantial property damage
WILL result if proper precautions are not taken.
Warning indicates that death, severe personal injury or substantial property damage
CAN result if proper precautions are not taken.
Caution indicates that minor personal injury or property damage CAN result if proper
precautions are not taken.
Note draws your attention to particularly important information on the product,
e.g. product operation or to a special part of the manual.
The safety instructions Danger, Warning and Caution stand out by the corresponding
warning labels.
Caut i on - Cor r osi ve Subst ance
This warning symbol indicates the possible presence of corrosive sub-
stances. When working with corrosive substances, always observe the lab-
oratory safety regulations and take protective measures (e.g. wearing
protective masks and gloves). Failure to do so may cause severe personal
injury or even death.
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GENERAL 2
VERTEX 70v is an evacuable, fully digital FT-IR spectrometer for demanding R&D
applications. The spectrometer is equipped with a number of features such as AAR
(Automatic Accessory Recognition) ACR (Automatic Component Recognition) and Per-
formanceGuard that facilitate performing spectroscopic measurements and ensure reli-
able measurement results. The function AAR identifies automatically the accessory
installed in the sample compartment, performs several tests and loads automatically the
corresponding experiment file including the pre-defined measurement parameters. The
feature ACR recognizes automatically the currently installed optical components like
source, detector and beamsplitter. These components are electronically coded so that
the spectrometer firmware can recognize them. This information is passed on to the
application software OPUS. The purpose of ACR is to enable the user to select the right
optics parameters in OPUS. In addition, the spectrometer components are monitored
permanently to ensure that they operate within the specification range. This feature is
called Performance Guard. Its purpose is to facilitate fault diagnostics and maintenance.
The data acquisition is based on a free running delta-sigma, dual-channel A/D converter
with 24-bit dynamic range. The A/D converter is integrated into the detector preamplifier
electronics. The DigiTect technology ensures a signal transmission free from interfer-
ences and guarantees the highest signal-to-noise ratio.
VERTEX 70v can be controlled by any data system (PC workstation, notebook etc.) on
which the operating system Microsoft Windows and the spectroscopic software OPUS is
installed. The Ethernet connection provides the possibility to control the spectrometer
also via your intranet or the internet.
The standard spectrometer configuration is designed for data acquisition in the mid IR
region. Optionally, VERTEX 70v can be equipped with additional optical components to
cover the whole spectral range - starting in the far infrared or THz region at 10cm
-1
up to
the ultraviolet region at 28,000cm
-1
. Due to the pre-aligned optical components and the
permanently aligned RockSolid interferometer, the spectral range can be changed eas-
ily. If you work with the advanced spectrometer configuration (i.e. two detector positions
and two source positions are available inside the spectrometer) you can select them
using the software. Removable vacuum-tight covers provide access to the detector and
beamsplitter if you want to exchange these components.
VERTEX 70v has five IR-beam outlet ports (on the right, front and left side) and two IR-
beam inlet ports (on the right and rear side) allowing the connection of a multitude of
optional accessories and/or components like:
TGA-coupling
PMA 50 (Polarization Modulation Accessory for VCD and PM-IRRAS)
HYPERION 1000/2000 IR microscope and HYPERION 3000 imaging
microscope with FPA detector (Focal Plane Array detector system)
IMAC module (Imaging Accessory with FPA detector)
2
GENERAL
External sample compartment (XSA)
HTS-XT module (High Throughput Screening Extension)
Fiber optic coupling module with MIR or NIR fiber probes for solid and
liquid samples
FT Raman module (e.g. RAM II)
FIR bolometer
External, water-cooled sources
There is also the possibility to connect several accessories simultaneously (e.g. a
water-cooled Hg-arc source at the rear side, the RAM II FT-Raman module at the right
side, a fibre optics coupling at the right front side, the HYPERION IR microscope at the
left side and a bolometer detector at the front side).
Diagnostic routines help to maintain optimum instrument status and performance. The
internal validation unit (IUV) is located inside the spectrometer. It contains standards
(test samples) used for the validation and testing of the instrument.
Note: Depending on the spectrometer configuration you have ordered,
your spectrometer may not include all options that are described in
this manual.
The evacuable VERTEX 70v spectrometer allows measurements under vacuum condi-
tions, i.e. unwanted atmospheric interferents (e.g. water vapor or carbon dioxide) are
eliminated nearly completely from the spectrometer interior. Evacuating the spectrome-
ter is more efficient than purging it or using desiccant cartridges. The result of an opti-
mal measurement under vacuum conditions is an IR spectrum in which no H
2
O or CO
2
absorptions mask weak spectral features of the sample.
The spectrometer design enables a separate evacuation of the spectrometer compart-
ments, i.e. either the complete spectrometer interior (sample compartment plus the opti-
cal bench) or only the optical bench can be evacuated. Vacuum shutters (so called
flaps), which can be equipped with optical or IR windows, allow a ventilation of only the
sample compartment in order to preserve the vacuum in the rest of the optics compart-
ment during a sample exchange or an accessory installation. Evacuating and venting
the sample compartment and/or optics are computer-controlled. Moreover, the spec-
trometer is equipped with two pressure sensors providing for the display of the current
pressure inside the spectrometer optics and/or sample compartment.
VERTEX 70v is supplied with an efficient vacuum pump that can evacuate the spec-
trometer optics within a few minutes. The oil-free vacuum pump prevents the spectrom-
eter optics from being contaminated by hydrocarbons.
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I NSTALLATI ON 3
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Unpacking and initial installation of VERTEX 70v is done by Bruker service engineers.
The operating company has to provide an installation site that meets the site require-
ments described in this chapter. (See also the technical document Installation Require-
ments for VERTEX 70v provided by Bruker Optik GmbH in advance.)
This chapter contains a list of the standard as well as the optional spectrometer compo-
nents and describes the procedures for connecting the spectrometer:
to the power supply,
to a PC,
to the vacuum pump and
to the purge gas supply line, if necessary.
For detailed information about how to install the computer, refer to the PC manual.
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DELI VERY SCOPE
The basic instrument of VERTEX 70v allows upgrading with additional components and/
or accessories. The delivery scope depends on the spectrometer configuration you
have ordered.
St andar d Component s
The basic instrument includes the following items:
VERTEX 70v spectrometer (including the user manual)
Power cord
PC compatible data system (if desired, the PC can also be provided by the
customer)
Data cable (Cat5, crossover cable for 10Base-T Ethernet standard)
Purge gas hose (OD: 6mm, length: approx. 5m)
Tool kit (slot-head screw driver, cross-head screwdriver and hex keys of several
sizes, sample preparation tools, 3x spare fuses, IR sensor card, metallic cap
shown in fig. 28)
Software package OPUS/IR (including the OPUS Reference Manual)
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I NSTALLATI ON
Delivery Scope
For installing the vacuum pump, the following items are included:
Vacuum pump (including the user manual)
Noise reduction hood
Vibration absorber
2x flexible metal hoses
4x hose clamps
4x sealing rings
Opt i onal Component s
Depending on the ordered spectrometer configuration, the delivery scope can also
include following optional components:
Optional spectrometer components (e.g. optional detectors) and/or accessories
Optional OPUS software packages (e.g OPUS/STEP) including the corresponding
manuals
I nspect i ng t he Packagi ng
After the receipt of the spectrometer, inspect the packaging for damages. If there are
any signs of damage, contact your local shipping representative before opening the
shipping box.
Warning: Do not put a spectrometer into operation that shows signs of
damage. Failure to do so may result in severe personal injuries
and/or property damage.
Tr anspor t at i on
Due to its weight (about 105kg), VERTEX 70v has to be carried by at least four persons
using the supplied transport handles. For transportation purposes, attach these handles
properly to the right and left spectrometer side as shown in figure 1 using 12 screws
(M5 x 16). Tighten the screws using a hex kex (size 4mm). After having transported the
instrument to the desired place, you can remove the transport handles again. Alterna-
tively, you can transport the instrument with a fork lifter.
Warning: Due to the high instrument weight, improper transportation can
lead to personal injuries and/or spectrometer damage.
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I NSTALLATI ON
Site Requirements
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SI TE REQUI REMENTS
Space Requi r ement s
The spectrometer dimensions are 85cm (w) x 71cm (d) x 32cm (h). (For exact spec-
trometer dimensions refer to appendix D.) At the rear side, the spectrometer requires a
clearance of at least 25cm (10). The spectrometer should be placed on a stable and
horizontal base. Note that the basic instrument has a weight of about 105kg.
When preparing the installation location for the spectrometer, take into consideration
that the mains power supply connection is easily accessible at any time. The mains
power supply can be interrupted, for example, either by disconnecting the safety plug or
switching off the mains switch on the spectrometer rear side or disconnecting the pri-
mary power receptacle.
Envi r onment al Requi r ement s
To ensure optimum spectrometer performance and long-term reliability the following
environmental conditions are essential:
Temperature Range: 18 - 35 C (64 - 95 F)
In case the vacuum pump is operated with installed noise reduction hood ensure the
ambient temperature does not exceed 32C (90F).
Humidity (non-condensing): 80% (relative humidity)
Temperature variations can impair the results of long-term measurements. Therefore,
the temperature variations should be less than 1C per hour and should not exceed 2C
per day for this type of measurement.
Figure 1: Installing the Transport Handles
Transport
Handles

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I NSTALLATI ON
Site Requirements
Vi br at i on
Ideally, the spectrometer should not be installed near vibration sources (e.g. ventilation
hoods, air conditioners, motors, elevator etc.) or in rooms with intense floor vibration.
Power Suppl y
The spectrometer power supply unit automatically adapts to the most common power
sources.
Valid voltage range: 100 V AC to 240 V AC
Valid frequency range: 50 to 60 Hz
VERTEX 70v is an instrument of the protection class I.
Caution: To avoid personal injury and spectrometer damage, connect the
spectrometer only to a socket outlet with earthing contact.
To provide for good data quality and a long spectrometer service life, ensure that the fol-
lowing site requirements are met:
Do not install the spectrometer near sources of potential inductive electrical
interference (e.g. pumps, switching motors, microwave ovens etc.), sources of
high energy pulses, and sources that might cause magnetic or radio frequency
interference.
Do not place devices such as large electric motors, heaters, welding equipment,
radio transmitting equipment, units emitting pulsed NMRs, or high powered lasers
in close vicinity to the spectrometer. These devices can interfere with the
spectrometer and cause spectrometer malfunction. Ensure that these types of
devices are not connected to the same electrical circuit as the spectrometer.
If a reliable mains power supply is a problem at your site (caused by brownouts,
power surges, frequent thunderstorms, for example), take precautions to ensure
an uninterruptible power supply.
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I NSTALLATI ON
Connecting VERTEX 70v to the Power Supply
CONNECTI NG VERTEX 70V TO THE POWER
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
SUPPLY
Power Cor d
Before connecting the power cord, make sure that the spectrometer is switched off, i.e.
the mains switch (B in figure 2) is in the O position. Connect the supplied power cord
to the primary power receptacle (C in figure 2) as well as to the mains socket outlet.
The power cord length should not exceed 3m. Depending on the local conditions, the
original power cord may need to be exchanged for a power cord that complies with the
standards of the country in question. The power cord must have approbation of at least
your local authority, UL for US, CSA for Canada or VDE for Europe. The spectrometer
power supply unit automatically adapts to the local voltage and frequency range. (See
section Site Requirements.)
Component
A Ethernet port
B Mains switch
C
Primary power receptacle (for connecting the
power cord)
Figure 2: Spectrometer Rear Side - Connections for Power Supply and PC
A
B
C
3
I NSTALLATI ON
Connecting VERTEX 70v to a PC
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
CONNECTI NG VERTEX 70V TO A PC
Dat a Cabl e
The data cable included in the spectrometer delivery scope is a CAT5 crossover cable
(labelled Cross-over) with two RJ-45 plugs. This cable is only used for the direct con-
nection of VERTEX 70v to a computer. If you intend to connect the spectrometer to a
network, a different type of cable (i.e. non-crossover, CAT 5 cable for the 10Base-T Eth-
ernet standard) is required. (See appendix E.) The data cable length should not exceed
100m (without repeater).
Connect one end of the data cable to the Ethernet port (ETH) (A figure 2) and the other
end of the data cable to the RJ-45 socket of the computer network interface card. (For
detailed information refer to the computer manual.)
After having set up the data cable connection, turn on the spectrometer using the mains
switch. After a few seconds, the spectrometer beeps once and starts a self test. After
the initialization has been completed successfully, the STATUS LED (figure 10) turns
from red to green. Now switch on the computer and the monitor. (For information on
how to install the computer and how to set up signal and power cable connections for
the computer, monitor etc. refer to the computer manual.)
Comput er Set up
VERTEX 70v and the delivered PC are already configured for the stand-alone opera-
tion. The spectrometer IP address is factory-set to 10.10.0.1. In case you have not pur-
chased the computer together with the VERTEX 70v spectrometer, you have to assign
an appropriate IP address to the computer to which you want to connect the spectrome-
ter. For detailed information about how to assign an IP-address to the computer refer to
appendix E.
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I NSTALLATI ON
Connecting VERTEX 70v to the Vacuum Pump
CONNECTI NG VERTEX 70V TO THE VACUUM
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
PUMP
The attachment flange (NW25 flange) for connecting the vacuum pump is at the spec-
trometer rear side. Figure 3 shows the valve block with removed cover.
The vent openings are covered by a plug made from sintered-powder metal which is air-
permeable (i.e. the spectrometer can be vented with the plugs installed on the vent
opening). (See figure 8.) The plug functions like a filter preventing particles from enter-
ing the spectrometer together with the influent air.
Note: For detailed information about the vacuum pump refer to the user
manual provided by the vacuum pump manufacturer.
Attachment Flange for the Vacuum Pump
Opening for venting
the optical bench
(Note: When purging the
spectrometer this port is
used as purge gas inlet for
the optical bench.
Valve for evacuating
the optical bench
Valve for evacuating
the sample compart-
ment
Figure 3: Valve Block (Spectrometer rear Side)
Opening for venting
the sample compart-
ment
(Note: When purging the
spectrometer this port is
used as purge gas inlet for
the sample compartment.
Valve for venting the
sample compartment
Valve for venting the
optical bench
3
I NSTALLATI ON
Connecting VERTEX 70v to the Vacuum Pump
I nst al l at i on Pr ocedur e
Remove the valve block cover shown in figure 4 by loosening the two Allen screws
using a hex key (size 3mm) and pulling off the cover.
Install the supplied sealing ring at the attachment flange. See figure 5.
Press the supplied flexible metal hose against the attachment flange (figure 6a)
and attach the hose to the flange using the supplied hose clamp (figure 6b).
Secure the hose clamp by fastening the wing screw.
Allen Screws
Valve Block Cover
Figure 4: Removing the Valve Block Cover
Figure 5: Connecting VERTEX 70v to Vacuum Pump - Step 1
Attachment Flange Sealing Ring
Flexible
Metal Hose
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I NSTALLATI ON
Connecting VERTEX 70v to the Purge Gas Line
During operation, the vacuum pump generates vibrations. In order to prevent these
vibrations from being transferred to the spectrometer via the flexible metal hose, the
supplied vibration absorber has to be installed between the vacuum pump and the
spectrometer. The procedure for connecting the flexible metal hose to the vacuum
pump and to the vibration absorber is identical to the procedure described above.
Note: Make sure that the vibrating metal hoses do not come into contact
with the table on which the spectrometer is placed.
During the operation, the vacuum pump produces an increased noise level. In order to
reduce the noise level install the supplied noise reduction hood over the vacuum pump.
For information about the noise reduction hood installation refer to instructions provided
by the pump manufacturer.
CONNECTI NG VERTEX 70V TO THE PURGE
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
GAS LI NE
As an alternative to the vacuum operation, VERTEX 70v can be purged with either dry
air or dry nitrogen gas. The spectrometer has two purge gas inlets; one for purging the
sample compartment and the other for purging the optical bench. The purge gas inlets
are at the spectrometer rear side. See figure 7.
Figure 6: Connecting VERTEX 70v to Vacuum Pump -Step 2
Hose Clamp
Wing Screw
3
I NSTALLATI ON
For detailed information about the required purge gas supply conditions refer to chapter
Operation, section Purging the Spectrometer.
I nst al l at i on Pr ocedur e
Note: In case the spectrometer is evacuated, first vent it before starting
the installation procedure. Otherwise, a warning message regarding
unstable pressure conditions inside the spectrometer will appear.
To connect the spectrometer to the purge gas supply you need a stiff hose with an
outer diameter of 6mm. Remove the plug (made from sintered-powder metal) from
the purge gas inlet by pressing the lock ring inwards (figure 8) and pulling out the
plug. Connect one end of the hose to your supply line for dry air or dry nitrogen
gas and insert the other end of the hose into the purge gas inlet for either the
sample compartment or optical bench.
If you want to purge both the sample compartment and the optical bench, you
need a T-shape connecting hose with two hose ends leading to the spectrometer.
After having connected the main end of the hose to the supply line, insert one of
the other two hose ends into the purge gas inlet for the sample compartment and
the other hose end into the purge gas inlet for the optical bench.
Figure 7: Purge Gas Inlets
Purge gas inlet for
optical bench.
(Note: In case of vacuum
operation - vent opening for
venting the optical bench.)
Purge gas inlet for
sample compartment.
(Note: In case of vacuum
operation - vent opening for
venting the sample com-
partment.)
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I NSTALLATI ON
Figure 8: Purge Gas Inlet with removed Plug
Plug
Lock Ring
3
I NSTALLATI ON
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
OVERVI EW 4
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
This chapter describes all relevant external and internal spectrometer components.
Note: The local indications right and left assume that the operator stands in
front of the spectrometer. The indications forward and backward refer
to the spectrometer front side and rear side, respectively.
Compartment
A Power Supply Connector
B Status Indicator Board
C Electronics Compartment
D Interferometer Compartment
E Detector Compartment
F Sample Compartment
G Laser
H Vacuum Pump Connection Port
I Beam Direction Control Compartment
A
B
C
D
E
F
G
H
I
Figure 9: General Overview
4
OVERVI EW
External Components
The detector compartment, the interferometer compartment and the beam direction
control compartment are not separated from each other but form one compartment. All
spectrometer compartments are accessible by removing the corresponding cover.
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
EXTERNAL COMPONENTS
St at us I ndi cat or Boar d
The status indicator board is in the left rear corner of the spectrometer, more precisely,
on the electronic compartment cover. (See figure 10.) The color of the LEDs gives a
general indication of the operating status of the corresponding spectrometer compo-
nent. Moreover, the color of the Vacuum LED indicates the current pressure situation
inside the spectrometer compartments (i.e it shows whether a certain compartment is
being evacuated/vented just now or is already evacuated/vented). In case one of these
LEDs lights up red indicating a spectrometer problem refer to chapter Troubleshooting.
This chapter shows possible causes of a problem and provides solutions.

