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PerkinElmer is the only GC supplier

that manufactures and sells a complete


single-vendor solution from sample
handling to data handling. This means
you will not struggle to find answers to
applications and service questions one
company provides the complete solution.

G a s C h ro m a t o g r a p h y

PerkinElmer continues to drive innovation


and performance in Gas Chromatography
(GC) instrumentation and software, with
a strong focus on making your lab more
productive. Backed by our worldwide,
world-class service and support team,
PerkinElmer GC products are a great fit
for your modern, fast-paced lab.

Gas Chromatography
QUICK-FIND INDEX

Page #

Autosampler Accessories
Vials, Caps and Septa

PerkinElmer offers a wide selection of superior quality products designed to work with
your PerkinElmer instruments. Our precision-designed products deliver the peace of
mind that comes from knowing that youll get the results you need.

89

Autosampler Syringes

88

The Quick Find Index to the left will help you find products fast. For your convenience,
products are alphabetized by category, sub-category, and family. There is also a more
complete Alphabetical INDEX on page 429 and a Part Number INDEX on page 407.

Capillary Columns Accessories

92

Capillary Columns

91

Capillary Injectors

150

Detectors

131

Ferrules

94

Gas Purification Systems

164

Gas Sampling Supplies

163

Headspace Accessories
and Supplies

143

Filters and Traps

163

Headspace Vials, Caps,


and Septa

148

Hydrogen Generators

165

Injector Liners

157

Injector Septa

159

Ozone Precursor

180

Headspace Vials, Caps, and Septa


PerkinElmers patented vial and cap design incorporates
pressure relief features which guarantee safe operation with
the high pressure typically developed during thermostatting.
These vials have a greater wall thickness and round base
which enables them to withstand pressure up to 60 psig.
PerkinElmer septa are designed for the patented pressure
release cap to ensure safe operation at higher temperatures. Available pre-assembled
into caps with starsprings.
Page 148

Capillary Columns
We use only the finest quality of high-strength fused silica in
the manufacture of our columns. Each column is individually
inspected and tested to guarantee you the highest
performance and to maximize reproducibility.
Page 91

Syringes
PerkinElmer TotalChrom
Software
Swagelok Fittings

173
95

Syringes

161

Thermal Desorber Stainless


Steel and Glass Tubes

181

Thermal Desorber Traps


and Fittings

182

Valves

168

Vial Crimping Tools

90

PerkinElmer Injector Syringes have been tested and


optimized for use with a 7 cm needle. This is critical for
depositing sample in the optimal zone. Syringes are
individually inspected for accuracy and performance.
Syringes for 0.5 L to 50 L capacity in two different point
styles are available. PerkinElmer ultra micro volume syringes are recommended for
sample injection of less than 5 L.
Page 161

Hydrogen Generators
The patented DBS PG-H2 series of Hydrogen Pure Gas
Generators is ideal for operation with gas analyzers as a
source of pure hydrogen in plasma chambers and other
isolated environments. Electrolytic membrane technology
is preferred over alternative hydrogen generating techniques
because it is clean, requires less maintenance, and there is
no need to store chemicals to maintain operation.
Page 165

Clarus GC
Sleek design and easy touch screen
revolutionize GC interaction
Gas chromatography started in 1952, with the seminal work of A.J.P.
Martin and A.T. James and, within a few years, it became one of the
most popular analytical techniques. PerkinElmer played a crucial role in
the development of the technique:
Dual-channel, real-time signal display

on the touch screen

Multiple-language support

Flexible configurations with

Enhanced Solvent Purge mode

integrated mass spectrometry,


headspace or thermal desorption
and pyrolysis samplers
Temperature-programmable inlets
Pneumatic Pressure Controllers (PPC)

Available in hundreds of configurations


ranging from dedicated analyzers for
petrochemical and air analysis to powerful
mass spectrometer units, the Clarus GC is
extremely flexible. For applications
requiring mass spectrometer detection,
the Clarus GC can be coupled to the
industrys easiest-to-use and widestmass-range quadrupole mass spectrometer.
The Clarus GC features the PerkinElmerexclusive PreVent operating mode. This
powerful mode uses the combined
features of the temperatureprogrammable PSS injector and the PPC,

PerkinElmers award-winning datahandling software makes managing


data easier than ever.
Combine the Clarus GC with the Clarus
Mass Spectrometer (MS), market-leading
PerkinElmer TurboMatrix samplehandling accessories, flexible user-friendly
TotalChrom software and world-class
service and support for an integrated,
complete analytical solution.
The totally integrated Clarus autosampler
provides flexibility and automation
capability for the gas chromatograph.
The autosampler accommodates three
autosampler syringe sizes (0.5, 5.0, and
50 L) and three injection speeds (slow,
normal, and fast), for complete application

Large-volume injection

to Asphalt

Air Toxics analysis

GC analysis at your fingertips

to increase analytical throughput, manage


difficult samples, protect the column and
chromatograph and lower detection limits

High-pressure pulse injection

Ozone Precursors analysis

provide accurate and highly


reproducible gas controls

The sleek Clarus Gas Chromatograph


from PerkinElmer offers a whole new
approach to the way you interact with
your GC instrument. An intuitive touchscreen interface features real-time signal
display and eight-language support.

Isolation mode

Petrochemical analysis from Hydrogen

maximize reproducibility

Clarus 500 GC

Easy setup/method development

Food and Beverage quality control

flexibility. Unobstructed access to either


injection port with one autosampler
permits any combination of analyses
for the most efficient utilization of
the gas chromatograph.
The Clarus MS features a wealth of
innovative technology to provide the most
complete characterization of samples.
PerkinElmer Selected Ion and Full Ion
(SIFI) scanning technology and high
scan speeds increase system accuracy.
The mass spectrometer boasts a fast
scanning speed with the widest mass
range available for GC/MS, providing
capability to analyze a greater scope
of applications.
The combination of a Clarus GC with a
data-handling system provides a total
laboratory solution from data collection
and analysis to reporting and storage.

87

Autosampler Accessories
Syringes and Accessories
Autosampler Replacement Parts

Autosampler Accessories

1
2
3

Description

Part No.

Each ()

Replacement Vial Locator (may require


service installation, not included)
Spring (pkg. 1)*
Shoulder Screw (pkg. 1)*

N6101182

14

N6101183
09907998

4
3

* Requires two for complete installation. See illustration.

5 L Syringe for Autosampler Part No. N6101390

Syringes
Replacement Needles for 0.5 L Syringes
Needle o.d. Part No.
0.47
0.63

Recommended Use

Autosampler Starter Kit


Includes: 5 L x 0.63 mm o.d. syringe, 2 mL clear sample
vials (100), 2 mL amber sample vials (100), blue crimp
caps with septa (100), green crimp caps with septa (100),
red crimp caps with septa (100), septa for waste/wash
vials (100), crimper 11 mm,
Part No.
Each ()
decapper 11 mm, 2 mL vial rack.
N6120105

791

Autosampler Thermostatting Accessory

Gas Chromatography

Allows thermostatting of Autosampler tray from 10 to 50 C.


Accessory includes: tubing, tie wraps,
Part No.
Each ()
clamp, and instructions.
(Circulating bath not included.)
N6120036
286

Part No.

Each ()

N6120181 10000

Part No.
N6120031

Each ()
287

Each ()

N6101253

210

N6101252

210

5 L Syringes
Recommended Use

Needle o.d. Part No.

0.53 capillary on-column injection


0.47
Plunger type: metal. Plunger in barrel
Routine analyses. Plunger type: metal 0.63
Plunger in barrel
Routine analyses. Shipped standard
0.63
with instrument. Plunger type: metal
Plunger in barrel with Teflon-tipped seal

Each ()

N6101380

113

N6101251

110

N6101390**

110

** Shipped standard with instrument

50 L Syringe
Recommended Use
Metal plunger in barrel type
Metal plunger in barrel type

AutoSystem XL Autosampler
Add-On Accessory (White Color)

88

Needle o.d. Part No.

Low injection volume. 0.53 capillary


0.47
on-column injection. Plunger type: Metal
Plunger in needle type
Low injection volume analyses
0.63
Plunger type: Metal
Plunger in needle type

Miscellaneous Accessories

Spare Autosampler Tray

74
74

0.5 L Syringes

Note: Cannot be installed on an AutoSystem.


Service installation is required.

N6101470
N6101469

Each ()

Needle o.d. Part No.


0.47
0.63

N9302799
N6101760

Each ()
223
200

Autosampler Accessories
Vials, Caps, and Septa
Crimp Caps and Septa

Screw Top Sample Vials and Caps


These vials are custom designed for the AutoSystem Series
and Clarus GC. (Not to be used with low-volume insert.)

Crimp Caps

Description

Part No.

Blue Crimp Caps and Septa (pkg. 100)


Green Crimp Caps and Septa (pkg. 100)
Red Crimp Caps and Septa (pkg. 100)
Silver Crimp Caps and Septa (pkg. 100)

N9302686
N9302684
N9302685
N9306015

Each ()
41
35
37
25

Viton Septa Crimp Caps


These Viton septa caps are recommended for applications
that require work with chloroform.
Part No.
Each ()
N9302784

Part No.

Cap, for Screw Top Vial (pkg. 100)


Septa for Screw Top Cap (pkg. 100)
PTFE-Coated Butyl Rubber
Vial, Clear Glass Screw Top (pkg. 100)

N9303441
N9303442

10
22

N9302945

41

Vial Holder Racks


Keep your samples organized and tip proof! These rugged,
plastic vial racks are great for holding vials while you load
and cap your samples. They stack away neatly when done.
Description

Part No.

36 vial capacity, 20 mm
50 vial capacity, 11 mm

N9301304
N9301303

Each ()

N9302680

31

Low-Volume Sample Inserts


200 L low volume glass inserts for crimp cap sample vials.
Supports required but not included.

Insert (pkg. 1000)


Support (pkg. 500)

N9302681
N9302682

33
33

Waste Vials
Part No.

Cap for Waste and Wash Vials (15 mm), (pkg. 1)


09923032
Clear Waste and Wash Vial 4 mL (15 mm), (pkg. 1) 09923031
Septa for Waste Wash Vials
N9302780
For use with viscous or toxic samples

Amber (11 mm) vial for photosensitive samples,


2 mL volume. Caps and septa not included.

Part No.

Each ()

1035

Crimp Top Sample Vials

Description

Each ()

Description

Description

Part No.

Autosampler Accessories

Aluminum crimp caps and


septa for 11 mm sample vial,
Teflon/rubber.

Each ()
1
1
37

Diffusers for Waste and Wash Vials


Diffusers are sold exclusively by PerkinElmer. The conical
shape allows the needle to penetrate into solvent or waste.
Reduces spillage and large losses
Part No.
Each ()
through evaporation.
N6101276

Each ()
471
77

Clear (11 mm) sample


vial, 2 mL volume.
Caps and septa not
included. (pkg. 100)

N9301385

Gas Chromatography

Part No.

Each ()
18

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

89

Autosampler Accessories
Vial Crimping Tools
Crimping Tools

Autosampler Accessories

Benchtop Crimper
Sturdy, rugged stand will accept three size jaws.
Jaws required but not included.
Part No.
N6621006

Each ()
1685

Jaws for Benchtop Crimpers


Description

Part No.

AutoSystem GC Vials, 11 mm
Headspace Vials, 20 mm

N6621008
N6621009

Each ()
391
344

Electronic Crimpers

Benchtop Crimper Part No. N6621006

Electronic crimpers and decappers are easy to use and


fully rechargeable. Ergonomically designed to alleviate
the potential for Carpal Tunnel Syndrome and provide a
consistent crimp pressure numerous times. The unit comes
with a standard Black and Decker VersaPak Gold battery
and charger, and will crimp several hundred vials on
one charge. Crimping pressure is fully adjustable for
precision control.
Description

Part No.

11 mm Electronic Crimper 120V


11 mm Electronic Crimper 200V
11 mm Electronic Crimper 230V
11 mm Electronic Crimper 240V
11 mm Electronic Decapper 120V
11 mm Electronic Decapper 200V
11 mm Electronic Decapper 230V
11 mm Electronic Decapper 240V
Electronic Crimper Replacement Battery

N9302567
N9302568
N9302569
N9302570
N9302575
N9302576
N9302577
N9302578
N9302585

Each ()
700
700
700
700
700
700
44

Hand Crimpers
Description

Part No.

1.5 mL (AutoSystem GC sample vials), 11 mm


6.0 mL and 20.0 mL (headspace vials), 20 mm

00090699
N9302785

Each ()
263
256

Gas Chromatography

Economy Cap Removal Tool


Electronic Crimper Part No. N9302567 (120 V)

90

Description

Part No.

11 mm Autosampler Crimp Caps


20 mm Headspace Crimp Caps

N9301390
N9301270

Each ()
64
64

Capillary Columns
Capillary Columns

Capillary Columns
Top 10 Reasons to Buy
PerkinElmer Elite Series
Capillary Columns
1

Finest quality of high-strength fused silica

Each column individually inspected and tested

Reproducible results

Crosslinked and bonded stationary phase

Robust column cage

Superior resolution

Wide selection of stationary phases available

Reduced baseline bleed

Lower baseline noise

10 Column lengths from 5 to 105 m

Why choose fused silica?

Selecting the right stationary phase

What length do I need?

Many factors influence the quality


of a column. Fused silica is considered
to be the purest form of glass, with fewer
metal oxides (Lewis acid sites) and
hydrogen bonding (surface silanol)
groups. The stationary phase is cross
linked (polymerized) and also bonded
to the surface of the column to provide
a high degree of stability, resulting in
lower bleeding of the stationary phase
at elevated temperatures. The superior
inertness of the column means that
acidic and basic compounds can be
analyzed on the same column.

The inherent efficiency (large number


of theoretical plates) of capillary columns
allows you to choose from relatively few
types of phases, compared to the many
varieties of packed columns previously
required. Perhaps more importantly,
because capillary columns are more
efficient, you will see superior resolution
resulting in narrower, taller peaks that
allow easier integration from your data
system. Identification of small peaks are
facilitated by a reduced baseline bleed
and lower baseline noise. Non-polar
Elite-1 columns from PerkinElmer will
preferentially retain non-polar
compounds, whereas the PerkinElmer
Elite-200 column phase provides
high selectivity for analytes containing
lone pair electrons, such as nitro and
carbonyl groups. Elite-WAX polyethylene
glycol columns are highly selective
toward polar compounds such as alcohols.

Typically, capillary columns are available


in lengths from 5 to 105 meters. The
longer the column the more resolving
power, but this also increases the analysis
time. Doubling a column length only
increases resolution by approximately
40% but, under isothermal conditions,
will double the analysis time. If using
a temperature programmed analysis,
retention times are more dependent on
the temperature than on the column
length. PerkinElmer provides columns
in the most popular lengths of 5, 10, 12,
15, 25, 30, 50, 60, 75, 100, and 105 m
depending upon the column i.d.

91

Capillary Column Accessories


Adapter Kits
Wide-Bore Kit
Replacement Parts

Capillary Column Accessories

Adapter Kit Accessories


Detector Receiver
1/8 to 1/16 in. detector receiver for
use when using capillary columns
with FID, ECD, NPD, and FPD.

Part No.
N6120020

Each ()
69

Column Nut 1/16 in.


Replacement 1/16 in. column nut.
Connects capillary column to adapter.

Part No.
09903392

Each ()
27

Flow Accessory 0-20 mL


For use when converting an
AutoSystem flow controller
to low-flow operation.

Part No.
N6101377

Each ()
261

Graphite/Vespel 1/16 in. Ferrule


1/16 in. x 0.8 mm i.d. For connecting
capillary columns to adapter liner.

Part No.
09920107

Each ()
84

Flow Accessory 0-100 mL


Shipped as standard with instrument.

Part No.
N6102190

Each ()
185

Injector/Detector Adapter for


Fused-Silica Capillary Columns

Wafer Scribe
The ceramic wafer scribe is inexpensive and ideal for
cutting polyimide fused-silica capillary columns. The scribe
is easy to hold and simple to use.
Part No.
Each ()
All four sides can be used. (pkg. 10)
N9301376

59

09903739

Each ()
21

Reverse ferrules used to connect 0.53 mm capillary columns


to wide-bore adapter kit. 1/16 in. fitting. Reverse ferrule
1/16 in. x 0.8 mm i.d. (pkg. 10)
Part No.
Each ()
09920141

Reverse ferrules used to connect 0.53 mm capillary columns


to wide-bore adapter kit. 1/16 in. fitting. Reverse ferrule
1/16 in. x 0.8 mm i.d. (pkg. 10)
Part No.
Each ()
09920107

AutoSystem GC wide-bore
replacement quartz liner.

AutoSystem GC Adapter Kit

Replacement glass liner (untreated)


for use with the wide-bore adapter
kit (0.53 mm columns).

523

84

Wide-Bore Quartz Liner

Wide-Bore Glass Liner

N6120001

59

Graphite/Vespel Ferrule

Wide-Bore Adapter Kit


The 0.53 mm Capillary Column
Adapter Kit from PerkinElmer
contains all the parts necessary to
adapt packed column injectors
quickly and easily for use with
wide-bore capillary columns. For accurate control of the
low flows used in wide-bore capillary columns (down to
1 mL/min.). Kit includes 0-20 mL/min. flow controller
element, wide-bore adapter with 1/16 in. fitting, wide-bore
glass liner and column support hanger. May be used in both
on-column or off-column modes.
Part No.
Each ()
(For AutoSystem GC Series only.)

Gas Chromatography

Part No.

For installing adapter liner into injector.

Graphite Ferrule

This 1/8 to 1/16 in. stainless steel


reducer can be easily installed. For
use when installing capillary columns
on the 1/8 in. split/splitless injector
and all 1/8 in. detector fittings. The
reducer allows the use of 1/16 in. graphite/vespel ferrules
rather than the larger 1/8 in. ferrule.
Part No.
Each ()
(Not compatible with AutoSystem
or Clarus Series.)
N9300063
130

92

Graphite/Vespel 1/4 in. Ferrule

Part No.
N6121003

Part No.
N6101375

Each ()
32

Each ()
29

Capillary Column Accessories


Connectors and Supplies

Union Connectors
Column i.d. (mm)

Qty.

Part No.

0.25*
0.32*

pkg. 10
pkg. 10
pkg. 5
pkg. 10
pkg. 5

N9301167
N9301169
N9301170
N9301171
N9301172

0.53*

High-quality, uncoated fusedsilica tubing is available in


standard capillary sizes.
Deactivated tubing is perfect for
making guard columns and
replacement Transfer Lines in HS
and TD samplers retention gaps;
available in 5 m lengths. Use our
SPLITTERS and CONNECTORS
to attach tubing to your
polyimide-coated columns.

Each ()
63
96
129
63
24

Reducing Connectors
Column i.d. (mm)

Qty.

Part No.

0.32 to 0.25*
0.53 to 0.25*
0.53 to 0.32*

pkg. 10
pkg. 10
pkg. 10
pkg. 5

N9301338
N9301340
N9301342
N9301341

Each ()
129
129
63
42

* Note: These connectors are not recommended


for use with aluminum-clad columns.

Tools

Capillary Column Accessories

Uncoated Deactivated
Fused-Silica Capillary Tubing

Column Connectors

Polyimide-Uncoated Deactivated Tubing


Tube i.d. (mm)

Length

Part No.

0.10
0.18
0.25
0.32
0.53

5m
5m
5m
5m
5m

N9301355
N9301354
N9301356
N9301357
N9301358

Each ()
114
75
37
37
63

Capillary Column Support for PerkinElmer GCs

Pin Vise and Drill Bits


For enlarging ferrule i.d. for capillary columns. Kit includes
a double-ended pin vise and a set of
Part No.
Each ()
12 drill bits, sizes No. 61 (0.99 mm)
through No. 80 (0.343 mm).
N9301346
51

Column supports delicate fused-silica columns


in the proper oven location for optimum
chromatographic performance.
Description

Part No.

AutoSystem Series/Clarus

N6101070

Each ()
51

Universal Connectors
Allows for fast, leak-free connections of fused-silica
columns. The new fused-silica tapered design allows
connection of any size column and its easy to use.
(0.1 to 0.53 mm columns can be used.)
Description

Part No.

Polyimide Sealing Resin* (5 g)


Universal Connector* (pkg. 5)
Universal Y Splitter* (pkg. 1)

N9301343
N9302149
N9303448

Each ()
39
81
96

* Note: These connectors are not recommended


for use with aluminum-clad columns.

Gas Chromatography

Pin Vise and Drill Bit Kit Part No. N9301346


Universal Connector
Part No. N9302149

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

93

Capillary Column Accessories


Ferrules
SilTite Metal
Nut and Ferrules Kit
SilTite
Ferrules

Capillary Column Accessories

Graphite and Vespel Ferrules


Graphite Ferrules
This is the ferrule of choice for high-temperature
applications. Of the three ferrule types available, graphite
is the softest, making it less damaging to capillary columns
when overtightened. Graphite seals easily and does not
stick to glass columns. Recommended for use with capillary
columns. Temperature limit is 450 C.
Nut Size (in.)

Ferrule i.d. (in.)

Qty.

Part No.

1/16
1/8
1/4

1/16
1/8
1/4

pkg. 10
pkg. 10
pkg. 10

02450972
09903915
09920140

Each ()
55
54
43

SilTite Metal Nut and


Ferrules provide a continuous
leak-free connection and are
perfect for connecting
your column to a GC/MS.
From the SilTite drawing it
can be seen that the taper of the inner nut is designed
specifically for the angle of the SilTite ferrule. This ensures
an even closure of the ferrule around the whole column to
eliminate leaks.
Features and Benefits:
No need to re-tighten the nut

Graphite/Vespel Ferrules

Eliminate contamination

Graphite/vespel ferrules (15% graphite/85% polyimide) are


recommended for use with GC/MS systems. Best choice for
glass columns and polyimide-coated, fused-silica capillary
columns. Can usually be removed easily from column.
Temperature limit is 350 C.

Reusable nut

Nut Size (in.)

Ferrule i.d. (in.)

Qty.

Part No.

1/16
1/8
1/4

1/16
1/8
1/4

pkg. 10
pkg. 1
pkg. 10

09920127
N9302081
09903739

Each ()
84
84
21

Vespel Packed Stainless Steel Column Ferrules


Vespel ferrules are not reusable; they tend to stick to
columns after use at upper temperature limit. Not
recommended for fused-silica capillary columns. Use these
vespel ferrules on 1/16 in. metal tubing and glass-lined
receivers (heated or ambient). Temperature limit is 350 C.
Nut Size (in.)

Ferrule i.d. (in.)

Qty.

Part No.

1/8
1/4

1/8
1/4

pkg. 10
pkg. 10

N9301360
N9301361

Each ()
64
65

Capillary Column Ferrules

Gas Chromatography

Package quantity: 10
Nut Size Column Ferrule
(in.)
i.d. (mm) i.d.(mm)

Graphite
Part No.

1/16

0.18-0.25 0.4

N/A

09920104

84

1/16

0.32

09903700

48 09920105

84

1/16

0.32

0.5 (2-hole) N9306001

55 N9306000

110

1/16

0.53

0.8

59 09920107

84

1/16

0.18-0.25 0.4 (2-hole) N/A

04972392

19

1/8

0.53

1.0

09903394

48 N/A

1/8

0.32

0.5 (2-hole) 09903395

75 N/A

1/8

0.32

0.5

48 N/A

0.5

09920141

09903981

Graphite/Vespel
Each () Part No.
Each ()

Note: 0.25-0.32 mm i.d. columns require 0.5 mm i.d. ferrules;


0.53 mm i.d. columns require 0.8 mm i.d. ferrules.

94

Leak-free seal
Starter kit contains 2 SilTite nuts and 10 ferrules
The metal SilTite ferrule and nut are manufactured from
the same material and will therefore not expand and contract
at different coefficient rates. The base of the SilTite ferrule
forms a perfect seal with the MS interface, covering the
whole transfer interface. SilTite metal ferrules have a
temperature limit well above the temperature capacity
of the injector, MS interface or GC oven.
Description

Qty.

Part No.

SilTite Ferrules Starter Kit 0.4 mm


SilTite Ferrules Starter Kit 0.5 mm
SilTite Ferrules Starter Kit 0.8 mm
SilTite Ferrules 0.4 mm
SilTite Ferrules 0.5 mm
SilTite Ferrules 0.8 mm
SilTite Nuts

pkg. 10
pkg. 10
pkg. 10
pkg. 10
pkg. 10
pkg. 10
pkg. 5

N9306090
N9306091
N9306092
N9306093
N9306094
N9306095
N9306096

Each ()
83
83
83
57
57
57
70

Capillary Column Accessories


Fittings
Capillary Column Accessories

Swagelok Fittings
SwagelokTM Fittings
Swagelok fittings from PerkinElmer are available in brass and stainless steel.
The patented advanced-geometry back ferrule design provides a leak-tight tube connection on all Swagelok stainless
steel tube fittings, in sizes 1/4 to 1/2 in., and 6 to 12 mm. Leak-tight seals that will withstand high-pressure, vibration,
vacuum and temperature changes depend upon close tolerances and consistent, exacting quality control in conjunction
with good design principles.
Ease of installation
Back ferrule axially advances the front ferrule
Vibration fatigue resistance
Wide variety of configurations
Brass
Part No.