VACUUM
The color of VACUUM LED depends on the current pressure situation inside the individ-
ual spectrometer compartments. The following table explains the meaning of the differ-
ent LED colors:
LED is off. Sample compartment and optical bench are vented.
LED flashes green. Sample compartment and optical bench are being either evacuated or vented.
LED lights up green. Sample compartment and optical bench are evacuated. The ultimate vacuum is
achieved.
LED flashes yellow. Sample compartment is being either evacuated or vented. (In case the sample
compartment is already vented, it flashes yellow also when the optical bench is
being vented.)
LED lights up yellow. Sample compartment is vented.
LED lights up red. When the spectrometer is being evacuated, but a certain threshold pressure value
is not reached within a certain period of time (i.e. the ultimate vacuum is not
achieved). A red VACUUM LED indicates a problem. See chapter Troubleshooting,
section Problem - Possible Cause - Solution, subsection Spectrometer problem
indicated by spectrometer status indicator.
Figure 10: Status Indicator Board
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OVERVI EW
External Components
LASER
The LASER LED lights green when the laser is in operation and the laser signal is OK.
The LASER LED lights up red if the laser power is too weak, the laser beam is blocked
or if the laser module is defective or out of alignment. (See chapter Troubleshooting,
section Problem - Possible Cause - Solution, subsection Spectrometer problem indi-
cated by spectrometer status indicator.) This control lamp also lights up red during the
spectrometer initialization phase. After the initialization is completed successfully, this
LED turns to green.
STATUS
A green STATUS LED indicates that the spectrometer is in proper operating condition.
The STATUS LED lights up red in case of a spectrometer malfunction or during the ini-
tialization phase. After the initialization is completed successfully, this LED turns to
green. (See chapter Troubleshooting, section Problem - Possible Cause - Solution, sub-
section Spectrometer problem indicated by spectrometer status indicator.)
Sampl e Compar t ment
Normally, you gain access to the sample compartment from the spectrometer top side
by removing the blue cover using the handle. See figure 11a. In exceptional cases, if
your measurement accessory requires access from the spectrometer front side (e.g. for
exchanging the sample), you can remove the blue front cover by loosening the six Allen
screws using a hex key size 3mm. See figure 11b.
Note: When performing measurements under vacuum condition do not
forget to reinstall the sample compartment front cover.
The sample compartment dimensions are 25.5cm (w) x 27cm (d) x 16cm (h). For more
information about the sample compartment interior refer to chapter Operation, section
QuickLock.
Figure 11: a) Sample Compartment Top Cover b) Sample Compartment Front Cover
Allen Screws Sample Compartment Cover Handle
4
OVERVI EW
External Components
I R Beam Por t s
VERTEX 70v has seven IR beam ports (five outlet ports and two inlet ports) allowing
the adaptation of external accessories and/or components (e.g. microscope, TG-IR cou-
pling or external light source). The IR beam ports are at the front and rear side as well
as at the left and right hand side of the spectrometer. For the exact dimensions of the IR
beam port positions refer to appendix D.

IR Beam Ports
A Outlet port for focussed beam (e.g. for connecting a bolometer)
B
Outlet port for parallel beam (e.g. for connecting a fiber optic coupling
module)
C Inlet port for connecting a light emission source (e.g. Hg source)
D Outlet port for parallel beam
E
Outlet port for parallel beam (e.g. for connecting a microscope, PMA50,
external sample compartment XSA)
F
Inlet port for connecting a light emission source (e.g. FT-Raman mod-
ule, water-cooled, high-power MIR source)
G
Outlet port for parallel beam (e.g. for connecting a microscope) or
focussed beam (e.g. for connecting a bolometer)
Figure 12: c) Right Side d) Left Side
Figure 12: a) Front Side b) Rear Side
A B
D
E F
G
C
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.
OVERVI EW
External Components
The IR beam ports are vacuum-tight sealed by circular covers. To remove a cover
loosen the six Allen screws using a hex key size 3mm. See figure 13.
Note: External accessories are installed by the Bruker service technicians.
Spect r omet er Rear Si de
Allen Screws
Figure 13: Removing an IR Beam Port Cover
Figure 14: Spectrometer Rear View
External Beam
Port
Vent Opening/
Purge Gas Inlet
Electronics
Panel
Mains Switch
CAN BUS
Port
Primary Power
Receptacle
Attachment Flange
for Vacuum Pump
4
OVERVI EW
External Components
EXTERNAL BEAM PORT
The inlet port is used for connecting a light source (e.g. Hg-Source) or an emission
sample.
VENT OPENI NG / PURGE GAS I NLET
Depending on whether you evacuate or purge the spectrometer, these two ports serve
different purposes. In case of evacuating the spectrometer these ports serve as vent
openings, whereas, when purging the spectrometer the purge gas supply lines are con-
nected to these ports. (For detailed information about installing the purge gas connec-
tion refer to chapter Installation.)
ELECTRONI CS PANEL
On the electronics panel are a number of ports (e.g. Ethernet port), the reset button as
well as LEDs indicating, for example, the status of the interferometer. For a detailed
description of the electronics panel refer to appendix F.
MAI NS SWI TCH AND PRI MARY POWER RECEPTACLE
The mains switch is used to turn the spectrometer on and off. The power supply socket
is used to connect the power cord to the spectrometer.
CAN BUS PORT
The CAN bus port is primarily used to connect external automated units to the spec-
trometer. For more information refer to appendix F.
ATTACHMENT FLANGE FOR VACUUM PUMP
The vacuum pump can be connected to this attachment flange (NW25) using the sup-
plied sealing ring, flexible metal hose and hose clamp. (For detailed information about
how to connect the vacuum pump to the spectrometer refer to chapter Installation.)
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.
OVERVI EW
Internal Components
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
I NTERNAL COMPONENTS
The following figure identifies only the most important internal components and their
location inside the spectrometer.

Component
A RockSolid interferometer (permanently aligned)
B DigiTect Detectors
C
Sample holder for transmission measurements (exchangeable
for other optional accessories with QuickLock baseplate)
D HeNe laser
E Two beamsplitters storage positions (optional)
F Beamsplitter (operation position)
G Optional NIR source (operating position)
H MIR source (operating position)
I QuickLock mechanism for accessories (including connectors)
Figure 15: Internal Spectrometer Components
B
D
E
A
F
G
H
I
C
4
OVERVI EW
Internal Components
Li ght Sour ce
The basic instrument is equipped with a MIR source (H in figure 15). The MIR light
source is a globar (i.e. an U-shaped silicon carbide piece) that emits mid-infrared light.
Apart from the standard air-cooled MIR source, the following optional sources are avail-
able:
VIS/NIR source (tungsten halogen lamp), installed in the spectrometer (G in
figure 15), air-cooled
FIR source (mercury lamp), connected externally to the spectrometer, water-
cooled
UV/VIS/NIR source (tungsten lamp), connected externally to the spectrometer,
water-cooled
UV source (deuterium lamp), connected externally to the spectrometer, air-cooled
High power MIR source (globar), connected externally to the spectrometer, water-
cooled
All external sources can be connected to one of the two inlet ports (C in figure 12b or F
in figure 12c). For the FIR source (mercury lamp), the preferred connection port is the
inlet port at the spectrometer rear side, C in figure 12b.
Det ect or
The basic spectrometer configuration is equipped with a DigiTect DLaTGS detector with
integrated preamplifier. This detector package contains an analog-to-digital-converter
that converts the analog signal from the detector directly into a digital signal. This digital
signal is transmitted to the data processing electronics unit of the spectrometer. The
standard detector is a pyroelectric DLaTGS detector which covers a spectral range from
12,000 to 250cm
-1
, operates at room temperature and has a sensitivity of D*>4x10
8
cm
Hz
1/2
W
-1
.
Apart from the standard detector, there is a large number of optional detectors. All
detectors are mounted on dovetail slides which allow an easy exchange. The following
optional detectors are available:
Detector
Spectral
Range (cm
-1
)
Sensitivity
Operating
Temperature
Mid-Infrared
DLaTGS with KBr
window
12,000 - 250
D*>4x10
8
cm Hz
1/2
W
-1
Temperature-sta-
bilized
DLaTGS with CsI
window
12,000 - 160
D*>4x10
8
cm Hz
1/2
W
-1
Room temperature
MCT narrow band,
with BaF
2
window
CAUTION - HARMFUL!
12,000 - 850
D*:>4x10
10
cm Hz
1/2
W
-1
Liquid N
2
cooled
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OVERVI EW
Internal Components
Warning: Some detectors are equipped with windows of which the material
is harmful or (very) toxic. During normal spectrometer operation,
these materials do not pose a health risk. However, should these
windows break caused by mechanical impact, be extremely
careful. Avoid generating dust. These materials are harmful or
toxic if swallowed or inhaled. Also avoid skin and eye contact.
MCT mid band, with
ZnSe window
CAUTION - TOXIC!
12,000 - 600
D*:>2x10
10
cm Hz
1/2
W
-1
Liquid N
2
cooled
MCT broad band,
with KRS-5 window
CAUTION - TOXIC!
12,000 - 420
D*:>5x10
9
cm Hz
1/2
W
-1
Liquid N
2
cooled
Photovoltaic MCT,
with BaF
2
window
CAUTION - HARMFUL!
12,000 - 850
D*:>2x10
10
cm Hz
1/2
W
-1
Liquid N
2
cooled
MCT/InSb Sandwich,
with ZnSe window
CAUTION - TOXIC!
10,000 - 600
D*:>2x10
10
cm Hz
1/2
W
-1
(MCT)
D*:>1.5x10
11
cm Hz
1/2
W
-1
(InSb)
Liquid N
2
cooled
Near-Infrared
InSb 10,000 - 1,850
D*:>1.5x10
11
cm Hz
1/2
W
-1
Liquid N
2
cooled
InSb with cold filter 10,000 - 3,100
D*>5x10
11
cm Hz
1/2
W
-1
Liquid N
2
cooled
Ge Detector (Raman) 11,750 - 5,900
NEP<10
-15
W Hz
-1/2
Liquid N
2
cooled
InGaAs Diode 12,800 - 5,800
NEP:<2x10
-14
W Hz
-1/2
Room temperature
InGaAs Diode 12,800 - 4,000
NEP:<2x10
-13
W Hz
-1/2
Peltier cooled
Ge Diode 15,000 - 5,300
NEP:<5x10
-12
W Hz
-1/2
Room temperature
Far Infrared
DLaTGS with PE win-
dow
700 - 10
D*>4x10
8
cm Hz
1/2
W
-1
Room temperature
Silicon Bolometer 600 - 10
NEP<10
-13
W Hz
-1/2
Liquid He cooled
Visible & UV
Silicon Diode 25,000 - 9,000
NEP:<10
-14
W Hz
-1/2
Room temperature
GaP Diode 33,000-18,000
No NEP available
Room temperature
Detector
Spectral
Range (cm
-1
)
Sensitivity
Operating
Temperature
4
OVERVI EW
Internal Components
Beamspl i t t er
The standard KBr beamsplitter covers a spectral range from 8000 to 350cm
-1
. Apart
from the standard beamsplitter, there are also optional beamsplitters. They allow data
acquisition in wavelength ranges other than MIR (standard) when used in conjunction
with the appropriate light source and detector. Note that the combination of light source,
detector, beamsplitter and sample compartment window material defines the IR mea-
surement range. The following optional beamsplitters are available:
Caution: The beamsplitter material CaF
2
is harmful if inhaled or swallowed.
Avoid also skin and eye contact.
Laser
VERTEX 70v is equipped with a HeNe laser (D in fig. 15) It emits red light with a wave-
length of 633nm. The rated power output is 1mW. The laser controls the position of the
moving interferometer mirror (also called scanner) and is used to determine the data
sampling positions. The monochromatic beam produced by the HeNe laser is modu-
lated by the interferometer to generate a sinusoidal signal. For information about how to
replace a defective laser module, refer to chapter Maintenance and Repair.
I nt er f er omet er
VERTEX 70v is equipped with a high stability interferometer with ROCKSOLID perma-
nent alignment. The ROCKSOLID interferometer incorporates dual retroreflecting cube
corner mirrors in pendulum arrangement. The high throughput design ensures the high-
est possible signal-to-noise ratio.
Beamsplitter Spectral Range (cm
-1
)
Color Coding of the
Beamsplitter Handle
Mid-Infrared
KBr (standard) 7,500 - 370 red
KBr (broad band) 10,000 - 400 red
Csl 5,000 - 210 red
Near-Infrared
CaF
2
CAUTION - HARMFUL!
15,500 - 1,200 black
Visible & UV
Quartz VIS/UV 25,000 - 9,000 white
Far-Infrared
Multilayer (far IR) 680 - 30 nickel-plated
Mylar 25m 120 - 20 nickel-plated
Mylar 50m 50 - 10 nickel-plated
Solid state 600 - 30 *
* limited to a spectral resolution of 0.5cm
-1
nickel-plated
Alignment Tool
Glass For alignment purposes only! nickel-plated
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OVERVI EW
Optical Path
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
OPTI CAL PATH
The beam path shown in figure 16 ist the beam path of the standard spectrometer con-
figuration.
D1 Standard detector
D2 Optional detector
BMS Beamsplitter
APT Aperture wheel
OPF Optical filter wheel
IN1 ... IN2 Beam inlet port 1 ... 2
OUT1 ... OUT5 Beam outlet port 1 ... 5
Figure 16: VERTEX 70v - Optical Path
4
OVERVI EW
Optical Path
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
OPERATI ON 5
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
After the spectrometer has been installed and connected to the power supply, the PC,
and the vacuum pump, the spectrometer is ready for operation. VERTEX 70v is com-
pletely computer-controlled, i.e. operating the spectrometer (e.g. selecting the corre-
sponding optical components) performing a measurement and evacuating/venting the
spectrometer is done using the spectroscopic software OPUS.
This chapter describes mainly the spectrometer related aspects of the operation. For
detailed information about the OPUS software refer to the OPUS Reference Manual.
The OPUS manual Getting Started explains step by step how to perform the first mea-
surement after the spectrometer has been set up.
The standard spectrometer configuration is designed for measurements in the mid infra-
red region. Optionally, the spectral region can be expanded by substituting the installed
MIR components (source, detector, beamsplitter and sample compartment windows, if
available) for the corresponding optical components that allow measurements in the far
or near infrared as well as in the visible or ultraviolet region. (For information about the
replacement procedure of these optional components refer to the corresponding sec-
tions in this chapter and in chapter Maintenance and Repair.)
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
SWI TCHI NG VERTEX 70V ON AND OFF
Gener al I nf or mat i on
The spectrometer is turned on and off using the mains switch at the spectrometer rear
side (figure 14). After having switched on the spectrometer, it starts booting. The boot
process takes about 30 seconds. As soon as this process is completed successfully, the
STATUS LED (figure 10) turns from red to green.
After having switched on the spectrometer wait at least ten minutes before starting the
first measurement. This allows for the electronics and the light source to stabilize ther-
mally.
Caution: After having switched the spectrometer off, wait at least 30 sec-
onds before switching the spectrometer on again. This measure
avoids peaks in the initial current which could lead to fuse blowing
and/or damaging the power switch.
5
OPERATI ON
Switching VERTEX 70v On and Off
Swi t ch- on Pr ocedur e
To put the spectrometer into operation again, proceed as follows:
1 Switch on the PC.
2 Switch on the spectrometer. The spectrometer begins to start up.
Note: After the spectrometer initialization is completed successfully, the
STATUS LED turns to green. Now the spectrometer is ready for
operation again.
3 Connect the the vacuum pump to the power supply.
Note: For information about how to operate the vacuum pump refer to the
supplied user manual of the vacuum pump manufacturer.
Swi t ch- of f Pr ocedur e
Ideally, the spectrometer should uninterruptedly be kept under vacuum, even during
times of nonuse. If, however, the circumstances require a switching-off of the vacuum
pump and/ or the spectrometer the following procedure is recommended:
1 Evacuate the optical bench.
2 As soon as the final pressure is reached, switch off the spectrometer.
Note: The evacuation will take about 5 minutes. In the electroless
spectrometer state, all valves (for venting as well as for evacuating
the spectrometer) are closed.
3 Disconnect the vacuum pump from the power supply.
In this state, the spectrometer interior is isolated from the laboratory environment and
the optical spectrometer components are protected against air humidity and they are no
longer current-carrying.
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OPERATI ON
QuickLock
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QUI CKLOCK
The sample compartment is equipped with a locking mechanism, called QuickLock, for
positioning and locking different measurement accessories. Therefore, you can use
only accessories that are mounted on a QuickLock baseplate. The QuickLock mecha-
nism enables a solid lock even for heavy and bulky accessories and allows a quick,
easy and reproducible positioning of the measurement accessories in the sample com-
partment.
When you insert and lock the accessory, all connections (purge gas connection and
electrical connection) are established and the accessory is automatically recognized by
the application software OPUS. This software feature is called AAR - Automatic Acces-
sory Recognition. In addition, the recommended measurement parameters are selected
automatically, provided that you have already stored the parameters for the accessory
in question. (See OPUS Reference Manual.)
The QuickLock mechanism also allows purging the sample compartment with dry air or
nitrogen gas. The purge gas enters the sample compartment via the gas diffusor
(figure 18).
Purge gas
connection port
QuickLock
locking device
Electronic
connectors
Figure 17: a) Sample Compartment - QuickLock Holder b) QuickLock Release Button
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QuickLock

To i nser t an accessor y wi t h Qui ckLock basepl at e:
1 Hold the accessory with the QuickLock