Qty.

Size

Bulkhead Adapter

pkg. 1

1/4 in. to 1/4 in. tube

Back Ferrule

pkg. 5

Cross Union

pkg. 1

1/16 in.
1/8 in.
1/4 in.
1/8 in.

N9300040
N9300036
N9300030
N9301259

Front Ferrule

pkg. 5

Male Adapter
Tube to Pipe

pkg. 1

1/16 in.
1/8 in.
1/4 in.
1/4 in. tube to 1/8 in. NPT

Male Connector

pkg. 1

Nut

pkg. 5

Plug

pkg. 1

1/8 in. to 1/8 in. NPT


1/8 in. to 1/4 in. NPT
1/4 in. to 1/8 in. NPT
1/4 in. to 1/4 in. NPT
1/16 in.
1/8 in.
1/4 in.
1/16 in.
1/8 in.
1/4 in.
1/16 in.
1/8 in.
1/4 in.
1/16 in.
1/8 in.
1/4 in.
1/8 in. to 1/16 in.
1/4 in. to 1/8 in.
1/4 in. to 1/16 in.

Union

pkg. 2

Union Tee

pkg. 1

Reducing Union

pkg. 1

Each ()

Stainless Steel
Part No.
Each ()
N9301267

48

12
5
6
40

N9300042
N9300038
N9300032

29
17
13

N9300041
N9300037
N9300031
N9301266

12
6
6
8

N9300043
N9300039
N9300033

30
19
13

N9301253
N9301254
N9301255
N9301269
N9300058
N9300056
N9300054

9
9
8
8
14
9
9

N9300060
N9301268
N9300048
N9300046
N9300044
N9301221
N9301222
N9301223
N9300051
N9300050
N9301227

9
5
31
25
17
37
27
27
27
22
14

N9300059
N9300057
N9300055
N9300053
N9300061
N9301233
N9300049
N9300047

54
33
30
70
44
17
99
69

N9301225
N9301226

47
36

Gas Chromatography

Product

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

95

Capillary Columns
Application Index
Environmental
Subject

Column

Amines and Phenols

Elite-5Amine

EPA Method 508 Pesticides

Elite-5

EPA Method 508


Organochlorine Pesticides

Capillary Columns

Forensic/Clinical Toxicology

Elite-CLPesticides
Elite-CLPesticides2

Page No.

Subject

Column

Page No.

99

Anabolic Steroids Underivatized

Elite-5

113

99

Blood Alcohol

Elite-BAC

114

Cannabinoids TMS Derivatives

Elite-5

113

100
100

Cocaine and Metabolites

Elite-5

115

Sympathomimetic Amines
HFBA Derivatives

Elite-5

115

Column

Page No.

EPA Method 524.2

Elite-624 (GC/MS)

101

EPA Method 551.1

Elite-5

101

EPA Method 551.1


Chlorinated Disinfection Byproducts

Elite-200

102

EPA Method 8021


Volatile Organics

Elite-Volatiles

104

EPA Method 8081


Pesticides

Elite-35

102

Elite-CLPesticides
Elite-CLPesticides2

103
103

EPA Method 8081A


Organochlorine Pesticides
EPA Method 8260B
Volatile Organics

Subject

Elite-VMS

105

EPA Method 8260B


Volatile Organics

Elite-VMS

106

EPA Method 8270


Semi-Volatile Organics

Elite-5 ms

107

Essential Oils
Citronella Java Oil

Elite-1

108

Nitrogen Containing Herbicides

Elite-5

Pesticides
Synthetic Essential Oil

Gas Chromatography

Alcohols and Aldehydes

Elite-WAX ETR

116

Alcohol Mixtures

Elite-WAX ETR

116

Aldehydes

Elite-WAX

117

Amines & Phenols

Elite-5Amine

117

Aromatics

Elite-WAX ETR

118

Industrial Solvents

Elite-MWAX

118

Industrial Solvents

Elite-WAX ETR

118

Petroleum
Subject

Column

108

Prudhoe Bay Crude Oil

Elite-1GC-79

119

Elite-5

109

Volatile Hydrocarbons

Elite-Q PLOT

119

Elite-1

109

Subject

Column

Page No.

Brewing Beer

Elite-BAC

110

Essential Oils Lemon Oil

Elite-5

110

Essential Oils Native Spearmint Oil

Elite-WAX ETR

111

Essential Oils
Synthetic Mushroom Aroma

Elite-WAX ETR

111

Sugars As Alditol Acetates

Elite-225

112

TCA in Wine

Elite-5 ms

112

Food and Flavors

96

Industrial Chemicals

Page No.

Capillary Columns
U.S. EPA Methods
U.S. EPA Drinking Water
Test Methods

U.S. EPA Organic Chemical


Analysis Waste Water Methods

Method Column Recommendations

N9316207
N9316208
N9316392
N9316393
N9316190
N9316207
N9316208
N9316392
N9316393
N9316190
N9316207
N9316392
N9316023
N9316207
N9316392
N9316024
N9316129
N9316076
N9316282
N9316234
N9316076
N9316282
N9316191
N9316234
N9316285
N9316296
N9316023
N9316086
N9316293
N9316243
N9316201
N9316207
N9316208
N9316087
N9316283
N9316392
N9316393
N9316086
N9316283
N9316076
N9316086
N9316282
N9316293
N9316392
N9316024
N9316283
N9316243

700
1249
764
1274
1210
700
1249
764
1274
1210
700
764
547
700
764
573
547
509
611
547
509
611
547
547
1084
1186
547
573
636
573
573
700
1249
547
611
764
1274
573
611
509
573
611
636
764
573
611
573

* Specified in EPA method.


** This column is highly recommended by PerkinElmer for this EPA method.
The choice of column for this purge-and-trap method may depend on your
sample concentrator to GC interface.

Method Column Recommendations


601 Elite-624
Elite-624**
Elite-Volatiles**
Elite-Volatiles**
Elite-502.2
602 Elite-624**
Elite-Volatiles**
Elite-502.2
603 Elite-624
Elite-Volatiles**
604 Elite-5ms**
606 Elite-1
607 Elite-5
Elite-5ms**
608 Elite-608**
609 Elite-5
Elite-5ms**
610 Elite-5
Elite-5ms**
611 Elite-5
Elite-5ms**
612 Elite-1
Elite-5ms**
613 Elite-5ms
Elite-5ms**
615 Elite-608**
Elite-1701
619 Elite-17
Elite-35**
622 Elite-5ms**
624 Elite-624
Elite-624
Elite-624
Elite-Volatiles**
Elite-Volatiles**
Elite-502.2
625 Elite-5ms**
680 Elite-5*
Elite-5ms**
1618 Elite-1
Elite-608**
Elite-1701
1624 Elite-624
Elite-624**
1625 Elite-5*
Elite-5ms**
1653 Elite-5*
Elite-5ms**

30 m x .53 mm i.d., 3.00 m


75 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
105 m x .53 mm i.d., 3.00 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
105 m x .53 mm i.d., 3.00 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
30 m x .53 mm i.d., 1.50 m
15 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 0.83 m
30 m x .53 mm i.d., 1.50 m
30 m x .25 mm i.d., 1.00 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
15 m x .53 mm i.d., 1.50 m
15 m x .53 mm i.d., 1.50 m
30 m x .32 mm i.d., 1.00 m
30 m x .25 mm i.d., 1.00 m
60 m x .25 mm i.d., 0.10 m
60 m x .32 mm i.d., 0.10 m
30 m x .53 mm i.d., 0.83 m
30 m x .53 mm i.d., 1.00 m
30 m x .53 mm i.d., 1.00 m
30 m x .53 mm i.d., 1.00 m
30 m x .53 mm i.d., 1.50 m
30 m x .25 mm i.d., 1.40 m
30 m x .53 mm i.d., 3.00 m
75 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
105 m x .53 mm i.d., 3.00 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 0.83 m
30 m x .53 mm i.d., 1.00 m
75 m x .45 mm i.d., 2.55 m
75 m x .53 mm i.d., 3.00 m
30 m x .25 mm i.d., 0.25 m
30 m x .25 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m

Part No.
N9316207
N9316208
N9316392
N9316393
N9316190
N9316207
N9316392
N9316190
N9316207
N9316392
N9316300
N9316046
N9316100
N9316300
N9316197
N9316100
N9316283
N9316086
N9316293
N9316098
N9316299
N9316024
N9316283
N9316285
N9316296
N9316197
N9316255
N9316136
N9316152
N9316300
N9316201
N9316207
N9316208
N9316392
N9316393
N9316190
N9316293
N9316086
N9316293
N9316050
N9316197
N9316255
N9316206
N9316208
N9316076
N9316282
N9316086
N9316293

Each ()
700
1249
764
1274
1210
700
764
1210
700
764
700
356
611
700
700
611
611
573
636
356
434
573
611
1084
1186
700
740
636
721
700
573
700
1249
764
1274
1210
636
573
636
636
700
740
1249
1249
509
611
573
636

Gas Chromatography

30 m x .53 mm i.d., 3.00 m


75 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
105 m x .53 mm i.d., 3.00 m
30 m x .53 mm i.d., 3.00 m
75 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
105 m x .53 mm i.d., 3.00 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
30 m x .32 mm i.d., 0.25 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
30 m x .32 mm i.d., 1.00 m
30 m x .32 mm i.d., 0.50 m
30 m x .25 mm i.d., 0.25 m
30 m x .25 mm i.d., 0.25 m
30 m x .25 mm i.d., 0.25 m
30 m x .25 mm i.d., 0.25 m
30 m x .25 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.50 m
30 m x .25 mm i.d., 0.25 m
60 m x .25 mm i.d., 0.10 m
60 m x .32 mm i.d., 0.10 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .25 mm i.d., 1.40 m
30 m x .53 mm i.d., 3.00 m
75 m x .53 mm i.d., 3.00 m
30 m x .32 mm i.d., 1.00 m
30 m x .25 mm i.d., 1.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
30 m x .32 mm i.d., 0.25 m
30 m x .25 mm i.d., 1.00 m
30 m x .25 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .25 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .45 mm i.d., 2.55 m
30 m x .32 mm i.d., 1.00 m
30 m x .25 mm i.d., 1.00 m
30 m x .32 mm i.d., 0.25 m

Each ()

Capillary Columns

501.3 Elite-624
Elite-624**
Elite-Volatiles**
Elite-Volatiles**
Elite-502.2
502.2 Elite-624*
Elite-624**
Elite-Volatiles
Elite-Volatiles**
Elite-502.2
503.1 Elite-624
Elite-Volatiles**
504 Elite-1*
Elite-624**
Elite-Volatiles**
505 Elite-1*
Elite-17
507 Elite-5*
Elite-5ms**
Elite-1701*
508 Elite-5*
Elite-5ms**
Elite-608**
Elite-1701*
513 Elite-5ms
Elite-5ms
515 Elite-1*
515.2 Elite-5*
Elite-5ms**
Elite-1701*
524.2 Elite-624*
Elite-624*
Elite-624*
Elite-5*
Elite-5ms**
Elite-Volatiles**
Elite-Volatiles**
525 Elite-5*
Elite-5ms**
548.1 Elite-5*
Elite-5*
Elite-5ms**
Elite-5ms**
Elite-Volatiles**
551 Elite-1*
Elite-5ms**
552 Elite-1701*

Part No.

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

97

Capillary Columns
U.S. EPA Methods

Gas Chromatography

Capillary Columns

U.S. EPA Solid Waste


Test Methods
Method Column Recommendations

Part No.

8010 Elite-624
Elite-Volatiles**
8015 Elite-624
Elite-Volatiles**
8020 Elite-624
Elite-Volatiles**
8030 Elite-624
Elite-Volatiles**
8040 Elite-5ms
8060 Elite-1
8080 Elite-608**
8081 Elite-5*
Elite-608**
Elite-1701*
8090 Elite-5
Elite-5ms**
8100 Elite-5
Elite-5ms**
8120 Elite-1
Elite-5ms**
Elite-5ms**
8140 Elite-1
Elite-1701**
8141 Elite-5*
Elite-5ms**
Elite-35**
8150 Elite-608**
Elite-1701
8240 Elite-624
Elite-624
Elite-Volatiles**
Elite-Volatiles**
8250 Elite-5
Elite-5ms**
8260 Elite-5*
Elite-624*
Elite-624
Elite-Volatiles**
Elite-Volatiles**
Elite-5ms**
8260B Elite-Volatiles**
8270 Elite-5*
Elite-5ms**
8280 Elite-5*
Elite-5ms**

N9316208
N9316393
N9316207
N9316392
N9316207
N9316392
N9316207
N9316392
N9316300
N9316046
N9316197
N9316100
N9316197
N9316255
N9316100
N9316300
N9316086
N9316293
N9316024
N9316283
N9316294
N9316050
N9316255
N9316098
N9316300
N9316153
N9316197
N9316255
N9316207
N9316208
N9316392
N9316393
N9316100
N9316300
N9316087
N9316207
N9316208
N9316392
N9316393
N9316283
N9316388
N9316087
N9316284
N9316076
N9316283

75 m x .53 mm i.d., 3.00 m


75 m x .45 mm i.d., 2.55 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
30 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
30 m x .53 mm i.d., 1.50 m
15 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 0.83 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 0.83 m
30 m x .53 mm i.d., 1.00 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 1.50 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 0.25 m
30 m x .32 mm i.d., 1.00 m
30 m x .25 mm i.d., 1.00 m
30 m x .32 mm i.d., 1.00 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 1.00 m
15 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 0.50 m
30 m x .53 mm i.d., 0.83 m
30 m x .53 mm i.d., 1.00 m
30 m x .53 mm i.d., 3.00 m
75 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
30 m x .53 mm i.d., 1.50 m
30 m x .53 mm i.d., 1.50 m
30 m x .32 mm i.d., 1.00 m
30 m x .53 mm i.d., 3.00 m
75 m x .53 mm i.d., 3.00 m
30 m x .45 mm i.d., 2.55 m
75 m x .45 mm i.d., 2.55 m
30 m x .25 mm i.d., 1.00 m
30 m x .25 mm i.d., 1.40 m
30 m x .32 mm i.d., 1.00 m
30 m x .25 mm i.d., 0.50 m
30 m x .25 mm i.d., 0.25 m
30 m x .25 mm i.d., 1.00 m

Each ()
1249
1274
700
764
700
764
700
764
700
356
700
611
700
740
611
700
573
636
573
611
636
636
740
356
700
611
700
740
700
1249
764
1274
611
700
547
700
1249
764
1274
611
638
547
611
509
611

* Specified in EPA method.


** This column is highly recommended by PerkinElmer for this EPA method.
The choice of column for this purge-and-trap method may depend on your
sample concentrator to GC interface.

98

Capillary Column Applications


Environmental

3
1

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.

Capillary Column Applications

Amines and Phenols

Diethylamine
Pyridine
Morpholine
Phenol
Aniline
2-Chlorophenol
Diethylenetriamine
Octylamine
1-Methyl-2-Pyrrolidinone
2-Nitrophenol
2, 6-Dimethylaniline
Nicotine
2-Nitroaniline

13
Column: Elite-5Amine
Dimensions: 30 m, 0.32 mm i.d., 1.0 m
Sample: 1.0 L split injection of
miscellaneous amines
and phenols in water
On-Column Conc.: 22 ng
Oven: 120 C to 220 C @ 10 C/min.
Injector & Detector: 305 C
Carrier Gas: Hydrogen
Linear Velocity: 38 cm/sec. set @ 120 C
FID Sensitivity: 6.4 x 10-11 AFS
Split Ratio: 25:1

11

8
10

12

10

Part No.

N9316677

TIME (MIN.)

U.S. EPA Method 508 Pesticides


Etridiazole (50 pg/L)
Chlorneb (1000 pg/L)
Propachlor (1000 pg/L)
Trifluralin (50 pg/L)
a-BHC (20 pg/L)
Hexachlorobenzene (10 pg/L)
b-BHC (20 pg/L)
g-BHC (30 pg/L)
PCNB (impurity) (100 pg/L)
PCNB (IS) (100 pg/L)
d-BHC (20 pg/L)
Chlorothalonil (50 pg/L)
Heptachlor (20 pg/L)
Aldrin (30 pg/L)
DCPA (50 pg/L)
DCB (SS) (5000 pg/L)
Heptachlor Epoxide (30 pg/L)
g-Chlordane (30 pg/L)
Endosulfan I (30 pg/L)
a-Chlordane (30 pg/L)

21.
22.
23.
24.
25.
26.
27.
28.
29.
30.
31.

Dieldrin (40 pg/L)


Endrin (30 pg/L)
Endosulfan II (30 pg/L)
Chlorobenzilate (1000 pg/L)
P, P'-DDD (50 pg/L)
Endrin Aldehyde (50 pg/L)
Endosulfan Sulfate (30 pg/L)
P, P'-DDD (120 pg/L)
Methoxychlor (100 pg/L)
cis-Permethrin (1000 pg/L)
trans-Permethrin (1000 pg/L)

N9316076

28

16

9 10

30 31

21

12

26

Column: Elite-5
Dimensions: 30 m, 0.25 mm i.d., 0.25 m
Sample: 2.0 L splitless injection of a pesticide mix
Splitless Hold: 0.75 min.
Oven Temperature: 60 C to 300 C @ 4 C/min.
(hold 10 min.)
Injector: 250 C
Detector: ECD, 320 C
Carrier Gas: Helium @ 30 cm/sec.

Part No.

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.

14

24
25
23
19
22
18 20

15 17

5
1

11
13
4

29

27
6
7

12

16

20

24

28

32

36

40

44

48

52

TIME (MIN.)

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

99

Capillary Column Applications


Environmental
Capillary Column Applications

U.S. EPA Method 508 Organochlorine Pesticides


14
18,19

1
5,6

13

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.

16,
17

8,9

24,25
15

22 26
28

10,11,12

32

23 27

31
20,
21
36
33
34
3

20.
21.
22.
23.
24.
25.
26.
27.
28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.

Hexachloropentadiene
Etridiazole
Chlorneb
Hexachlorobenzene
Propachlor
a-BHC
Simazine
g-BHC
Atrazine
Trifluralin
Pentachloronitrobenzene
b-BHC
d-BHC
Metribuzin
Heptachlor
Aldrin
Chlorothalonil
4, 4'-Dibromobiphenyl
Alachlor

Metalachlor
DCPA (Dacthal)
Heptachlor Epoxide
g-Chlordane
Cyanazine
a-Chlordane
4, 4'-DDE
Endosulfan I
Dieldrin
Endrin
Chlorobenzilate
4, 4'-DDD
Endosulfan II
4, 4'-DDT
Endrin Aldehyde
Methoxychlor
Endosulfan Sulfate
cis-Permethrin
trans-Permethrin

30
29

38
35
37

10

17

4 6

12

14
TIME (MIN.)

16

18

14

20
8,11 13

16

22

Gas Chromatography

Part No.

N9316664

Part No.

N9316662

26

25
23

Column: Elite-CLPesticides
Dimensions: 30 m, 0.32 mm i.d., 0.50 m,
Elite-CLPesticides (N9316664)
Dimensions: 30 m, 0.32 mm i.d., 0.25 m,
Elite-CLPesticides2 (N9316662)
EPA 508.1 list w/added compounds
Oven: 120 C (hold 1 min.) to 300 C @ 9 C/min.
(hold 10 min.)
Injector: Direct, Uniliner inlet liner, 200 C
Dead Time: 1.797 (Elite-CLPesticides),
1.663 (Elite-CLPesticides2)
Head Pressure: 12 psi (constant)
Carrier Gas: Helium
Flow: 2.1 mL/min. @ 120 C

27
28

32

18,21

36

3
12

31

24

33
34

19
29,
30

10
2

20

38
35

9
37
5
7

100

10

12

14
TIME (MIN.)

16

18

20

Capillary Column Applications


Environmental
51,52
35,36

Column: Elite-624 (GC/MS)


Dimensions: 75 m, 0.53 mm i.d., 3.0 m
Sample: 20 ppm of 502.2 Standards Calibration Mixes 1-6
Oven: 35 C (hold 8 min.) to 220 C at 10 C/min. (hold 3 min.)
Detector: MS, 250 C
Scan Range: 45-300AMU
Purge: 11 min.
Purge and Trap: Tenax, Silica Gel, charcoal
Desorb Preheat: 220 C, 2 min. desorb at 225 C
Desorb Flow Rate: 10 mL/min.

Part No.

33,34
37,38
43,44

40
25

Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane

8 9

10

39

30

16,17 18

58
59 60

45
22
27

11,12 13
14

Standards used are 524 Volatiles Kit:

32

28

20

N9316208

1 3
2

57
54
50 53
49
46
55
48
47

41,42

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.

Capillary Column Applications

U.S. EPA Method 524.2

21

23

24

31

26

19

10

56

29

15

15

20

25

TIME (MIN.)
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.

1, 1-Dichloroethene
Methylene Chloride
trans-1, 2-Dichloroethene
1, 1-Dichloroethane
cis-1, 2-Dichloroethene
2, 2-Dichloropropane
Bromochloromethane
Chloroform
1, 1, 1-trichloroethane
Carbon Tetrachloride

28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.

1, 1-Dichloropropene
Benzene
1, 2-Dichloroethane
Trichloroethene
1, 2-Dichloropropane
Dibromomethane
Bromodichloromethane
cis-1, 3-Dichloropropene
Toluene
trans-1, 3-Dichloropropene
1, 1, 2-Trichloroethane

Tetrachloroethene
1, 3-Dichloropropane
Dibromochloromethane
1, 2-Dibromoethane
Chlorobenzene
1, 1, 1, 2-tetrachloroethane
Ethylbenzene
m-Xylene
p-Xylene
o-Xylene
Styrene

U.S. EPA Method 551.1

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.

3
4

39.
40.
41.
42.
43.
44.
45.
46.
47.
48.
49.

Bromoform
Isopropylbenzene
Bromobenzene
1, 1, 2, 2-Tetrachloroethane
1, 2, 3-Trichloropropane
Propylbenzene
2-Chlorotoluene
1, 3, 5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1, 2, 4-Trimethylbenzene

Chloroform
1, 1, 1-Trichloroethane
Carbon Tetrachloride
Trichloroacetonitrile
Trichloroethylene
Bromodichloromethane
Chloral Hydrate
Dichloroacetonitrile
1, 1-Dichloro-2-Propanone
1, 1, 2-Trichloroethane
Chloropicrin

12.
13.
14.
15.
16.
17.
18.
19.
20.
21.

50.
51.
52.
53.
54.
55.
56.
57.
58.
59.
60.

sec-Butylbenzene
1, 3-Dichlorobenzene
p-Isopropyltoluene
1, 4-Dichlorobenzene
n-Butylbenzene
1, 2-Dichlorobenzene
1, 2-Dibromo-3-Chloropropane
1, 2, 4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1, 2, 3-Trichlorobenzene

Dibromochloromethane
1, 2-Dibromoethane (EDB)
Tetrachloroethylene
Bromochloroacetonitrile
1, 1, 1-trichloro-2-propanone
Bromoform
Dibromoacetonitrile
1, 2, 3-Trichloropropane
4-Bromofluorobenzene (I.S.)
1,2-Dibromo-3-Chloropropane (DBCP)

16

19
6
11

21
15

2
9

18

7
1

20

12

13
17
10

10

20
TIME (MIN.)

Gas Chromatography

14

30

Column: Elite-5
Dimensions: 30 m, 0.25 mm i.d., 1.0 m
Sample: 1.0 L split injection, 1 ng on-column concentration
Oven: 35 C (hold 22 min.) to 200 C at 10 C/min.
Injector: 200 C
Detector: ECD, 290 C
Carrier: Helium at 30 cm/sec.
Split Ratio: 10:1

Part No.

N9316077

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

101

Capillary Column Applications

Capillary Column Applications

Environmental
U.S. EPA Method 551.1 Chlorinated Disinfection Byproducts
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.

3
8, 14

12.
13.
14.
15.
16.
17.
18.
19.
20.
21.