baseplate front edge slightly tilted
upwards. Then, gently push the electrical connectors of the baseplate
against their counterpart of the QuickLock holder. Put the baseplate down.
Ensure that the baseplate is horizontally aligned to the QuickLock holder.
2 Gently press the front edge of the baseplate downward until it snaps into
place. To facilitate the insertion of the accessory, press the release button
outside the sample compartment. (See figure 17b.)
To r emove an accessor y wi t h Qui ckLock basepl at e:
1 Press the QuickLock release button outside the sample compartment. (See
figure 17b.)
2 While pressing the QuickLock release button, lift the front edge of the
QuickLock baseplate until the baseplate snaps free.
3 Carefully lift the accessory off the QuickLock holder to avoid damages to the
electrical connectors at the baseplate rear side.
Figure 18: Accessory with QuickLock Baseplate
Purge gas
diffusor
Electronic connectors
for AAR and CAN bus
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Automatic Accessory Recognition
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AUTOMATI C ACCESSORY RECOGNI TI ON
As soon as an accessory is locked into the QuickLock holder, the OPUS/AAR software
(Automatic Accessory Recognition) starts and recognizes automatically the accessory
in question, provided you have activated the AAR function in the OPUS software. (For
information about how to activate the AAR function refer to the OPUS reference man-
ual, OPUS manual part Automatic Accessory Recognition).
The OPUS/AAR software identifies the accessory, performs several tests, adapts the
measurement parameters and opens the Measurement dialog window to start a mea-
surement. If the automatic accessory recognition has been completed successfully,
OPUS displays a corresponding message.
Each time you start OPUS, the AAR program checks whether an accessory is installed
into the sample compartment. If AAR detects an accessory, the corresponding dialog
box is displayed. It also appears when the accessory is substituted by another one.
Note: When installing a new accessory for the first time, it is not yet
registered so that the OPUS/AAR software can not recognize it. In
this case, you first have to register the new accessory in question.
(See OPUS Reference Manual.)
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PERFORMI NG A MEASUREMENT
The measurement procedure described in the following refers exclusively to measure-
ments under vacuum conditions. In case you want to perform a measurement not under
vacuum ignore the steps regarding evacuating and venting the spectrometer.
Specify the measurement parameters in the OPUS programme. To do this, select
in the OPUS Measure menu the Advanced Measurement function and select or
enter the corresponding parameter values. (The standard parameter values are
listed in appendix C.)
Evacuate the spectrometer as described in the following section. (Wait until the
ultimate vacuum is achieved.)
Acquire a background spectrum without the sample in the sample compartment by
clicking in OPUS on the Background Single Channel button. (See figure 19.)
Vent the sample compartment as described in the following section.
Put the sample in the sample compartment. (For information about how to install a
QuickLock accessory into the sample compartment refer to the section QuickLock
in this chapter. For information about sample preparation refer to appendix G.)
Evacuate the sample compartment again. (Wait until the ultimate vacuum is
achieved.)
Acquire a sample spectrum by clicking in OPUS on the Sample Single Channel
button (figure 19) and calculate the ratio (transmittance spectrum).
Note: Use the same parameter values for the background and the sample
measurement. Ensure that both measurements are performed under
identical ambient conditions.
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OPERATI ON
Evacuating and Venting the Spectrometer
For detailed information about OPUS functions for data acquisition, manipulation and
evaluation refer to the OPUS Reference Manual.
EVACUATI NG AND VENTI NG THE
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SPECTROMETER
VERTEX 70v is primarily designed for vacuum operation, but it can be purged as well.
To activate the vacuum mode, select in the OPUS Measure menu the Optic Setup and
Service function. Click on the Devices/Options tab and make sure that the Purge Mode
check box is not ticked off. See figure 20.
Figure 19: OPUS Measurement Dialog Window
Figure 20: Activating the Vacuum Mode
With this checkbox
being deactivated,
the vacuum mode is
activated.
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The flaps and the venting and evacuating valves are controlled automatically via the
OPUS software. So evacuating and venting the sample compartment and/or optical
bench is done using the OPUS software. The corresponding buttons are at the Basic
page of the Measurement dialog window. See figure 21.
Let us assume the following initial situation: both the sample compartment and the opti-
cal bench are vented. In this case, it is not possible to evacuate only the sample com-
partment. (The evacuation of only the sample compartment is not possible as in this
case the pressure difference between the sample compartment and the optical bench
would damage the flaps, i.e. the flaps are not designed for such an operation condition.)
So, clicking on either button effects the evacuation of both compartments. The evacua-
tion process is indicated by the message Sample / Optics Evacuating that appears in
the fields below the buttons. The progress of the evacuation is shown by the perma-
nently updated pressure readings in the lower fields. See figure 22.
Note: After you have clicked on a button, the labeling of this button
changes immediately showing the action that can be performed next
(i.e. Evacuate... turns to Vent... and versa vice).
Current state in the
individual compart-
ments including the
current pressure
reading
Command that can be
executed next by
clicking on this button.
Figure 21: Optical bench and sample compartment are vented.
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OPERATI ON
As soon as the evacuation process is completed, the message Sample / Optics Evacu-
ated appears in the lower fields. See figure 23.
Note: If the sample compartment is evacuated you can not open it.
Note: To prevent OPUS from starting a measurement while the
spectrometer is being evacuated or vented proceed as follows: Click
in the Measurement dialog window on the Optic tab and select in the
Optical bench ready drop-down list the option Pressure stable. See
figure 24.
Figure 22: Optical bench and sample compartment are being evacuated.
Figure 23: Both compartments are evacuated.
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When both compartments are evacuated you can vent the sample compartment sepa-
rately (for example, if you want to open the sample compartment in order to exchange
the sample) by clicking on the Vent Sample button.
Note: When both compartments are evacuated, venting only the optical
bench is not possible as the pressure ratio inside the spectrometer
would damage the flaps. For safety reasons, the instrument does not
perform this operation. In this case, clicking on the Vent Optics
button effects the ventilation of the sample compartment as well. This
precaution prevents the instrument from being operated wrongly.
Figure 24: Defining the Measurement Start Precondition
Figure 25: Sample compartment is vented and optical bench is evacuated.
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Optimizing the Vacuum Operation of the Spectrometer
OPTI MI ZI NG THE VACUUM OPERATI ON OF
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THE SPECTROMETER
To get optimum measurement results under vacuum conditions, there are some aspects
that need to be taken into consideration:
The thermal conditions in an evacuated optics bench and in a purged optics bench
are completely different, i.e., under vacuum there is no thermal conduction at all
due to the lack of the purge gas. This aspect has consequences on the
reproducibility of the measurement results.
Water molecules are very polar. Due to this property, they tend to stick at the inner
wall of the optics compartment. For this reason, it takes time to get the water
vapor pumped off completely.
The purpose of the following advice is to help you in achieving optimum measurement
results.
Repr oduci bi l i t y of t he Resul t s
After having evacuated the spectrometer, it is highly recommended that you allow the
spectrometer to stabilize long enough. An optimally stabilized spectrometer is able to
achieve an extreme high 100%-line stability in the sub-%-level with the standard optical
components designed for MIR measurements. (Note: A precondition is that the room
temperature does not vary by more than 1C per hour and 2C per day. Typically, this
condition can be fulfilled in an air-conditioned environment.)
Recommendat i ons:
For demanding experiments, a stabilization period of at least 4 hours is
recommended. After this period, the maximum instrument stability is achieved.
For non demanding experiments, a stabilization time of 0.5 hour is sufficient.
During a long-term experiment, it is recommended to repeat the background
measurement in regular interval, at least every hour.
Ideally, the spectrometer should be kept under vacuum overnight.
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Resi dual Wat er Vapor
Longer evacuation times will further reduce the residual water vapor concentration
inside the spectrometer:
Note: Besides the necessity of a water vapor concentration being as low as
possible, there is another aspect regarding water vapor you have to
take into consideration: The water vapor line intensity in the sample
spectrum does not depend on the absolute residual water vapor
concentration in the spectrometer but on the different water vapor
concentrations during the background and the sample measurement.
Therefore, it is of crucial importance that the residual water vapor
concentration is (nearly) identical during both the background
measurement and the sample measurement.
Evacuat i on Ti me
As mentioned above, water molecules are very polar. Due to this property, they tend to
stick at the inner wall of the optics compartment, even under vacuum. For this reason, a
long evacuation time is recommended. Ideally, the evacuation of the spectrometer
should not be interrupted overnight. This action will further reduce the residual water
vapor content.
Evacuat i on Pr ocedur e
Before acquiring a background spectrum, simulate a sample exchange in the same way
as you will do it later for the real sample measurement:
1 Vent the sample compartment.
2 Afterwards, evacuate the sample compartment for about 5 to 10 minutes.
(An evacuation time longer than 10 minutes is not necessary because after
that period, the final pressure of < 0.2hPa (< 0.2mbar) will be achieved.)
Note: As soon as the pressure falls below < 1hPa, the message Sample
Evacuated, including the current pressure value, is displayed in the
Measure dialog window (figure 26). The achievement of the final
pressure is also indicated by the VACUUM LED at the spectrometer
top side, i.e. this LED lights green.
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Important Note:The evacuation times before the background measurement
and before the sample measurement have to be more or less
identical. To ensure reproducible evacuation times, specify
in OPUS a Delay before Measurement. See the figure 27.
3 Acquire a single channel background spectrum.
4 Afterwards, vent the sample compartment and place the sample in the
sample compartment.
5 Evacuate sample compartment for about 5 to 10 minutes.
6 Acquire a single channel sample spectrum.
Figure 26: OPUS dialog window Measurement - page Basic
Current state inside the
individual compartments,
including the current pres-
sure reading
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Purging the Spectrometer
Note: Take into account that the intensity of the water vapor band in the
sample spectrum does not depend on the absolute residual water
vapor concentration but results from a water vapor concentration
difference during the background and the sample measurement.
With the above described operation conditions and a spectral resolution of 4cm
-1
, typi-
cally a residual water vapor band intensity in the range of significantly less than 0.1%T
can be achieved.
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PURGI NG THE SPECTROMETER
Purging the spectrometer is not necessarily required, especially when you perform
measurements under vacuum conditions. However, if the spectrometer is not evacu-
ated, purging is recommended, especially when you frequently open the compartment
covers (e.g. due to a detector or beamsplitter replacement or a sample substitution) or if
the ambient air humidity content is too high because this measure reduces the level of
water vapor, CO
2
or other components of the ambient air inside the spectrometer.
Note: Water vapor, CO
2
and other atmospheric contaminants cause
unwanted absorption. Therefore, open the sample compartment, the
detector compartment and/or the interferometer compartment only if
necessary in order to prevent water vapor, CO
2
or other contaminants
from entering the above mentioned compartments.
Figure 27: OPUS Measurement dialog
Specifying the
measurement
delay time
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Purge the spectrometer, for example, with dry air or low pressure nitrogen gas. Provide
the following purge gas conditions:
Dry (dew point < -40C corresponds to a degree of dryness of 128ppm humidity),
oil-free and dust-free air or nitrogen gas
Maximum pressure of 2 bar (29 psi)
Initial purge gas flow rate should not exceed 500 liters/hour
Sustained purge gas flow rate should not exceed 200 liters/hour
Danger: Do not use flammable gases for purging the spectrometer. Some
spectrometer components become very hot during operation. If
flammable gases come in contact with hot components there will
be the risk of fire and/or explosion!
For information about how to connect the spectrometer to a purge gas supply line, refer
to chapter Installation.
If you want to purge an enclosed accessory (e.g. micro ATR unit) you have to cover the
opening, which is also intended for evacuating and venting the sample compartment
(see figure 28), using the supplied cap in order to ensure a sufficient purge of the
accessory. Put the cap over opening and screw on the cap.
Attention: If you want to perform measurements under vacuum conditions
do not forget to remove this cap again! Otherwise, the evacuation
of sample compartment via the small purge gas inlet in the Quick-
Lock clamping device (figure 28) will take too long causing a red
VACUUM LED after a certain period of time.
This opening is intended for evacu-
ating, venting and purging the sam-
ple compartment.
Purge gas inlet for purging an enclosed accessory
mounted on a QuickLock baseplate
Figure 28: Sample Compartment
Cap with screw thread
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Cont r ol l i ng t he Fl aps
VERTEX 70v is primarily designed for vacuum operation, but it can be purged as well.
To activate the purge mode, select in the OPUS Measure menu the Optic Setup and
Service function. Click on the Devices/Options tab and make sure that the Purge Mode
check box is activated. See figure 29.
This operating mode allows you to control (open and close) the flaps in order to purge
either the sample compartment or the optical bench or both. The flaps are controlled via
the OPUS software. The corresponding buttons are at the Basic page of the Measure-
ment dialog window. See the following figure.
Figure 29: Activating the Purge Mode
Purge mode is
activated.
Current state of the
flaps
Next possible action
that can be performed
by clicking on this
button.
Figure 30: Controlling the Flaps
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OPERATI ON
Exchanging the Beamsplitter
The flaps can be opened or closed only if the pressure difference between the sample
compartment and the optical bench is below the threshold value of 5 hPa.
Speci al Case
Besides the normal purge mode in which the optical bench and/or the sample compart-
ment are only purged, the following special case is also possible: the vented sample
compartment is purged while the optical bench is evacuated. For the realization of this
special case, the spectrometer needs to be equipped with windows mounted on either
the sample compartment walls or the flaps which are closed in this case. To realize this
special case, proceed as follows:
Make sure that the purge mode is deactivated in OPUS. (See figure 20.)
Evacuate the optical bench and the sample compartment. (See chapter Opera-
tion, section Evacuating and Venting the Spectrometer.)
Afterwards, vent the sample compartment again. (In this condition, the flaps are
closed.)
Connect a hose to the purge gas inlet for the sample compartment. (The purge
gas inlet is at the spectrometer rear side. See chapter Installation, section Con-
necting VERTEX 70v to the Purge Gas Line, figure 7.)
Now start the purge gas supply.
Note: The flaps isolate the sample compartment hermetically from the
optical bench.
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EXCHANGI NG THE BEAMSPLI TTER
The standard version and the optional version of VERTEX 70v differ from each other
with regard to the interferometer compartment cover design (see fig. 33a and 33b) and
the availability of the beamsplitter storage positions (see fig. 31) inside the interferome-
ter compartment.

Feature Standard Version Optional Version (S239/V)
Interferometer compartment
cover design
A beamsplitter exchange
requires the removal of the
complete interferometer com-
partment cover.
Wing-shaped cover provides
for easy access to the beam-
splitter.
Availability of the beamsplitter
storage positions inside the
interferometer compartment
No Yes
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The standard spectrometer version is equipped with a MIR beamsplitter (made of KBr).
If your measurement requires a different spectral range, you can exchange the beam-
splitter manually. For a list with all available beamsplitters (including their spectral
ranges) refer to chapter Overview, section Internal Components.
Note: Make sure that the spectral ranges of the installed optical
components (source, beamsplitter, detector and sample
compartment windows, if installed) correspond with each other!
Changing the beamsplitter is easy because a precise locking mechanism automatically
fixes the beamsplitter at its pre-aligned position, as soon as you move the release lever
(figure 34) into the locked position (i.e. backward).
All beamsplitters for VERTEX 70v are electronically coded enabling the spectrometer
firmware to auto-detect the beamsplitter type. The information about the component is
passed on to the OPUS software. This feature is called ACR (Automatic Component
Recognition)
1
. Its purpose is to prevent you from selecting a wrong component in
OPUS when you set up a measurement. (Note: A wrongly selected component is indi-
cated in OPUS by a red colored entry field of the corresponding drop-down list. See
also the OPUS Reference Manual.)
1. ACR is restricted only to the optical components beamsplitter, detector and source.
Figure 31: VERTEX 70v - Beamsplitter Installation Positions (only In case of option S239/v)
Beamsplitter
(Operating position)
Two additional Beamsplitters
(Storage position)
Knob
Wing-shaped
cover
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OPERATI ON
Handl i ng I nst r uct i ons
Caution: The beamsplitter is a very delicate component. Handle it with
utmost care and observe the following handling instructions to
ensure a long service life.
Do not touch the beamsplitter surface as this will damage the surface and, as a
consequence, the beamsplitter may become useless. Hold the beamsplitter using
always the handle (figure 32).
Some beamsplitter materials are hygroscopic. Never expose them to humidity or
water vapor. Store the beamsplitter either in a dry and sealed container (e.g. in the
beamsplitter storage box) or inside the spectrometer (storage position, figure 31).
Do not try to loosen or fasten the screws as this will impair the optical quality of the
beamsplitter and lead to malfunctions.
Do not try to clean the beamsplitter.
Do not expose the beamsplitter (especially beamsplitters made of KBr) to temper-
ature changes.

Figure 32: Beamsplitter
Handle
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Exchange Pr ocedur e
1 The procedure for gaining access to the beamsplitter depends on the
interferometer compartment cover design. Standard cover (fig. 33a): Take
off the complete cover. Optional cover (fig. 33b): Turn the knob counter-
clockwise until the stop and rotate the wing-shaped cover aside as shown in
figure 31.
Caution: Class 2 laser radiation. When the cover is removed do not stare
into the laser beam.
2 Move the release lever into the unlocked position (i.e. backward).
3 Carefully pull the beamsplitter straight upwards without catching an edge.
4 Take the other beamsplitter out of the storage position and insert it with the
electrical contacts facing to the front side (figure 34).
5 Push down the beamsplitter completely until you feel resistance.
6 Move the release lever into the locked position, i.e. forward. (See figure 34.)
Note: A beep indicates that the beamsplitter has been recognized by the
electronics. After a few seconds the spectrometer will start scanning.
7 Insert the beamsplitter, you have taken out of the operating position, either
into the storage position holder (figure 31) or store it in the intended box.
8 Standard cover: Place the cover on the interferometer compartment again.
Optional cover: Rotate the wing-shaped cover over the openings and
secure it by turning the knob clockwise.
9 Check whether a signal is detected and the optics works correctly. (For
detailed information refer to the OPUS reference manual.)
Figure 33: a) Standard Cover b) Wing-shaped Cover (in case of option S239/V)
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Exchanging the Detector
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EXCHANGI NG THE DETECTOR
The basic spectrometer configuration is equipped with a DigiTect DLaTGS detector. If
your measurement requires a different spectral range or another detector sensitivity you
can install another detector into the second detector position, which is an optional spec-
trometer feature, or exchange the installed DigiTect DLaTGS detector for another Digi-
Tect detector, such as a MCT with a higher sensitivity or a NIR detector. (For the list
with all available detectors including their spectral ranges refer to chapter Overview,
section Internal Components.)
Note: Make sure that the spectral ranges of the installed optical
components (source, beamsplitter, detector and sample
compartment windows, if installed) correspond with each other!
A removable cover provides access to the detector compartment. The dovetail detector
mounting facilitates the exchange. A re-alignment is not necessary. All detectors for
VERTEX 70v are electronically coded, enabling the spectrometer firmware to auto-
detect the type of detector currently installed. This information is passed on to the
OPUS software. This feature is called ACR (Automatic Component Recognition)
1
. Its
purpose is to prevent you from selecting a wrong component in OPUS when you set up
a measurement. (Note: A wrongly selected component is indicated in OPUS by a red
colored entry field of the corresponding drop-down list. See also the OPUS Reference
Manual.)
Figure 34: Beamsplitter (Operating Position)
Release lever
(in locked position)
Beamsplitter handle
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Exchanging the Detector
Exchange Pr ocedur e
1 Take off the detector compartment cover (E in figure 9).
Caution: If there is a MCT detector installed in the detector compartment
(including a vacuum-tight closure at the filling hole in the detector
compartment cover) the detector compartment cover can not be
taken off. In this case, do not try to remove the cover forcibly as
this may cause a spectrometer damage! Therefore, first screw off
the sealing adapter mating part (figure 39) before you take off the
detector compartment cover. (See chapter Operation, section
Cooling an MCT Detector, subsection Detector Compartment
Cover Preparation Procedure.)
2 Loosen the locking screw (allen screw) that secures the detector using a
hex key (size 6mm). See figure 35. Depending on which detector you want
to remove, the allen screw is on the left or right side of the detector.
3 Pull the detector straight upwards out of the dovetail guide.
Caution: Remove the detector carefully in order not to damage the detector
and/or the mirrors.
4 Insert the other detector precisely into the dovetail guide and push the
detector downwards until you feel a resistance.
Figure 35: Detector Compartment
MCT detector
DLaTGS
detector
Moveable mirror
Locking screw
of the detector
installed in
position 1
Locking screw of
the detector in-
stalled in position 2
Fixed mirror
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OPERATI ON
Cooling an MCT Detector
Note: A beep indicates that the detector has been recognized by the
electronics. The electrical connections are established automatically.
5 Fasten the allen screw slightly using a hex key (size 6mm).
6 Place the cover on the detector compartment. Make sure that the four
plastic pins in the corners at the bottom side of the detector compartment
cover engage into the corresponding hole of the spectrometer case.
Note: If there is a MCT detector in the detector compartment do not forget
to reinstall the vacuum-tight closure at the filling hole in the detector
compartment cover. For information about it refer to chapter
Operation, section Cooling an MCT Detector, subsection Detector
Compartment Cover Preparation Procedure.)
7 Check whether a signal is detected and the optics works correctly (For
detailed information refer to the OPUS reference manual).
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COOLI NG AN MCT DETECTOR
To ensure operating ability, MCT detectors have to be cooled regularly with liquid nitro-
gen. The typical hold time depends on the detector. There are MCT-detectors with a
hold time of 8, 12 or 24 hours.
To fill the detector with liquid nitrogen you need neither to remove the detector from the
spectrometer nor even open the detector compartment. The supplied funnel facilitates
the filling in of the liquid nitrogen in the detector. See figure 40.
Det ect or Compar t ment Cover Pr epar at i on Pr ocedur e
In case the MCT detector has been delivered together with VERTEX 70v, the detector
compartment cover is already prepared for the funnel insertion. If you have ordered the
MCT detector at a later date you need to prepare the cover as described in the follow-
ing.
In accordance with the number of detectors that can be installed in the VERTEX 70v
detector compartment, there are two filling holes in the cover. See figure 36. These
holes are intended to accommodate the funnel. Upon delivery, these holes are closed
vacuum-tightly by a cap plus O-ring.
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OPERATI ON
Proceed as follows:
1 Take off the detector compartment cover and turn it upside down.
2 Remove the cap from the filling hole that corresponds with the position of
the MCT detector you want to cool. To do this, loosen the nut using a
wrench (size 24mm) and remove the O-ring and the cap. See figure 37.

3 By default, the sealing adapter is already factory-mounted on the MCT
detector. If not, screw the sealing adapter on the MCT detector filling piece.
See figure 38.
Filling holes
closed by caps
Figure 36: Detector Compartment Cover (Top Side)
Figure 37: Detector Compartment Cover (Bottom Side)
Open filling hole
Closed filling hole
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OPERATI ON
4 Put the cover on the detector compartment again.
5 Screw the white sealing adapter mating part on the threaded end fitting of
the sealing adapter. See figure 39.
Note: When you perform a measurement in vacuum, the sealing adapter
and its mating part ensure a vacuum-tight closure at the filling hole in
the detector compartment cover.
Caution: With the installed vacuum-tight closure at filling hole, the detector
compartment cover can not be removed. In this case, do not try to
remove the cover forcibly as this may cause a spectrometer
damage.
6 Insert the funnel as shown in figure 40.
Figure 38: Detector Compartment
Sealing adapter
MCT detector
Figure 39: Installing a vacuum-tight closure
Threaded end fitting of
the sealing adapter
Sealing adapter mating part
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OPERATI ON
Saf et y Not es
MCT detectors have to be cooled with liquid nitrogen. The temperature of liquid nitrogen
is minus 196C (minus 320.8F). Therefore, handling liquid nitrogen requires the obser-
vance of the following safety notes:
Warning: Handle liquid nitrogen always with utmost care. Due to its
extremely low temperatures, skin contact can cause severe
frostbites! Also the gases escaping from the liquid nitrogen are
extremely cold and can cause frostbite. The delicate eye tissue
can be damaged if exposed to this cold gas even for a short time.
Protect your eyes by wearing a face shield or safety goggles! Note
that goggles without side shields do not provide adequate
protection!
Warning: High nitrogen gas concentrations in an enclosed area can cause
asphyxiation! Use liquid nitrogen only in well-ventilated areas.
Nitrogen gas is colorless, odorless and tasteless. Therefore, it can
not be detected by human senses and will be inhaled as if it were
normal air.
Cool i ng Pr ocedur e
1 Fill in slowly liquid nitrogen. See figure 40. At first the liquid nitrogen
evaporates and streams out again.
Warning: Liquid nitrogen boils and splashes when it is filled a warm
container. Therefore, fill in the liquid nitrogen slowly to minimize
boiling and splashing. Stand clear of boiling and splashing liquid
nitrogen and its issuing gas.
Figure 40: Filling in liquid Nitrogen
5
OPERATI ON
2 Wait until the funnel is empty before refilling. When the liquid nitrogen stops
streaming out the dewar has reached liquid nitrogen temperature. Then, fill
the funnel again with liquid nitrogen. Avoid spilling the liquid on the housing.
3 Repeat this procedure until the detector dewar has been filled to maximum.
(As a rough rule of thumb for the standard MCT detector: the maximum
dewar capacity is about the quantity of two to three funnel fillings. Note that
the first two funnel filling will evaporate almost completely.) Avoid overfilling.
In this case the liquid flows out of the filling port.
4 After having filled in sufficient liquid nitrogen, remove the funnel and insert
the supplied plug instead. See figure 41.
5 Wait about 20 minutes before starting the measurement to allow the
detector to stabilize.
Figure 41: Closed Filling Hole
Plug
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
MAI NTENANCE AND REPAI R 6
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
VERTEX 70v is a low-maintenance instrument equipped with easy-to-replace compo-
nents. The operator can replace components with a limited service life (e.g. IR source)
without requiring the assistance of the Bruker service personnel. The following mainte-
nance and repair procedures are described in this chapter:
Evacuating a MCT detector dewar
Replacing a defective laser module
Replacing a defective IR source
Replacing fuses
Replacing the sample compartment windows
Cleaning the instrument
Maintaining the vacuum pump
Perform only the maintenance and repair works which are described in this manual.
Adhere strictly to the described procedures and observe all relevant safety precautions.
Otherwise, personal injury and/or spectrometer damage can be the result. In this case,
Bruker does not assume any liability. Maintenance and repair works that are not
described in this manual should only be performed by Bruker service personnel. (For
service addresses and telephone numbers refer to appendix I.)
Caution: Avoid electrostatic discharges (ESD) to prevent ESD sensitive
electronic components from being damaged.
Electronic components (like semiconductor chips and boards) are very susceptible to
electrostatic discharges caused by the operator. Even the slightest electrostatic dis-
charge that is imperceptible to the operator can damage electronic components. There-
fore, it is of crucial importance that you are connected to ground with respect to the
spectrometer before you touch any electronic component inside the spectrometer. Elec-
trical grounding can be accomplished either by using a grounded wrist strap or touching
a grounded object (e.g. radiator). The grounded wrist strap is the most effective (and the
preferred) grounding method.
Note: After having exchanged a defective optical component e.g. laser unit,
light source we recommend running the OQ test using the OVP
software to check the spectrometer performance. (For the test
procedure refer to the OPUS Reference Manual.)
6
MAI NTENANCE AND REPAI R
Evacuating the MCT Detector Dewar
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
EVACUATI NG THE MCT DETECTOR DEWAR
Most liquid nitrogen cooled detectors are mounted in re-pumpable vacuum dewars
(except for those which are sealed permanently). Evacuating the detector dewar
becomes necessary if the hold time decreases considerably (i.e. a hold time of less
than four hours). The existence of condensation water on the detector outside indicates
that the dewar must be evacuated soon. If there is frost on the detector outside the
dewar must be evacuated immediately. Before evacuating the dewar, the detector must
be removed from the spectrometer.
To evacuate the dewar the following evacuating equipment is required:
turbo molecular pump / oil-free high-vacuum pump (that generates an vacuum of
at least < 10
-5
mbar)
vacuum adapter
Note: Bruker offers suitable evacuating equipment (# S105-V). In case you
do not want to purchase this equipment, Bruker also offers the
service of evacuating the MCT detector (# D128). So, alternatively you
can send the complete MCT detector in to Bruker.
Component
A Vacuum Adapter (D126)
B Flange
C Flexible Metal Hose
D NW25 Flange
Figure 42: a) Vacuum Adapter b) Vacuum Adapter with flexible Metal Hose and Flange
A
B C D
.

.

.

.

.
Evacuat i on Pr ocedur e
1 Remove the MCT detector from the spectrometer. See chapter Operation,
section Exchanging the Detector.
2 Connect the connecting piece of the vacuum adapter (E in figure 43) to the
vacuum pump. (The connecting piece has an OD of 9.7mm.)
3 Pull the knob (H in figure 43) to the open position and loosen the coupling
nut (A in figure 43).
4 Push the vacuum adapter carefully over the connection nozzle of detector
dewar and fasten the coupling nut finger-tight. Additional tightening is not
necessary.
5 Push the knob in the closed position until the threaded rod (D in figure 43) of
the vacuum adapter is in contact with the dewar evacuation valve.
6 Screw the threaded rod in the evacuation valve closure of the dewar by
turning the knob clockwise; 2 to 3 rotations are sufficient.
7 Evacuate the vacuum adapter using the vacuum pump.
Note: The dewar should not contain any liquid nitrogen and should be at or
slightly above room temperature (max. 60C).
8 Pull the knob to the open position in order to open the dewar evacuation
valve. Evacuate the detector dewar using the vacuum pump.
Note: Evacuating the dewar takes several hours. Therefore, it is
recommendable to evacuate the dewar overnight. The final pressure
in the dewar should be less than 10
-5
mbar.
9 When the desired vacuum is achieved, push the knob to the closed position
in order to close the dewar evacuation valve.
10 Vent the section between vacuum pump and vacuum adapter.
11 Rotate the knob several turns counterclockwise in order to screw the
threaded rod off the dewar evacuation valve. Be careful not to vent the
dewar.
12 Pull the knob to the open position, loosen the coupling nut and remove the
vacuum adapter from the connection nozzle of the dewar.
13 Reinstall the MCT detector in the spectrometer.
6
Component
A Coupling nut
B O-ring retainer
C O-ring
D
Threaded rod (to remove the valve closure of the
detector dewar)
E Connecting piece for vacuum pump (OD = 9,7mm)
F Vacuum adapter
G Washer and O-ring packing
H Knob
Figure 43: Vacuum Adapter - Cross Section
open
closed
A
B
C
D
E
F
G
H
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Replacing the Laser Module
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
REPLACI NG THE LASER MODULE
The laser module needs to be replaced only if it is defective. A defective laser is indi-
cated by a red LASER LED (fig. 10). For detailed information about fault diagnosis refer
to chapter Troubleshooting, section Diagnostic Means.
The replacement laser module consists of the laser tube and the laser power supply
unit, i.e. in case of a defective laser you have to replace both components. For the order
number of the replacement laser module refer to appendix B.
Saf et y Not es
The interferometer is equipped with a HeNe laser. This laser emits red light with a
wavelength of 633nm. The rated power output is 1mW. According to EN 60825-1/
10.2003, the laser is laser class 2 product. Laser class 2 means that the accessible
laser radiation can cause eye injuries. Therefore, when replacing the laser, observe the
following safety notes:
Caution: Do not stare into the beam! A long-standing exposure to laser
class 2 radiation can lead eye injuries.
Always switch off the spectrometer and disconnect the power plug
before beginning the laser removal. Be aware of the fact that the
laser is active as soon as the spectrometer is switched on.
Do not put the spectrometer into operation if the covers are
removed or show signs of damage.
Repl acement Pr ocedur e
The laser module is accessible from the spectrometer rear side. For the exact location
of the laser, see to chapter Overview, section Internal Components, fig. 15. Proceed as
follows:
1 In case the spectrometer is evacuated, vent it first
2 Switch off the spectrometer using the mains switch at the spectrometer rear
side and unplug the power cord. See chapter Installation, fig. 2.
3 Remove the interferometer compartment cover.
4 Remove the valve block cover shown in fig. 44 by loosening the two Allen
screws (using a hex key, size 3mm) and pulling off the cover.
6
5 Disconnect the laser power supply cable from the laser module by loosening
the two slotted screws at the green plug shown in figure 45 and pulling off
the plug.
6 Loosen the Allen screw (A in fig. 46) using the supplied hex key (size 3mm)
and rotate the holding plate (B fig. 46) aside.
Allen Screws Valve Block Cover
Figure 44: Removing the Valve Block Cover
Figure 45: Disconnecting the Laser Power Supply Cable
Laser power
supply cable
2 slotted screw
(at the green plug)
.

.

.

.

.
7 Grasp the laser module with both hands as shown in fig. 47 and pull it out of
the holder. (Note: To do this, you have to apply some force in order to
overcome the holding force of the fixing pins.)
8 Install the replacement laser module and connect the laser power supply
cable. (See step 3 to 4.)
Figure 46: Laser module - Top view
B
A
Figure 47: Removing the Laser Module
Fixing pins
6
Important: When inserting the replacement laser module in the spectrometer
pay attention to the following potential installation errors:
Insert the laser module in such a way that the white labels at
both laser tube ends (fig. 48a) do not come in contact with the
two locking pins. Otherwise, the laser beam will be out off
alignment.
Make sure that the outlet of the black cable is orientated as
shown in fig. 48b.
9 Reinstall the valve block cover. (See step 2.)
10 Reconnect the spectrometer to the power supply and switch on the
spectrometer. (See step 1.)
Laser Par amet er Reset
After having replaced the laser, do not forget to reset the laser parameters (operating
time and laser dropouts, if necessary) using the OPUS software. To do this, proceed as
follows:
Select in the OPUS Measure menu the Optic Setup and Service function. A dialog
window opens. Click on the Service tab and then on the Laser Replaced (Rest
Parameters) button. (See fig. 49.) Alternatively, either click on the green status
light (at the right end of the status bar) or select in the Measure menu the Optics
Diagnostics function. The Instrument Status window opens. Click the on HeNe
laser icon and then on the Service Info button. The diagnostics page of the HeNe
laser opens. (See chapter Troubleshooting, fig. 60.) Click on the Reset button.
If the previous laser has shown sporadic power fluctuations, these fluctuations
have been recorded automatically by an internal counter. After having replaced
the laser, reset this counter to 0 by clicking on the Reset Laser Dropouts button,
OPUS dialog window Optic Setup and Service page Service. (See fig. 49.)
Figure 48: a) Replacement Laser Module (side view) b) Laser Module (front view)
Cable
outlet
Laser
tube
White labels
.

.

.

.

.
Note: After a laser replacement, it is highly recommended to perform an OQ
test using OVP. For detailed information about this topic refer to the
OPUS Reference Manual.
Figure 49: OPUS dialog window - Optic Setup and Service
Laser parameters
Source parameters
6
Replacing a defective IR Source
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
REPLACI NG A DEFECTI VE I R SOURCE
The basic spectrometer configuration is equipped with a MIR source (standard). Option-
ally, a NIR source can be installed inside the spectrometer. The replacement procedure
is identical for both IR sources. The IR sources are pre-aligned and electrically coded
enabling the spectrometer firmware to auto-detect the source type. This information is
passed on to the OPUS software. This feature is called ACR (Automatic Component
Recognition)
1
. Its purpose is to prevent you from selecting a wrong component in
OPUS when you set up a measurement. (Note: A wrongly selected component is indi-
cated in OPUS by a red colored entry field of the corresponding drop-down list. See
also the OPUS Reference Manual.)
Saf et y Not es
During the spectrometer operation, the IR source becomes very hot. Therefore, after
having switched off the spectrometer, wait until the IR source has cooled down suffi-
ciently before you remove it.
Caution: Avoid any skin contact with a hot IR source. Risk of skin burn!
The IR sources are situated in the interferometer compartment. See chapter Overview,
figure 15. The replacement procedure is identical for both IR source types, MIR and
NIR source.
1 Switch off the spectrometer.
2 Take off the interferometer compartment cover. Wait until the IR source has
cooled down sufficiently.
3 Loosen the knurled thumb screw of the release lever (approx. one turn). See
figure 50.
.

.

.

.

.
Replacing a defective IR Source
4 Press the IR source slightly downwards while swiveling the release lever
aside.
5 Take out the IR source.
6 Insert the replacement IR source into the seating hole. Note that the two
pins shown in figure 51 have to snap in the corresponding holes at the IR
source bottom side to ensure the correct position of the source.
7 Gently press the IR source downwards and swivel the release lever over the
source to secure it. A beep indicates that the source has been recognized
by the electronics.
8 Tighten the knurled thumb screw of the release lever.
9 Place the cover again on the interferometer compartment.
10 Switch on the spectrometer.
11 Check whether a signal is detected and the optics works correctly using the
OPUS software.
Figure 50: IR Sources
Release levers
Knurled thumb
screws
Source seating
hole
Pins
Figure 51: Installing a MIR Source
6
Replacing the Fuses
Sour ce par amet er Reset
After having replaced the source, reset the operating hour meter. Proceed as follows:
Select in the OPUS Measure menu the Optic Setup and Service function. The
corresponding dialog window opens. Click on the Service tab and then on the
Source Replaced (Rest Parameters) button. (See figure 49.)
Alternatively, either click on the green status light (at the right end of the status
bar) or select in the Measure menu the Optics Diagnostics function. The
Instrument Status window opens. Click the on source icon and then on the Service
Info button. The diagnostics page of the source opens. (See figure 61.) Click on
the Reset button.
Note: After a source replacement, it is highly recommended to perform an
OQ test using OVP. For detailed information about this topic refer to
the OPUS Reference Manual.
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
REPLACI NG THE FUSES
If the voltage status LEDs (A in fig. 83) at the spectrometer rear side do not light,
although the spectrometer is switched on (assuming sufficient power is supplied to the
spectrometer), a blown fuse of the spectrometer mains power supply can be the cause.
The fuse box is at the spectrometer rear side below the mains switch. (See figure 52a.)
1 Switch off the spectrometer by turning the mains switch to the O position
(figure 52a) and unplug the spectrometer power cable.
2 Open the fuse box flap by inserting a small flat-ended screwdriver into the
groove and gently prying out the fuse block flap. (See figure 52b.) Turn the
fuse box downwards. (See figure 52c.)
3 The fuse box contains two fuses. Replace both fuses with 5x20 mm fuses
with a rated current of 4A, slow blow (according to IEC 60 127-2).
Note: We recommend fuses of the manufacturer WICKMANN. (See
www.wickmannusa.com). Alternatively, you can order single fuses at
BRUKER.
4 Close the fuse box by turning the box upwards and pressing it against the
housing until the spring clip engages.
5 Reconnect the spectrometer to the mains.
.

.

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.

.
Replacing the Sample Compartment Windows
REPLACI NG THE SAMPLE COMPARTMENT
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
WI NDOWS
Provided the sample compartment of your spectrometer is equipped with windows, they
are mounted either on the sample compartment walls or on flaps which can be move in
and out of the beam path. With the flaps in the beam path, the windows separate the
sample compartment from the detector compartment and the beam direction control
compartment. The flap movement is computer-controlled.
In the course of time, the opaqueness of the windows can reach such a degree that the
transparency (infrared transmittance) is seriously reduced. If this is the case, the win-
dows need to be replaced.
Note: When installing new windows, make sure that their transmission
range corresponds with the spectral range of the other installed
components (detector and beamsplitter). For information about the
transmission range of the available window materials refer to the
table below. The spectral range of the available detectors and
beamsplitters is listed in the corresponding tables in chapter
Overview, section Internal Components.
Figure 52: a) Fuse Box b) Opening the Fuse Box c) Opened Fuse Box
Fuse
Box
Mains
Switch
6
Handl i ng I nst r uct i ons
The windows are very fragile. Moreover, contaminations on the window surface can
decrease the transparency significantly. Therefore, follow the following instructions:
Caution: Handle the windows with great care because they are made of
fragile material that cracks under influence of mechanical
pressure. Do not touch the window surface. This may lead to
irreversible contamination.
Saf et y Not es
Some window materials are harmful or (very) toxic. (See the following table.) During
normal operation, these window materials do not pose a health risk. However, should
these windows break, be extremely careful. Avoid generating dust.
Warning: Observe the safety instructions on the packaging, and the safety
data sheets attached. Non-observance may cause serious health
problems or even death.
The following table lists the available window materials including their transmission
range, refraction index and chemical properties.
Material
Transmission
Range (cm
-1
)*
Refraction Index
n (at 2000cm
-1
)
Chemical Properties
Quartz (Infrasil)
SiO
2
57,000 - 2,800 1.46 Insoluble in water;
soluble in HF
Silicon
Si
10,000 - 100 3.42 Insoluble in most acids and
bases; soluble in HF and HNO
3
Calcium Fluoride
CaF
2
66,000 - 1,000 1.40 Insoluble in water; resistant to
most acids and bases; soluble
in NH
4
salts
Barium Fluoride
BaF
2
CAUTION - HARMFUL!
50,000 - 800 1.45 Low water solubility; soluble in
acid and NH
4
Cl
Sodium Chloride
NaCl
28,000 - 580 1.50 Hygroscopic; slightly soluble in
alcohol and NH
3
Zinc Selenide
ZnSe
CAUTION - TOXIC!
20,000 - 500 2.43 Soluble in strong acids and in
HNO
3

Silver Chloride
AgCl
CAUTION - HARMFUL!
23,000 - 400 2.00 Insoluble in water; soluble in
NH
4
OH
Potassium Bromide
KBr
33,000 - 280 1.54 Soluble in water, alcohol, and
glycerine; hygroscopic
.

.

.

.

.
* 50% value at a window thickness of 4mm
Repl acement Pr ocedur e f or Wi ndows mount ed on Fl aps:
1 Take off the sample compartment cover.
2 To gain access to the flaps, first remove the cover by loosening the two Allen
screws using a hex key (size 2mm). See figure 53.
3 Remove the window retaining ring by loosening the three slotted screws.
See figure 54.
4 Take out the window and install the new one.
5 Attach the window retaining ring by fastening the three slotted screws. See
figure 54.
6 Reinstall the cover using the two Allen screws. See figure 53.
Cesium Iodide
CsI
CAUTION - HARMFUL!
33,000 - 180 1.74 Soluble in water and alcohol;
hygroscopic
KRS-5 (TIBr/I thallium
bromide-iodide)
CAUTION - VERY TOXIC!
16,000 - 250 2.38 Soluble in warm water and
bases; insoluble in acids
Polyethylene
PE (high density)
600 - 10 1.52 Resistant to most solvents
Silver bromide
AgBr
CAUTION - HARMFUL!
22,000 - 300 2.22 Soft crystal; insoluble in water;
darks upon exposure to UV
radiation
Material
Transmission
Range (cm
-1
)*
Refraction Index
n (at 2000cm
-1
)
Chemical Properties
Figure 53: Removing the Cover
Cover
Allen screws
6
Repl acement Pr ocedur e f or Wi ndows mount ed on t he
Sampl e Compar t ment Wal l s:
1 Take off the sample compartment cover.
2 Remove the complete window assembly by loosening the three Allen
screws using the hex key (size 2mm) See figure 55. (The window assembly
consists of the retaining ring, the window and the flange ring. See
figure 56b)
3 Loosen the three slotted screws shown in figure 56a and remove the
retaining ring.
4 Take the window out of the flange ring and insert a new one.
Window
Figure 54: Replacing a Window
Slotted
Screws
Retaining ring
Figure 55: Removing the Window Assembly
Allen screws
.

.

.

.