Chloroform
1,1,1-Trichloroethane
Carbon Tetrachloride
Trichloroacetonitrile
Trichloroethylene
Bromodichloromethane
Chloral Hydrate
Dichloroacetonitrile
1,1-Dichloro-2-Propanone
1,1, 2-Trichloroethane
Chloropicrin

Dibromochloromethane
1, 2-Dibromoethane (EDB)
Tetrachloroethylene
Bromochloroacetonitrile
1,1,1-Trichloro-2-Propanone
Bromoform
Dibromoacetonitrile
1, 2, 3-Trichloropropane
4-Bromofluorobenzene (IS)
1, 2-Dibromo-3-Chloropropane (DBCP)

5,6
16 18,19
21

Column: Elite-200
Dimensions: 30 m, 0.25 mm i.d., 1.0 m
Sample: 1.0 L split injection,
1 ng on-column concentration
Oven: 35 C (hold 22 min.) to 200 C
@ 10 C/min.
Injector/Detector: 200 C/290 C
Carrier Gas: Helium
Linear Velocity: 30 cm/sec. @ 50 C
ECD Sensitivity: 20 kHz full scale
Split Ratio: 10:1

2
12
1

20

11,13

15
17

10
10

20

30

Part No.

TIME (MIN.)

N9316623

U.S. EPA Method 8081 Pesticides


1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.

2,4,5,6-tetrachloro-m-xylene
a-BHC
g-GHC (lindane)
b-BHC
d-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
g-Chlordane
a-Chlordane
4,4'-DDE

12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.

Endosulfan I
Dieldrin
Endrin
4,4'-DDT
Endosulfan II
4,4'-DDD
Endrin Aldehyde
Methoxychlor
Endosulfan Sulfate
Endrin Ketone
Decachlorobiphenyl

22

1
11

13

9 10

7
3

Gas Chromatography

N9316147

18
17
14 15

5
6

Part No.

20
21

Column: Elite-35
Dimensions: 30 m, 0.32 mm i.d., 0.50 m
Oven Temperature: 120 C (hold 1 min.) to 285 C
@ 8.5 C/min. (hold 6 min.)
Injector: 200 C
Detector: ECD, 300 C
Carrier Gas: Helium

12

12

15

18
TIME (MIN.)

102

19

16

21

24

Capillary Column Applications


Environmental
Capillary Column Applications

U.S. EPA Method 8081A Organochlorine Pesticides


3

26

29
17
19
16
15

6,7
4

20,22
23
24

11 12

28

21

2
14
13

10

25
18

27

9
5

10

15
TIME (MIN.)

20

25

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
29.

Dibromochloropropane
Hexachlorocyclopentadiene
2, 4, 5, 6-Tetrachloro-m-Xylene
Hexachlorobenzene
cis-Diallate
a-BHC
trans-Diallate
g-BHC
b-BHC
d-BHC
Heptachlor
Aldrin
Isodrin
Heptachlor Epoxide
g-Chlordane
a-Chlordane
4, 4'-DDE
Endosulfan I
Dieldrin
Chlorobenzilate
Endrin
4,4'-DDD
Endosulfan II
4, 4'-DDT
Endrin Aldehyde
Methoxychlor
Endosulfan Sulfate
Endrin Ketone
Decachlorobiphenyl

29

17

23
26

16
18

6
15
8

25

27

13

9
2

Gas Chromatography

21

14
11

24

22

10 12

Column: Elite-CLPesticides and


Elite-CLPesticides2
Dimensions: 30 m, 0.32 mm i.d., 0.50 m,
Elite-CLPesticides (N9316664)
Dimensions: 30 m, 0.32 mm i.d., 0.25 m,
Elite-CLPesticides2 (N9316670)
On-Column Conc.: 16160 pg
Oven: 80 C (hold 1 min.) to 300 C @ 10 C/min.
(hold 15 min.)
Injector: Direct, Uniliner inlet liner
Detector: ECD, 300 C, with Anode Purge
Dead Time: 1.9 min.
Head Pressure: 8.7 psi (constant)
Flow Rate: Helium @ 1.3 mL/min. @ 120 C

28

19

1
7
20

Part No.

N9316664

Part No.

N9316670

10

15
TIME (MIN.)

20

25

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

103

Capillary Column Applications

Capillary Column Applications

Environmental
U.S. EPA Method 8021 Volatile Organics
39/40

Column: Elite-Volatiles
Dimensions: 20 ppb in 5 mL of RO Water. 75 m, 0.45 mm i.d., 2.55 m
Concentrator: Purge and Trap
Trap: Vocarb 3000
Purge: 11 min. at 40 mL/min.
Dry Purge: 1 min. at 40 mL/min. (MCS bypassed with Silcosteel tubing)
Desorb Preheat: 245 C
Desorb: 250 C for 2 min.
Bake: 260 C for 8 min.
Interface: direct
Transfer Line: 0.32 mm i.d.
Oven: 35 C (hold 12 min.) to 60 C at 5 C/min. (hold 1 min.) to 220 C at 17 C/min.
(hold 3 min.)
Carrier: Helium at 9 mL/min.
Detectors: PID/ELCD
PID: makeup 7 mL/min., purge 7 mL/min., set at 0.35 mV base temp 200 C
ELCD: Reaction Gas 25mL/min.
Reaction Temp.: 940 C, propanol flow 470 L/min.

Part No.

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
29.
30.

enlarged
view from
PID
52

62
48

42

45

37

51
50

54 57

49

59
58

38

60

53

47

N9316393

31.
32.
33.
34.
35.
36.
37.
38.
39.
40.
41.
42.
43.
44.
45.
46.
47.
48.
49.
50.
51.
52.
53.
54.
55.
56.
57.
58.
59.
60.

Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1, 1-Dichloroethene
Methylene Chloride
Freon113
trans-1, 2-Dichloroethene
Methyl-tert-Butyl-Ether
1, 1-Dichloroethane
cis-1, 2-Dichloroethene
Bromochloromethane
Chloroform
2, 2-Dichloropropane
1, 2-Dichloroethane
1, 1, 1-Trichloroethane
1, 1-Dichloropropene
Carbon Tetrachloride
Benzene
Fluorobenzene
Dibromomethane
1, 2-Dichloropropane
Trichloroethene
Bromodichloromethane
2-Chloroethylvinylether
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
1, 1, 2-Trichloroethane

Toluene
1, 3-Dichloropropane
Dibromochloromethane
1, 2-Dibromoethane
Tetrachloroethene
1, 1, 1, 2-Tetrachloroethane

61.
62.
63.
64.
65.
66.

1, 2-Bromo-3-Chloropropane
4-Bromo-1-Chlorobenzene

22.5

1, 2, 4-Trichlorobenzene

25.0

Hexachlorobutadiene
1, 2, 3-Trichlorobenzene

Chlorobenzene
Ethyl Benzene
m-Xylene
p-Xylene
Bromoform
Styrene
1, 4-Dichlorobutane
1, 1, 2, 2-Tetrachloroethane
1, 2, 3-Trichloropropane
Isopropyl Benzene
Bromobenzene
n-Propyl Benzene
2-Chlorotoluene
4-Chlorotoluene

57

1, 3, 5-Trimethylbenzene

30

sec-Butylbenzene
1, 3-Dichlorobenzene

10

1, 4-Dichlorobenzene

2
1

p-Isopropyl Toluene
1, 2-Dichlorobenzene

15

12

25

63
64
66
65

14

32

37 44

29
28

13

n-Butylbenzene

16

24

62
33

26

18
17 19

34

51
50
46
43
41 48

35

23

21
22

11

25

19

27

ELCD

29
27 28

61

22
5

10

15

20

25

5
TIME (MIN.)

104

66
59

1, 2, 4-Trimethylbenzene

13

63

56

tert-Butylbenzene

10

65

35 36

o-Xylene

20

PID

27.5

Naphthalene

31

55 56

10

15

20

25

Capillary Column Applications


Environmental
Capillary Column Applications

U.S. EPA Method 8260B Volatile Organics


77,78
96,97

90-92
73-75

101,102

86-89
95

82

98

94

79 80
84

103
100

104

93

83

76

99

85
81

11.5

11.6

11.7

11.8

11.9

12.0

12.1

12.2 12.3 12.4


TIME (MIN.)

Column: Elite-VMS
Dimensions: 40 m, 0.18 mm i.d., 1.0 m
Conc.: 5 ppb each in 25 mL of RO water
Trap: Vocarb 3000
Purge: 11 min. @ 40 mL/min.
Dry Purge: 1 min. @ 40 mL/min. (MCS by-passed
with Silcosteel Tubing)
Desorb Preheat: 245 C
Desorb: 2 min. @ 250 C
Desorb Flow Rate: 45 mL/min. Helium
Bake: 8 min. @ 260 C
Interface: Plumbed through injection port

Part No.

12.7

12.8

12.9

13.0

Transfer Line: Silcosteel transfer line


Mount Temperature: 40 C
Split Ratio: 1:40 split
Injector: 250 C
Carrier Gas: 1.1 mL/min. Helium, constant flow
Linear Velocity: 32 cm/sec. @ 40 C
Oven: 35 C (hold 2 min.) to 60 C @ 4 C/min.
(hold 0 min.) to 225 C @ 40 C/min.
(hold 5 min.)
Source Temperature: 280 C
Scan Range: 35260 amu
Ionization: EI

62-64

66,67
65

N9316651

1
2 3 5
4
2.0

Carbon Dioxide
Dichlorodifluoromethane
Freon 114
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
Ethanol
Diethyl Ether
1, 1-Dichloroethene
Lodomethane
Carbon Disulfide
Freon 113
Acrolein
Allyl Chloride
Methylene Chloride
Acetone
trans-1,2-Dichloroethene
Methyl Acetate
Methyl tert-Butyl Eether
tert-Butyl Alcohol

108
106,107 109 110

60
59
69 72
58
49 50
45
51
68 71
42,43
54 53 57
46
35-38
28,29
70
55
40,41
21
44
52 56
47
11-13 1617 19 20 24 25,26
30 31 3334 39
32
61
8
10 14
18
6 7
22 23 27
9
15
48
3.0

4.0

23.
24.
25.
26.
27.
28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.
39.
40.
41.
42.
43.
44.

5.0

Acetonitrile
Diisopropyl Ether
Chloroprene
1, 1-Dichloroethane
Acrylonitrile
Vinyl Acetate**
Ethyl-tert-Butyl Ether**
cis-1, 2-Dichloroethene
2, 2-Dichloropropane
Bromochloromethane
Chloroform
Carbon Tetrachloride
Ethyl Acetate
Methyl Acrylate
Dibromofluoromethane
Tetrahydrofuran
1, 1, 1-Trichloroethane
2-Butanone
1, 1-Dichloropropene
Benzene
Propionitrile
Methacrylonitrile

6.0

7.0

45.
46.
47.
48.
49.
50.
51.
52.
53.
54.
55.
56.
57.
58.
59.
60.
61.
62.
63.
64.
65.
66.

8.0
9.0
TIME (MIN.)

Pentafluorobenzene
tert-Amyl-Methyl Ether
1, 2-Dichloroethane
Isobutyl Alcohol
Isopropyl Acetate
Trichloroethene
1, 4-Difluorobenzene
Dibromomethane
1, 2-Dichloropropane
Bromodichloromethane
Methyl Methacrylate
n-Propyl Acetate
2-Chloroethyl Vinyl Ether
cis-1, 3-Dichloropropene
Toluene-d8
Toluene
2-Nitropropane
Tetrachloroethene
4-Methyl-2-Pentanone
trans-1, 3-Dichloropropene
2-Bromo-1-Chloropropane
1, 1, 2-Trichloroethane

10.0

67.
68.
69.
70.
71.
72.
73.
74.
75.
76.
77.
78.
79.
80.
81.
82.
83.
84.
85.
86.
87.
88.

11.0

105

12.0

Ethyl Methacrylate
Dibromochloromethane
1, 3-Dichloropropane
1, 2-Dibromoethane
n-Butyl Acetate
2-Hexanone
Chlorobenzene-d5
Chlorobenzene
Ethylbenzene
1, 1, 1, 2-Tetrachloroethane
m-Xylene
p-Xylene
o-Xylene
Styrene
Bromoform
Isopropylbenzene
n-Amyl Acetate
4-Bromo-1-Fluorobenzene (ss)
cis-1,4-Dichloro-2-Butene
n-Propylbenzene
Bromobenzene
1, 4-Dichlorobutane

13.0

89.
90.
91.
92.
93.
94.
95.
96.
97.
98.
99.
100.
101.
102.
103.
104.
105.
106.
107.
108.
109.
110.

14.0

15.0

1, 1, 2, 2-Tetrachloroethane
2-Chlorotoluene
1, 3, 5-Trimethylbenzene
1, 2, 3-Trichloropropane
trans-1, 4-Dichloro-2-Butene
4-Chlorotoluene
tert-Butylbenzene
Pentachloroethane
1, 2, 4-Trimethylbenzene
sec-Butylbenzene
p-Isopropyltoluene
1, 3-Dichlorobenzene
1, 4-Dichlorobenzene-d4
1, 4-Dichlorobenzene
n-Butylbenzene
1, 2-Dichlorobenzene
1, 2-Dibromo-3-Chloropropane
Nitrobenzene
Hexachlorobutadiene
1, 2, 4-Trichlorobenzene
Naphthalene
1, 2, 3-Trichlorobenzene

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.

12.5 12.6

* 2-Chloroethanol in 8260B mix requires lower scan range for identification;


1, 4-Dioxane requires fortification or identification using single-point high-calibration standard.
** Peaks 28 & 29 share ion (43).

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

105

Capillary Column Applications

Capillary Column Applications

Environmental
U.S. EPA Method 8260B Volatile Organics
Column: Elite-Volatiles
Dimensions: 30 m, 0.25 mm i.d., 1.40 m
Conc.: TurboMatrix 110 Headspace Trap
Trap: Air Monitoring
Thermostating Time: 80 C
Needle Temperature: 90 C
Dry Purge: 5 min.
Desorb Temperature: 280 C
Desorb Time: 0.5 min.
Oven Temperature: 40 C (hold 2 min.) to 100 C @ 10 C/min. (hold 0 min.)
to 240 C @ 30 C/min. (hold 5 min.)
Carrier Gas: Helium at 1 mL/min.
Detector: MS
Scan Time: 0.10 sec.
Transfer Line Temperature: 200 C
Source Temperature: 200 C
Trap Emission: 75 A

Part No.

N9316388

TIME (MIN.)

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.

106

Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
Ethanol (2500 ppb)
1,1-Dichloroethene
Carbon Disulfide (40 ppb)
Allyl Chloride
Methylene Chloride
Acetone
trans-1, 2-Dichloroethene
Methyl tert-Butyl Ether
tert-Butyl Alcohol (100 ppb)
Disopropyl Ether
1,1-Dichloroethane
Acrylonitrile
Vinyl Acetate
Allyl Alcohol (250 ppb)
Ethyl-tert-Buyl Ether
cis-1, 2-Dichloroethene
2, 2-Dichloropropane
Bromochloromethane
Chloroform

26.
27.
28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.
39.
40.
41.
42.
43.
44.
45.
46.
47.
48.
49.
50.

Ethyl Acetate
Carbon Tetrachloride
Methyl Acrylate
Propargyl Alcohol (500 ppb)
Dibromofluoromethane (SMC)
Tetrahydrofuran
1,1,1-Trichloroethane
2-Butanone
1,1-Dichloropropene
Benzene
Pentafluorobenzene (IS)
tert-Amyl-Methyl Ether
1, 2-Dichloroethane
Isobutyl Alcohol (500 ppb)
Isopropyl Acetate
Trichloroethene
1, 4-Difluorobenzene (SMC)
Dibromomethane
1, 2-Dichloropropane
Bromodichloromethane
Methyl Methacrylate
n-Propyl Acetate
2-Chloroethanol (2500 ppb)
cis-1, 3-Dichloropropene
Toluene-d8 (SMC)

51.
52.
53.
54.
55.
56.
57.
58.
59.
60.
61.
62.
63.
64.
65.
66.
67.
68.
69.
70.
71.
72.
73.
74.
75.

Toluene
Pyridine (250 ppb)
Tetrachloroethene
4-Methyl-2-Pentanone
trans-1, 3-Dichloropropene
1,1, 2-Trichloroethane
Ethyl Methacrylate
Dibromochloromethane
1, 3-Dichloropropane
1, 2-Dibromoethane
n-Butyl Acetate
2-Hexanone
2-Picoline (250 ppb)
Chlorobenzene-D5 (IS)
Chlorobenzene
Ethylbenzene
1,1,1, 2-Tetrachloroethane
m-Xylene
p-Xylene
o-Xylene
Stryrene
Bromoform
Isopropylbenzene
4-Bromo-1-Fluorobenzene (SMC)
Bromobenzene

76.
77.
78.
79.
80.
81.
82.
83.
84.
85.
86.
87.
88.
89.
90.
91.
92.
93.
94.
95.
96.
97.

n-Propylbenzene
1,1, 2, 2-Tetrachloroethane
2-Chlorotoluene
1, 3, 5-Trimethylbenzene
1, 2, 3-Trichloropropane
4-Chlorotoluene
tert-Butylbenzene
Pentachloroethane
1, 2, 4-Trimethylbenzene
sec-Butylbenzene
p-Isopropyltoluene
1, 3-Dichlorobenzene
1, 4-Dichlorobenzene-d4 (IS)
1, 4-Dichlorobenzene
n-Butylbenzene
1, 2-Dichlorobenzene
1, 2-Dibromo-3-Chloropropane
Nitrobenzene (250 ppb)
Hexachlorobutadiene
1, 2, 4-Trichlorobenzene
Naphthalene
1, 2, 3-Trichlorobenzene

Capillary Column Applications


Environmental
Capillary Column Applications

U.S. EPA Method 8270 Semi-Volatile Organics

Column: Elite-5 ms
Dimensions: 30 m, 0.25 mm i.d., 0.5 m
Sample: 80 ng splitless injection of CLP standard
Oven: 40 C (hold 2 min.) to 290 C at 20 C/min.
(hold 0 min.) to 303 C at 2 C/min. (hold
0 min.) to 330 C at 6 C/min. (hold 1 min.)
Injector: 300 C
Detector: MS, 280 C, scan range 35-550 AMU
Carrier: Helium at 1.0 mL/min.

47

10
34

58

6,7

Part No.

89
67

N9316284

87,88

81

85
82

93
95,96
97
90 91

84
1,2
86

5
3

100
99

98

94

101

104,105 106

92
102 103

83

10

11

12

13

14

15

16

17

18

19

20

21

22

23

24

47

10,11
16,17
34

41

27,28

20 21,22

6,7

42
58

13,14
12

38

32
18

25

15

67
68,69
72

35,36

66
46

26

31

61

48

39

45

33

19

43

37

54

8.5

9.0

9.5

10.0

64

57

73

77
76

59

8.0

71

53

7.5

70

65

80 81

74 75

51 52

50

7.0

62,63

44

40

29,30

23 24

55

49

10.5

79
78

60

11.0

11.5

12.0

12.5

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.

n-Nitrosodimethylamine
Pyridine
Methyl Methanesulfonate
2-Fluorophenol
Ethyl Methanesulfonate
Phenol-d6
Phenol
Aniline
Bis(2-chloroethyl)ether
2-Chlorophenol-d4
2-Chlorophenol
1, 3-Dichlorobenzene
1, 4-Dichlorobenzene-d4
1, 4-Dichlorobenzene
Benzyl Alcohol
1, 2-Dichlorobenzene-d4
1, 2-Dichlorobenzene
2-Methylphenol

19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
29.
30.
31.
32.
33.
34.
35.

Bis(2-chloroisopropyl)ether
4-Methylphenol/
3-Methylphenol
n-Nitroso-di-n-Propylamine
Acetophenone
Hexachloroethane
Nitrobenzene-d5
Nitrobenzene
Isophorone
2, 4-Dimethylphenol
2-Nitrophenol
Benzoic Acid
Bis (2-Chloroethoxy) Methane
2, 4-Dichlorophenol
1, 2, 4-Trichlorobenzene
Naphthalene-d8
Naphthalene
2, 6-Dichlorophenol

36.
37.
38.
39.
40.
41.
42.
43.
44.
45.
46.
47.
48.
49.
50.
51.
52.
53.

4-Chloroaniline
Hexachloropropene
Hexachlorobutadiene
4-Chloro-3-Methylphenol
Isosafrole
2-Methylnaphthalene
1-Methylnaphthalene
Hexachlorocyclopentadiene
1 ,2, 4, 5-Tetrachlorobenzene
2, 4, 6-Trichlorophenol
2, 4, 5-Trichlorophenol
2-Fluorobiphenyl
Safrole
2-Chloronaphthalene
2-Nitroaniline
1, 4-Naphthoquinone
Dimethylphthalate
1, 3-Dinitrobenzene

54.
55.
56.
57.
58.
59.
60.
61.
62.
63.
64.
65.
66.
67.
68.
69.
70.
71.

2, 6-Dinitrotoluene
Acenaphthylene
3-Nitroaniline
Acenaphthene-d10
Acenaphthene
2, 4-Dinitrophenol
4-Nitrophenol
Pentachlorobenzene
2,4-Dinitrotoluene
Dibenzofuran
2, 3, 4, 6-Tetrachlorophenol
Diethyl Phthalate
4-Chlorophenyl Phenyl Ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-Methylphenol
Diphenylamine
Azobenzene

72.
73.
74.
75.
76.
77.
78.
79.
80.
81.
82.
83.
84.
85.
86.
87.
88.
89.

2, 4, 6-Tribromophenol
Phenacetin
4-Bromophenyl-Phenyl ether
Hexachlorobenzene
Pentachlorophenol
Pentachloronitrobenzene
Dinoseb
Phenanthrene-d10
Phenanthrene
Anthracene
Di-n-Butylphthalate
4-Nitroquinoline-1-Oxide
Isodrin
Fluoranthene
Benzidine
Pyrene
Aromite
p-Terphenyl-d14

Gas Chromatography

TIME (MIN.)
90. Chlorbenzilate
91. Butyl Benzyl Phthalate
92. Kepone
93. Bis(2-ethylhexyl)phthalate
94. 3, 3'-Dichlorobenzidine
95. Benzo (a) Anthracene
96. Chrysene-d12
97. Chrysene
98. Di-n-Octyl Phthalate
99. Benzo (k) Fluoranthene
100. Benzo (b) Fluoranthene
101. Benzo (a) Pyrene
102. Perylene-d12
103. 3-Methylcholanthrene
104. Indeno (1, 2, 3-cd) Pyrene
105. Dibenzo (a, h) Snthracene
106. Benzo (g, h ,i) Perylene

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

107

Capillary Column Applications


Environmental
Column: Elite-1
Dimensions: 60 m, 0.25 mm i.d., 0.25 m
Sample: 1.0 L split injection of Citronella Java Oil
Oven: 100 C to 260 C at 4 C/min. (hold 1 min.)
Injector: 250 C
Detector: MS, 280 C
Carrier: Helium at 30 cm/sec.
Split Vent: 100 cc/min.

Capillary Column Applications

Essential Oils Citronella Java Oil

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.

Limonene
Citronellal
Linalool
Borneol
-Elemene
-Caryophyllene
Neryl Acetate
-Terpineol
Germancrene-
-Citronellol
Geranyl Acetate
-Cadenene
Nerol
Geraniol
Eugenol
-Bergamotene

10 14
1

11
7

Part No.

N9316013
16

12

15
3
13

10

12

14

16

18

20

22

24

26

28

TIME (MIN.)

Nitrogen Containing Herbicides


1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.

Eptam
Sutan
Vernam
Tillam
Ordram
Propachlor
Ro-Neet
Treflan
Balan
Simazine
Atrazine

Gas Chromatography

12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.

Propazine
Tolban
Terbacil
Sencor
Bromacil
Dual
Paarlan
Prowl
Oxadiazon
GOAL
Hexazinone

2 4
3

Column: Elite-5
Dimensions: 30 m, 0.53 mm i.d., 5.0 m
Sample: 0.2 L direct injection of nitrogen containing herbicides.
Concentration approximately 10 ng per component.
Oven Temperature: 60 C (hold 1 min.) to 290 C @ 15 C/min.
(hold 5 min.)
Injector: 290 C
Detector: FID, 290 C
Carrier Gas: Helium @ 40 cm/sec.

Part No.

67
17 19
9
8

18

13
12
15
11
10 14

10
TIME (MIN.)

108

N9316102

12

20 21

22

16

14

16

18

Capillary Column Applications


Environmental

1.
2.
3.
4.
5.
6.
7.
8.

9.
10.
11.
12.
13.
14.
15.
16.

Tetrachloro-m-xylene
a-BHC
g-BHC
Heptachlor
Aldrin
b-BHC
d-BHC
Heptachlor Epoxide

17.
18.
19.
20.
21.
22.

Endosulfan I
g-Chlordane
a-Chlordane
P, P'-DDE
Dieldrin
Endrin
P, P'-DDD
Endosulfan II

Column: Elite-5
Dimensions: 30 m, 0.53 mm i.d., 5.0 m
Sample: 1.0 L direct injection of a pesticide mix.
Concentration: 80-800 ppb (ng/mL)
Oven Temperature: 150 C (hold 5 min.) to 275 C
@ 4 C/min. (hold 5 min.)
Injector: 200 C
Detector: ECD, 275 C
Carrier Gas: Helium @ 40 cm/sec.

Part No.

Capillary Column Applications

20

Pesticides

22

P, P'-DDT
Endrin Aldehyde
Endosulfan Sulfate
Methoxychlor
Endrin Ketone
Decachlorobiphenyl

12
13

21
14
16
15
18

17
19

9
2

10 11

N9316102
6

10

20

30

TIME (MIN.)

Synthetic Essential Oil Mixture

29 31

3,4
20,21

42

35
27

14
19
18

23,24
38

6,7

15

30

22

16
5
10

8
11,12
13
9

39

41

32,33
34

25
26
17

37

10

15

20
TIME (MIN.)

25

22.
23.
24.
25.
26.
27.
28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.
39.
40.
41.
42.

Nerol
Carveol
Anisaldehyde
Carvone
Geraniol
Anethole
Cinnamic Alcohol
Eugenol
Neryl Acetate
Geranyl Acetate
Vanillin
Coumarin
-Ionone
Ethyl Vanillin
-Caryophyllene
-Caryophyllene
-Ionone
Valencene
Ethyl Laurate
Amyl Cinnamic Aldehyde
Nootketone

Column: Elite-1
Dimensions: 60 m, 0.25 mm i.d., 0.25 m
Sample: 1.0 L split injection of 42 flavor components
Oven: 100 C to 260 C at 4 C/min. (hold 1 min.)
Injector: 250 C
Detector: 280 C
Carrier: Helium at 30 cm/sec.
Split Vent: 100 cc/min.

40

36

Ethyl Butyrate
trans-2-Hexenol
-Pinene
Benzaldehyde
Camphene
Octanol
-Myrcene
-Pinene
-Phellandrene
p-Cymene
l-Limonene
Camphor
trans-Sabinene Hydrate
Linalool
Citronellal
l-Menthone
Menthofuran
l-Menthol
-Terpineol
Linalyl Acetate
-Citronellol

Gas Chromatography

28

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.

30

Part No.

N9316013

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

109

Capillary Column Applications


Food and Flavors
Capillary Column Applications

Brewing Beer
1.
2.
3.

Column: Elite BAC-1


Dimensions: 30 m x 0.32 mm x 1.8 m
Instrument: Headspace TurboMatrix 40

Chloroform
2, 3-Butanedione (Diacetyl)
2, 3-Pentanedione

Table 2: HS Conditions
Sample Temperature: 60 C
Needle Temperature: 80 C
Transfer Line Temperature: 100 C
Equilibration Time: 15 min.
Pressurization Time: 1.0 min.
Injection Time: 0.1 min.
Withdrawal Time: 0.0 min.
Carrier Pressure: 35 psi

3
180
160
140
2
120
100
80
60
40
1
20

0.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

1.6

1.8

2.0

2.2

2.4

2.6

2.8

3.0

3.2

3.4

3.6

3.8

Table 3: GC with ECD Conditions


Initial Temperature: 45 C
Time 1: 1.3 min.
Rate 1: 40 C/min.
Final Temperature: 150 C
Hold: 0.6 min
Injector Temperature: 100 C
Liner: Zero Dilution
Split: 25 mL/min.
ECD: 150 C
ECD Attenuation: 1
Makeup Gas (Argon/Methane) 30 mL/min.

TIME (MIN.)

Part No.

N9316579

Essential Oils Lemon Oil


7,8
14 15

2 3 56

29

38

32
33

36

17

Column: Elite-5
Dimensions: 30 m, 0.32 mm i.d., 0.25 m
Sample: Wet needle split injection of
a neat lemon oil
Oven: 75 C (hold 8 min.) to 250 C
at 4 C/min.
Injector: 250 C
Detector: FID, 250 C
Carrier: Hydrogen at 40 cm/sec.
Split Ratio: 100:1

Part No.

26

N9316086

13
35

12

Gas Chromatography

10
4

20

11

21 22

18 19

24
23

1
2

1.
2.
3.
4.
5.
6.
7.
8.

110

16
4

Heptanol
-Thujene
-Pinene
Camphene
Sabinene
-Pinene
6-Methyl-5-Hepten-2-One
Myrcene

9.
10.
11.
12.
13.
14.
15.
16.

10

Octanal
-Phellandrene
3-Carene
-Terpinene
-Cymene
Limonene
-Terpinene
Octanol

12

25

27,28

37

31

30

14
16
TIME (MIN.)
17.
18.
19.
20.
21.
22.
23.
24.

34
18

Terpinolene
Linalool
Nonanal
Citronellal
Terpinen-4-ol
-Terpineol
Decanol
Octyl Acetate

20

22

25.
26.
27.
28.
29.
30.
31.
32.

24

26

Nerol
Neral
Carvone
Geraniol
Geranial
Nonyl Acetate
Citronellyl Acetate
Neryl Acetate

28

33.
34.
35.
36.
37.
38.

Geranyl Acetate
Dodecanal
-Caryophyllene
trans--Bergamotene
-Humulene
-Bisabolene

Capillary Column Applications


Food and Flavors

2 4 67

15

13

Column: Elite-WAX ETR


Dimensions: 60 m, 0.25 mm i.d., 0.25 m
Sample: 0.2 L split injection of a neat spearmint oil
Oven: 75 C (hold 4 min.) to 200 C at
4 C/min. (hold 10 min.)
Injector: 250 C
Detector: FID, 250 C
Carrier: Hydrogen at 40 cm/sec.
Split Ratio: 100:1

25

19

16

Part No.

18

N9316551

28

21

17

Capillary Column Applications

Essential Oils Native Spearmint Oil

29
24
9
8 1011

1.
2.
3.
4.
5.
6.

-Pinene
-Pinene
Sabinene
Myrcene
-Terpinene
L-Limonene

30

12

20 22

7.
8.
9.
10.
11.
12.

23

14

10

12

26 27

14

16
18
TIME (MIN.)
13.
14.
15.
16.
17.
18.

1, 8-Cineole
cis-Ocimene
-Terpinene
p-Cymene
Terpinolene
3-Octyl Acetate

20

22

24

26

19.
20.
21.
22.
23.
24.

3-Octanol
L-Menthone
trans-Sabinenehydrate
-Bourbonene
Linalool
Terpinene-4-ol

28

30

32

-Caryophyllene
Dihydrocarvone
trans-Dihydrocarvyl Acetate
trans--Farnesene
-Terpineol
Germacrene-

25.
26.
27.
28.
29.
30.

Carvone
cis-Carvyl Acetate
trans-Carveol
cis-Carveol
cis-Jasmone
Viridiflorol

Essential Oils Synthetic Mushroom Aroma


20

3
17

14
10

15
12

9
7

18

13

19

1
11
2

16

4
5

Acetone
Ethyl Acetate
Methylene Chloride
Hexanal
Amyl Acetate
1-Butanol
3-Methyl-1-Butanol
1-Pentanol
3-Octanone
3-Octanol
Nonanal
1-Octen-3-ol
Furfural
Benzaldehyde
Octyl Alcohol
Phenylacetaldehyde
-Terpineol
2, 4-Nonadienal
2, 4-Decadienal
Benzyl Alcohol

10

12

14

16
TIME (MIN.)

18

20

22

24

26

28

30

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.

Column: Elite-WAX ETR


Dimensions: 30 m, 0.32 mm i.d., 1.0 m
Sample: 1.0 L split injection of a synthetic mushroom aroma,
concentration 10 ng per component
Oven: 40 C to 220 C at 6 C/min.
Injector: 260 C
Detector: FID, 260 C
Carrier: Hydrogen at 40 cm/sec.
Split Ratio: 100:1

Part No.

N9316557

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

111

Capillary Column Applications


Food and Flavors
Capillary Column Applications

Sugars As Alditol Acetates


1.
2.
3.
4.
5.
6.
7.
8.

78
2
1

Rhamnitol
Fucitol
Ribitol
Arabinitol
Mannitol
Galactitol
Glucitol
Inositol

56

4
3

Column: Elite-225
Dimensions: 15 m, 0.25 mm i.d., 0.25 m
Sample: 0.5 L split injection of alditol
acetate derivatives
Oven: 190 C (hold 5 min.) to 250 C
at 8 C/min. (hold 5 min.)
Injector: 260 C
Detector: 260 C
Carrier: Helium at 42 cm/sec.
Split Ratio: 50:1

Part No.
2.5

7.5

10

N9316175

12.5

TIME (MIN.)

TCA in Wine

1.
2.

Natural Wine Separation Products


TCA

TCA 12127
100

SIR of 2 Channels El+ 1


TIC
35166

Gas Chromatography

Column: Elite-5ms
Dimensions: 30 m x 0.25 mm x 0.25 m
Instrument: Clarus 500 GC/MS
Oven: 50 C (hold 4 min.) to 240 C at
40 C/min. (hold 5 min.)
Injector: 150 C
Carrier: Helium (99.999%)
Instrument: TurboMatrix Headspace
HS-40 Trap
Needle Temperature: 75 C
Transfer Line Temperature: 75 C
Oven Temperature: 75 C
Trap Low Temperature: 40 C
Trap High Temperature: 280 C
Dry Purge Time: 5 min.
Trap Hold Time: 5 min.
Desorb Pressure Time: 0 min.
Thermostatting Time: 30 min.
Pressurization: 1 min., 3 cycles
Decay Time: 1.2 min.
Vial Pressure: 40 psi
Column Pressure: 25 psi
Trap Sorbent: CarboPack Y

Part No.

1
0
4.49

112

4.69

4.89

5.09

5.29

5.49

5.69

5.89

6.09 6.29 6.49


TIME (MIN.)

6.69

6.89

7.09

7.29

7.49

7.69

7.89

8.09

N9316282

Capillary Column Applications


Forensics/Clinical Toxicology
Capillary Column Applications

Anabolic Steroids Underivatized

Column: Elite-5
Dimensions: 30 m, 0.25 mm i.d., 0.10 m
Sample: 0.5 L split injection of anabolic steroids
Concentration 1000 ng/L
Oven: 180 C to 340 C at 10 C/min. (hold 3 min.)
Injector: 280 C
Detector: FID, 340 C
Carrier: Helium at 35 cm/sec.
Split Ratio: 50:1

10,11

Part No.

N9316075

1 3
5

13
7

6
15
12

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.

19

17

18

14

10

16

12

14

16

18

TIME (MIN.)

5-Androstene-3,17-diol
17-Methyl-5-Androstene-3,17-Diol
5-Androstan-17-ol-3-One
19-Nortestosterone
17-Methylandrostan-17-ol-3-One
Mesterolone
Testosterone
17-Methyltestosterone
1-Dehydrotestosterone
1-Dehydro-17-Methyltestosterone
Bolasterone
Oxymethalone
19-Nortestosterone-17-Propionate
Testosterone Propionate
Fluoxymesterone
4-Chlorotestosterone-17-Acetate
Testosterone-17-Cypionate
1-Dehydrotestosterone Benzoate
1-Dehydrotestosterone Undecylenate

Cannabinoids TMS Derivatives


Column: Elite-5
Dimensions: 15 m, 0.25 mm i.d., 0.25 m
Sample: 1.0 L splitless injection of cannabinoids,
concentration 100 g/mL
Oven: 50 C (hold 0.5 min.) to 225 C at 30 C/min.,
to 325 C at 10 C/min.
Injector: 225 C
Detector: MS, 320 C
Carrier: Helium at 40 cm/sec.
Splitless Hold Time: 0.75 min.
Scan Range: 40-500 AMU

Part No.

4
1

2
5

N9316073
3

Cannabidiol
8-Tetrahydrocannabinol
9-Tetrahydrocannabinol
Cannibinol
11-Hydroxy-9-Tetrahydrocannabinol
11-Nor-9-Tetrahydrocannabinol Carboxylic Acid
11-Nor-8-Tetrahydrocannabinol Carboxylic Acid

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.

10

11

12

13

14

15

TIME (MIN.)

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

113

Capillary Column Applications

Capillary Column Applications

Forensics/Clinical Toxicology
Blood Alcohol
Conc. w/v
1.
2.
3.
4.
5.
6.

Methanol
Acetaldehyde
Ethanol
Isopropanol
Acetone
n-Propanol

0.1%
0.2%
0.2%
0.1%
0.01%
0.1%

6
2
1

5
3

1.0

1.2

1.4

1.6

1.8
2.0
TIME (MIN.)

2.2

2.4

2.6

2.8

3.0

Column: Elite-BAC-1
Dimensions: 30 m x 0.32 mm x 1.8 m
Sample: 1.0 mL Blood Alcohol Mix
Oven: 40 C Isothermal
Injector: 200 C
Carrier: Helium
Sample Equilibration Temperature: 70 C
Sample Equilibration Time: 15 min.
Vial Pressure: 30 psi
Vial Pressurization Time: 0.15 min.
Vial Sampling Time: 0.01 min.
Transfer Line: 0.32 mm i.d. FS Hydroguard TM Tubing (N9301357)
Transfer Line Temperature: 200 C
Injection Port Sleeve: 2 mm i.d.
Split Flow: 20 mL per min.

Part No.

N9316579

Blood Alcohol
Conc. w/v
1.
2.
3.
4.
5.
6.

Methanol
Acetaldehyde
Ethanol
Isopropanol
Acetone
n-Propanol

0.1%
0.2%
0.2%
0.1%
0.01%
0.1%

1
6
4
2

Gas Chromatography

1.0

1.2

1.4

1.6

1.8

2.0

TIME (MIN.)

2.2

2.4

2.6

2.8

3.0

Column: Elite-BAC-2
Dimensions: 30 m x 0.32 mm x 1.2 m
Sample: 1.0 mL Blood Alcohol Mix
Oven: 40 C Isothermal
Injector: 200 C
Carrier: Helium
Sample Equilibration Temperature: 70 C
Sample Equilibration Time: 15 min.
Vial Pressure: 30 psi
Vial Pressurization Time: 0.15 min.
Vial Sampling Time: 0.01 min.
Transfer Line: 0.32 mm i.d. FS Hydroguard Tubing (N9301357)
Transfer Line Temperature: 200 C
Injection Port Sleeve: 2 mm i.d.
Split Flow: 20 mL per min.

Part No.

114

N9316577

Capillary Column Applications


Forensics/Clinical Toxicology
Capillary Column Applications

Cocaine and Metabolites

2
1.
2.
3.
4.
5.

Ecgonine Methyl Ester (TMS)


Ecgonine (TMS)
Cocaine
Coca Ethylene
Benzoylecgonine (TMS)

5
4
3

Column: Elite-5
Dimensions: 30 m, 0.25 mm i.d., 0.25 m
Sample: 1.0 L split injection of cocaine
and cocaine metabolites
Oven: 150 C to 320 C at 10 C/min.
Injector: 250 C
Detector: FID, 300 C
Carrier: Helium at 30 cm/sec.
Split Ratio: 30:1

Part No.
2

10

12

14

N9316076

16

TIME (MIN.)

Sympathomimetic Amines HFBA Derivatives


1.
2.
3.
4.
5.
6.
7.
8.
9.
10.

Amphetamine - HFBA
Phentermine - HFBA
Phenylpropanolamine - HFBA
Ephedrine - HFBA
Methamphetamine - HFBA
Fenfluramine - HFBA
Pseudoephedrine - HFBA
Methylenedioxyamphetamine - HFBA
Methylenedioxymethamphetamine - HFBA
Methylphenidate - HFBA

Column: Elite-5
Dimensions: 30 m, 0.25 mm i.d., 0.25 m
Sample: 1.0 L splitless injection of sympathomimetic amines
Concentration approximately 2.5 ng/L
Oven: 40 C (hold 1 min.) to 150 C at 30 C/min., to 300 C at 5 C/min.
Injector: 225 C
Detector: MS, 275 C
Carrier: Helium at 20 cm/sec.
Splitless Hold Time: 1 min.

Part No.

N9316076

4
2

Gas Chromatography

6
9
8
10

10

12

14

16

18

TIME (MIN.)

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

115

Capillary Column Applications

Capillary Column Applications

Industrial Chemicals
Alcohols and Aldehydes
Column: Elite-WAX ETR
Dimensions: 60 m, 0.53 mm i.d., 1.0 m
Sample: 1.0 L split injection of alcohols
and aldehydes
Oven: 45 C (hold 10 min.) to 250 C
at 12 C/min. (hold 20 min.)
Injector: 250 C
Detector: MS, 285 C
Carrier: Helium at 50 cm/sec.
Split Ratio: 7:1

Part No.

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.

N9316571

14.
15.
16.
17.

Pentane
Heptane
Acetaldehyde
Dimethoxy Methane
Butyraldehyde
3-Pentanol
1-Penten-3-ol
3-Octanol
Cyclohexanol
Furfural
Pentadecane
Benzaldehyde
Ethylene Glycol and
2-Methyl-2, 4-Pentanediol
Furfuryl Alcohol
Nonadecane
1, 4-Butanediol
Diethylene Glycol

11

9
14
12,13
7
15

17
8
16

6
1 2
3

5
10
4

10

15
TIME (MIN.)

20

25

Alcohol Mixtures
Column: Elite-WAX ETR
Dimensions: 60 m, 0.53 mm i.d., 1.0 m
Sample: 1.0 L split injection of alcohols
Oven: 45 C (hold 10 min.) to 250 C
at 12 C/min. (hold 20 min.)
Injector: 250 C
Detector: MS (EI), 250 C
Carrier: Helium at 51 cm/sec.
Split Ratio: 8:1

Part No.

15

N9316571

10

18

16

13

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.

Pentane
Methanol
2-Methyl-2-Propanol (tert-Butylalcohol)
2-Methyl-3-Buten-2-ol
3-Buten-2-ol
Undecane
2, 2-Dimethyl-1-Propanol (Neopentanol)
1-Penten-3-ol
2-Methoxyethanol
2, 2, 2-Trifluoroethanol

11.
12.
13.
14.
15.
16.
17.
18.
19.
20.

17

2-Ethoxyethanol
1-Pentanol
2-Methyl-1-Pentanol
2, 2-Dimethyl-1-Pentanol
Tetradecane
trans-2-Hexen-1-ol
1-Octanol
Ethylene Glycol
1-Undecanol
1, 4-Butanediol
19

17
12

14

11
2

15
16

3
7 8

14

Gas Chromatography

12
11
4

20

13

10
2
5
1.
2.
3.
4.
5.
6.

116

Pentane
Hexane
Heptane
Ethanol
Decane
1-Propanol

10
7.
8.
9.
10.
11.
12.

15
TIME (MIN.)
1-Butanol
Dodecane
1-Pentanol
1-Hexanol
Tetradecane
1-Heptanol

20

3
4

25

18

5
7

13.
14.
15.
16.
17.
18.

1-Octanol
Hexadecane
1-Nonanol
1-Decanol
1-Undecanol
1-Dodecanol

10

15
TIME (MIN.)

20

25

Capillary Column Applications


Industrial Chemicals
Capillary Column Applications

Aldehydes
2

6
3

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.

4
5
9

Ethanal
Propanal
Butenal
Pentanal
Hexanal
Heptanal
Octanal
Nonanal
Decanal
Undecanal

8
Column: Elite-WAX
Dimensions: 30 m, 0.25 mm i.d., 0.50 m
Sample: Split injection of C2-C11 aldehydes mixture,
on-column concentration: 250 ng
Oven: 40 C (hold 5 min.) to 200 C at 10 C/min.
Injector: 200 C
Detector: 200 C
Carrier: Hydrogen at 35 cm/sec.
Split Ratio: 100:1

10

Part No.

10
TIME (MIN.)

15

N9316404

20

Amines and Phenols

3
1

13

12

10

Part No.

Gas Chromatography

Column: Elite-5Amine
Dimensions: 30 m, 0.32 mm i.d., 1.0 m
Sample: 1.0 L split injection of miscellaneous
amines and phenols in water
On-Column Conc.: 22 ng
Oven: 120 to 220 C @ 10 C/min.
Injector: 305 C
Linear Velocity: 38 cm/sec. set @ 120 C
FID Sensitivity: 6.4 x 10-11 AFS
Split Ratio: 25:1

10

Diethylamine
Pyridine
Morpholine
Phenol
Aniline
2-Chlorophenol
Diethylenetriamine
Octylamine
1-Methyl-2-Pyrrolidinone
2-Nitrophenol
2, 6-Dimethylaniline
Nicotine
2-Nitroaniline

11

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.

N9316677

TIME (MIN.)

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

117

Capillary Column Applications


Industrial Chemicals
Capillary Column Applications

Aromatics

1.
2.
3.
4.
5.
6.
7.
8.

Column: Elite-WAX ETR


Dimensions: 60 m, 0.53 mm i.d., 1.0 m
Sample: 1.0 L split injection of an
aromatics mixture
Oven: 40 C (hold 10 min.) to 245 C
at 4 C/min. (hold 20 min.)
Injector: 250 C
Detector: MS, 280 C
Carrier: Helium at 50 cm/sec.
Split Ratio: 7:1

trans-Decahydronaphthalene
1, 2-Xylene
cis-Decahydronaphthalene
1, 3, 5-Trimethylbenzene
p-Cymene or p-Isopropyltoluene
1, 2, 4-Trimethylbenzene
-Methyl Benzene
1, 2, 3-Trimethylbenzene
10

9.
10.
11.
12.
13.
14.
15.

Diisopropylbenzene
Triethylbenzene
Pentadecane
Nitrobenzene
Nonadecane
o-Cresol
Bibenzyl

14

15

12

4
6
13
2

11

Part No.

N9316571
3
1

15

20

30

35

40

45

50

55

TIME (MIN.)

Industrial Solvents

Gas Chromatography

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.

Pentane
Hexane
Methyl Formate
Acetone
Tetrahydrofuran
1, 1, 1-Trichloroethane
Ethyl Acetate
Methanol
Methylethyl Ketone
Methylene Chloride
Chloroform
Benzene
n-Propyl Alcohol
sec-Butyl Alcohol
Toluene
n-Butyl Acetate
Isobutyl Alcohol
n-Butyl Alcohol
o-Xylene
Ethoxyethane

10,11
6,7

16

14
13

17 18
20

12

6
TIME (MIN.)

Column: Elite-MWAX
Dimensions: 30 m, 0.53 mm i.d., 1.0 m
Sample: Wet needle injection of neat solvents
Oven: 50 C to 220 C at 10 C/min.
Injector: 250 C
Detector: FID, 250 C
Carrier: Helium at 20 cm/sec.

Part No.

118

N9316478

6,7
10,11

8,9

Industrial Solvents

19
15

10

1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.

Pentane
Hexane
Methyl Formate
Acetone
Tetrahydrofuran
1, 1, 1-Trichloroethane
Ethyl Acetate
Methanol
Methylethyl Ketone
Methylene Chloride
Chloroform
Benzene
n-Propyl Alcohol
sec-Butyl Alcohol
Toluene
n-Butyl Acetate
Isobutyl Alcohol
n-Butyl Alcohol
o-Xylene
Ethoxyethane

19

15

1
8,9
16
5
14
13 17

18
20

12

8
TIME (MIN.)

10

Column: Elite-WAX ETR


Dimensions: 30 m, 0.53 mm i.d., 1.0 m
Sample: Wet needle injection of neat solvents
Oven: 50 C to 220 C at 10 C/min.
Injector: 250 C
Detector: 250 C
Carrier: Helium at 20 cm/sec.

Part No.

N9316569

Capillary Column Applications


Petroleum
Capillary Column Applications

Prudhoe Bay Crude Oil


1.
2.
3.
4.
5.
6.
7.
8.
9.
10.

11.
12.
13.
14.
15.
16.
17.
18.
19.
20.

Benzene
Heptane
Toluene
Octane
m-Xylene and p-Xylene
o-Xylene
Nonane
Decane
Undecane
Dodecane

21.
22.
23.
24.
25.
26.
27.
28.

Tridecane
Tetradecane
Pentadecane
Hexadecane
Heptadecane
Pristane
Octadecane
Phytane
Nonadecane
Eicosane

Column: Elite-1
Dimensions: 30 m, 0.53 mm i.d., 3.0 m
Sample: 0.4 L split injection of Prudhoe Bay crude oil
Oven: 40 C to 285 C at 5 C/min. (hold 30 min.)
Injector: 285 C
Detector: 285 C
Carrier: Hydrogen at 40 cm/sec.
Split Ratio: 50:1

Heneicosane
Docosane
Tricosane
Tetracosane
Pentacosane
Hexacosane
Heptacosane
Octacosane

Part No.