.
Cleaning the Instrument
5 Reassemble the window assembly and attach it to the sample compartment
wall. (Note: While reassembling the window assembly, tighten the slotted
screws alternately.)
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
CLEANI NG THE I NSTRUMENT
Only the outer surface of the spectrometer can be cleaned with a dry or damp cloth. Do
NOT use detergents with organic solvents, acid or base!
Warning: Do not clean the spectrometer interior. This may lead to serious
spectrometer damage.
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
MAI NTAI NI NG THE VACUUM PUMP
The vacuum pump needs to be maintained regularly. For detailed information about the
maintenance procedure and service intervals refer to the supplied vacuum pump user
manual.
Figure 56: Window Assembly (a) assembled (b) disassembled
Slotted screws
Retaining ring Flange ring
6
Maintaining the Vacuum Pump
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
TROUBLESHOOTI NG 7
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
This chapter describes the most common potential spectrometer problems, their possi-
ble causes and recommended solutions.
1
Depending on how a spectrometer problem
becomes apparent, they are subdivided into the following categories:
Spectrometer problem indicated by the spectrometer status indicator
Spectrometer problem indicated by an instrument status message in OPUS or
other OPUS messages
No interferogram displayed in the OPUS dialog Check Signal
A failed OVP test
Spectrometer problem indicated by various diagnostic LEDs at the spectrometer
rear side (e.g. ERR LED, voltage status LEDs)
No data transfer between spectrometer and computer
The available diagnostic means (e.g. spectrometer status indicator, error messages in
OPUS, diagnostics pages of the firmware) enable the operator to identify and solve
many spectrometer problems without requiring the support of the Bruker service, or at
least to narrow down a problem.
If the solutions listed below do not solve a problem contact the Bruker service. (For ser-
vice addresses and telephone numbers refer to appendix I.)
With OPUS version 6 or higher, it is possible to send the complete spectrometer status
report by e-mail to the Bruker service. This report allows the Bruker service technician a
first remote fault diagnostics. To do this, proceed as follows:
1 Click on the OPUS status light. (The status light is in the lower right corner of
the OPUS interface.)
2 The Instrument Status dialog window opens. Click on the Send Report
button. (See figure 58.) The report is sent by e-mail to
opusreports@brukeroptics.de.
Note: This function requires an e-mail program installed on your computer
and a set-up mail account. In addition, your spectrometer needs to be
connected to a network computer.
1. Not all possible spectrometer problems and causes are listed in this chapter. If the recommended solutions do
not solve the problem, contact your local Bruker service. For service addresses and telephone numbers refer to
appendix I.
7
TROUBLESHOOTI NG
Diagnostic Means
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
DI AGNOSTI C MEANS
For a spectrometer fault diagnosis, the following diagnostic means are available:
Spectrometer status indicator on the spectrometer top side
OPUS dialog window Instrument Status
Instrument status messages in OPUS
Diagnostics pages for the following spectrometer components: laser, source,
interferometer
1
, electronic, automation and detector
Several diagnostic LEDs at the spectrometer rear side
Spect r omet er St at us I ndi cat or Boar d
The status indicator board (figure 57) is in the left rear corner on the spectrometer top
side.

These LEDs can light up in different colors. Depending on the LED in question, they
indicate the following status/condition:
VACUUM LED
The color of VACUUM LED depends on the current pressure situation inside the individ-
ual spectrometer compartments.
1. The terms Interferometer and Scanner are used synonymously.
LED is off. Sample compartment and optical bench are vented.
LED flashes green. Sample compartment and optical bench are being either evacuated
or vented.
LED lights up green. Sample compartment and optical bench are evacuated. The ulti-
mate vacuum is achieved.
LED flashes yellow. Sample compartment is being either evacuated or vented. (In case
the sample compartment is already vented, it flashes yellow also
when the optical bench is being vented.)
Figure 57: Status Indicator Board
.

.

.

.

.
TROUBLESHOOTI NG
Diagnostic Means
LASER LED
STATUS LED
Note: The diagnostic LED Status corresponds for the most part with the
instrument status indicator in OPUS. (The difference between both is
that the spectrometer Status LED does not light up yellow whereas
the instrument status indicator in OPUS does.) The instrument status
indicator is in lower right corner of the OPUS user interface. For
detailed information about it, refer to the OPUS Reference Manual.
For detailed information about the diagnostic LEDs of the status indicator board refer to
chapter Overview, section External Components.
OPUS Di al og Wi ndow I ns trument Status
The OPUS dialog window Instrument Status allows you to diagnose which spectrometer
component has caused the failure or to find out whether an OVP test
1
has expired or
failed.
To perform a fault diagnosis, proceed as follows:
LED lights up yellow. Sample compartment is vented.
LED lights up red. When the spectrometer is being evacuated, but a certain threshold
pressure value is not reached within a certain period of time (i.e.
the ultimate vacuum is not achieved). A red VACUUM LED indi-
cates a problem.
LED lights green. Laser is OK.
LED lights up red. Possible causes are:
Laser power is too weak.
Laser beam is blocked.
Laser module is defective.
Laser tube is out of alignment.
LED lights green. Spectrometer is OK.
LED lights up red. Possible causes are:
Spectrometer is still initializing.
There is a general spectrometer problem (e.g. a defective
spectrometer component).
1. OVP test is a collective term for all tests (e.g. OQ, PQ, PHEUR2240) that can be performed with OVP. OVP
(OPUS Validation Program) is part of OPUS. The general purpose of these OVP tests is to check whether the
spectrometer system achieves the specified performance. For detailed information about OVP refer to the
OPUS Reference Manual.
7
TROUBLESHOOTI NG
Diagnostic Means
1 Either click on the OPUS status light or select in the OPUS Measure menu
the Optics Diagnostics function. The following dialog window opens:
A The status of the hardware components, e.g. source, laser, interferometer etc.
is displayed in the upper icon line. The status can be as follows:
B The second row of icons refer to the possible active test channel and indicates
the result of the last OVP test performed. The results can be as follows:
Green check mark:
Component is okay.
WARNING (light blue):
The exact meaning of a warning depends on the compo-
nent in question. For example, in case of the source, a
warning means:
End of the specified lifetime of the component is nearly
reached. In this case, measuring is still possible.
ERROR (red):
Component is defective. In this case, measuring is no
longer possible.
Figure 58: Optics Diagnostics - Instrument Status dialog
A
B
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TROUBLESHOOTI NG
Diagnostic Means
2 To perform a fault diagnosis of a particular spectrometer component click on
the respective icon in the first row of the Instrument Status dialog. The
Instrument Status Message dialog opens. (See figure 59.)
I nst r ument St at us Messages i n OPUS
Some spectrometer problems are indicated additionally by a corresponding instrument
status message displayed in OPUS. (See fig. 59) These messages appear when you
click on the icon of the optical component in question in the Diagnose window.

PASSED (green):
OVP test passed. Test is still valid.
EXPIRED (light blue):
The validity period of an OVP test has
expired.
What to do in this case?
Perform the OVP test in question. (See
OPUS Reference Manual.)
FAILED (red):
OVP test failed.
What to do in this case?
Try to find out the cause of a failed OVP
test by performing a systematic fault
diagnosis. Solve the problem and then
repeat the OVP test in question.
Figure 59: Instrument Status Message in OPUS indicating a Source Problem
Component
in question
Status message for
the component in
question
Status indication for the component in question
(green: OK, yellow: warning, red: error)
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TROUBLESHOOTI NG
Diagnostic Means
Di agnost i cs Pages
When you click on the Service Info button (figure 59), the diagnostics page for the com-
ponent in question opens. The diagnostics pages of the spectrometer firmware contain
all relevant information about the current operating state of the respective spectrometer
component. In the following figures, the information important for fault diagnostics are
highlighted by a rectangle.
The following figures show the diagnostics pages of the spectrometer components
listed above. These pages provide information relevant to fault diagnostics.
Figure 60: Laser Diagnostics Page
Date of initial laser
operation
Current reading of the laser
operating hour counter
Figure 61: Source Diagnostics Page
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TROUBLESHOOTI NG
Diagnostic Means
Figure 62: Scanner Diagnostics Page
Figure 63: Electronics Diagnostics Page
7
TROUBLESHOOTI NG
Diagnostic Means
Figure 64: Automation Diagnostics Page
e.g. Flaps Note: A missing
cross indicates a
disconnected flap.
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TROUBLESHOOTI NG
Diagnostic Means
Vol t age St at us LEDs
The voltage status LEDs (A in figure 83) are at the spectrometer rear side, labeled +5V,
+12V and -12V. These diagnostic LEDs indicate the state of the secondary voltages of
the electronics unit.
Di agnost i c LEDs RX and TX
These LEDs (S and T in figure 82) indicate the data transfer direction between the
spectrometer and the data system via the Ethernet connection. In case of the stand-
alone configuration, the green RX LED signals that the spectrometer receives data. In
case the spectrometer is connected to an Ethernet network, the green RX LED indi-
cates that a data packet is transmitted on the Ethernet. (It does not necessarily mean
that the data packet is destined for the spectrometer!) The yellow TX LED lights when
the spectrometer transmits a data packet. This indicates that the spectrometer is
accessed by a computer.
Di agnost i c LEDs SR and SG
These two LEDs (red SR LED and green SG LED, P and Q in figure 82) indicate the
internal operating state of the spectrometer communication processor. (The abbrevia-
tion SR stands for Status Red and SG for Status Green.) If the SR LED lights up the
spectrometer is busy and not ready for communication.
Figure 65: Detector Diagnostics Page
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TROUBLESHOOTI NG
Diagnostic Means
Di agnost i c LED ERR
The red ERR LED (K in figure 82) indicates an interferometer error (e.g. a missing laser
signal). As long as this LED lights, data acquisition is not possible.
Di agnost i c LED CR, CY and CG
These LEDs (D, E and F in figure 82) are status and diagnose LEDs for the step scan
option. They indicate the status of the controlling device. (The abbreviation CR stands
for Controller Red, CY for Controller Yellow and CG for Controller Green.) (For
detailed information refer to the Step Scan Manual.)
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TROUBLESHOOTI NG
Problem - Possible Cause - Solution
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
PROBLEM - POSSI BLE CAUSE - SOLUTI ON
Spect r omet er pr obl em i ndi cat ed by spect r omet er st at us
i ndi cat or .
RED VACUUM LED
During a spectrometer evacuation, a red VACUUM LED indicates that the ultimate vac-
uum inside the spectrometer is not reached (i.e it lights up red if a certain threshold
pressure value is not reached within a certain period of time).
Possible causes Solutions
There is a leakage that allows air to enter the
spectrometer. During the evacuation, a leak-
age may become apparent by a hiss. Possible
leakages are:
sample compartment cover has not been
placed correctly on the spectrometer,
flaps do not close properly,
the wing-shaped cover is not secured
properly (after the beamsplitter has been
exchanged),
a beam port cover is not reinstalled properly
(after an accessory has been removed from
an IR beam port).
Find the leakage and close it. (In case of
defective flaps contact the Bruker service. See
appendix I.)
Vacuum pump is defective. See the user manual of the vacuum pump.
Vacuum pump is not connected properly. Check the vacuum pump connection. (For
information about how to connect the vacuum
pump to the spectrometer refer to chapter
Installation, section Connecting the Vacuum
Pump.)
Venting valve(s) do(es) not close. This prob-
lem is accompanied by a hissing sound at the
spectrometer rear side.
Contact the Bruker service. (See appendix I.)
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TROUBLESHOOTI NG
RED LASER LED
RED STATUS LED
A red STATUS LED indicates a spectrometer problem which can be caused by a num-
ber of spectrometer components (e.g. laser, source, detector). In order to be able to
narrow down the problem, it is highly recommended to open the OPUS dialog window
Instrument Status. See figure 58.
Spectrometer is still initializing. (In this case,
there is no spectrometer problem.)
Wait until the spectrometer has completed the
initialization successfully (i.e. the LED turns to
green).
Laser beam inside the interferometer compart-
ment is blocked.
Note: This problem is indicated by the following instru-
ment status message HeNe-Laser is off or no laser sig-
nals.
After a laser replacement, the laser beam is
out of alignment due to the white labels at both
laser tube ends (fig. 48a) being in contact with
the fixing pins (fig. 47).
Install the laser correctly as described in chap-
ter Maintenance and Repair, section Replac-
ing the Laser Module.
Laser tube is not orientated correctly. Correct the laser tube orientation as shown in
fig. 48b. (See chapter Maintenance and
Repair, section Replacing the Laser Module.)
Laser is defective.
Note: This problem is indicated by the following instru-
ment status message HeNe-Laser is off or no laser sig-
nals.
Have a look at the laser diagnostic page. (See
section Diagnostics Pages.)
In case of a defective laser:
order a replacement laser module (For the
order number of the spare part, refer to
appendix B.)
replace the laser module as described in
chapter Maintenance and Repair, section
Replacing the Laser Module.
Laser signal is too weak because the average
laser lifetime is nearly over.
Note: In this case, the OPUS message End of average
life time is nearly reached, spare part will be required
appears.
If the average laser lifetime is exceed (signifi-
cantly) the laser module needs to be replaced.
To do this:
order a replacement laser module (For the
order number of the spare part, refer to
appendix B.)
replace the laser module as described in
chapter Maintenance and Repair, section
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TROUBLESHOOTI NG