N9316051

4
5

12

11

10

13

14
15
17

19
20 21
22

16

23

18

24
25

26
27

12

16

20

24

28

32

36

40
44
TIME (MIN.)

48

52

56

60

28

64

68

72

76

80

Volatile Hydrocarbons

1.
2.
3.
4.
5.
6.
7.
8.
9.

8,9

17

14

2,3

10.
11.
12.
13.
14.
15.
16.
17.

Isobutane
1, 3-Butadiene
1-Butene
n-Butane
cis-2-Butene
trans-2-Butene
Isopentane
n-Pentane

11

13
12

5 7

Methane
Ethylene
Acetylene
Ethane
Propylene
Propane
Cyclopropane
Propadiene
Propyne

15
16

6
10

10

11

12

13

Gas Chromatography

Column: Elite-Q PLOT


Dimensions: 30 m, 0.32 mm i.d.
Sample: 300 L split injection (40:1), 1000 ppm
Oven: 50 C (2 min.) to 220 C at 15 C/min.
Injector: 250 C
Detector: FID, 250 C
Carrier: Helium at 42 cm/sec.
Split Flow: 40 mL/min.

14

TIME (MIN.)

Part No.

N9316359

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

119

Capillary Columns
Phase Cross-Reference
Phase

Phase Description

Equivalent Phase

Elite-1, Elite-1ht

100% Dimethyl

Packed: OV-1, OV-101, SP-2100, DC-200, UC-W982, S 96, CP-Sil 5, SE-30


Capillary: DB-1, DB-1ht, HP-1, HP-101, Ultra-1, SPB-1, CP-Sil 5CB, Cl-Sil5CBMS,
RSL-150, RSL-160, Rtx-1, BP-1, CB-1, OV-1, 007-1(MS), SP-2100, SE-30

Elite-5, Elite-5ht,

5% Diphenyl 95% Dimethyl

Elite-5ms

Packed: OV-3, OV-73, Dexsil 300, Fluorolube, CP-Sil 8


Capillary: DB-5, DB-5ms, DB-5ht, HP-5, Ultra-2, SPB-5, CP-Sil 8CB, RSL-200, Rtx-5,

Capillary Columns

BP-5, CB-5, OV-5, 007-2(MPS-5), SE-52, SE-54, XTI-5, Rtx-5 ms, PTE-5, HP-5MS
Elite-5Amine

5% Diphenyl 95% Dimethyl Polysiloxane

Rtx-5Amine; PTA-5

Elite-17, Elite-17ht,

50% Phenyl 50% Methyl

Packed: OV-17, OV-11, OV-22, SP-2250, DC-710

Elite-17ms

Capillary: DB-17, DB-17ht, HP-17, RSL-300, Rtx-50, 007-17(MPS-50),


SP-2250, HP-50+

Elite-35, Elite-35ms

35% Phenyl 65% Methyl

Capillary: DB-35, DB-35ms, Rtx-35, SPB-35, AT-35, Sup-Herb

Elite-200

Trifluoropropylmethyl Polysiloxane

DB-210; AT-210; VF-200MS; 007-210; Rtx-200

Elite-225

50% Cyanopropylmethyl

Packed: OV-225, Silar 5 CP

50% Phenylmethyl

Capillary: DB-225, HP-225, SP-2330, CP-Sil 43CB, RSL-500, Rtx-225,


BP-225, CB-225, OV-225, 007-225

Elite-608

Specialty phase for semivolatile


pesticides (U.S. EPA 608)

Capillary: SPB-608, NON-PAKD Pesticide, DB-608, 007-608, HP-608

Elite-624,

Specialty phase for volatiles

Capillary: DB-624, DB-VRX, VOCOL, NONPAKD AT-624, Rtx-Volatiles,

Elite-Volatiles

(U.S. EPA 624 and 502.2)

Rtx-502.2, 007-624, 007-502, HP-624, CP-624, Rtx-624

Elite-1301

6% Cyanopropylphenyl 94% Methyl

Capillary: DB-1301, Rtx-1301, CP-624

Elite-1701

14% Cyanopropylphenyl 86% Dimethyl

Packed: OV-1701
Capillary: DB-1701, SPB-7, CP-Sil 19CB, Rtx-1701, BP-10, CB-1701,
OV-1701, 007-1701

Elite-Alumina

PLOT phase for analysis

Packed: Alumina

of light hydrocarbons

Capillary: GS-Alumina, Al2O3/KC1, Al2O3/Na2SO4, RT-Alumina

Elite-Betacydex

Betacyclodextrin for chiral separations

Capillary: Cyclodex-B, LIPODEX C, Chirasil-D/L-Val, Rt-bDEXm

Elite-CLPesticides

Specialty phase for chlorinated pesticides

Rtx-CLPesticides

Elite-CLPesticides2

Specialty phase for chlorinated pesticides

Rtx-CLPesticides

Elite-FFAP

Polyethylene Glycol Acid Modified

Packed: OV-351, FFAP, Carbowax 20M-Terephthalic acid


Capillary: DB-WAX, HP-FFAP, Nukol, SUPEROX FA, STABILWAX-DA, 007-FFAP,
OV-351, DB-FFAP

Gas Chromatography

Elite-Molesieve

Elite-PONA

Elite-Q

PLOT phase for analysis

Packed: Molesieve 5A

of permanent gases

Capillary: GS-Molesieve, Molesieve 5A, #PLT-5A, Rt-Molesieve 5A

Dimethylpolysiloxane processed for


detailed analysis of petroleum naphtha

Capillary: DB-Petro100, Petrocol DH, HP-PONA, SPB-1, 007-1, Rtx-1 PONA

PLOT phase for analysis

Packed: Chomosorb 101, HayeSep Q, Porapak Q

of light gases and hydrocarbons

Capillary: GS-Q, PoraPLOT Q, Rt-QPLOT

Elite-VMS

Specialty phase for U.S. EPA Volatile Organics

Rtx-VMS

Elite-WAX

Polyethylene Glycol

Packed: Carbowax 20M, SUPEROX, SUPELCOWAX 10, PEG


Capillary: DB-FFAP, HP-20M, SUPELCOWAX 10, CP-WAX 52CB, SUPEROX II,
CB-WAX, STABILWAX, BP-20, Elite-CW, 007-CW, Carbowax, HP-Innowax

120

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-1 Dimethylpolysiloxane
100% Dimethyl Polysiloxane phase:
The 100% Dimethyl Polysiloxane is a highly versatile phase
that is extremely rugged, exhibiting long column lifetime,
low bleed, and high maximum operating temperatures.

Primary applications:

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.05
0.05
0.10
0.10
0.18
0.18
0.18
0.18
0.18
0.20
0.20
0.20
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.45*
0.45*
0.45*
0.45*
0.45*
0.45*
0.45*
0.45*
0.45*

10
10
10
20
10
10
20
20
40
12
25
50
15
15
15
30
30
30
60
60
60
100
15
15
15
15
15
25
30
30
30
30
30
60
60
60
60
60
5
15
15
15
15
15
30
30
30

0.05
0.20
0.10
0.40
0.18
0.40
0.18
0.40
0.40
0.33
0.33
0.33
0.10
0.25
1.00
0.10
0.25
1.00
0.10
0.25
1.00
0.50
0.10
0.25
1.00
3.00
5.00
0.52
0.10
0.25
1.00
3.00
5.00
0.10
0.25
1.00
3.00
5.00
4.25
0.13
0.42
1.27
2.55
4.25
0.42
1.27
2.55

-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 330/350
-60 to 320/340
-60 to 330/350
-60 to 320/340
-60 to 320/340
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 300/320
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 280/300
-60 to 260/280
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 280/300
-60 to 260/280
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 280/300
-60 to 260/280
-60 to 260/280
-60 to 340/360
-60 to 310/330
-60 to 310/330
-60 to 270/290
-60 to 260/280
-60 to 310/330
-60 to 310/330
-60 to 270/290

Part No.
N9316056
N9316057
N9316058
N9316061
N9316001
N9316002
N9316003
N9316004
N9316005
N9316062
N9316063
N9316064
N9316006
N9316007
N9316008
N9316009
N9316010
N9316011
N9316012
N9316013
N9316014
N9316015
N9316016
N9316017
N9316018
N9316019
N9316020
N9316021
N9316022
N9316023
N9316024
N9316025
N9316026
N9316027
N9316028
N9316029
N9316030
N9316031
N9316032
N9316033
N9316037
N9316034
N9316035
N9316036
N9316041
N9316038
N9316039

Each ()
650
650
574
625
332
332
523
445
944
325
445
738
357
318
318
606
547
547
1046
930
891
1057
381
356
389
389
356
483
573
547
573
573
445
1141
1122
993
1122
993
147
402
402
402
402
402
721
721
721

Film
Thickness
(m)

Temperature
Limits
(C)

0.45*
0.45*
0.45*
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53

30
60
105
5
15
15
15
15
15
30
30
30
30
60

4.25
1.27
2.55
5.00
0.15
0.50
1.50
3.00
5.00
0.50
1.50
3.00
5.00
1.50

-60 to 260/280
-60 to 310/330
-60 to 270/290
-60 to 270/290
-60 to 320/340
-60 to 310/330
-60 to 310/330
-60 to 270/290
-60 to 270/290
-60 to 310/320
-60 to 310/320
-60 to 270/290
-60 to 270/290
-60 to 310/330

Part No.
N9316040
N9316042
N9316043
N9316044
N9316045
N9316049
N9316046
N9316047
N9316048
N9316053
N9316050
N9316051
N9316052
N9316054

Each ()
721
1148
1836
147
356
356
356
292
402
636
636
636
636
993

* Ferrule size same as 0.53.

Elite-1ht (High-Temp)
Dimethylpolysiloxane
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.25
0.25
0.32
0.32

15
30
15
30

0.10
0.10
0.10
0.10

-60 to 380
-60 to 380
-60 to 380
-60 to 380

N9316268
N9316269
N9316270
N9316271

Each ()
383
573
414
636

Gas Chromatography

Inner
Diameter
(mm i.d.)

Length
(m)

Capillary Columns

Elite columns are ideal for the analysis of non-polar


petrochemical samples, such as detailed hydrocarbon
analysis, hydrocarbon gases, petroleum oxygenates,
petroleum aromatics, fuels, waxes, oils, sulfur compounds,
mercaptans, and carbon disulfide. It also is an excellent
phase for solvents, chemicals, flavors, fragrances, essential
oils, air toxins, chlorofluorocarbons, arson analysis, and
high-temperature applications.

Inner
Diameter
(mm i.d.)

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

121

Capillary Columns
PerkinElmer Elite Series Capillary Columns

Capillary Columns

Elite-5 (5% Diphenyl)


Dimethylpolysiloxane
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.05
0.05
0.10
0.10
0.18
0.18
0.18
0.18
0.18
0.20
0.20
0.20
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.45*
0.45*
0.45*
0.45*
0.45*
0.45*
0.53
0.53
0.53
0.53
0.53
0.53

10
10
20
20
20
10
10
20
40
12
25
50
15
15
15
30
30
30
60
60
60
15
15
15
25
30
30
30
50
60
60
60
15
15
30
30
30
60
15
15
30
30
30
60

0.05
0.20
0.10
0.40
0.18
0.18
0.40
0.40
0.40
0.33
0.33
0.33
0.10
0.25
1.00
0.10
0.25
1.00
0.10
0.25
1.00
0.10
0.25
1.00
0.52
0.10
0.25
1.00
1.00
0.10
0.25
1.00
0.42
1.27
0.42
1.27
4.25
1.27
0.50
1.50
0.50
1.50
5.00
1.50

-60 to 325/350
-60 to 325/350
-60 to 330/350
-60 to 320/340
-60 to 325/340
-60 to 325/340
-60 to 315/330
-60 to 315/330
-60 to 315/330
-60 to 320/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 330/350
-60 to 330/350
-60 to 320/340
-60 to 330/350
-60 to 330/340
-60 to 320/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 310/330
-60 to 310/330
-60 to 310/330
-60 to 310/330
-60 to 270/290
-60 to 310/330
-60 to 310/330
-60 to 310/330
-60 to 310/330
-60 to 310/330
-60 to 270/290
-60 to 310/330

Elite-5ht (High-Temp)
(5% Diphenyl)
Dimethylpolysiloxane
Part No.
N9316104
N9316105
N9316108
N9316109
N9316068
N9316066
N9316067
N9316069
N9316071
N9316110
N9316111
N9316112
N9316072
N9316073
N9316074
N9316075
N9316076
N9316077
N9316078
N9316079
N9316080
N9316081
N9316082
N9316083
N9316084
N9316085
N9316086
N9316087
N9316088
N9316089
N9316090
N9316091
N9316093
N9316092
N9316096
N9316094
N9316095
N9316097
N9316099
N9316098
N9316102
N9316100
N9316101
N9316103

Each ()
650
650
547
625
523
332
292
445
829
325
445
848
357
318
292
573
509
509
1046
891
891
389
356
389
509
547
573
547
828
1141
993
993
402
402
721
721
721
1148
363
356
636
611
636
993

* Ferrule size same as 0.53.

Gas Chromatography

Elite-5Amine

122

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.53
0.53
0.53
0.25

30
15
30
15
30
15
30
30
15
30
15

0.50
1.00
1.00
1.00
1.00
1.50
1.50
1.00
3.00
3.00
0.50

-60 to 300/315
-60 to 300/315
-60 to 300/315
-60 to 300/315
-60 to 300/315
-60 to 290/305
-60 to 290/305
-60 to 290/305
-60 to 280/305
-60 to 280/305
-60 to 300/315

Part No.
N9316673
N9316674
N9316675
N9316676
N9316677
N9316678
N9316679
N9316680
N9316681
N9316682
N9316684

Each ()
675
445
675
458
713
458
713
789
483
789
445

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.25
0.25
0.32
0.32

15
30
15
30

0.10
0.10
0.10
0.10

-60 to 400
-60 to 400
-60 to 400
-60 to 400

N9316272
N9316273
N9316274
N9316275

Each ()
383
611
356
611

Elite-5ms (5% Diphenyl)


Dimethylpolysiloxane
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.18
0.18
0.20
0.20
0.20
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.53
0.53

20
40
12
25
50
15
15
15
30
30
30
30
60
60
60
15
15
15
25
30
30
30
30
60
60
60
15
30

0.18
0.18
0.33
0.33
0.33
0.10
0.25
1.00
0.10
0.25
1.00
0.50
0.10
0.25
1.00
0.10
0.25
1.00
0.52
0.10
0.25
1.00
0.50
0.10
0.25
1.00
1.50
1.50

-60 to 325/340
-60 to 325/340
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 325/350
-60 to 330/350
-60 to 330/350
-60 to 325/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 325/350
-60 to 330/350
-60 to 330/350
-60 to 325/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 325/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 330/350
-60 to 310/330
-60 to 310/330

Part No.
N9316276
N9316277
N9316301
N9316302
N9316303
N9316278
N9316279
N9316280
N9316281
N9316282
N9316283
N9316284
N9316285
N9316286
N9316287
N9316288
N9316289
N9316290
N9316291
N9316292
N9316293
N9316294
N9316295
N9316296
N9316297
N9316298
N9316299
N9316300

Each ()
547
930
344
483
828
402
402
402
638
611
611
611
1084
1019
993
421
421
421
561
695
636
636
636
1186
1083
1186
434
700

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-17ms (Low Bleed)
(50% Phenyl)
Methylpolysiloxane

Elite-17 (50% Phenyl)


Methylpolysiloxane
Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.05
0.05
0.10
0.10
0.10
0.10
0.18
0.18
0.18
0.18
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.45*
0.45*
0.45*
0.45*
0.53
0.53
0.53
0.53

10
10
10
10
20
20
10
10
20
20
15
15
15
30
30
30
60
15
15
15
30
30
30
5
15
30
60
5
15
30
60

0.05
0.10
0.10
0.02
0.10
0.20
0.18
0.30
0.18
0.30
0.15
0.25
0.50
0.15
0.25
0.50
0.25
0.15
0.25
0.50
0.15
0.25
0.50
1.70
0.85
0.85
0.85
2.00
1.00
1.00
1.00

40 to 280/300
40 to 280/300
40 to 280/300
40 to 280/300
40 to 280/300
40 to 280/300
40 to 310/300
40 to 300/320
40 to 310/330
40 to 300/320
40 to 300/320
40 to 300/320
40 to 290/310
40 to 300/320
40 to 300/320
40 to 290/310
40 to 290/310
40 to 300/320
40 to 300/320
40 to 290/310
40 to 300/320
40 to 300/320
40 to 290/310
40 to 260/280
40 to 270/290
40 to 270/290
40 to 260/280
40 to 250/270
40 to 260/280
40 to 260/280
40 to 260/280

Part No.
N9316138
N9316139
N9316140
N9316141
N9316142
N9316143
N9316113
N9316114
N9316115
N9316116
N9316117
N9316118
N9316119
N9316120
N9316121
N9316122
N9316123
N9316124
N9316125
N9316126
N9316127
N9316128
N9316129
N9316130
N9316131
N9316132
N9316133
N9316134
N9316135
N9316136
N9316137

Each ()
650
650
574
574
625
625
332
332
523
523
357
357
357
606
547
547
891
389
389
389
644
644
547
147
402
721
1148
147
356
636
1148

* Ferrule size same as 0.53

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.18
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32

20
15
15
30
30
60
15
15
30

0.18
0.15
0.25
0.15
0.25
0.25
0.15
0.25
0.15

40 to 320/340
40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320

Part No.
N9316534
N9316535
N9316536
N9316537
N9316538
N9316539
N9316540
N9316541
N9316542

Each ()
599
434
434
611
701
1205
471
472
759

Capillary Columns

Inner
Diameter
(mm i.d.)

Elite-35 (35% Diphenyl)


Dimethylpolysiloxane
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.25
0.32
0.32
0.45*
0.45*
0.45*
0.53
0.53
0.53

30
30
30
30
15
30
30
15
30
30

0.15
0.25
0.25
0.50
0.85
0.42
0.85
1.00
0.50
1.00

40 to 300/320
40 to 300/320
40 to 300/320
40 to 290/310
40 to 280/300
40 to 290/310
40 to 280/300
40 to 260/280
40 to 260/280
40 to 260/280

Part No.
N9316144
N9316145
N9316146
N9316147
N9316148
N9316150
N9316149
N9316151
N9316153
N9316152

Each ()
606
606
547
644
402
721
721
402
611
721

Elite-35ms (35% Phenyl)


Methylpolysiloxane

Elite-17ht (High-Temp)
(50% Phenyl)
Methylpolysiloxane
Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.25
0.32
0.32
0.32

15
30
15
30
60

0.15
0.15
0.15
0.15
0.15

40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320
40 to 300/320

Part No.
N9316263
N9316264
N9316265
N9316266
N9316267

Each ()
383
625
414
676
1173

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.20
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.53
0.53
0.53

25
15
30
30
60
15
30
60
15
30
30

0.33
0.25
0.15
0.25
0.25
0.25
0.25
0.25
1.00
1.00
0.50

50 to 320/340
50 to 320/340
50 to 320/340
50 to 320/340
50 to 320/340
50 to 320/340
50 to 320/340
50 to 320/340
50 to 290/310
50 to 290/310
50 to 300/320

Part No.
N9316446
N9316436
N9316437
N9316438
N9316439
N9316440
N9316441
N9316442
N9316443
N9316444
N9316445

Each ()
536
402
644
644
1019
421
636
1186
434
759
759

Gas Chromatography

Inner
Diameter
(mm i.d.)

Inner
Diameter
(mm i.d.)

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

123

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-225 (50%
Cyanopropylmethyl)
Phenylmethylpolysiloxane

Gas Chromatography

Capillary Columns

Elite-200 Trifluoropropylmethyl
Polysiloxane
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.18
0.18
0.18
0.18
0.18
0.18
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53

10
20
40
10
20
40
15
30
15
30
15
30
15
30
60
15
30
15
30
15
30
60
15
30
60
15
30
60
15
30
60
15
30
60
15
30
60
15
30
60

0.20
0.20
0.20
0.40
0.40
0.40
0.10
0.10
0.25
0.25
0.50
0.50
1.00
1.00
1.00
0.25
0.25
0.50
0.50
1.00
1.00
1.00
1.50
1.50
1.50
0.25
0.25
0.25
0.50
0.50
0.50
1.00
1.00
1.00
1.50
1.50
1.50
3.00
3.00
3.00

-20 to 310/330
-20 to 310/330
-20 to 310/330
-20 to 310/330
-20 to 310/330
-20 to 310/330
-20 to 320/340
-20 to 320/340
-20 to 320/340
-20 to 320/340
-20 to 310/330
-20 to 310/330
-20 to 290/310
-20 to 290/310
-20 to 290/310
-20 to 320/340
-20 to 320/340
-20 to 310/330
-20 to 310/330
-20 to 290/310
-20 to 290/310
-20 to 290/310
-20 to 280/300
-20 to 280/300
-20 to 280/300
-20 to 310/330
-20 to 310/330
-20 to 310/330
-20 to 300/320
-20 to 300/320
-20 to 300/320
-20 to 290/310
-20 to 290/310
-20 to 290/310
-20 to 280/300
-20 to 280/300
-20 to 280/300
-20 to 260/280
-20 to 260/280
-20 to 260/280

Part No.
N9316610
N9316611
N9316612
N9316613
N9316614
N9316615
N9316616
N9316617
N9316618
N9316619
N9316620
N9316621
N9316622
N9316623
N9316624
N9316625
N9316626
N9316627
N9316628
N9316629
N9316630
N9316631
N9316632
N9316633
N9316634
N9316635
N9316636
N9316637
N9316638
N9316639
N9316640
N9316641
N9316642
N9316643
N9316644
N9316645
N9316646
N9316647
N9316648
N9316649

Each ()
343
522
917
343
522
917
381
611
369
598
369
598
369
598
993
420
636
420
636
420
636
1095
420
636
1095
445
726
1185
445
726
1185
445
726
1185
445
726
1185
445
726
1185

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.05
0.10
0.18
0.18
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.45*
0.45*
0.53
0.53

10
20
10
20
15
15
30
30
15
15
30
30
15
30
15
30

0.05
0.10
0.20
0.20
0.15
0.25
0.15
0.25
0.15
0.25
0.15
0.25
0.85
0.85
1.00
1.00

45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
45 to 220/240
40 to 200/220
40 to 200/220
40 to 200/220
40 to 200/220

N9316186
N9316187
N9316172
N9316173
N9316174
N9316175
N9316176
N9316177
N9316178
N9316179
N9316180
N9316181
N9316182
N9316183
N9316184
N9316185

Each ()
636
625
332
523
363
318
619
547
402
402
670
573
395
740
395
636

Elite-502.2 Specialty Phase for


Analysis of Volatiles (U.S. EPA 502.2)
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.25
0.45*
0.45*
0.53

60
105
75
105

1.40
2.55
2.55
3.00

0 to 250/270
0 to 250/270
0 to 250/270
0 to 250/270

N9316498
N9316189
N9316188
N9316190

Each ()
1065
1836
1338
1210

Elite-608 Specialty Phase for


Semivolatile Pesticides (U.S. EPA 608)
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.32
0.45*
0.45*
0.45*
0.45*
0.53
0.53
0.53
0.53

30
15
15
30
30
15
15
30
30

0.50
0.42
0.70
0.42
0.70
0.50
0.83
0.50
0.83

40 to 290/310
40 to 270/290
40 to 260/280
40 to 270/290
40 to 260/280
40 to 270/290
40 to 260/280
40 to 270/290
40 to 260/280

* Ferrule size same as 0.53

124

Part No.

Part No.
N9316191
N9316194
N9316192
N9316195
N9316193
N9316198
N9316196
N9316199
N9316197

Each ()
547
402
402
721
721
402
402
611
700

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-624 Specialty Phase for
Analysis of Volatiles (U.S. EPA 624)
Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.18
0.20
0.25
0.25
0.32
0.32
0.45*
0.45*
0.53
0.53

20
25
30
60
30
60
30
75
30
75

1.00
1.12
1.40
1.40
1.80
1.80
2.55
2.55
3.00
3.00

-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240

N9316200
N9316209
N9316201
N9316202
N9316203
N9316204
N9316205
N9316206
N9316207
N9316208

Each ()
510
445
573
1065
611
1057
829
1249
700
1249

* Ferrule size same as 0.53

Elite-1301
(6% Cyanopropylphenyl)
Methylpolysiloxane
Inner
Diameter
(mm i.d.)
0.18
0.18
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.45*
0.45*
0.53
0.53

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

10
20
15
15
30
30
60
60
15
30
60
15
30
60
15
30
15
30

0.40
0.40
0.25
1.00
0.25
1.00
0.25
1.00
0.25
0.25
0.25
1.00
1.00
1.00
0.85
0.85
1.00
1.00

-20 to 280
-20 to 280
-20 to 280
-20 to 260/280
-20 to 280
-20 to 260/280
-20 to 280
-20 to 260/280
-20 to 280
-20 to 280
-20 to 280
-20 to 260/280
-20 to 260/280
-20 to 260/280
-20 to 260/280
-20 to 260/280
-20 to 260/280
-20 to 260/280

Part No.
N9316210
N9316211
N9316212
N9316213
N9316214
N9316215
N9316216
N9316217
N9316218
N9316220
N9316222
N9316219
N9316221
N9316223
N9316224
N9316225
N9316226
N9316227

Each ()
332
523
363
363
619
619
1065
1065
402
670
1173
402
670
1173
395
740
395
636

Film
Thickness
(m)

Temperature
Limits
(C)

0.05
0.05
0.10
0.10
0.18
0.18
0.25
0.25
0.25
0.25
0.25
0.25
0.25

10
10
20
20
10
20
15
15
15
30
30
60
60

0.05
0.20
0.10
0.40
0.40
0.40
0.15
0.25
1.00
0.25
1.00
0.15
0.25

-20 to 280
-20 to 280
-20 to 280
-20 to 270/280
-20 to 270/280
-20 to 270/280
-20 to 280
-20 to 280
-20 to 260/280
-20 to 260/280
-20 to 260/280
-20 to 280
-20 to 280

Temperature
Limits
(C)

0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.45*
0.45*
0.45*
0.45*
0.53
0.53
0.53
0.53

60
15
15
15
30
30
30
50
60
60
60
15
15
30
30
15
15
30
30

1.00
0.15
0.25
1.00
0.15
0.25
1.00
1.00
0.15
0.25
1.00
0.42
0.85
0.42
0.85
1.00
0.50
0.50
1.00

-20 to 260/280
-20 to 280
-20 to 280
-20 to 260/280
-20 to 280
-20 to 280
-20 to 260/280
-20 to 260/280
-20 to 280
-20 to 280
-20 to 260/280
-20 to 260/270
-20 to 250/270
-20 to 260/270
-20 to 250/270
-20 to 250/270
-20 to 260/270
-20 to 260/270
-20 to 250/270

Part No.
N9316238
N9316239
N9316240
N9316241
N9316242
N9316243
N9316244
N9316245
N9316246
N9316247
N9316248
N9316250
N9316249
N9316252
N9316251
N9316253
N9316254
N9316256
N9316255

Each ()
930
402
402
402
573
573
573
828
1173
828
1019
395
395
740
740
356
395
740
740

Elite-BAC Blood Alcohol Analysis


Columns for GC and High-Speed
Headspace Gas Chromatography
Now using the PerkinElmer Blood Alcohol columns,
standard separations and automated separations of less than
1.5 minutes can be accomplished. Sample concentrations
range from 0.01 to 0.05% with quantitative precision
of <3% RSD. A full range of analytes with a choice of
internal standards can be used with excellent quantitative
performance. Two columns may be used in parallel for
confirmation of peak identity.

Description

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Elite BAC-1
Elite BAC-2
Elite BAC-3

0.18
0.18
0.18

10
10
10

1.00
0.63
0.30

Part No.
N9316573
N9316574
N9316575

Each ()
292
292
332

Part No.
N9316257
N9316258
N9316259
N9316260
N9316228
N9316229
N9316230
N9316231
N9316232
N9316234
N9316235
N9316236
N9316237

Each ()
650
650
547
625
332
523
318
363
363
547
547
1065
1057

Description

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Elite BAC-1
Elite BAC-1
Elite BAC-2
Elite BAC-2

0.32
0.53
0.32
0.53

30
30
30
30

1.80
3.00
1.20
2.00

Part No.
N9316579
N9316578
N9316577
N9316576

Each ()
587
625
587
625

Gas Chromatography

Length
(m)

Film
Thickness
(m)

Standard Blood Alcohol GC Columns

Elite-1701
(14% Cyanopropylphenyl)
Methylpolysiloxane
Inner
Diameter
(mm i.d.)

Length
(m)

Capillary Columns

Inner
Diameter
(mm i.d.)

Inner
Diameter
(mm i.d.)

Elite-Betacydex Betacyclodextrin
for Chiral Separations
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25

30

0.25

40 to 230

Part No.
N9316319

Each ()
547

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

125

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-CLPesticides

Capillary Columns

Elite-CLPesticides is specially designed to overcome the


coelutions and analyte breakdown typically encountered in
chlorinated pesticide analyses for U.S. EPA methods 8081,
608, and CLP. Column bleed measured by ECD is extremely
low at temperatures greater than 300 C, which is critical for
baking out the column to remove high-boiling compounds
commonly found in pesticide/PCB extracts.

Primary Applications
Chlorinated Pesticides and Herbicides. U.S. EPA Methods
504, 608, 619, 8081, 8151, and CLP.
Features and Benefits:
Thermally stable to 340 C
Low column bleed ideal for ECD or GC/MS analysis
Exceeds performance criteria for U.S. EPA Methods
8081, 608, CLP
Baseline separation in less than 15 minutes
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

0.25
0.25
0.32
0.32
0.53
0.53

15
30
15
30
15
30

0.25
0.25
0.50
0.50
0.50
0.50

Part No.
N9316661
N9316662
N9316663
N9316664
N9316665
N9316666

Each ()
432
636
458
687
483
764

Gas Chromatography

Elite-CLPesticides 2

126

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

0.25
0.25
0.32
0.32
0.53
0.53

15
30
15
30
15
30

0.20
0.20
0.25
0.25
0.42
0.42

Part No.
N9316667
N9316668
N9316669
N9316670
N9316671
N9316672

Each ()
432
624
483
687
483
764

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-FFAP Nitroterephthalic
Acid Modified Polyethylene
Glycol (Bonded)

Elite-SimDist
Dimethylpolysiloxane Processed
for Simulated Distillation

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.25
0.32
0.32
0.45*
0.45*
0.53
0.53

15
30
15
30
15
30
15
30

0.25
0.25
0.25
0.25
0.85
0.85
1.00
1.00

40 to 250
40 to 250
40 to 250
40 to 250
40 to 240/250
40 to 240/250
40 to 240/250
40 to 240/250

Part No.
N9316351
N9316352
N9316353
N9316354
N9316355
N9316356
N9316357
N9316358

Each ()
318
547
356
547
356
721
402
611

Elite-HT SimDist
for High-Temperature
Simulated Distillation
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.53

0.15

-60 to 400

N9316572

Each ()
318

Elite-MTBE Low Polarity


Stationary Phase
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.45
0.53

30
30

2.55
3.00

10 to 250
10 to 250

Part No.
N9316520
N9316521

Each ()
797
797

Elite-PONA Dimethylpolysiloxane
Processed for Detailed Analysis
of Petroleum Naphtha
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.20

100
50

0.50
0.50

-60 to 300/320
-60 to 300/320

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.45*
0.53

10
10

2.55
3.00

-60 to 360
-60 to 360

N9316261
N9316262

Each ()
281
254

Elite-TPH Specialty
Phase for Analysis of
Total Petroleum Hydrocarbons
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.32
0.45*

30
30

0.25
1.00

-10 to 320
-10 to 290

N9316386
N9316387

Part No.

Each ()
611
752

Elite-VMS
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.18
0.18
0.25
0.25
0.32
0.32
0.45
0.45
0.53
0.53
0.53

20
40
30
60
30
60
30
60
30
60
75

1.00
1.00
1.40
1.40
1.80
1.80
2.55
2.55
3.00
3.00
3.00

-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260
-40 to 240/260

N9316650
N9316651
N9316652
N9316653
N9316654
N9316655
N9316656
N9316657
N9316658
N9316659
N9316660

Each ()
547
942
624
1019
675
1121
764
1223
764
1223
1338

Part No.
N9316015
N9316065

Each ()
1057
764

Film
Thickness
(m)

Temperature
Limits
(C)

0.33
0.33

-60 to 330/350
-60 to 330/350

N9316345
N9316346

325
445

0.33
0.33

-60 to 330/350
-60 to 330/350

N9316349
N9316350

344
483

0.33
0.33

40 to 330/320
40 to 330/320

N9316347
N9316348

325
445

Part No.

Each ()

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.25
0.25
0.32
0.32
0.45*
0.45*

30
60
30
60
30
75

1.40
1.40
1.80
1.80
2.55
2.55

-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240
-20 to 240

N9316388
N9316389
N9316390
N9316391
N9316392
N9316393

Each ()
638
802
714
1083
764
1274

Gas Chromatography

Phase: Elite-1-RX
0.20
12
0.20
25
Phase: Elite-5ms-RX
0.20
12
0.20
25
Phase: Elite-17-RX
0.20
12
0.20
25

Length
(m)

Elite-Volatiles Specialty Phase


for Analysis of Volatile
Organic Compounds

Elite-RX for Analysis


of Drugs of Abuse
Inner
Diameter Length
(mm i.d.)
(m)

Inner
Diameter
(mm i.d.)

Capillary Columns

Inner
Diameter
(mm i.d.)

* Ferrule size same as 0.53

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

127

Capillary Columns
PerkinElmer Elite Series Capillary Columns
Elite-WAX ETR
(Extended Temperature Range)
Polyethylene Glycol

Elite-MWAX
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.53

30

1.00

20 to 240/250

Part No.
N9316478

Each ()
721

Gas Chromatography

Capillary Columns

Elite-WAX Polyethylene Glycol

128

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.05
0.05
0.10
0.10
0.10
0.10
0.18
0.18
0.18
0.18
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.45*
0.45*
0.45*
0.45*
0.45*
0.45*
0.53
0.53
0.53
0.53
0.53

10
10
10
10
20
20
10
10
20
40
15
15
15
30
30
30
60
60
60
15
15
15
30
30
30
60
60
5
15
15
30
30
60
15
15
30
30
60

0.05
0.10
0.10
0.20
0.10
0.20
0.18
0.30
0.18
0.30
0.15
0.25
0.50
0.15
0.25
0.50
0.15
0.25
0.50
0.15
0.25
0.50
0.15
0.25
0.50
0.25
0.50
1.70
0.42
0.85
0.42
0.85
0.85
0.50
1.00
0.50
1.00
1.00

20 to 240/250
20 to 240/250
20 to 240/250
20 to 240/250
20 to 240/250
20 to 240/250
20 to 240/250
20 to 240/250
20 to 240/250
20 to 250/260
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
20 to 250
50 to 230
20 to 250
20 to 240/250
20 to 250
20 to 240/250
20 to 240/250
20 to 250
20 to 240/2540
20 to 250
20 to 240/250
20 to 240/250

Part No.
N9316430
N9316431
N9316432
N9316433
N9316434
N9316435
N9316394
N9316395
N9316396
N9316398
N9316399
N9316400
N9316401
N9316402
N9316403
N9316404
N9316405
N9316406
N9316407
N9316408
N9316409
N9316410
N9316411
N9316412
N9316413
N9316416
N9316417
N9316418
N9316420
N9316419
N9316422
N9316421
N9316423
N9316426
N9316425
N9316428
N9316427
N9316429

Each ()
650
650
574
574
625
625
332
332
523
944
357
357
356
606
547
547
1019
738
930
389
389
389
644
573
573
993
993
147
402
402
721
721
1148
402
356
721
611
1019

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.32
0.45
0.45
0.45
0.45
0.53
0.53
0.53
0.53
0.53
0.53

15
15
30
30
60
15
15
15
30
30
30
50
60
60
60
5
15
30
60
5
15
15
30
30
60

0.25
0.50
0.25
0.50
0.25
0.25
0.50
1.00
0.25
0.50
1.00
1.00
0.25
0.50
1.00
1.70
0.85
0.85
0.85
2.00
1.00
2.00
1.00
2.00
1.00

40 to 250
40 to 250
40 to 250
40 to 250
40 to 250
40 to 250
40 to 250
40 to 240/250
40 to 260
40 to 250
40 to 240/250
40 to 240/250
40 to 250
40 to 250
40 to 240/250
40 to 230/250
40 to 240
40 to 240
40 to 240
40 to 220/230
40 to 240/250
40 to 220/230
40 to 240/250
40 to 220/230
40 to 240/250

Part No.
N9316547
N9316548
N9316549
N9316550
N9316551
N9316552
N9316553
N9316554
N9316555
N9316556
N9316557
N9316558
N9316559
N9316560
N9316561
N9316562
N9316563
N9316564
N9316565
N9316566
N9316567
N9316568
N9316569
N9316570
N9316571

Each ()
363
363
612
612
1071
396
396
396
676
676
547
828
1180
1180
993
147
396
746
1193
147
395
396
611
746
1192

* Ferrule size same as 0.53

Elite-XLB Specialty Phase


for GC/MS with
Exceptionally Low Bleed
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.18
0.20
0.20
0.25
0.25
0.25
0.25
0.25
0.25
0.32
0.32
0.32
0.32
0.32
0.32
0.53
0.53

20
12
25
15
15
30
30
30
60
15
30
30
30
30
60
15
30

0.18
0.33
0.33
0.25
1.00
0.10
0.25
1.00
0.25
0.25
0.10
0.25
0.50
1.00
0.25
1.50
1.50

30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 340/360
30 to 320/340
30 to 320/340

Part No.
N9316480
N9316496
N9316497
N9316481
N9316482
N9316483
N9316484
N9316485
N9316487
N9316488
N9316489
N9316490
N9316492
N9316491
N9316493
N9316494
N9316495

Each ()
548
351
536
402
402
636
611
636
1019
421
695
636
674
674
1057
445
759

Capillary Columns
PerkinElmer Elite Series Guard and PLOT Columns
Elite Guard Columns

Elite-Alumina/KCI* PLOT

Guard Columns
Maintain the integrity of your capillary column
with a fused silica Guard Column.

PerkinElmer offers both the Intermediate-polarity deactivated


guard column and the Siltek deactivated guard column
as it is important to match the polarity of the solvent
and the polarity of the surface deactivation. The Elite-Guard
intermediate polarity deactivated column has an operating
temperature up to 325 C. Siltek deactivation creates a
highly inert surface for very active compounds such as
chlorinated pesticides with a maximum temperature
range up to 380 C.
Features and Benefits:
Increases the life of the capillary column
Maintains retention time and resolution on capillary column
Traps nonvolatile particles
Improves column performance
Elite-Guard temperature range to 325 C

Elite-Guard
Length
(m)

0.10
0.18
0.25
0.32
0.45
0.53

5
5
5
5
5
5

Part No.
N9316601
N9316602
N9316603
N9316604
N9316605
N9316606

Each ()
106
70
56
64
84
84

Elite-Siltek Guard
Length
(m)

0.25
0.32
0.53

5
5
5

Part No.
N9316607
N9316608
N9316609

Temperature
Limits
(C)

0.53

50

N/A

up to 200

Part No.

Each ()

N9316544

802

* Lower Polarity than Elite Alumina.

Elite-Alumina PLOT Phase for


Analysis of Light Hydrocarbons
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.53
0.53

30
50

N/A
N/A

-60 to 200
-60 to 200

N9316304
N9316305

Each ()
636
1019

Note: -60 C is the lowest temperature used on this phase in our lab.
Lower temperatures may be used depending on the sample.

Elite-Cyclosil B PLOT for Chiral Separations


Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

0.25
0.32

30
30

0.25
0.25

35 to 230
35 to 230

Part No.

Each ()

N9316545
N9316546

650
649

Each ()
70
77
106

Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.53

30

N/A

-60 to 300

N9316361

Each ()
611

Note: -60 C is the lowest temperature used on this phase in our lab.
Lower temperatures may be used depending on the sample.

Elite-Q PLOT Phase for Analysis of


Light Gases and Hydrocarbons
Inner
Diameter
(mm i.d.)

Length
(m)

Film
Thickness
(m)

Temperature
Limits
(C)

Part No.

0.32
0.53

30
30

N/A
N/A

-60 to 250
-60 to 250

N9316359
N9316360

Gas Chromatography

Inner
Diameter
(mm i.d.)

Film
Thickness
(m)

Elite-Molesieve PLOT Phase for


Analysis of Permanent Gases

Elite-Siltek Guard temperature range to 380 C

Inner
Diameter
(mm i.d.)

Length
(m)

Capillary Columns

Using the Elite-Guard or Elite-Siltek Guard Column


lengthens the life of the capillary column and improves the
analyte focusing. The 5 m length of deactivated uncoated
fused silica is connected to the inlet end of the capillary
column and traps nonvolatile residues, preventing them
from collecting at the head of the analytical column. This
length of fused silica contains no stationary phase, adding
only a minimal amount of time to the analysis.

Inner
Diameter
(mm i.d.)

Each ()
509
636

Note: -60 C is the lowest temperature used on this phase in our lab.
Lower temperatures may be used depending on the sample.

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

129

Capillary Columns
PerkinElmer Packed Columns

Capillary Columns

Packed Columns
Instrument Type

Material

AutoSystem GC
Clarus
(not on-column)

Stainless
Steel

Glass

AutoSystem GC/XL Glass


(on-column)

Shape

Length o.d.
(ft.)
(in.)
3
6
12
3
6
12
3
6
12
3
6
12

1/8
1/8
1/8
1/4
1/4
1/4
1/4
1/4
1/4
1/4
1/4
1/4

Packed
2 mm i.d.
Part No.
N9305012
N9305013
N9305014

Each ()

Packed
4 mm i.d.
Part No.

Empty
2 mm i.d.
Each () Part No.

126
165
254

N9305018
N9305019

228
190

N9305047
N9305048

255
332

N9304012
N9304013
N9304014
N9305016
N9305017

228
356

N9305022

292

N9304018
N9304019
N9304020

Empty
4 mm i.d.
Each () Part No.

Each ()

87
88
101

114
114
325

N9304016
N9304017
N9304021
N9304022
N9304023
N9304046
N9304047
N9304048

88
134
114
114
325
126
126
268

Note: Stainless steel columns are metal-fitted at both ends to contain the packing.
For on-column applications, please request glass wool plugs instead of metal frits when ordering.

Gas Chromatography

Choose the appropriate part number from table above. Follow form at bottom of page to choose support material, % liquid
phase, and mesh size. This information is required to place an order.

130

Detectors
Electron Capture Detectors (ECD)
ECD Add-On Kit (PPC Pneumatics)

Add-On Kit
The ECD is a versatile, nondestructive detector which
responds strongly to halogen-containing compounds as
well as to certain other electron-capturing substances. The
ECDs high sensitivity and selectivity make it an ideal
choice for pesticide-residue analysis and for detection
of halogen-derivatized compounds.

Voltage

Part No.

120 V
230 V

N6120122
N6120123

Vent Tube Assembly


Flexible tube to safely vent
toxic sample effluent.

Part No.
N6100161

Each ()
4037

Each ()

Detectors

The ECD has an independent temperature range of 100 450 C. The detector contains thermal protection that
prevents heating the Ni63 source to temperatures beyond
safe operating limits. Two ECDs can be installed and
operated simultaneously on the AutoSystem Series and
Clarus GCs. Nitrogen or argon/methane is the required
detector operating gas. The base of the detector terminates
in a 1/8 in. fitting.

Kit includes detector, heater, sensor, heater block, and


programmable pneumatic control for makeup gas. Requires,
but does not include, ECD amplifier (N6120014). The
AutoSystem XL or Clarus GCs must be PPC ready. If not,
a PPC upgrade kit (N6120146) is required. (See page 166
for more information.) Installation by PerkinElmer Service
is required, but not included.

47

Column Adapters

Collector Anode
To Amplifier

Capillary Column Adapter/Receiver


Adapter converts 1/8 in. fitting to
1/16 in. for use with capillary columns.

Ni Foil (Source)
63

Note: Glass-lined tubing reduces background from


polyimide coating in high-temperature applications.

PID/ECD Series Operation Kit


Kit for directing effluent from
PID to ECD.

Part No.
N6000968

Part No.
N6120059

Each ()
249

Each ()
293

Makeup Gas In

1/4 in. Packed Column Adapter


Column Connection

For use with 1/4 in. packed columns.


1/8 to 1/4 in. adapters fit both injector
and detector ends. (Pkg. 2)

ECD Add-On Kit (Manual Pneumatics)


Kit includes all parts necessary to install an ECD on the
AutoSystem Series or Clarus GCs. Includes detector,
heater, sensor, heater block, 1/16 in. makeup gas line,
makeup gas needle valve, and vent tube assembly.
Requires but does not include ECD amplifier (N6120014).
Installation by PerkinElmer Service is recommended.
Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120011
N6120026
N6520020
N6520021

ECD Amplifier
Required for use with ECD detector
with add-on kit.

Each ()
5400
3136

00080100

N6120014

172

ECD Wipe Test Kit


U.S. Federal law requires that all ECDs be wipe-tested
periodically as described in the instrument operators
manual. In the U.S., possession and use of ECD is regulated
by N.R.C. and/or state regulatory agencies. Licensing by
regulatory agencies is required. Outside of the U.S., check
with governing bodies for licensing and regulations
covering possession and use. This kit contains everything
necessary to do a complete wipe test. For use on any
model GC ECD.
Part No.
Each ()
00091667

Part No.

Each ()

Gas Chromatography

Voltage

Part No.

Each ()
712

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

131

Detectors
Flame Ionization Detector (FID) Auto-Ignite
Add-On Kits

Detector Series Operation Kit

Auto-Ignite FID with PPC Add-On Kit

TCD/FID Series Operation Kit

Kit includes detector assembly with heater and sensor,


heater block, igniter, programmable pneumatics, and
controls for detector combustion gases. Requires but does
not include amplifier (N6120162) and AutoSystem XL
firmware revision 3.3 or higher. The AutoSystem XL must
be PPC ready. If not, a PPC upgrade kit (N6120146)
is required.

Used to direct sample effluent


from the TCD to the FID.

Detectors

Note: AutoSystem XL GCs shipped prior to January 1997 require a new


detector cover. Installation by PerkinElmer Service is required, but not included.
Voltage

Part No.

120 V
240 V

N6120167
N6120168

3172

Kit includes detector assembly with heater and sensor,


heater block, igniter, hydrogen pressure regulator, and
needle valve. Requires, but does not include, amplifier
(N6120162). Requires AutoSystem XL to have firmware
revision 3.3 or higher.
Note: AutoSystem XL GCs shipped prior to January 1997 require a new
detector cover (N6103151).
Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120165
N6120166
N6520018
N6520019

FID Amplifier
Required for use with
FID Detector Add-On Kit.

Part No.
N6120162

Used to direct sample effluent


from the PID to the FID.

N6120006

Part No.
N6120059

Each ()
166

Each ()
293

FID Miscellaneous Accessories

Each ()

Auto-Ignite FID Add-On Kit (Manual Pneumatics)

Voltage

PID/FID Series Operation Kit

Part No.

Each ()
4158
1762

Each ()
754

Description

Part No.

Each ()

Auto-Ignite Nozzle Replacement Tool


For removing nozzle from auto-ignite FID body
Auto-Ignite FID Catalytic Reactor Accessory
Capillary Column Adapter
For capillary column use with the
FID 1/8 to 1/16 in. detector adapter
Ceramic Column Cutter
Cotton Applicators
Detector Cover (Brown Color)
Detector Cover (White Color)
Eraser Brush-Pencil
Jet Assembly
Jet Replacement Tool
1/4 in. nut driver for removing jet
from auto-ignite FID body
Quartz Wool
Replacement Stainless Steel Glow Plug
for Auto-ignite FID
Septa, low bleed (pkg. 50)**
1/4 in. Packed Column Adapter
For use with 1/4 in. packed columns. 1/8 to 1/4 in.
adapter fits both injector and detector ends

N6103188

17

N6120161
N6120020

612
69

N9301376
N9301272
N6103225
N6103151
09923078
N6100194
N6101297

59
4
43
43
64
376
51

N6102354
N6103089

26
9

N9302972
00080100

103
172

** For more Septa see page 159.

Auto-Ignite FID
Replacement Parts
2
1

Gas Chromatography

2
3
4
5
6
7
8
9

Description

Part No.