Spectrometer is still initializing. (In this
case, there is no spectrometer problem.)
Wait until the spectrometer has completed the ini-
tialization (i.e. the LED turns to green).
If the laser is the cause of the problem
either:
the laser beam is blocked or
the laser tube is not orientated correctly
or
the laser is defective.
Note: These causes are also indicated by a red
LASER LED.
Blocked laser beam: Contact the Bruker service.
(See appendix I.)
Incorrect laser tube orientation: Correct the
laser tube orientation as shown in fig 48. See
chapter Maintenance and Repair, section Replac-
Defective laser: Order a replacement laser. (For
the order number of the spare part, refer to
appendix B.) Replace the laser as described in
chapter Maintenance and Repair, section Replac-
If the source is the cause of the problem it
is either not installed or defective.
Note: This problem is indicated by the following
instrument status message Source is broken or not
connected.
Check whether the source is installed properly.
If the source is defective it needs to be replaced.
Proceed as follows:
order a replacement source (For the order
number of the spare part, refer to appendix B.)
replace the source as described in chapter
Maintenance and Repair, section Replacing a
defective IR Source.
If the detector is the cause of the problem
it is either not cooled down (instrument
status message: Detector not ready) or it
is not installed correctly (instrument status
message: Device not connected. No ana-
log board selected).
Cool down the MCT detector by filling liquid nitro-
gen into the detector dewar. (See chapter Opera-
tion, section Cooling an MCT Detector.)
Check whether the detector is installed correctly.
(See chapter Operation, section Exchanging the
Detector.)
If the interferometer is the cause of the
problem there are a number of possible
causes. For example, the beamsplitter is
not locked. This problem is also indicated
by the instrument status message BMS
door is open in OPUS.
(Note: In case there is no beamsplitter installed at
all, also the LASER LED is red.)
To narrow down the cause of the problem, see
section below Spectrometer Problem indicated by
an Instrument Status Message, messages regard-
ing the interferometer.
If an unlocked beamsplitter is the cause of the
problem lock it. See chapter Operation, section
Exchanging the Beamsplitter.
If the electronics is the cause of the prob-
lem the electronics unit is defective or
there is a short circuit, for example.
Check whether the voltage status LEDs labeled
+5V, +12V and -12V (A in fig. 83) at the spectrom-
eter rear side are on. (See also section Voltage
Status LEDs below in this chapter.) In case of a
defective power supply unit contact the Bruker
service. (See appendix I.)
7
TROUBLESHOOTI NG
Spect r omet er Pr obl em i ndi cat ed by an I nst r ument St at us
Message
I NSTRUMENT STATUS MESSAGE REGARDI NG THE LASER
If the automation is the cause of the prob-
lem there are a number of possible
causes.
To narrow down the cause of the problem, open
the Automation Diagnostics Page (figure 64) in
OPUS. See also section Spectrometer Problem
indicated by an Instrument Status Message below
in this chapter; Instrument status messages
regarding the automation. If you can not solve the
problem contact the Bruker service. (See
appendix I.)
Instrument status message Possible causes Solutions
HeNe laser is off or no laser
signal.
Laser tube is not orientated
correctly.
OR
Power supply to the laser is
interrupted because the
green plug of the laser power
supply cable is not plugged in
at all or not secured properly.
(See fig. 45.)
OR
Laser is defective.
Correct the laser tube orienta-
tion as shown in fig. .48. (See
chapter Maintenance and
Repair, section Replacing the
Laser Module.)
Plug in the green plugs and
secure them properly by fas-
tening the two slotted screws.
See chapter Maintenance
and Repair, section Replacing
the Laser Module.
Order a replacement laser
module and replace the
defective laser module as
described in chapter Mainte-
nance and Repair, section
(For the order number of the
replacement laser refer to
appendix B.)
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TROUBLESHOOTI NG
I NSTRUMENT STATUS MESSAGE REGARDI NG SOURCE
End of average lifetime is
nearly reached, spare part will
be required.
The end of the specified life-
time of the laser is nearly
reached.
Order a replacement laser
module. (For the order num-
ber refer to appendix B.) After
the receipt, replace the laser
module. (See chapter Mainte-
Replacing the Laser Module.)
Note: Despite this warning mes-
sage, measuring is still possible.
To turn the OPUS status light green
again click on the Ignore button in
the Instrument Status Message dia-
log (fig. 59). The message will be
repeated in certain intervals until you
have replaced the laser module.
Source is broken or not con-
nected.
Source is not installed at all or
not installed properly.
OR
Source is defective (e.g. burnt
out).
Install the source as
described in chapter Mainte-
Replacing a defective
IR Source.
Order a replacement source
and replace the defective
source as described in chap-
ter Maintenance and Repair,
section Replacing a defective
IR Source.
End of average lifetime is
nearly reached, spare part will
be required.
The end of the specified life-
time of the source is nearly
reached.
Order a spare source. (For
the order number refer to
appendix B.) After the receipt,
replace the laser module.
(See chapter Maintenance
and Repair, section Replacing
a defective IR Source..)
Note: Despite this warning mes-
sage, measuring is still possible.
To turn the OPUS status light green
again click on the Ignore button in
the Instrument Status Message dia-
log (fig. 59). The message will be
repeated in certain intervals until you
have replaced the source.
7
TROUBLESHOOTI NG
I NSTRUMENT STATUS MESSAGE REGARDI NG THE
I NTERFEROMETER
I NSTRUMENT STATUS MESSAGE REGARDI NG DETECTOR
Scanner initialization mode. This error message appears
only if you try to start a mea-
surement while the spectrom-
eter is still initializing.
Note: Also other error messages
can be displayed. As in this case
there is not a spectrometer problem
you can ignore them.
Before starting a measure-
ment, wait until the spectrom-
eter has completed the
initialization successfully.
BMS door is open. Beamsplitter is not installed
properly (i.e. the beamsplitter
release lever is not in the
locked position).
Put the beamsplitter release
lever in the locked position.
(See chapter Operation, sec-
tion Exchanging the Beam-
splitter.)
Laser-A timing error / Laser-B
timing error
OR
Laser-A modulation too small /
Laser-B modulation too small
OR
Laser signals modulation too
small
OR
Laser period too slow or
modulation too small
Interferometer is out of adjust-
ment caused by strong vibra-
tions, for example.
Contact the Bruker service.
(See appendix I.)
Detector not ready. The MCT detector is not
cooled down to its operating
temperature.
Cool down the MCT detector
by filling liquid nitrogen into
the detector dewar. (See
chapter Operation, section
Cooling an MCT Detector.)
Device not connected. No
analog board selected.
OR
No analog board found.
Detector is not installed. Install the detector as
described in chapter Opera-
tion, section Exchanging the
Beamsplitter.
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TROUBLESHOOTI NG
I NSTRUMENT STATUS MESSAGE REGARDI NG AUTOMATI ON
Pressure in interferometer
compartment is unstable. /
Pressure in sample compart-
ment is unstable.
Note: These messages are dis-
played if the defined ultimate pres-
sure is not reached in the
compartment in question when
evacuating or venting it.
A valve jams.
OR
Vacuum pump is defective /
does not work properly.
OR
There is a leakage that allows
air to enter the interferometer
compartment. During the
evacuation, a leakage may
become apparent by a hissing
sound. Possible leakages
are:
detector compartment
cover / sample
compartment cover has not
been placed correctly on
the spectrometer or
the flaps do not close
properly or
the wing-shaped cover is
not secured properly (after
the beamsplitter has been
exchanged) or
an beam port cover is not
reinstalled properly (after
an accessory removal).
See appendix I.
See the user manual of the
vacuum pump.
Find the leakage and close it.
(In case of defective flaps
contact the Bruker service.)
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TROUBLESHOOTI NG
OTHER ERROR MESSAGES I N OPUS
If an error message appears which is not listed above contact the Bruker service. See
appendix I.
Error message Possible causes Solutions
Error message from Optical
Bench. Should this message
be ignored? Fatal 50200
Flaps Device error.
Note: As a flap malfunction leads to
unstable pressure conditions inside
the spectrometer during venting or
evacuating it, this kind of problem is
also indicated by a red VACUUM
LED and a red STATUS LED. More-
over, the instrument status message
Pressure in interferometer compart-
ment / sample compartment is
unstable is displayed in OPUS as
well. (See section Diagnostic
Means.)
Upon closing the flaps, a flap
is blocked by an object. (For
example, an object has got in
the opening while you have
worked in the sample com-
partment.)
OR
Flaps malfunction (i.e. one or
both flaps do not open / close
properly.)
OR
One or both flaps are not con-
nected.
Check whether there is some-
thing that blocks the flaps. If
so, remove it.
(See appendix I.)
To find out whether a discon-
nected flap is the cause of the
problem, consult the automa-
tion diagnostics page. See
fig. 64. If so, Contact the
Bruker service.
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TROUBLESHOOTI NG
Ther e i s no I nt er f er ogr am di spl ayed i n OPUS Di al og
Check Si gnal
Assuming that, firstly, the computer can access the spectrometer and secondly, there is
an optical connection between the interferometer outlet and the detector inlet, this prob-
lem can have the following possible causes:
Possible Causes Solutions
Optical path is blocked. Check whether the accessory in the sample
compartment blocks the IR beam.
Detector is not cooled down at operating tem-
perature.
Note: This problem is indicated by the instrument status
message Detector not ready.
Cool down the detector. In case of a liquid
nitrogen cooled detector, fill liquid nitrogen into
the dewar. (See chapter Operation, section
Cooling an MCT Detector.)
Detector is not or incorrectly installed.
message Device not connected. No analog board
selected.
Manually Changed Detectors: Check
whether the detector is inserted properly in its
holder. (See chapter Operation, section
Exchanging the Detector.)
External detectors: Examine the cable con-
nection at the detector as well as at the spec-
trometer rear side.
Defective or not correctly installed IR source.
message Source is broken or not connected.
Check whether the IR source is installed prop-
erly or replace the IR source, if it is defective.
(See chapter Maintenance and Repair, section
Replacing a defective IR Source.)
Beamsplitter is not properly installed.
message BMS door is open.
Check whether the beamsplitter is properly
installed. (See chapter Operation, section
Exchanging the Beamsplitter.)
Beamsplitter has become opaque or is dam-
aged.
Replace the beamsplitter and check the signal.
(See chapter Operation, section Exchanging
the Beamsplitter.)
Note: If a replacement beamsplitter is not available, you
need to order a new one.
The red ERR LED on the spectrometer rear
side lights up, i.e. there is a spectrometer
error, for example, strong mechanical shocks
have caused a temporary or permanent optics
misalignment or the laser is defective. (In case
of a defective laser, the LASER LED lights up
red.)
In case of an optics misalignment, contact the
Bruker service.
In case of a defective laser order a replace-
ment laser module. (For the order number
refer to appendix B.) After the receipt, replace
the laser module. (See chapter Maintenance
and Repair, section Replacing the Laser Mod-
ule.)
7
TROUBLESHOOTI NG
A f ai l ed OVP t est
OVP test is a collective term for all tests (e.g. OQ test, PQ test, PHEUR2240) that can
be performed with OVP (OPUS Validation Program). The general purpose of these
OVP tests is to check whether the spectrometer system achieves the specified perfor-
mance. For detailed information about OVP refer to the OPUS Reference Manual.
Defective power supply unit. Check the voltage status LEDs on the spec-
trometer rear side. If none of the LEDs lights,
the power supply unit probably needs to be
replaced. Contact the Bruker service. See
appendix I.
Detector oversaturation or ADC overflow Either reduce the light source intensity by
using a smaller aperture or reduce the gain
settings.
There is a sample in the spectrometer sample
compartment which blocks the IR beam.
Take the sample out of the sample compart-
ment and repeat the OVP test.
Source performance has decreased because
the end of its service lifetime is nearly reached.
Note: This problem is indicated by the following mes-
sage End of average lifetime is nearly reached, spare
part will be required.
Note: To find out of which component - either laser or
source - the end of the average lifetime is nearly
reached, open in OPUS the Instrument Status dialog win-
dow (fig. 58) The component in question has the status
WARNING.
Order a replacement source. (For the order
number refer to appendix B.) After receipt,
replace the source as described in chapter
Maintenance and Repair, section Replacing a
defective IR Source.
Sample compartment windows are dirty or
have become opaque.
Order new windows and replace them as
described in chapter Maintenance and Repair,
section Replacing the Sample Compartment
Windows.
Beamsplitter is dirty, opaque or damaged. Replace the beamsplitter as described in
chapter Operation, section Exchanging the
Beamsplitter.
Regarding the spectral range of the selected
optical components source, beamsplitter and
detector, the wrong sample compartment win-
dows are installed in the sample compartment.
Install windows made from a material that cor-
responds with the spectral range of the other
selected components. See chapter Mainte-
nance and Repair, section Replacing the Sam-
ple Compartment Windows.
Possible Causes Solutions
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The spectral ranges of the selected optical
components - source, beamsplitter and detec-
tor - do not correspond with each other.
Check whether the spectral ranges of the
selected optical components correspond with
each other. (For information about the spectral
range of the available detectors and beam-
splitters refer to chapter Overview, section
Internal Components.)
Ice formation in the MCT detector dewar.
Note: This problem becomes apparent by a failed ice
band test. This test is part of the PQ test procedure.
Evacuate the MCT detector dewar as
described in chapter Maintenance and Repair,
section Evacuating the MCT Detector Dewar.
Air humidity content inside the spectrometer is
too high.
Note: This problem becomes apparent by a failed water
vapor test. This test is part of the OQ test procedure.
Reduce the air humidity content inside the
spectrometer by either evacuating the spec-
trometer or purging it with dry air or nitrogen
gas. See chapter Operation, section Evacuat-
ing and Venting the Spectrometer or section
Purging the Spectrometer.
Peak position has shifted. Save the new peak position using the OPUS
software. Proceed as follows: Select in the
Measure menu the Advance Measurement
function, click on the Check Signal tab.
(Ensure that the option button Interferogram is
activated.) If the peak position is constant save
it by clicking on the Save Peak Position button.
If a failed OVP test has a different cause (e.g.
detector sensitivity has weakened or interfer-
ometer is out of adjustment due to shock etc.)
...
... contact the Bruker service. (See
appendix I.)
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TROUBLESHOOTI NG
Vol t age St at us LEDs
ALL VOLTAGE STATUS LEDS ARE OFF
ONE VOLTAGE STATUS LED I S OFF
Spectrometer is not turned on. Turn on the spectrometer using the mains
switch.
Power cord is not connected. Connect the power cord to the power outlet as
well as to the appliance inlet connector.
No voltage is applied. Check whether the proper voltage is applied at
the outlet to which the spectrometer is con-
nected.
Defective fuse. Replace the fuse as described in chapter
Maintenance and Repair, section Replacing
the Fuses.
Short circuit in the power supply unit. Typically, a short circuit is accompanied by a
ticking sound in the power supply unit. Dis-
connect the power supply unit immediately.
If there are additional external circuitry con-
nected to the CAN bus or the MPE port, dis-
connect them and try it again. If this measure
solves the problem the external circuitry has
caused the short circuit. Otherwise, it is an
internal problem of the spectrometer electron-
ics. Contact the Bruker service. (See
appendix I.)
Defective power supply unit. If the voltage status LEDs do not light cor-
rectly, probably the power supply unit needs to
be replaced. If they do not light at all, contact
the Bruker service. (See appendix I.)
An external device shortens the power supply
unit.
Disconnect all external devices from the CAN
bus or the MPE port and try it again.
Temporary short circuit in the spectrometer. Switch off the spectrometer, wait about 30 sec-
onds and switch it on again. After the initializa-
tion cycle the STATUS LED will turn to green.
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TROUBLESHOOTI NG
ERR LED
Generally, a red ERR LED indicates a scanner malfunction, i.e. all components and/or
conditions that are involved in the scanner functioning (laser, beamsplitter, air bearing
pressure etc.) can cause a red ERR LED.
A defective LED. In this case, there is no spectrometer malfunc-
tion and the spectrometer operates properly.
Only the defective LED needs to be replaced.
If the laser is the cause of the problem either
the laser beam is blocked or the laser tube is
not orientated correctly or the laser is defec-
tive.
Note: These causes are also indicated by a red LASER
LED.
Blocked laser beam: Contact the Bruker ser-
vice. (See appendix I.)
Incorrect laser tube orientation: Correct the
laser tube orientation as shown in fig. 48. See
chapter Maintenance and Repair section
Defective laser: Order a replacement laser
module. (For the order number refer to
appendix B.) After the receipt, replace the
laser module. (See chapter Maintenance and
Repair, section Replacing the Laser Module.)
In case the beamsplitter is the cause of the
problem either:
no beamsplitter is installed in the operating
position or
the beamsplitter is not locked properly or
it is damaged or
has become opaque.
Note: The second cause is also indicated by the instru-
ment status message BMS door is open.
Install a beamsplitter in the operating position
or check whether the beamsplitter is locked
properly (i.e. the release lever (fig. 34) has to
be in the front position. (See chapter Opera-
tion, section Exchanging the Beamsplitter.)
In case of an opaque or damaged beamsplitter
replace it as described in chapter Operation,
section Exchanging the Beamsplitter.
Note: Probably you need to order a replacement beam-
splitter.
Strong mechanical shocks have caused a per-
manent optics misalignment.
7
TROUBLESHOOTI NG
The SR LED l i ght s per manent l y
The SR LED indicates whether the instrument is busy and not available for communica-
tion.
No Dat a Tr ansf er bet ween Spect r omet er and Comput er
In this case the troubleshooting procedure depends on the connection topology. The
default connection (stand-alone configuration) is established using a crossover cable
between the PC and the spectrometer 10Base-T Ethernet port (see appendix E,
figure 79). Alternatively, the spectrometer can be connected directly to an Ethernet net-
work using the 10Base-T port. The direction of the data transfer is indicated by the RX
and TX LEDs on the spectrometer rear side. The TX LED lights during the spectrometer
sends data and the RX LED lights during the spectrometer receives data.
THE GREEN RX LED DOES NOT LI GHT AT ALL
This indicates a problem with regard to the physical connection between the spectrome-
ter and the PC or the network.
Spectrometer is still in the initialization phase.
(In this case, there is no spectrometer prob-
lem.)
After having switched on the spectrometer wait
about one minute until the initialization proce-
dure is completed.
Spectrometer control hangs. Reset the spectrometer using the reset button
(R in fig. 82) at the spectrometer rear side and
wait for initialization to terminate. If this mea-
sure does not solve the problem, contact the
Bruker service. (See appendix I.)
Wrong cable type is used. To connect the spectrometer directly to the PC
use a CAT 5 crossover cable for the 10Base-T
Ethernet standard.
To connect the spectrometer to an existing
network use a regular CAT-5 10Base-T cable
(ask your network administrator).
Defective cable or unstable connection. Check the RJ-45 connection to the Ethernet
port (ETH) and at the other end of the cable.
Replace the cable, if necessary.
Spectrometer does not start up. Check the main power supply. At least the volt-
age status LEDs +5V, +12V and -12V must
light when the spectrometer is switched on.
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TROUBLESHOOTI NG
DURI NG THE CONNECTI ON ESTABLI SHMENT THE
GREEN RX LED LI GHTS BUT THE YELLOW TX LED
DOES NOT
There is no logical connection between the spectrometer and network or computer.
Wrong IP address has been assigned to the
spectrometer.
Assign the correct IP address to the spectrom-
eter. You find the correct IP address on a label
on the spectrometer rear side. (See figure 82.)
For detailed information refer to appendix E.
TCP/IP settings mismatch between spectrom-
eter and computer/network.
Refer to appendix E.
7
TROUBLESHOOTI NG
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SPECI FI CATI ONS A
Spect r omet er
Parameter Specification
Weight approx. 105kg (depends on the individual instrument configuration)
Dimension 85cm (W) x 71cm (D) x 32cm (H)
Power
Consumption
Spectrometer: 100 - 240 VAC 10%; 50 - 60 Hz; 80W typical, 180 W max.
Vacuum pump: approx. 500 W
Complete power consumption (but without data station): ca. 700 W
VERTEX 70v is a protection class I product.
Spectral Range standard:
With the standard optical components (KBr beamsplitter, DLaTGS detector and
MIR source) the following spectral range is achieved:
Middle IR: 8,000 to 350cm
-1
optional:
With the corresponding optional optical components, the following spectral
ranges can be achieved:
Far IR/THz: 680 to 10cm
-1
Near IR: 15,500 to 4,000cm
-1
UV/VIS: 28,000 to 9,000cm
-1
Spectral Resolution
standard: better than 0.4cm
-1
(apodized)
optional: better than 0.2cm
-1
(apodized)
Wavenumber
Accuracy
better than 0.01cm
-1
@ 2,000cm
-1

Photometric
Accuracy
better than 0.1% T
Scan Speed standard: 0.1 to 3.75 cm/sec (opd - optical phase difference)
optional: 0.1 to 10 cm/sec (opd - optical phase difference)
Environmental
Conditions
Operational temperature range of VERTEX 70v: 18 - 35C (64 - 95F)
In case the vacuum pump is operated with installed noise reduction
hood ensure the ambient temperature does not exceed 32C (90F).
Temperature variation: max. 1C per hour and max. 2C per day
Humidity (non condensing): 80% (relative humidity)
Installation site: in a closed room, max. 2000m above sea level
Overvoltage category: II
Degree of pollution: 2

A
SPECI FI CATI ONS
Detector standard: High sensitivity DLATGS detector with KBr window
optional: various detectors for measurements in the NIR, MIR, FIR, UV and
VIS region (See also chapter Overview.)
Laser VERTEX 70v is a laser class 2 product containing a laser class 2 laser
according to EN 60825-1/10.2003.
Divergence angle: 1.77 mrad 5%
Interferometer Permanently aligned RockSolid interferometer
Sample
Compartment
25.0cm (W) x 27.0cm (D) x 16.0cm (H)
Optionally, the evacuable and purgeable sample compartment can be sepa-
rated from the optical bench by KBr windows mounted on either the flaps or the
sample compartment walls.
Electronics Microprocessor-controlled optics bench with digital speed control, system diag-
nostics, advanced system check, 80 kHz A/D converter with 24 bit dynamic
range. Industry standard Ethernet connection
Housing Vacuum-tight cast aluminum housing
Vacuum Evacuable below 0.2mbar
Parameter Specification
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CONSUMABLE SPARES B
Spar e Par t s - St andar d Component s
Spar e Par t s - Opt i onal Component s
Part # Description
Q 328/7 MIR source, mounted, 12 V, replacement unit
Q 101/B HeNe laser module (laser tube plus laser power supply unit)
Part # Description
Q 428/7 NIR source with QuickSwitch mount, 12 V
average lifetime > 9000 hours
Q 402 NIR source (24V, 150W), connected externally and water-cooled
Q 302 MIR source (24V, 150W), connected externally and water-cooled
Q 202/6 FIR source (Hg-arc), connected externally and water-cooled
B
CONSUMABLE SPARES
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DEFAULT PARAMETER C
Note that depending on the spectrometer configuration, different default parameter sets
may apply. In the following table you will find a list of the measurement parameters that
apply to the standard spectrometer configuration (MIR). Select in the OPUS Measure
menu the Select Measurement Parameters function and enter following measurement
parameters.
Advanced Parameters Settings
Resolution 4
Sample/Background Scan Time 6 scans
Save Data from 7500 to 400cm
-1
Result Spectrum Transmittance
Data Blocks to be saved Transmittance and Single Channel
Optics Parameter Settings
Source Setting MIR source (#1)
Beam splitter KBr
Optical Filter Setting open
Aperture Setting 6mm
Sample/Background Measurement
Channel
Sample Compartment
Detector Setting RT-DLaTGS (#1)
Scanner Velocity 10 kHz
Sample Signal Gain automatic
Background Signal Gain automatic
Delay after Device Change 3
Delay before Measurement 0
Acquisition Parameters Setting
Wanted High Frequency Limit 15.500cm
-1
Wanted Low Frequency Limit 0cm
-1
C
DEFAULT PARAMETER
The OPUS software provides the option to set the optics parameters Source Setting,
Detector Setting and Measurement Channel also interactively using the schematic pre-
sentation of the beam path. To do this, click in the Setup Measurement Parameters dia-
log box on the Beam Path tab. The following window opens:
To select the detector position 2, for example, place the cursor on this detector so that
the label Detector 2 occurs and double-click on this position. The setting will switch to
detector 2. See figure 67. As soon as you click on the Check Signal tab the spectrome-
ter implements the settings.
High Pass Filter open
Low Pass Filter 10kHz
Acquisition Mode Double Sided - Forward/Backward
Correlation Mode OFF
FT-Parameters Settings
Phase Correction 32cm
-1
Phase Correction Mode Power Spectrum
Apodization Function Blackman-Harris3-Term
Zerofilling Factor 2
Advanced Parameters Settings
Figure 66: OPUS Dialog Window - Beam Path
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DEFAULT PARAMETER
In this way, you can also change the Source Setting and Measurement Channel.
Note: The parameters you have set in the schematic presentation of the
beam path are realized automatically by the software also in the
corresponding fields on the Optics page and vice versa.
Figure 67: Changing the Detector Position interactively
C
DEFAULT PARAMETER
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DI MENSI ONAL DRAWI NGS D

Figure 68: VERTEX 70v - Isometric View
D
DI MENSI ONAL DRAWI NGS
Figure 69: VERTEX 70v - Top View
Figure 70: VERTEX 70v - Top View Showing Sample Compartment Dimensions
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Figure 71: VERTEX 70v - Right Side View
Figure 72: VERTEX 70v - Left Side View
D
Figure 73: VERTEX 70v - Front View
Figure 74: VERTEX 70v - Rear View
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Figure 75: VERTEX 70v - Sample Compartment Interior (Right Side View)
Figure 76: VERTEX 70v - Sample Compartment Interior (Front View)
D
Figure 77: VERTEX 70v - Sample Compartment Interior (Top View)
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CONNECTI NG VERTEX 70V TO PC E
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The connection of the spectrometer to a PC involves the following steps:
1 Defining a connection topology
2 Defining the corresponding network addresses
3 Assigning the network addresses
4 Checking the connection
Depending on the connection typology, two different data cable types are required:
Data cable type
For realizing the following
connection topology
Included in the delivery
scope
crossover cable
1. Stand-alone topology, i.e. spec-
trometer is connected to a
stand-alone PC. See fig. 79.
2. Spectrometer is connected to a
network computer. See fig 81.
Yes (1 piece)
straight through cable
1. Spectrometer and PC are con-
nected to a network. See fig. 80.
2. Spectrometer is connected to a
network computer. See fig 81.
No
Note: A straight data cable, category
5, with RJ45 plugs for the Ethernet
standard 10Base10 is required.
1
2
3
6
1
2
3
6
1
2
3
6
1
2
3
6
Straight through cable
Crossover cable
Figure 78: Schematic presentation of the different data cable types
E
CONNECTI NG VERTEX 7 0 V TO PC
Possible Connection Topologies
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POSSI BLE CONNECTI ON TOPOLOGI ES
Basically, the following connection topologies are possible:
Connecting the spectrometer directly to a stand-alone PC (It is the standard
connection topology.) See fig. 79.
Connecting both the spectrometer and PC to a network. See fig. 80.
Connecting the spectrometer to a network computer. See fig. 81.
a) Conf i gur at i on f or st and- al one Oper at i on ( St andar d)
The spectrometer is connected directly to the standalone computer, i.e. neither the PC
nor the spectrometer is connected to a network.
By default, the supplied PC is equipped with two network interface cards labelled
OPTIC CONECTOR and LAN. For the stand-alone configuration, connect the crossover
cable to the OPTIC CONNECTOR at the PC rear side. See figure 79.
Advantages:
Easy to install.
Full bandwidth available for data transfer between the spectrometer and PC.
No access conflicts with other PCs that try to access the spectrometer as well.
No data transfer rate problems.
Disadvantages:
No remote access to the spectrometer from other PCs on which OPUS is
installed.
No computer network connection.
A local printer is required to print out the measurement results.
Spectrometer
10.10.0.1
PC
Crossover cable