Collector Head Assembly


Silicone Rubber O-Ring* (not shown)
Polarizer Nozzle
Spring Washer
Nozzle Insulator
Nozzle Collector
FID Jet Contact/Spring
Jet Assembly
FID Body
Nozzle Assembly

N6100357
09902143
N6103167
09907827
N6101085
N6103175
N6001204
N6100361
N6100364
N6100430

Each ()
1161
1
49
1
59
55
10
301
573
199

1
3

5
6

132

Detectors
Flame Ionization Detector (FID) External Igniter
2

Add-On Kits
External Igniter FID with PPC Add-On Kit
Kit includes detector, heater and sensor, heater block,
igniter, programmable pneumatics, and controls for
detector combustion gases. Requires but does not include
FID amplifier (N6120162). The AutoSystem XL must be
PPC ready. If not, PPC upgrade kit (N6120146) is required.
(See page 166 for more information.) Installation by
PerkinElmer Service is required, but not included.
Voltage

Part No.

120 V
230 V

N6120120
N6120121

Each ()

4489

Kit includes detector assembly with heater and sensor,


heater block, igniter, hydrogen pressure regulator,
and air needle valve. Requires, but does not include,
FID amplifier board (N6120162).
Part No.

120 V
240 V

N6120010
N6120024

Detectors

External Igniter FID Add-On Kit (Manual Pneumatics)

Voltage

Each ()
2516
7

FID Amplifier

Part No.

Required for use with FID


Detector Add-On Kit.

N6120162

Each ()
754

Replacement Parts
1
2
3
4
5
6
7
8
9

Part No.

Collector Head Assembly


*Collector Assembly O-Ring (not shown)
Collector Cap
Nozzle Insulator
Nozzle Ring
FID Nozzle
FID Jet Contact
Jet Assembly
Polarizer Replacement Kit
FID Body
Collector Adapter, Teflon ** (not shown)

N6100170
09902143
N6101037
N6101085
09912223
N6101100
N6001204
N6100038
N9300089
N6100037
N6101547

Each ()
574
1
17
59
1
59
10
147
65
682
43

Gas Chromatography

Description

** Note: If instrument was purchased prior to March 1993, the following


items must also be ordered: one each of N6101546 and 09912223.
8

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

133

Detectors
Flame Ionization Detector (FID) Replacement Parts
Catalytic Reactor Accessory

Miscellaneous Accessories

The catalytic reactor converts CO and CO 2 to methane


conveniently and efficiently. The lower detection limit
is extended to well below 0.1 ppm.

External Ignite Nozzle Replacement Tool


For removing nozzle from
External Ignite FID body.

The catalytic reactor consists of a special catalytic reactor


base which replaces the FID base. The reactor body
contains a quantity of catalyst held in place by a quartz
wool plug.

Part No.
N6100102

Hydrogen Regulator
Replacement Kit

Part No.
N6100289

Each ()
125
Each ()
548

Kits include base assembly, reactor tube, and instructions.

Detectors

External Igniter FID Catalytic


Reactor Accessory

Part No.
N6120070

Each ()

Hydrogen/Air Replacement
Needle Valve

Part No.
N6120161

Each ()
612

Catalytic Reactor Replacement Parts


Description

Part No.

Catalyst
Jet Assembly
Quartz Wool

N9302698
N6100194
N6102354

FID Base

Gas Chromatography

Catalyst

134

N6101412

Each ()
396

810

Igniter Assembly
Auto-Ignite FID Catalytic
Reactor Accessory

Part No.

Complete replacement igniter


assembly with glow plug.

Part No.
N6100016

Replacement Glow Plug


for External Ignite FID

00091279

FID Flow Measurement Adapter

Part No.

Part No.

Each ()
191

Each ()
6

Each ()
55
376
26

N6101345

Each ()
29

Detectors
Flame Photometric Detector (FPD)
FPD Add-On Kit (Manual Pneumatics)

Add-On Kits
The FPD is a highly sensitive and selective detector for both
sulfur and phosphorus compounds. It is especially suitable
for environmental monitoring of H2S and sulfur gases in
general and for organophosphorus compounds present at
trace levels in pesticide analysis. Alkyl tin compounds can
also be analyzed by changing the filter assembly. The sulfur
filter is shipped standard.
The FPD mounts in either the front or rear detector position.
This allows many detector combinations, such as FPD/FPD,
FPD/TCD, and FPD/ELCD.
The AutoSystem also includes a linearizer function for the
sulfur mode and convenient control of the photomultiplier
tube from the keyboard.

Voltage

Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120088
N6120089
N6520028
N6520029

Each ()
8900
5400

FPD Amplifier

Detectors

The FPD is capillary-column compatible. The detector will


accept columns of 0.530 mm i.d. or less. The standard jet
shipped with the FPD does not have a glass-lined tail pipe.
If an all-glass system is required and glass packed columns
will be used, then a glass-lined tail pipe should be ordered
(N6100264). As a reminder, use of packed 1/4 in. columns
requires a 1/8 to 1/4 in. adapter.

Kit includes detector, heater, sensor, heater block,


hydrogen needle valve, air pressure regulator, and
sulfur photomultiplier filter. Requires but does not
include FPD amplifier (N6120095). Firmware revision
1.6 or greater required. Firmware must be PerkinElmer
Service installed. AutoSystem operators manual
(09938559) revision E or higher required.

Firmware revision 1.6 or greater required. Firmware must


be PerkinElmer Service installed. AutoSystem operators
manual (09938559) revision E or higher required.
Part No.
N6120095

Each ()
660

FPD Replacement Parts for AutoSystem Series GCs


1
2
3
4
5
6

Filter Assembly

1
3
4
6
5

7
8

Hydrogen

Phosphorus Lens (Yellow)


Sulfur Lens* (Blue)
Tin Lens (Orange)

N6000981
N6000637
L4135472

* Shipped standard.

O-Ring
Seal Assembly and Window
(heat shield)
Liner (window)
FPD Body (upper)
Window Holder
FPD Jet,
Glass-lined Jet Tailpipe
(for all-glass system)
FPD Body (lower)
Photomultiplier Tube

09902247
N9300096

2
105

N6003057
N6100243
N6003066
N6100245
N6100264

34
650
22
128
376

N6100244
09972321

612
1256

Each ()
465
670
721

Voltage

Part No.

120 V
230 V

N6120128
N6120129

Packed Column Adapter


1/8 to 1/4 in. adapter for use with
1/4 in. packed columns. (Set of 2)

Part No.
00080100

Gas Chromatography

Filters
Part No.

Each ()

Kit includes detector, heater, sensor, heater block,


programmable pneumatic control for detector combustion
gases, and sulfur photomultiplier filter. Requires but does
not include FPD amplifier (N6120095). AutoSystem XL GC
must be PPC ready. If not, a PPC upgrade kit (N6120146)
is required. (See page 166 for more information.)
Installation by PerkinElmer Service is required,
but not included.

Description

Part No.

FPD with PPC Add-On Kit

Air
8

Description

Each ()
6700

Each ()
172

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

135

Detectors
Mass Spectrometer Detector

The Clarus

Mass Spectrometer
The Clarus mass spectrometer is the fastest
sampling and widest-mass-range quadrupole mass
spectrometer available for GC/MS. State-of-the-art
Pentium electronics process more scans across each
peak, resulting in unmatched accuracy and precision,
and better overall spectral fidelity. This, coupled
with unique productivity tools, provides the
functionality necessary to achieve optimum
performance, completing work quickly, easily, and
efficiently. The wide mass range and flexible data
acquisition modes help tackle the most complex
applications while rugged instrument design delivers
maximum uptime, easy maintenance, and lower
operating cost.
Combine the Clarus mass spectrometer with the
Clarus gas chromatograph, market-leading
TurboMatrix sample handling accessories, flexible
user-friendly TotalChrom software, and worldclass service and support for an integrated,
complete analytical solution from one familiar
name PerkinElmer. Whatever your application
Environmental, Chemical, Petrochemical, Flavor
and Fragrance, Food, Beverage, Forensic,
Pharmaceutical PerkinElmer delivers the
accuracy and precision you need.

Clarus Mass Spectrometer

Flexible Column Choices

Clarus Mass Spectrometer Benefits:

Because the Clarus mass spectrometer allows a carrier gas flow of up to 5 mL


per minute in EI, you have more column choices than with other GC/MS systems.
Narrow-, medium-, and wide-bore columns can be used, with almost unlimited choice
of stationary phase, diameter, and analytical method with Clarus mass spectrometer.

Fastest Scan Rates unprecedented speed with


better chromatographic peak definition ensuring
better quality results. Opens the use of quadrupole
technology to fast GC applications.

Column

Internal Diameter

Typical Flows

Clarus Mass Spectrometer

Others

Narrow-bore

0.10 to 0.18 mm i.d.

0.1 to 0.8 mL/min.

Medium-bore

0.25 mm i.d

1 to 1.5 mL/min.

Wide-bore*

0.32 to 0.53 mm i.d.

3 to 5 mL/min.

* Columns with low pneumatic impedance may require attachment of additional length of deactivated
fused-silica capillary tubing to provide proper pressure drop from injector to mass spectrometer
(Part Nos. N9301354, N9302149, and N9301343).

Widest Mass Range uncompromised performance


over a wide mass range.
SIFI Scanning Mode selected Ion Monitoring (SIM)
and full scan in the same run resulting in the most
complete characterization of the sample. No need
to run the sample twice.
Gold Component Technology improved stability
and reduced maintenance.
Easy Access Ion Source less than
15-minute changeover.
Sealed, Long-Life Photomultiplier eliminates
expensive replacement costs of electron multipliers.
Better reliability.

136

Detectors
Mass Spectrometer Detector
Cables

Miscellaneous Accessories
Each ()

Description

Part No.

Cable, RS232, 7 ft. Length (185 cm)


Personal Computer to AutoSystem XL Integral LINK
(included with TurboMass Gold)
Cable, RS232, 25 ft. Length (660 cm)
Personal Computer to AutoSystem XL Integral LINK
Computer to MS Cable
For use with TurboMass Mass Spectrometers only
Ethernet Cable
For TurboMass Gold Mass and
Clarus 500 Spectrometers only
GC Start/Ready Cable
GC to MS Interface Cable

S5010025

46

S5010030

52

E6400251

672

09991463

58

E6400247
E6400242

599
1022

BTOTM (Bleed Temperature Optimized) Injector Septa


Maximum recommended operating
temperature 300 C. Low bleed,
high temperature. 11 mm diameter.

Part No.

CI Ion Exit Plate


Extra EI Electron Trap
Extra CI Ion Volume
Extra EI Ion Volume
Extra EI Repeller
Ion Exit Plate
Filament Assembly and Standard Tungsten Filament
For use with TurboMass Spectrometers only
Inner Source Heater Assembly
Inner Source O-Ring Seal
Inner Source Thumbscrew
Standard Rhenium Filament
Trap Contact

E6401214
E6401220
E6401208
E6400211
E6401219
E6401213
E6400209

52
137
988
1784
242
66
220

E6400265
E5711272
E6070836
N6470012
E6401217

255
22
6
191
157

Ionizer Replacement Parts

103

Includes standard solutions of benzophenone,


hexachlorobenzene, and octafluoronaphthalene
for testing instrument sensitivity.
Part No.
E6401017

High molecular weight


test standard. 100 mg.

Part No.
N9301730

Each ()
59

Detectors

Each ()

Description

N9302972

Each ()

GC/MS Sensitivity Test Mix

GC/MS Test Mix Triazine

Inner Source Replacement Parts

Part No.

Each ()
107

Forepump Vacuum Filter Kits


Includes: Foreline Adsorption Trap (09923493), Nipple
NW25 Extension Tube (09920864), NW25 Clamp Ring
(09923491), NW25 Centering Ring (09923490), Installation
Instructions (09936442), and
Part No.
Each ()
Activated Alumina Reagentreplacement (09923504).

E6420021

Outlet Mist Filter

Part No.
09923518

912
Each ()
643

Replacement Parts

Description

Part No.

Each ()

Clarus 500 and TurboMass Extra EI Inner source


Assembly (Tungsten)
Clarus 500 and TurboMass Gold Extra EI Inner Ion
Source Assembly (Rhenium)
Clarus 500 and TurboMass Gold Extra PCI/NCI
Inner Ion Source Assembly (Rhenium)
Requires PCI or PCI/NCI configuration option
Extra Outer Ion Source and Optics Assembly

N6470207

2064

E6400207

2171

E6400208

1615

E6400206

4438

Manuals
Part No.

Clarus 500 MS Manual Set


TurboMass Gold Manual Kit
Includes: Users Guide-EPCAS software,
Users Guide-EPCAS hardware, and TurboMass
Gold Tutorial
TurboMass Software Users Manual
TurboMass Hardware Users Manual

09934562
09934472

Each ()
179
257

Part No.

Centering Ring
Clamp
Copper Tubing, Precleaned (50 ft.)
FC-43 Tuning Compound
Filament Allen Wrench
Forepump Oil
Gas Purifier for GC/MS
Glass Bulb for Reference Gas
Penning Gauge Spares Kit
Vacuum line (7 ft.)
Eraser Brush-Pencil
Ceramic Column Cutter
Cotton Applicators
Septa, low bleed (pkg. 50)*

09923490
09923491
N9300077
N6212407
09907222
09923492
N6471025
E6401384
N6471031
E6400223
09923078
N9301376
N9301272
N9302972

Each ()
54
43
120
115
9
117
293
62
1305
1058
64
59
4
103

* For more septa see page 159.

Gas Chromatography

Description

Description

Vent Kit
S2701610
09936341

217
96

The Mass Spectrometer Vent Kit eliminates the introduction


of oxygen, water vapor, and other airborne contaminants
which can degrade sensitivity and performance of the mass
spectrometer. The Clarus GCs should be vented with UHP
nitrogen (99.9995%). Helium should not be used as Helium
molecules penetrate the glass sleeve on the photomultiplier
tube, compromising the vacuum
Part No.
Each ()
and lowering sensitivity.
N6470045

446

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

137

Detectors
Mass Spectrometer Detector
TurboMass Single Additional Workstation License
Allows TurboMass software to be run on one additional
computer. Does not include manuals.
Part No.
Each ()
Note: Network setup is the responsibility
S2701017
1512
of the customer.

Clarus MS

Wiley Mass Spectral Library

Part No.

Does not include the NIST library.

E6420003

Each ()
6400

Detectors

Transfer Line
Description

Part No.

Transfer Line Carrier Tube


Transfer Line O-Ring
Transfer Lines 1/8 in. Nut

E6401308
E5711269
E6401309

Each ()
982
11
370

Upgrade Kits
MSVent Add-On Kit for the Clarus GC/MS

EI to PCI/NCI Upgrade

Includes: all the necessary parts to add an MSVent


accessory to a Clarus GC/MS. Requires a PreVent option
(N6120144) to be already installed
Part No.
Each ()
in the Clarus gas chromatograph.

Includes: Cl ion source, reagent gas tubing, flow regulators,


valves and solenoids, and dual-polarity electronic options.
Installation by PerkinElmer Service
Part No.
Each ()
is required, but not included.

N6120179

E6420007

714

8600

TurboMass Gold Computer Upgrade

Software
TurboMass 5.1 Software Kit
Includes: the TurboMass 5.1 software
CD, TurboMass Users Manual CD,
and Utilities CD.

Part No.
N6520206

Description

Part No.

NIST Mass Spectral Library (2002)


NIST98 to 2002 Upgrade Kit
Pfleger/Maurer/Weber Drug and Pesticide
Spectral Library

N6520220
N6520240
04308523

Each ()
1915
Each ()
2082
878
4712

TotalChrom Workstation Reprocess-Only Kit


for TurboMass Mass Spectrometers Only

Gas Chromatography

Allows data collected from a conventional detector via


TurboMass software to be analyzed with TotalChrom
Workstation Chromatography Data System software.
Includes: CD and 3.5 in. diskette
Part No.
Each ()
media, user manuals, mouse pad,
and installation instructions.
S2701116
822

138

Upgrade kit includes: Dell GX270 computer plus 17" flat


panel monitor and Windows XP SP2.
Part No.
Each ()
TurboMass 5.1 software is included free.
Service installation is not required.
N6470070
4285

TurboMass Upgrade Kit


Upgrade kit includes: Dell GX270 computer with Windows
XP SP2, 17" flat panel monitor, TurboMass 5.1 software
and manual plus all necessary electronic and hardware
components. Installation by a
Part No.
Each ()
PerkinElmer Service professional
is required, but not included.
N6470080 10700

Detectors
Nitrogen Phosphorus Detector (NPD)
Add-On Kits

Replacement Parts

NPD Add-On Kit (Manual Pneumatics)


The NPD can be used for the analysis of organic compounds
containing nitrogen or phosphorus down to the picogram
level. The NPD has become the detector of choice for
low-level drug and pesticide applications because of its
sensitivity and selectivity.
Kit includes detector, heater, sensor, heater block, air
needle valve, and hydrogen pressure regulator with snubber
and two beads. Requires but does not include amplifier. For
AutoSystem GC Firmware revision 1.4 or greater is required.
Firmware must be PerkinElmer Service installed.

1
2
3
4

Description

Part No.

Collector Head
Bead Assembly (pkg. 5)
Single pkg.
Jet Assembly
NPD Body

N6100253
N6120093
N6120092
N6100038
N6100228

Each ()
574
689
185
147
504

1
Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120090
N6120091
N6520024
N6520025

Each ()

Detectors

Voltage

5300
1730
2

NPD Amplifier

Part No.

Required for use with


NPD Add-On Kit.

N6120094

Each ()

Air in

400

Hydrogen in

NPD with PPC Add-On Kit


Kit includes detector, heater, sensor, heater block, and
programmable pneumatic control for detector combustion
gases and two beads. Requires but does not include amplifier
(N6120094). The AutoSystem XL or Clarus GC must be PPC
ready. If not, the PPC upgrade kit (N6120146) is required.
(See page 166 for more information.) Installation by
PerkinElmer Service is required, but not included.
Voltage

Part No.

120 V
240 V

N6120126
N6120127

Each ()

Column Connection

3045

Column Adapter
1/4 in. Packed Column Adapter
1/8 to 1/4 in. detector receiver adapter
for use with 1/4 in. packed columns.
Two included (injector/detector).

Part No.
00080100

Each ()
172

Gas Chromatography

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

139

Detectors
Photoionization Detector (PID)
Add-On Kits

Detector Series Operation Kits

PID Add-On Kit (Manual Pneumatics)

Description

Part No.

The PID utilizes a high-intensity ultraviolet light source to


ionize the sample components eluting from the column in
order to generate the chromatographic signal. The PID has
a maximum recommended operating temperature of 250 C.
The lamp can be replaced with a blanking disk to allow
bake-out operation (up to 350 C).

PID/FID, PID/ECD
Series kit for directing effluent
from a PID to an FID or an ECD

N6120059

Detectors

Kit includes detector, heater, sensor, makeup gas needle


valve, and all necessary mounting hardware for installation
on an AutoSystem GC. Requires but does not include
amplifier (N6120061) and lamp power supply (N6120062).
Firmware revision 1.2 or greater is required. Firmware must
be PerkinElmer Service installed. AutoSystem operators
manual (09908559) is required if not revision or higher.
Voltage

Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120047
N6120057
N6520026
N6520027

PID Amplifier
Required for use with
PID Add-On Kit.

PID Lamp Power Supply


Required for use with
PID Add-On Kit.

Part No.
N6120061

Part No.
N6120062

Each ()

Description

Part No.

Bakeout Disk
Lamp Cleaning Compound
1/4 in. Detector Receiver
1/8 in. Detector Receiver

03302989
03302775
03300866
03300865

Each ()
398

Gas Chromatography

Voltage

Part No.

Each ()

120 V
230 V

N6120130
N6120131

12900

2
3
4
5
6
7
8

Part No.

PID Lamp (10.2eV), For most applications


including aromatics, alkenes, and aliphatics
higher than C4. Shipped standard with PID
PID Lamp (9.5eV), Improved selectivity for
multiple ring aromatic, sulfur compounds
PID Lamp Window Seal
PID Lower Lamp Seal
Shoulder Pin
Cap Nut
Base Assembly
Spring
Cap with Harness

03303599

721

03303598

593

03302778
03302777
03302976
03303773
03302979
03302973
N6101696

47
79
110
46
2753
13

2
4

140

62
172
261
261

Description

PID with PPC Add-On Kit


Kit includes detector, heater, sensor, heater block, and
programmable pneumatic control for makeup gas. Requires
but does not include amplifier (N6120061) and power
supply (N6120062). The GC must be PPC ready. If not, a
PPC upgrade kit (N6120146) is required. (See page 166 for
more information.) Installation by PerkinElmer Service is
required, but not included.

Each ()

Replacement Lamps and Parts

Each ()
396

293

Miscellaneous Accessories

8900
7300

Each ()

Each ()

Detectors
Thermal Conductivity Detector (TCD)
Add-On Kits
Lower Internal Volume and Smaller Overall Size
No Makeup Gas Required with 0.53 mm and 0.32 mm i.d.
Capillary Columns
Series Connection Option
Excellent Sensitivity Over a Wide Dynamic Range

TCD Add-On Kit (Manual Pneumatics)


Kit includes all necessary items to install the TCD into the
instrument: detector, heater, sensor, heater block, 1/16 in.
gas line, and flow controller pneumatics. Requires, but does
not include, amplifier (N6120015). The TCD can only be
installed in the rear detector position.
Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120012
N6120027
N6520022
N6520023

TCD Amplifier

Part No.
N6120015

Detectors

Voltage

Each ()
4260

Thermal Conductivity Detector

2400
Each ()
610

TCD/FID Series Operation Kit


TCD and FID series operation kit for
directing effluent from a TCD to an FID.

Part No.
N6120006

TCD with PPC Add-On Kit


Kit includes detector, heater, sensor, heater block, and
programmable pneumatic control for reference gas. Requires
but does not include amplifier (N6120015). The TCD can
only be installed in the rear detector position. The GC must
be PPC ready. If not, a PPC upgrade kit (N6120146) is
required. (See page 166 for more information.) Installation
by PerkinElmer Service is required, but not included.
Voltage

Part No.

120 V
230 V

N6120124
N6120125

Each ()

Each ()
166

TCD Detector Makeup Gas Kit (Manual Pneumatics)


For use with TCD (at low flow rates). Required when using
0.25 mm i.d. and recommended when using 0.32 mm i.d.
capillary columns. Kit includes 1 m of 1/16 in. tubing to
connect to gas supply, graphite/vespel
Part No.
Each ()
ferrules, manual pneumatics,
and installation instructions.
N6120080
510

2827

TCD with PPC Makeup Gas Kit


Includes parts required to add PPC controlled makeup
gas to an existing TCD. Includes tubing, tee-piece, PPC
pneumatics module, and PPC frit #4
Part No.
Each ()
(N6120155). Requires PPC capability
in the GC.
N6120150
1441

Gas Chromatography

Column Adapters
Description

Part No.

Each ()

1/8 to 1/4 in.


Column adapter for use with 1/4 in.
packed columns
1/8 to 1/16 in.
Column adapter for use with capillary columns

00080100

172

N6120020

69

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

141

Headspace Accessories and Supplies


Headspace Instruments

PerkinElmer TurboMatrix
Headspace Samplers
PerkinElmer TurboMatrix Headspace Samplers eliminate tedious and error-producing steps required
in other GC sample preparation techniques, enabling you to analyze volatile compounds in less time.
The intuitive touch-screen graphical user interface provides easy control of the sampler.

TurboMatrix 16

TurboMatrix 40

The TurboMatrix Headspace (HS)


system is fully self-contained and
can be interfaced to almost any gas
chromatograph, giving you access to
PerkinElmers proven headspace
technology, regardless of the brand or
model GC you have in your laboratory.
The TurboMatrix system maximizes
sample throughput. The system can
simultaneously thermostat up to 12
samples, ensuring that the next sample
is always ready for analysis upon
completion of the previous run. This
adds up to a significant time saving since
there is no need to wait for the next
sample to heat.
Volatile compounds in almost any
sample matrix can be analyzed simply
and quickly by headspace gas
chromatography. Only PerkinElmer
headspace samplers utilize a pneumatic-

142

pressure-balanced system, a proven


technology thats been used in all
PerkinElmer headspace samplers for
more than 35 years. This unique,
patented technique provides higher
sensitivity and better performance
than alternative techniques.
The pressure-balanced sampling technique:
Produces sharper peaks by rapidly transferring
a narrow sample band to the GC column.
Increases sensitivity since there is no carrier gas
dilution of sample.
Avoids fractionation due to pressure changes
in the syringe.
Eliminates multiport valves that are prone to
adsorption and may introduce dead volumes.
Provides exceptional reproducibility equal to that
obtainable with liquid.

TurboMatrix
Headspace Trap

The TurboMatrix system is available


in your choice of entry-level, mid-range,
or high-capacity systems. And, since
upgradeability is built in, you can adapt
your system to changing requirements
by upgrading from one model to the
next or adding accessories that provide
more capabilities.