OPTIC CONNECTOR
10.10.0.100
Figure 79: Stand-alone Configuration of the Spectrometer
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CONNECTI NG VERTEX 70 V TO PC
b) Connect i ng bot h Spect r omet er and PC t o a Net wor k:
Both the spectrometer and the PC, on which the OPUS software is installed, are con-
nected directly to the network.
OPTIC CONECTOR and LAN. For this connection topology, connect the straight
through cable(s) to the LAN connector at the PC rear side. See figure 80.
Advantages:
Remote access to the spectrometer via the internet or the intranet is possible.
The PC can access to all network resources (provided that you have the
corresponding access right).
Disadvantages:
Data cables are required which are not included in the delivery scope of the
spectrometer. They have to be provided by your network administrator.
Only a fraction of the bandwidth is available for the data transfer between the
spectrometer and the PC. Due to data transmission delays, the measurement time
may increase.
Access conflicts caused by other PCs that try to access the spectrometer as well.
Your network administrator must be involved in configuring the connection.
PC 1 Spectrometer
Straight through Cables
PC 2
Hub

LAN LAN
Figure 80: Integration of the Spectrometer into a 10Base-T Ethernet Network
E
c) Connect i ng t he Spect r omet er t o a Net wor k Comput er :
This topology combines the advantages of the other two connection topologies, but it
requires additional hardware (straight trough cable).
OPTIC CONECTOR and LAN. For this connection topology, connect the crossover
cable to the OPTIC CONNECTOR and the straight through cable to the LAN connector
at the PC rear side. See figure 81.
Advantages:
Full bandwidth is available for the data transfer between the spectrometer and PC.
Remote access to the spectrometer via internet or intranet is possible (provided
that you have the corresponding access rights).
The PC has access to all network resources (provided that you have the
corresponding access rights).
Different data transfer rates for the data exchange between the spectrometer
(10Base-T) and the network (no restriction) are possible.
Disadvantages:
For connecting the PC to a hub, a straight through data cable is required which is
not included in the delivery scope of the spectrometer. It has to be provided by
your network administrator.
Your network administrator must be involved in configuring the connection.
Spectrometer PC 1
Straight through cable
Hub
Crossover cable

LAN
OPTIC
CONNECTOR
Figure 81: Integration of the Spectrometer into a 10Base-T Ethernet Network via a PC
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Selecting Network Addresses
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
SELECTI NG NETWORK ADDRESSES
Depending on the connection topology, use the following network addresses:
a) Net wor k Addr esses f or t he St and- al one Oper at i on:
Spectrometer: IP-address 10.10.0.1
Subnet Mask 255.255.255.0
Gateway 0.0.0.0 (no entry in case of Windows 2000 or XP)
PC: IP-address 10.10.0.100
The delivered spectrometer and the delivered PC are factory-configured for the
stand-alone operation, i.e. all network addresses for a stand-alone operation are
already assigned, provided that you have acquired the PC by Bruker.
b) Net wor k Addr esses f or connect i ng bot h Spect r omet er
and PC t o a Net wor k:
For this connection topology, both the spectrometer and the PC must have a unique
IP address. These addresses depend on your intranet and have to be assigned by your
network administrator. To ensure that the spectrometer can be accessed via internet
also a gateway address has to be assigned. The gateway links your intranet domain to
other domains (e.g. domains being part of the internet). Otherwise, set the gateway
address to 0.0.0.0. In case of the operating system Windows 2000 or XP do not specify
a Gateway.
Note: A wrong IP address can cause problems with other devices
connected to the network.
c) Net wor k Addr esses f or Connect i ng t he Spect r omet er t o
a Net wor k Comput er
This connection topology requires two network interface cards and three addresses
sets: the first set for the spectrometer, the second for the network interface card com-
municating with the spectrometer and the third for the network interface card linking the
computer to the intranet.
Spectrometer: IP-address 10.10.0.1
PC and network interface card connected to the spectrometer:
IP-address 10.10.0.100
PC and network interface card connected to the network/hub:
IP-address assigned by your network administrator
Subnet Mask assigned by your network administrator
Gateway assigned by your network administrator
E
Assigning Network Addresses
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
ASSI GNI NG NETWORK ADDRESSES
This section describes how to assign an IP address to an instrument, not yet config-
ured, using the FCONF program (Firmware Configuration). The program is part of the
OPUS software. You will find it in the OPUS directory or directly on the OPUS CD.
Note: Among other things, the FCONF program also allows for updating the
spectrometer firmware. These program options are described in
detail in appendix G.
Start the FCONF program.

Select the option Modify IP settings and click on the Next button.
Accept the settings by clicking on the Next button.
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Activate the radio button Assign a new address to the spectrometer and click on
the Next button.
The IP address assignment window opens:

Specify the MAC address (Media Access Control), the IP address and the
gateway address. The Help buttons provide information on what to enter in the
different lines.
The MAC address is the unique hardware name of the network interface adapter
installed inside the spectrometer. You will find this address on the label at the
spectrometer rear side (see the above figure.). In this example, the MAC address
is 00 00 AD 02 AC 11. Enter this code into the first line of the IP assignment
window.
E
If this label is missing or the MAC address proves to be incorrect, you will find this
address also on a label inside the electronics unit. It is placed on the black 26-pole
connector at the EWS15-board.
Note: Always keep the MAC address on the label at the spectrometer rear
side up to date! Ensure that the MAC address on the label is legible.
The entries for the remaining three lines depend on the chosen connection
topology. For more information see section Selecting Network Addresses. The
default entries are shown in the above figure. Use them for the direct connection
of the spectrometer to the PC. After entering all addresses, click on the Next
button.
Now you are asked to set the spectrometer into BootP-mode. Follow the
instructions on the screen.
Note: The reset button (R in figure 82) is on the spectrometer rear side.
When the spectrometer is in BootP mode, click on the Next button to start the
procedure. Otherwise, the BootP-mode will be canceled automatically after 2
minutes.
The assigning process starts immediately and may take several minutes.
After a successful completion, a message appears and the spectrometer reboots
automatically.
Now the spectrometer starts up with the newly assigned IP setting and can be
accessed by the computer.
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Checking the Connection
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CHECKI NG THE CONNECTI ON
To check the connection you can use either the internet explorer provided as part of
Windows or any other internet browser program installed on your PC. Proceed as fol-
lows:
2 Wait about one minute to allow the spectrometer to boot. A dark SR LED (P
in figure 82) indicates that the spectrometer is ready.
3 Start your internet browser.
4 Check that the internet browser is not in offline mode. In case of the
Microsoft Internet Explorer, the offline mode is indicated by a tick in front of
Offline Mode in the File menu of the browser.
5 Ensure that the internet browser does not use a proxy server, or at least not
for addresses of direct access in the 10.10.x.x.-range. In case of the
Microsoft Internet Explorer, you can check this by selecting the Internet
Options function in the Extra browser menu. Click on the Connections tab.
Then, click in the LAN-Settings group field on the Settings button.
6 Enter the IP address of the spectrometer in the corresponding browser entry
field (for stand-alone configuration: 10.10.0.1).
7 Press the enter button.
Now the Internet Explorer should display the home page of your spectrometer.
In case the Internet Explorer shows a blank page and is not able to access the
instrument home page, check the IP address you have just assigned for correct
spelling. If the problem is persistent, refer to chapter Troubleshooting.
E
Checking the Connection
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
ELECTRONI CS AND POWER SUPPLY F
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
ELECTRONI CS PANEL
The electronics panel at the spectrometer rear side includes cable connections (e.g.
Ethernet connection) and LEDs. The LEDs serve for instrument diagnostics purposes.
Each LED indicates a specific operating state (e.g. interferometer mirror movement,
data transfer).
Figure 82: Electronics Panel
B
C
D
E
J
K
L
M
N
O
P
Q
R
F
G
H
I
S
T
U
A
V
F
ELECTRONI CS AND POWER SUPPLY
Electronics Panel
TRG PORT
The 15-pin TRG port (A in figure 82) is intended for the connection of a triggering
device. This port is only used in conjunction with the Step Scan option for step scan and
time-resolved measurements. (The abbreviation TRG stands for Trigger.) (For detailed
information refer to the Step Scan Manual.)
EDI S PORT
The EDIS port (B in figure 82) has no function at the moment. (The abbreviation EDIS
stands for External Display.)
PORT DDC 1/ 2/ 3/ 4
The ports DDC 1 to 4 (C, G, I and N in figure 82) are versatile ports to connect external
optical modules and detectors. These ports include a complete CAN-Bus, transmits all
required remote trigger signals and establishes a complete connection to DDC (Digital
Detector Connection) compatible detectors. (Note that the DDC 4 port can not be used
if a detector is connected to the DDC 4 port inside the spectrometer. In this case, a cap
is fixed to the DDC 4 port.)
CR, CY AND CG LEDS
These LEDs (D, E and F in figure 82) are status and diagnose LEDs for the step scan
option. They indicate the status of the controlling device. (The abbreviation CR stands
for Controller Red, CY for Controller Yellow and CG for Controller Green.) (For
detailed information refer to the Step Scan Manual.)
LAS TEST
The port LAS TEST (H in figure 82) is intended for service and diagnostic purposes
only. Do not connect a device to this port!
COM1 PORT
The COM1 port (J in figure 82) is technically similar to a conventional, PC-compatible
serial port, however, it does not have the complete functionality like serial port of a PC.
It is only used for special applications.
ERR LED
The red ERR LED (K in figure 82) indicates an interferometer error (e.g. a missing laser
signal). As long as this LED lights, data acquisition is not possible. See chapter 7 for
troubleshooting.
FWD LED
The yellow FWD LED (L in figure 82) indicates the current interferometer mirror move-
ment. As long as the interferometer mirror moves forward this yellow LED lights. During
the backward movement the LED does not light. Thus, the LED flashes in the rhythm of
the interferometer mirror forward and backward movement. This rhythm depends on the
chosen measurement parameters (e.g. resolution and velocity). (The abbreviation FWD
stands for forward.)
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Electronics Panel
TKD LED
The green TKD LED (M in figure 82) indicates that the interferometer mirror is within the
data acquisition range. Typically, it flashes with twice the frequency and synchronous to
the FWD LED. During data acquisition the light intensity changes to bright green. (The
abbreviation TKD stands for take data.)
LPT1 PORT
This parallel port (O in figure 82) is reserved for diagnostic purposes. Do not connect
any device to this port! (The abbreviation LPT stands for Line Printer.)
SR LED AND SG LED
These 2 LEDs (red SR LED and green SG LED, P and Q in figure 82) indicate the inter-
nal operating state of the spectrometer communication processor. See also chapter 7.
(The abbreviation SR stands for Status Red and SG for Status Green.)
RES BUTTON
The spectrometer is equipped with a reset button (R in figure 82) similar to the one you
know from a PC. Pressing this button longer than 1 second resets the spectrometer
without the need to turn it off. The effect is identical to switching the spectrometer off
and on again. In addition, this button can be used to assign an IP address to the spec-
trometer. Refer to appendix E.
TX LED AND RX LED
These LEDs (S and T in figure 82) indicate the data transfer between the spectrometer
and the data system via the Ethernet connection. In case of the stand-alone configura-
tion, the green RX LED signals that the spectrometer receives data. In case the spec-
trometer is connected to an Ethernet network, the green RX LED indicates that a data
packet is transmitted on the Ethernet (this does not necessarily mean that the data
packet is destined for the spectrometer!)
The yellow TX LED lights if the spectrometer transmits a data packet. This indicates
that the spectrometer is accessed by a computer.
Note: Use these LEDs to test the operational reliability of the Ethernet
connection.
10BASE- T ETHERNET PORT
The ETH port (U in figure 82) is primarily used to connect the spectrometer to a com-
puter on which the application software (e.g. the OPUS software) is installed. The spec-
trometer can be connected either to a 10Base-T intranet or directly to the computer
using a crossover cable (stand-alone configuration). This is a standard cable in which
the TX and RX lines are cross-linked.
F
Power Supply Panel
VERTEX 70v is factory-configured for stand-alone operation. The IP address is on a
label on the spectrometer rear side. The Ethernet port (ETH) is designed for RJ-45
plugs and complies with the 10Base-T standard. Use a CAT 5 cable (SSTP) to realize
the connection; the cable length should not exceed 100 meters. Alternatively, a gateway
can be used to connect the spectrometer to the internet. In this case a unique
IP address must be assigned to the spectrometer. For detailed information on how to
assign an IP address refer to appendix E.
Note: Keep in mind that the interface speed is 10 Mbit/s. In this case a
100BASE-T connection does not work!
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POWER SUPPLY PANEL

A
B
C
Figure 83: Power Supply Panel
D
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Power Supply Panel
VOLTAGE STATUS LEDS ( +5V, +12V, - 12V)
These LEDs (A in figure 83) indicate the state of the secondary voltages of the electron-
ics unit.
Note: A dark power supply LED indicates a major electronics problem.
CAN BUS PORT
The CAN bus port (B in figure 83) is primarily used to connect external automated units
(e.g. sample changer, moving mirror unit, etc.) to the spectrometer. The CAN bus also
provides power to these units. Thus, most external units can be operated without
connecting them to the power supply. Furthermore, the CAN bus can be used as a
communication link to control these external units via the spectrometer. (The
abbreviation CAN stands for Controller Area Network.)
MAI NS SWI TCH
The mains switch (C in figure 83) is used to switch the spectrometer on and off. This
switch interrupts the primary voltage supply.
PRI MARY POWER RECEPTACLE
Connect the supplied power cord to the primary power receptacle at the spectrometer
rear side (D in figure 83) as well as to the mains socket outlet.
POWER CORD
Replace the power cord if there are any visible signs of insulation, connectors or cable
damage. Do not repair it! Replace the power cord only with cords rated for at least
250VAC, 10A. The cord must have approbation of at least your local authority, UL for
US, CSA for Canada or VDE for Europe.
F
Power Supply Panel
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FI RMWARE UPDATE G
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
The spectrometer firmware needs to be updated in order to make new features (e.g. a
higher scanner velocity) available. It is updated using the FCONF program (Firmware
Configuration Tool). This program performs automatically all the necessary actions.
The FCONF program facilitates:
updating the firmware,
restoring a previous firmware version,
backing up the current firmware version,
initializing the firmware (For service purposes only!),
modifying IP settings (See appendix E, section Assigning Network Addresses.),
running a custom script (For service purposes only!).
Firmware updates are typically delivered on CD or by e-mail. If the firmware update has
been delivered on a CD start the FCONF program directly from the CD by double-click-
ing on the fconf.exe file and proceed as described below. If the firmware update has
been delivered via e-mail, store the delivered files into a temporary directory, start the
FCONF program by double-clicking on the fconf.exe file and proceed as described
below.
After having double-clicked on the fconf.exe file, the following window appears:

G
FI RMWARE UPDATE
Updating the Firmware
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
UPDATI NG THE FI RMWARE
To update the firmware, proceed as follows:
Activate the Update firmware option button and click on the Next button. The
following window appears:
If there is no reason why another directory (run folder) than the displayed default
directory should be specified, accept the default directory by clicking on the Next
button. The following window appears:
In this window you have to specify the spectrometer of which the firmware is to be
updated. To do this, activate the Enter custom address option button and enter the
corresponding IP address in dotted notation.
Note: In case of a stand-alone operated instrument, the default IP address
is 10.10.0.1. If the spectrometer is integrated into a network and
therefore the operating company has assigned a different than the
default IP address you will find it at the spectrometer rear side. In this
case, it is the operating companys duty to inscribe the IP address on
the provided label at the spectrometer rear side.
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FI RMWARE UPDATE
Updating the Firmware
After having entered the IP address, check whether the intended spectrometer is
addressed by clicking on the Beep button. The addressed spectrometer will beep
shortly three times.
Click on the Next button. The following window will appear:
Press the Finish button to start the update procedure.
Note: The update procedure may take several minutes, depending on the
available bandwidth and the amount of files to be updated.
During the update procedure, a log window is displayed showing all actions performed
by the FCONF program. (The log-file is stored in the same directory as the backup
files.)
At the end of the update procedure, the FCONF program resets the spectrometer (tell-
ing it in the log window: Resetting the spectrometer... done.). After a successful spec-
trometer initialization, the firmware version is displayed in the log window.
G
FI RMWARE UPDATE
Restoring a previous Firmware Version
After the firmware updating has been completed successfully, the following message
appears:

Click on the OK button of the message window and on the Close button of the log
window.
Note: The delivered Firmware update performs automatically all the actions
necessary to properly replace the existing firmware version by the
new one. It also generates automatically backup information to allow
the restoration of the previous firmware version, in case the new
firmware version does not ensure a trouble-free operation. For
information on how to restore a previous firmware version refer to
the next section.
Note: In case of error during the update procedure, the FCONF program
terminates the procedure and proposes to restore the previous
firmware version.
RESTORI NG A PREVI OUS FI RMWARE
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
VERSI ON
Restoring a previous firmware version is only possible if an update has been performed
from that PC before.
To restore the previous firmware version, proceed as follows:
Activate the Restore previous firmware option button and click on the Next button.
The following window appears:

.

.

.

.

.
FI RMWARE UPDATE
Backing up the current Firmware Version
The FCONF program asks you to select the directory containing the backup
information of the last firmware version (previous run folder). By default, this
directory is displayed automatically.
Note: If you click on the View Log button a log window appears displaying
detailed information about the last update including errors, warnings
or other irregularities.
Press on the Next button.
In the next window you are asked to specify a directory for the backup files of the
restoration procedure. It is recommended to accept the directory proposed by the
FCONF program.
The rest of the restoration procedure is identical to the update procedure
described above.
BACKI NG UP THE CURRENT FI RMWARE
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
VERSI ON
To backup the current firmware version, proceed as follows:
Activate the Backup current firmware option button and click on the Next button.
The following backup procedure is identical to the update procedure described
above.
G
FI RMWARE UPDATE
Backing up the current Firmware Version
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
SAMPLE PREPARATI ON H
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Proper sample preparation is crucial to obtain good and meaningful spectra. This sec-
tion describes several sample preparation technique that cover a wide range of sam-
ples. It will give you some help in choosing the most suitable sample preparation
technique for a given sample.
The adequate sample preparation technique depends on the state of aggregation and
the spectral absorptivity of the sample. Regardless of the state of aggregation, the sam-
ple material has to be homogeneous because variations in concentration or composition
within the sample area to be analyzed can result in misleading or erroneous data.
Sometimes the trial-and-error procedure is required to obtain an acceptable spectrum.
St at e of Aggr egat i on
Depending on the state of aggregation of the sample, there are different sample prepa-
ration and measurement techniques. If you have to analyze a solid sample you can
either prepare a solution, a Nujol mull or a KBr pellet. Liquid samples can be analyzed
either as a thin film between plates or in a liquid cell. Gaseous samples require dedi-
cated cells with different path lengths.
Absor pt i vi t y
The absorptivity of the sample is a critical factor in choosing a suitable sample prepara-
tion method. To get a meaningful spectrum of a strongly absorbing sample, the sample
has to be either:
very thin or
diluted by a solvent or powder that is not strongly absorbing.
According to Beers Law, the absorbance (i.e. peak intensity) in an absorbance spec-
trum is directly proportional to the component concentration in the sample, pathlength of
the sample and the absorptivity.
A bC =
H
SAMPLE PREPARATI ON
General Information
If the absorbance A (i.e. peak intensity) is too strong, decrease the sample concentra-
tion C by diluting it or diminish the pathlength b by reducing the sample thickness. If the
absorbance A (i.e. peak intensity) is too weak, increase the sample concentration C or
the pathlength b correspondingly to obtain a reasonable peak intensity.
To find out whether a sample is strongly absorbing in the wavelength range of interest
or not you have to acquire a test transmission spectrum. The figure below shows a
transmission spectrum of a strongly absorbing sample.
Symbol Description Typical Units
A Absorbance at a given wavelength None
Molar absorptivity (a proportionality constant)
l
.
mol
-1.
cm
-1
b
Pathlength of the sample (cell length for sam-
ples in a cell or sample thickness for films,
pressed pellets)
cm
C Component concentration in the sample mol/l)
Figure 84: Transmission Spectrum of a strongly absorbing Sample
Regions of total
Absortion
.

.

.

.

.
SAMPLE PREPARATI ON
Sample Preparation Techniques
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
SAMPLE PREPARATI ON TECHNI QUES
There is a large number of possible sample preparation techniques. For lack of space,
however, not all possible techniques can be described in detail in this chapter. There-
fore, we restrict our explanations only to the most common techniques. (For more
detailed information about this topic refer to the relevant specialist literature
1
.) More-
over, we give you a general guideline for choosing the adequate sample preparation
technique.
To find the most adequate method we recommend trying several sample preparation
techniques and acquiring spectral data. On the basis of these data, you can assess
which sample preparation technique is the most suitable one for your application. In
case of doubt ask your application specialist.
Some of the most common sample preparation techniques are:
No sample preparation (e.g. self supporting film or measurement using a micro-
ATR accessory)
Thin film of liquid sample solution between two IR-transparent
2
plates
Preparing a solution
Preparing a Nujol mull
3
Pressing a KBr pellet
Liquid cell and gas cell
Note: Most of the described sample preparation techniques involve the use
of hygroscopic materials (such as NaCl or KBr), i.e. if these materials
come in contact with water or alcoholic solvents, they begin to
dissolve or become cloudy and thus, impair the measurement
results. Therefore, avoid all sources of water and even alcohols
(ethanol and methanol).
No Sampl e Pr epar at i on
The easiest samples to analyze are film and polymer samples with a thickness of less
than approx. 100 micrometers. They can be simply placed in a magnetic holder and
immediately scanned. The same procedure can be used for samples which can be
sliced to an appropriate thickness.
A large number of solid and liquid samples can also be analyzed without requiring a
preparation using a micro-ATR accessory. Attenuated Total Reflectance (ATR) units are
a very versatile accessory for FT-IR measurements. In many cases, the micro-ATR unit
can be used for liquid and semi-liquid materials instead of the constant path transmis-
1. e.g. Gnzler, Helmut / Gremlich, Hans-Ulrich (2002): IR Spectroscopy - An Introduction. Weinheim:
WILEY-VCH Verlag.
2. i.e. IR-transparent within the frequency range of interest
3. A mull is a mixture (more precisely a suspension) of two substances, one of which (i.e. the sample)
is finely divided and dispersed in the other (e.g. the paraffin oil Nujol).
H
SAMPLE PREPARATI ON
sion cells and the salt plates. In addition, this measurement accessory can also be used
for analyzing polymer films, pastes and powders. Due to the reproducible effective path-
length, they are well suited for both qualitative and quantitative analyses. Depending on
the sample material and the objective of the analysis, there are different ATR-crystal
materials (e.g. ZnS, ZnSe, Ge and diamond). The sample penetration depth ranges
between 0.1 and 2m and depends on the wavelength, the refractive index of the ATR-
crystal material and the incidence angle of the beam. (For more information about
attenuated total reflectance refer to the respective specialist literature.)
Thi n Fi l m bet ween t wo Pl at es
Preparing a thin film of a liquid sample between two IR-transparent plates is an easy
sample preparation method. Choose this method if your sample is either a liquid or an
oil. An advantage of this method is that only a small amount of the sample is required.
Apply a drop of the sample on one of the plates using a pipet.
Place a second plate on the top and make a quarter turn to obtain a nice even film
of the liquid sample. Sandwich the plates carefully together to remove all air
bubbles. Note that these plates are very fragile and can break easily. (The space
between the two plates is very small (typically < 0.01mm).
If the sample amount proved to be too much, separate the plates, wipe one side
clean and fit the plates together again.
Slot the plates in the sample holder of the spectrometer and start the
measurement.
Note: The plates (made of NaCl or KBr) are extremely moisture sensitive.
Therefore, do not use samples that contain water, keep the plates
always dry, clean them only with chloroform or high purity acetone
and polish them carefully after each use. In the course of time they
will absorb moisture from the atmosphere and deteriorate. Therefore,
proper storage (e.g. in an exicator) is extremely important.
Sol i d Sampl e as Sol ut i on
Use this sample preparation method if your sample is a soluble solid (e.g. a soluble
powder). To obtain an IR spectrum, you have to prepare a concentrated solution of your
sample using a suitable solvent. The concentration of the solution needed for a good
spectrum depends on the sample.
Dissolve the sample or sample powder in a solvent and apply the sample solution
between two support plates, as described above. Depending on the available
amount of sample material you can either apply a small amount of your sample
powder directly on the plate and add one drop of the solution or dissolve the
sample in a test tube and apply the solution with a pipet on the plate.
A second variant is to apply the sample solution on an IR-transparent plate and
allow the solvent to evaporate leaving a thin sample film on the plate. Then, slot
the plate in the sample holder of the spectrometer and start the measurement.
.

.

.

.

.
SAMPLE PREPARATI ON
A third variant is to fill the sample solution in a liquid cell and acquire a sample
spectrum. To acquire a background spectrum measure the liquid cell containing
only the solvent. The volumes of these liquid cells are between 0.1 and 1ml.
Microcells with a much lower capacity are also available.
Do not forget to acquire a background spectrum from the solvent as well.
Note: The plates (made of NaCl or KBr) are extremely moisture sensitive.
(See above.)
The major problem in preparing a solution is choosing an appropriate solvent. Most sol-
vents have a strong absorptivity and so their absorption bands will superimpose those
of the solute. Therefore, you have to ensure that the used solvent is not strongly
absorbing in the wavelength range of interest. Use only spectrophotometrically pure sol-
vents and solvents that are not infrared active in the spectral region of interest.
No solvent is perfect but if some information about the sample is known, the solvent can
be chosen accordingly. Commonly used solvents are carbon tetrachloride, carbon disul-
phide, chloroform, cyclohexane, acetonitrile, and tetrachloroethylene. Never use water
as solvent because, firstly, it will dissolve the salt plates and secondly, it exhibits a
broad OH-peak. Consult the relevant reference books for the absorptivity of the various
solvents.
Pr epar i ng a Mul l
This sample preparation method is suitable if the solid sample can be ground into fine
particles but a suitable solvent is not available. In this case the sample powder is sus-
pended in a mulling agent (i.e. a liquid in that the solid is not soluble). A suitable mulling
agent is Nujol, a paraffin oil, which is transparent in the infrared region, except for nar-
row bands at 2900, 1450 and 1375cm
-1
. (An alternative mulling agent, which does not
absorb in these regions, is a perfluorokerosene, such as Fluorolube.)
The advantage of this technique is that it is a relatively quick and simple procedure. The
disadvantage is the interference resulting from the absorption bands of the mulling
agent. (Both Nujol and Fluorolube have characteristic spectral features and in most
cases have to be used as a pair in order to generate a complete MIR spectrum. Nujol is
used below 1330cm
-1
, Fluorolube above 1330cm
-1
.)
Put a small amount of your solid sample in an agate mortar.
Grind the sample thoroughly into fine powder (particles smaller than 500 mesh)
using a pestle.
Note: A common mistake when preparing a Nujol mull is to spend too little
time grinding the powder. Note that a mull prepared from a coarsely
ground solid will yield only a poorly resolved spectrum. Grinding the
sample into very fine particles is also important to reduce light
scattering and salt plate scratching.
H
SAMPLE PREPARATI ON
Add 1 or 2 drops of Nujol. Be careful not to add too much Nujol.
Mix the ground sample with the mulling agent until a uniform paste with a
vaseline-like consistency is formed.
Apply some mull on the surface of a NaCl plate using a suitable tool (e.g. a small
spatula or a rubber policeman). Be careful not to scratch the plate.
Place the second plate over the mull. To ensure an even and thin sample
thickness between the plates, rotate and press the plates together in order to
squeeze out the excess of the paste. Exclude also air bubbles.
Slot the plates in the plate holder installed in the spectrometer sample
compartment and start the measurement.
Do not forget to acquire also a background spectrum of the pur Nujol.
Pr essi ng a KBr Pel l et
This sample preparation technique is very suitable for solid samples in terms of the
information yield from an IR spectrum because KBr is significantly more IR transparent
than most solvents or Nujol oil. KBr has no absorption in the region 4000cm
-1
to
250cm
-1
so that a good sample spectrum (i.e. a spectrum that does not contain spectral
information about the dispersing agent) is obtained.
The success of this technique strongly depends on the grain size of the ground sample.
Grind the sample as fine as possible (particle size of at least 200 mesh, better 500
mesh) to minimize the infrared light scattering on the particle surface, also called Chris-
tiansen effect. This effect is caused by a refraction index mismatch between the salt
(KBr) and the sample powder that leads to reflections at the salt-sample interface.
Therefore, proper grinding is required to ensure a good contact between KBr and sam-
ple powder and to minimize the portion of the reflected light.
Another important factor in this technique is to keep everything moisture free as the KBr
material is hygroscopic. To prevent the KBr material from absorbing moisture, keep the
KBr material and the die in a drying oven at a temperature of 50 to 60C. Failure to do
so will result in cloudy pellets that yield distorted spectra. A correctly prepared KBr pel-
let will be transparent to IR light.
To sum it up, the KBr-pellet technique yields good quality spectra with a wide spectral
range and no interfering peaks. Disadvantages include tedious and time consuming
sample preparation and cleanup, interference of water bands (3,960 to 3,480cm
-1
and
1,950 to 1,300cm
-1
and below 500cm
-1
) and in same cases structural changes caused
by high pressure applied to the KBr/sample mix.
Put a small amount of the sample in an agate mortar and grind it up as fine as
possible.
Add a spatula full of oven-dry KBr material to the ground sample and mix it until a
uniform mixture is obtained. Do not grind the mixture as this may increase the
absorption of water by KBr.
.

.

.

.

.
SAMPLE PREPARATI ON
Note: A common mistake is to use to much sample. The concentration of
the sample in KBr should be in the range of 0.2% to 1% (i.e. typically a
300:1 dilution by mass).
Transfer the mixture into a die of a hydraulic or hand press and subject it to very
high pressure (ca. 20,000 psi) for a few minutes (2 to 5 minutes). The result
should be a translucent pellet with an ideal thickness of 0.5 to 1mm.
Carefully remove the pellet from the die, place it in the pellet holder and put the
pellet holder in the spectrometer sample compartment.
Note: The KBr pellet is very hygroscopic and fragile. Handle it with care
and use gloves to avoid contact with moisture from your hands.
Measure the KBr pellet immediately after removing it from the press
as the pellet will fairly rapidly begin to absorb moisture from the air
and becomes cloudy.
Li qui d Cel l
Liquid cells produce excellent results for most liquids. Especially for liquid samples that
are very volatile, using a liquid cell is highly recommended. A liquid cell consists of two
IR transparent windows with a precision spacer in between. One of the windows has
two drilled holes for the introduction and evacuation of the liquid. A large number of cell
options are available including permanently sealed cells, demountable cells with differ-
ent window material and a wide selection of spacers.
Note: Take into consideration that KBr is hygroscopic and the pathlength of
the KBr cell will change when exposed to a wet sample (this may
affect quantitative results). In addition, water will reduce the cell
throughput by clouding the windows. Note that many liquid cells
contribute a fringe pattern to the spectrum. Matching the refraction
index of the window material with that of the sample can minimize
this effect.
Gas Cel l
To obtain an infrared spectrum of a gaseous sample a gas cell with windows at each
end is required. It is important to select a suitable window material (e.g. KBr, NaCl, or
CaF
2
) that does not absorb infrared light. The cell usually has an inlet and outlet port
with a tap to facilitate the filling with the gas to be analyzed. Simple demountable cells
(50 mm to 100 mm) are recommended for samples in a 5 - 10% concentration range.
For diluted samples (ppm to ppb concentrations) a long path cell should be used. The
long path cell reflects the IR beam several times through the sample using a set of mir-
rors positioned on the opposite ends of the cell. Note that the cell thickness, the pres-
sure of the gas (proportional to concentration) inside the cell, and the molar absorptivity
determine the peak intensity.
H
SAMPLE PREPARATI ON
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
SERVI CE ADDRESSES I
Bruker Optik has an international network of branch offices and representations to
ensure worldwide a competent customer service. Below the addresses of the Bruker
headquarters are listed.
For a complete list with the addresses and telephone numbers of the Bruker branch
offices and representations worldwide refer to the internet: http://www. brukerop-
tics.com/contacts/worldwide.html
No responsibility can be taken for the correctness of this information. Subject to change.
North America
Bruker Optics Inc
19 Fortune Drive
Billerica, MA 01821
USA
Phone: +1-978-439-9899 (ext. 5227)
Fax: +1-978-663 9177
www.brukeroptics.com
info@brukeroptics.com
Europe
Bruker Optik GmbH
Rudolf-Plank-Str. 27
76275 Ettlingen
Germany
Phone: +49 7243/504-619 / -600
Fax: +49 7243/504-698
www.brukeroptics.de
ir_service@brukeroptics.de
Asia
Bruker Optik Asia Pacific Ltd.
Unit 505, 6/F, Tower III
Enterprise Square No. 9
Sheung Yuet Road
Hong Kong
Phone: +852 2796 6100
Fax: +852 2796 6109
asiapacific@brukeroptics.com.hk
I
SERVI CE ADDRESSES
VERTEX 70v User Manual
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
INDEX
Numerics
10Base-T Ethernet network 117, 118
10Base-T Ethernet port 98, 127
10Base-T Ethernet standard 7, 12, 98
A
AAR 5, 33, 35
ACR 5, 47, 50, 66
Air humidity content 43, 95
Aperture wheel 29
Automatic accessory recognition 5, 35
Automatic component recognition 5, 47,
50, 66
Automation diagnostics page 82, 88
B
Beam direction control compartment 19
Beam path 106
Beamsplitter 25, 28, 29, 47, 50, 90, 93,
94, 97
Color coding of the handle 28
Exchange procedure 49
Handling instructions 48
Operating position 47
Spectral range 28
Storage position 47
C
CAN bus port 23, 24, 96, 129
CAT 5 cable 98, 128
CG LED 84, 126
COM1 port 126
Computer network interface card 12
Connection topology 116
Connecting VERTEX 70v and PC to a
network 117
Connecting VERTEX 70v to a network
computer 118
For stand-alone operation 116
CR LED 126
Crossover cable 7, 12, 98, 127
CY LED 84, 126
D
Data cable 7, 12, 115
DDC ports 126
Detector 25, 26, 28, 29, 50, 87, 90, 93,
102
Exchange procedure 51
Operating temperature 26
Sensitivity 26
Spectral range 26
Detector compartment 19, 50, 52
Detector dewar 56
Detector diagnostics page 83
Diagnostic LEDs 75
Diagnostics page 75, 80
DLaTGS detector 26, 51
E
EDIS port 126
Electronics 87, 102
Electronics compartment 19
Electronics diagnostics page 81
Electronics panel 23, 24, 125
Electronics unit 129
Electrostatic discharges 57
ERR LED 84, 93, 97, 126
Ethernet 24, 98
Ethernet connection 5
Ethernet network 83, 127
Ethernet port 11, 98, 127, 128
Evacuating valve 13, 37
Evacuation time 41
F
FCONF program 120, 131
FIR source 26
Firmware 120, 131
Backing up the current version 135
Modifying IP settings 120
Restoring a previous version 134
Updating the firmware 132
Flaps 6, 37, 45, 69, 71, 85, 91
Controlling 45
I nde x
Fuses
Replacement procedure 68
FWD LED 126
G
Gas cell 139, 143
Gaseous sample 137
Globar 26
H
HeNe laser 103
I
Inlet port 5, 22, 24, 26, 29
Instrument status message 75, 79, 88
Interferogram 75
Interferometer 28, 87, 90, 102
Interferometer compartment 19
Internet 117
Intranet 117
IP address 12, 99, 123, 127, 128
IP addresses
for the stand-alone configuration 119
IR beam port 22, 23, 85
IR-transparent plate 139, 140
K
KBr pellet 137, 139, 142, 143
L
LAS TEST port 126
Laser 19, 25, 28, 61, 86, 88, 93, 97, 102
Parameter reset 64
Safety notes 61
Laser beam 86, 87, 97
Laser diagnostics page 64, 80
Laser LED 21, 61, 77, 86, 87, 93, 97
Laser power supply unit 61
Laser tube 86, 87, 97
Liquid cell 139, 143
Liquid nitrogen 52, 55, 93
Safety notes 55
Liquid sample 137
LPT1 Port 127
M
MAC address 121
Mains switch 11, 23, 24, 31, 68, 96, 129
MCT detector 26, 51, 52, 53, 55, 56, 87,
90, 95
Cooling procedure 55
Evacuation procedure 59
Measurement parameters 105
MIR source 25, 26, 66, 103
MPE port 96
N
Network 116
Network interface card 118, 119
NIR source 25, 26, 66, 103
Noise reduction hood 8, 15
Nujol mull 137, 139, 141
O
Optical path 29
OQ test 57, 94
Outlet port 5, 22, 29
OVP 94
OVP software 57
OVP test 75, 77, 78, 94
P
Peak position 95
Photometric accuracy 101
Power 101
Power cord 7, 11, 96, 129
Power supply
Frequency range 10
Voltage range 10
Power supply connector 19
Power supply panel 128
Power supply unit 94, 96
PQ test 94
Pressure sensor 6
Primary power receptacle 11, 23, 24, 129
Primary voltage supply 129
Purge gas 33
Degree of dryness 44
Flow rate 44
Maximum pressure 44
Purge gas connection 33
Purge gas hose 7
Purge gas inlet 15, 16, 24
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
INDEX
Q
QuickLock 25, 33, 34
Inserting a QuickLock accessory 34
Removing a QuickLock accessory 34
R
Reset button 24, 98, 127
Residual water vapor 41
RJ-45 connection 98
RX LED 83, 98, 127
S
Sample compartment 19, 21, 33, 102
Dimensions 110
Sample compartment windows 28, 50, 69,
94
Chemical properties 70
Handling instructions 70
Refraction index 70
Safety notes 70
Transmission range 70
Sample holder 25
Sample preparation 137
Sample preparation techniques 139
Sample spectrum 141
Sanner diagnostics page 81
Scan speed 101
SG LED 83, 127
Site requirements
Environmental requirements 9
Humidity 9
Power supply 10
Space requirements 9
Temperature range 9
Vibration 10
Solid sample 137, 140
Source 26, 28, 31, 89, 93, 94
Parameter reset 68
Safety notes 66
Source diagnostics page 68, 80
Spectral range 101
Spectral resolution 101
Spectrometer
Connecting the vacuum pump 13
Connecting to a PC 12
Connecting to the power supply 11
Connecting to the purge gas supply 15
Evacuating procedure 36
Initialization 21, 77, 86, 87, 96, 98
Purging 43
Rear side 23
Switching-on/off-procedure 31
Venting procedure 36
Spectrometer status indicator 75
SR LED 83, 98, 123, 127
Stand-alone configuration 123, 127
Status indicator board 19, 20, 76
Status LED 12, 21, 31, 32, 77, 86, 96
Step scan option 126
T
Temperature range 101
Time-resolved measurement 126
TKD LED 127
Tool kit 7
Transport handles 8
TRG port 126
TX LED 83, 98, 127
U
UV source 26
V
Vacuum 102
Vacuum LED 20, 76, 85
Vacuum pump 6, 8, 9, 13, 15, 32, 73, 85
Vacuum pump connection port 13, 19, 23,
24
Valve block 13
Vent opening 13, 23, 24
I nde x
Venting valve 13, 37, 85
Vibration absorber 8, 15
VIS source 26
Voltage status LED 68, 83, 87, 94, 96, 98,
129
W
Wavenumber accuracy 101

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