Headspace Accessories and Supplies


Headspce Add-On Kits

Vial Shaker Add-On Kit,


Headspace and Headspace Trap

Cryofocusing Add-On Kit, TurboMatrix HS

Adds a Frequency Scanning Shaker to a TurboMatrix 40


or TurboMatrix 110 headspace sampler. Note: Requires,
but does not include, an options board to be installed in
the TurboMatrix 40 headspace sampler. Installation by
PerkinElmer Service is required,
Part No.
Each ()
but not included.

Adds cryofocusing capability to a TurboMatrix 40 or


TurboMatrix 110 headspace sampler. Includes water trap
to remove the water from headspace samples taken from
aqueous solutions. Note: Requires but does not include,
LN2 Dewar (B0500924). Also requires, but does not include,
an options board to be installed in the TurboMatrix 40
headspace sampler. Installation
Part No.
Each ()
by PerkinElmer Service is required,
but not included.

M0413550

3941

Consists of cryofocusing module, firmware, required tubing


unions, and water trap to be installed in AutoSystem GC.
Requires liquid nitrogen storage tank.
Part No.
Each ()
Installation by PerkinElmer Service
is required, but not included.
N1010047
2716
Part No.
B4000057

1314

HS 40XL Shaker Accessory Add-On Kit


Adds Frequency Scanning Shaker to vibrate all samples in
thermostatting chamber. Installation by PerkinElmer Service
is required, but not included.

HS 40XL Cryofocusing Accessory (White Color)

Replacement Water Trap


for Cryofocusing Accessory

M0413549

Headspace Accessories and Supplies

Add-On Kits

Color

Part No.

Blue
Red

N1010050
B0505475

Each ()
4336
3941

Each ()
402

Options Board/BCD Output Board, TurboMatrix HS


Required for installation of the following options on
the TurboMatrix 40 headspace sampler Vial Shaker
and Cryofocusing and when upgrading a TurboMatrix
16 or 40 headspace sampler to a TurboMatrix 110. Also
provides output of BCD information regarding tube position
numbers and six relays for timed control of external
devices. Installation by PerkinElmer Service is required, but
not included. (Fitted as standard
Part No.
Each ()
on TurboMatrix 110 HS).
M0413551

988

HS 40 Options Board
Allows up to six optional control ICs.
Installation by PerkinElmer Service
is required, but not included.

Part No.
B0184142

Each ()
261

TurboMatrix Headspace PPC Add-On Kit

M0413548

Gas Chromatography

Includes parts to convert a headspace sampler from manual


pneumatics to electronic Programmable Pneumatic Control
(PPC). Installation by PerkinElmer
Part No.
Each ()
Service is required, but not included.
3418

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

143

Headspace Accessories and Supplies


Headspace Accessories and Supplies

Headspace Accessories
TurboMatrix HS Trap Cold Trap Tube (Carbotrap C)

Miscellaneous Accessories
TurboMatrix HS Standard Length
Heated Transfer Line (960 mm)

Part No.

For operation up to 210 C.

M0413643

TurboMatrix HS/HS Trap Long


Heated Transfer Line (1650 mm)

Part No.

For operation up to 210 C.

M0413552

Each ()

Standard cold trap (M0410094)


packed with Carbopack C.

Part No.
N6200150

Each ()
317

1314

O-Ring

Part No.

7 mm

09200091

TurboMatrix Headspace
Sampler Users Manual

Part No.

Each ()
30

Each ()
2168

M0413401

Each ()
93

FusedSilica Capillary Transfer Line


Tube i.d. (mm)

Length (m)

Part No.

0.25
0.32

5
5

N9301356
N9301357

Each ()
37
37

Siltek Deactivated Fused Silica Transfer Line


Tube i.d. (mm)

Length (m)

Part No.

0.25
0.32

5
5

N9316607
N9316608

Each ()
70
77

Cool Platen
For storage of vials below ambient down to +5 C. Contains
cool platen and tubing. Requires a thermostatted external
cooling circulation water bath. Installation by PerkinElmer
Service is required, but not included.
Part No.
Each ()
Note: Requires, but does not include,
B0500778
2270
Cryostat Liquid Immersion Cooler.

Extended Transfer Line (1650 mm HS 40/40XL)


Zero Dilution Inner Liner
To be used with zero dilution outer liner. The powerful
zero dilution liner combination allows you to achieve lower
detection limits, sharpen peak shape, and increase throughput
for many routine analyses. Installed in an AutoSystem Series
or Clarus GC standard capillary or PSS injector, this optional
special hourglass insert connects the fused-silica transfer
line from the headspace sampler to the capillary column,
permitting undiluted and efficient sample transfer. The
insert provides the advantages of a
Part No.
Each ()
direct connection, while maintaining
the capability to perform split injections.
N1011446
41

Zero Dilution Capillary Injector Outer Liner

Gas Chromatography

To be used with zero dilution inner liner. The powerful


zero dilution liner combination allows you to achieve lower
detection limits, sharpen peak shape, and increase throughput
for many routine analyses. Installed in an AutoSystem Series
or Clarus GC standard capillary injector, this optional special
hourglass insert connects the fused-silica transfer line from
the headspace sampler to the capillary column, permitting
undiluted and efficient sample transfer. The insert provides
the advantages of a direct connection,
Part No.
Each ()
while maintaining the convenience of
using a split injector as an interface.
N1011445
74

Zero Dilution PSS


Injector Outer Liner

Part No.
N1011447

Each ()

Extra-long transfer line to allow installation of HS 40XL on


the right side of the AutoSystem Series/Clarus GC or to any
gas chromatograph where the HS 40XL
Part No.
Each ()
is situated at an extended distance.
B4000046

High Pressure Sampling Accessory


Used for operation with capillary columns requiring a
low head pressure. Also used for carrier gas flow control.
Accessory includes high-pressure sampling module with
pressure regulator, gauge, firmware, tubing, and unions.
Installation by PerkinElmer Service
Part No.
Each ()
is required, but not included.
Note: Requires, but does not include, Options Board.

144

3278

HS 40XL to AutoSystem Series


Left Side Mounting Kit (White Color)
For connecting the HS 40XL transfer line through the left
side of the AutoSystem XL GC directly to the column in the
oven instead of via the injection port. Includes a new GC
side panel and parts for attaching the transfer line to the
GC. Requires, but does not include, some type of zero dead
volume connector to connect to the column (for example,
a universal capillary column connector,
Part No.
Each ()
N9302149). Installation by PerkinElmer
Service is recommended.
N1010048
510

HS 40XL Instruction Manual

N1011210

B0505271

90

Gas Chromatography Theory and Practice,


Static Headspace Book by L. Ettre and B. Kolb
Part No.

2168

Part No.
09935404

Each ()
153

Each ()
73

Headspace Accessories and Supplies


Internal Carrier Gas Pressure Control

TurboMatrix HS Trap PC (RCS) v2.0

For carrier gas control. Includes regulator, gauge, tubing, and


unions. Installation by PerkinElmer
Part No.
Each ()
Service is required, but not included.

NOTE: This software requires the HS unit to have firmware version 2.00.
Provides full external control of a TurboMatrix headspace sampler from a
personal computer running under Windows XP SP1 or Windows 2000 SP3.
Methods and sequences can be generated, stored, edited, printed and executed.
Functions include setup, diagnostics, user defined access levels and run
reports. Includes control of the TurboMatrix Trap if present on the HS unit. Onscreen interactive help function is available. Cable included. RCS version 2.0
is available for those who do not wish to update from TotalChrom (TC) 6.2.1
and/or for those who need to use a TurboMatrix
Part No.
Each ()
HS unit with revision 2.0 or lower firmware.

B0505268

1314

Recycle Mode Accessory


Continuously repeats sequence with setup method. Installation
by PerkinElmer Service is required, but not included.
Note: Requires, but does not include, Options Board.

Part No.
B0197336

N6700200

Each ()
606

TurboMatrix 40 Mid-Range Sample Tray

HS 40XL Control Software

40-position sample tray for use on


the mid-range headspace sampler.

B0510984

745

Sample Trays

Remote Control Software (RCS)


Windows -based, flexible, easy-to-use external control software
for the HS 40 and HS 40XL. The user can develop and store
methods and sequences. Run reports can be obtained, stored,
and printed. On-screen, context sensitive help available. Can
be operated in combination with PerkinElmer TotalChromTM
Software. Requires RS-232
Part No.
Each ()
Interface for the HS 40XL.

Headspace Accessories and Supplies

Headspace Accessories

Part No.
M0413592

Each ()
112

TurboMatrix 110 High-Capacity Sample Tray


110-position sample tray for use on
the high-capacity headspace sampler.

Part No.
M0413593

Each ()
332

844

Tools
TurboMatrix HS PC (RCS) v1.1 for WIN NT
NOTE: This software version is only supported under Windows NT4.0 Service
Pack 6a. Windows 2000 users should order Version 1.2 (see Part Number
N6200200 below). This software requires the HS unit to have firmware
version 1.87 or earlier. Provides full external control of a TurboMatrix
headspace sampler from a personal computer running under Windows 95, 98
or NT. Methods and sequences can be generated, stored, edited, printed and
executed. Functions include setup, diagnostics, user
Part No.
Each ()
defined access levels and run reports. On-screen
interactive help function is available. Cable included.
M0413348
822

TurboMatrix HS PC (RCS) v1.2 for WIN 2000

For replacing O-Rings in upper


and lower seal assemblies.

Headspace Vial Gauge

Part No.
B0147449

Part No.

Used to check 20 mL headspace


vials for correct dimensions.

B0151737

Adapter Sleeve Torsion Bar

Part No.

For loosening upper seal.

B0135485

Thumbscrew Removal Tool

Part No.

For removing lower seal assembly.

B0131410

Spigot Key

Part No.

For loosening lower seal.

B0500843

Open End Wrench, 1/4 - 5/16 in.

Part No.

For use in mounting the Transfer Line.

09907233

Each ()
20

Each ()
102
Each ()
26
Each ()
20
Each ()

Gas Chromatography

NOTE: This software requires the HS unit to have firmware version 1.87 or
earlier. Provides full external control of a TurboMatrix headspace sampler
from a personal computer running under Windows 2000 SP2. Methods and
sequences can be generated, stored, edited, printed and executed. Functions
include setup, diagnostics, user defined access
Part No.
Each ()
levels and run reports. On-screen interactive help
function is available. Cable included.
N6200200
819

O-Ring Removal Tool

39
Each ()
23

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

145

Headspace Accessories and Supplies


Headspace Accessories and Supplies

Headspace Accessories
Open End Wrench, Sw-7

Part No.
B0510251

Transfer Line End Cap

Part No.
B0510403

PE Injector Transfer Line Adapter

Part No.
B0505266

Each ()
10
Each ()
53

Each ()
186

For connecting a TurboMatrix or HS 40 (XL) headspace


sampler to the following Shimadzu gas chromatographs:
GC 9a for capillary columns, 14A
Part No.
Each ()
packed columns, 14B packed columns,
17A packed, and capillary columns.
B0505889
140

Headspace Adapter Kit for Shimadzu GC14A/B


For connecting a TurboMatrix or HS 40 (XL) headspace
sampler to a Shimadzu GC 14A/14B gas
Part No.
Each ()
chromatograph with capillary columns.

TurboMatrix and HS 40XL


Adapter Kits for Non-PerkinElmer
Gas Chromatographs

Headspace Adapter Kit for Shimadzu GC16

All kits include a Modified Septum Nut Adapter and the instructions for
physical installation and interfacing of the two instruments. Use the standard
PerkinElmer cables (N1011206, 2 needed) for ready/run connections.

For connecting a TurboMatrix or


HS 40 (XL) headspace sampler to a
Shimadzu GC 16 gas chromatograph.

Headspace Adapter Kit for Carlo Erba

Headspace Adapter Kit for Thermo Trace GC

For connecting a TurboMatrix or HS 40


(XL) headspace sampler to a Carlo Erba
Mega or Vega gas chromatograph.

B4000033

Part No.
B0506603

Each ()
147

Headspace Adapter Kit for Fisons Series 8000


For connecting a TurboMatrix or HS
40 (XL) headspace sampler to a Fisons
Series 8000 gas chromatograph.

Part No.
B4000012

Each ()
140

Headspace Adapter Kit for Gerstel CIS Injector


For connecting a TurboMatrix or HS 40 (XL) headspace
sampler to a Gerstel Cooled Injector System Inlet. As the
Gerstel injector can be installed on several GC models,
customer should contact the GC
Part No.
Each ()
manufacturer for the appropriate
Remote Start/Stop Cable.
B0506539
198

Headspace Adapter Kit for HP 6890,


HP 6850, or HP 5890 On-Column
For connecting a TurboMatrix or HS 40 (XL) headspace
sampler to an on-column injector of an HP 6890, HP 6850,
HP 5890, or HP 5890 Series 2 gas chromatograph.

Gas Chromatography

Headspace Adapter Kit for Shimadzu

Note: Installation on HP 6890 and HP 6850 requires a TurboMatrix/HS 40 (XL)


to HP 6890/6850 GC Ready/Start Cable (N610-0410). For installation on
HP 5890, customer should contact Hewlett-Packard
Part No.
Each ()
for the appropriate Remote Start/Stop Cable.
B0507944

140

For connecting a TurboMatrix or


HS 40(XL) headspace sampler to a
Thermo Trace gas chromatograph.

Part No.

147

Each ()

B0508521

Part No.

147

Each ()

N6201030

143

Headspace Adapter Kit


for Varian Capillary Column Injector
For connecting a TurboMatrix or HS 40(XL) headspace
sampler to a Varian 3400 or 3800 gas chromatograph
capillary column injector. Customer
Part No.
Each ()
should contact Varian for the
appropriate Remote Start/Stop Cable.
N6201001
168

Headspace Adapter Kit


for Varian Packed Column Injector
For connecting a TurboMatrix or HS 40(XL) headspace
sampler to a Varian 3400 or 3800 gas chromatograph
packed column injector. Customer
Part No.
Each ()
should contact Varian for the
appropriate Remote Start/Stop Cable.
B0505978
140

Headspace Adapter Kit for Varian/Finnigan ITS40


For connecting a TurboMatrix or
HS 40(XL) headspace sampler to a
Varian/Finnigan ITS40 GC/MS System.

Part No.
B0507942

Each ()
217

Installation Instructions: Headspace to


Non-PerkinElmer Gas Chromatographs
Instructions for physical installation and interfacing
of the TurboMatrix or HS 40(XL) headspace sampler
to non-PerkinElmer GCs.
Part No.
Each ()
Note: This kit is intended for GCs not listed above.
B0508738
77

146

Headspace Accessories and Supplies


TurboMatrix Headspace to HP 6890
GC Ready Start Cable

TurboMatrix Upgrade Kits

Connects a TurboMatrix Headspace Sampler to an


HP 6890 or HP 6850 GC.

TurboMatrix 16 to 40 Upgrade Kit (Headspace Only)

Note: Customer should contact gas chromatograph manufacturer for the


appropriate Remote Start/Stop Cable.
Part No.
Each ()
N6100410

149

Headspace Accessories and Supplies

Headspace Accessories

Includes parts to upgrade an entry-level headspace sampler


to a mid-range headspace sampler that can perform automated
analysis of up to 40 vials with overlapping themostatting of
up to 12 vials. Installation by
Part No.
Each ()
PerkinElmer Service is required,
but not included.
M0413545
5300

Start/Ready Cables
Description

Part No.

HS 40XL to Agilent 6890 GC


For all PerkinElmer GCs and HP 5890 (2 needed)

N6100410
N1011206

Each ()
149
35

TurboMatrix Headspace/HS 40/


HS 40XL Replacement Parts
and Needle Identification

Includes parts to upgrade a mid-range headspace sampler


to a high-capacity headspace sampler that can perform
automated analysis of up to 1100 vials with overlapping
themostatting of up to 12 vials.
Part No.
Each ()
Installation by PerkinElmer Service
is required, but not included.
M0413547 15100

The number of rings engraved into the needle top


in various types of needles.

Needle Type

Number of Rings
for Stainless Steel

Number of Rings
for Platinum Iridium

Wide-Bore
Small-Bore
Jet

none
none
3

1
2
4

Note: Requires, but does not include, an options board (M0413551) to be installed
in the headspace sampler. Installation by PerkinElmer Service is required,
but not included.

Replacement Parts
Part No.

1 Platinum/Iridium Needle, Wide-Bore


Platinum/Iridium Needle, Small-Bore
Platinum/Iridium Needle, Jet
Silcosteel Needle, for Headspace Trap Only
Stainless Steel Needle, Wide-Bore
Stainless Steel Needle, Small-Bore
Stainless Steel Needle, Jet (ships with instrument)
2 Needle Seal Assembly (without O-Rings)
3 O-Ring for Needle Seal Assembly (pkg. 10)
4 Vespel Ferrule 116 in. (pkg. 10)

9 Fused-Silica Capillary Transfer Line:


0.25 mm i.d. x 5 m length
0.32 mm i.d. x 5 m length

Each ()

B0144169
B0500959
B0510364
N6700130
B0131385
B0500987
B4000011

2371
2032
1084
994
268
1024
547

B0500833

74

B0198110

42

09920127

84

N9302832

B0503956
N6700113

207
529

09920104

84

09903700

48

N9300059

54

Gas Chromatography

5 Male Nut 116 in.


6 GLT Adapter Tube
GLT Adapter Tube, Silcosteel
7 Graphite/Vespel Ferrule 116 in. x 0.4 mm
(for use with 0.25 mm i.d. transfer line, pkg. 10)
Graphite/Vespel Ferrule 116 in. x 0.5 mm
(for use with 0.32 mm i.d. transfer line, pkg. 10)
8 Nut 1 16 in. Swagelok

Includes parts to upgrade an entry-level headspace sampler


to a high-capacity headspace sampler that can perform
automated analysis of up to 110 vials with overlapping
themostatting of up to 12 vials.
Part No.
Each ()
Installation by PerkinElmer Service
is required, but not included.
M0413546 18400

TurboMatrix 40 to 110 Upgrade Kit


(Headspace and Headspace Trap)

Needle Identification

Description

TurboMatrix 16 to 110 Upgrade Kit (Headspace Only)

9
8
7

5
4
2
3

N9301356
N9301357

37
37

2
3

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

147

Headspace Accessories and Supplies


Headspace Accessories and Supplies

Headspace Vials, Caps, and Septa


Headspace Caps and Septa

Headspace Septa Recommended


Temperature Chart

Patented safety springs and caps designed to


release at vial headspace pressures above 73 psi.

Aluminum-Coated Silicone
Rubber Headspace Septa
Includes caps and starsprings
(19 mm diameter). Maximum
temp. 120 C.
Description

Part No.

pkg. 100
pkg. 1000
pkg. 1000 (preassembled)

B0104243
B0104244
B4000028

Each ()
101
906
952

Butyl Rubber Headspace Septa


Includes caps and starsprings
(19 mm diameter). Maximum
temp. 100 C.

Description

Part No.

pkg. 100
pkg. 1000
pkg. 1000 (preassembled)

B0159356
B0159357
N1010070

Material

Upper Temperature
Limit at Vial

Inertness

Butyl Rubber
PTFE-Coated Butyl Rubber
Aluminum-Coated Silicone
PTFE-Coated Silicone

100 C
100 C
120 to 210 C
210 C

Poor
Good
Good
Good

Headspace Vials
Headspace Starter Kit
Consisting of 1000 vials (B0104236), two sets of septa,
each with aluminum caps and starsprings: 200 PTFE-coated
butyl rubber septa (B0104239), 200 PTFE-coated silicon
rubber septa (B0104241). Also included are: hand crimper
(N9302785), pressure gauge with needle for vials
(B0501377), two needle seal assemblies (B0500833),
10 O-Rings (B0198110), and a book by B. Kolb and L.S.
Ettre, Static Headspace Gas Chromatography Theory and
Practice (N1011210).
Part No.
Each ()

Each ()
B0505601
51
460
507

PTFE-Coated Butyl Rubber


Headspace Septa
Includes caps and starsprings
(19 mm diameter). Maximum
temp. 100 C.
Description

Part No.

pkg. 100
pkg. 1000
pkg. 1000 (preassembled)

B0104239
B0104240
B4000025

Each ()
68
614
645

PTFE-Coated Silicone Rubber


Headspace Septa

Gas Chromatography

Includes caps and starsprings


(19 mm diameter). Maximum
temp. 210 C.

148

Description

Part No.

pkg. 100
pkg. 1000
pkg. 1000 (preassembled)

B0104241
B0104242
B4000022

Each ()
86
772
810

1339

Headspace Safety Sample Vials


Description

Part No.

pkg. 1000

B0104236

Each ()
370

Headspace Accessories and Supplies


Headspace Accessories and Supplies

Headspace Vials, Caps, and Septa


Vial Crimping Tools

Hand Crimper
Part No. N9302571

Electronic Crimpers

Benchtop Crimper
The PerkinElmer Benchtop Crimper with interchangeable
jaws provides a fast and consistent crimp on each vial, every
time. Once crimping pressure is set, the lever action will
repeatedly afford the user a perfectly crimped vial, with little
effort. Jaws and decrimping jaws are available for 11 mm
and 20 mm crimp caps.
Description

Part No.

Benchtop Crimper with 20 mm Jaw


Benchtop Crimper without Jaws
Jaws for Benchtop Crimper, 11 mm
Jaws for Benchtop Crimper, 20 mm

N6620065
N6621006
N6621008
N6621009

Each ()
1685
1685
391
344

New from PerkinElmer, the 20 mm electronic crimpers


and decappers are easy to use and fully rechargeable.
Ergonomically designed to alleviate the potential for Carpal
Tunnel Syndrome and provide a consistent crimp pressure
numerous times. The electronic crimper is provided with
a standard Black and Decker VeraPak Gold battery and
charging unit. This hand-held device will crimp several
hundred vials from one charge. Crimping pressure is fully
adjustable for precision control. Also available in 11 mm.
See page 90.
Features and Benefits:
Precision control crimping
Ergonomically designed grip
Numerous reproducible crimps from a single charge
Includes standard Black and Decker VersaPak Gold
battery and charger
Description

Part No.

20 mm Electronic Hand Crimper, 120 V


20 mm Electronic Hand Crimper, 200 V
20 mm Electronic Hand Crimper, 230 V
20 mm Electronic Hand Crimper, 240 V
20 mm Electronic Hand Decapper, 120 V
20 mm Electronic Hand Decapper, 200 V
20 mm Electronic Hand Decapper, 230 V
20 mm Electronic Hand Decapper, 240 V
Electronic Crimper Battery

N9302571
N9302572
N9302573
N9302574
N9302579
N9302580
N9302581
N9302585
N9302582

Each ()
700
700
700
700
700
700
44

Hand Crimpers
Part No.

Hand Held Crimper, 20 mm


Hand Held Decapper, 20 mm

N9302785
N9301270

Gas Chromatography

Description

Each ()
256
64

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

149

Injectors
Capillary Injectors
Injector Replacement Parts
Components
Manual Gas Control
1
2
3

1
2
3
4
5
6

Injectors

6
6

18
8

11

17
10

14
15
16
19

10
11
12
13
14
15
16
17
18
19

Part No.

Injector Cover
N6101482
Septum Cap
N6100153
ThermogreenTM Septum (pkg. 50)*
N6621028
Injector Top Nut
N6101358
Injector Head
N6100158
O-Ring, Silicone for Glass Liner (pkg. 10) N6101374
Maximum injector temperature 250 C,
O-Ring, Graphite for Glass Liner (pkg. 5) N6101378
Maximum injector temperature 450 C.
O-Ring, KALREZ for Glass Liner (pkg. 1) N9302782
Maximum injector temperature 450 C.
O-Ring, Viton for Glass liner (pkg. 1)
N9302783
Maximum injector temperature 250 C,
recommended for use with Mass Spec.
ships with instrument
Quartz Liner (2 mm) for Splitless Operation N6121002
Quartz Liner (4 mm) for Split Operation
N6121001
or Large Volume Splitless Injection
Glass Liner (2 mm) for Splitless Operation N6101372
Glass Liner (4 mm) for Split Operation
N6101052
Deactivated Liner for Splitless Operation N6121021
2 mm, packed with wool. (pkg. 5)
Deactivated Liner for Split Operation
N6121020
4 mm, packed with wool. (pkg. 5)
Deactivated Uniliner
N6121022
4 mm, packed with wool. (pkg. 5)
Injector Body
N6100047
N9300056
1/8 in. SwagelokTM Nut Brass (pkg. 5)
Restrictor
N6101034
1/8 in. Graphite/Vespel Ferrule (pkg. 10) 09920301
1/4 in. Graphite Ferrule (pkg. 10)
09920140
1/4 in. Swagelok Nut, Stainless Steel (pkg. 5) N9300055
Injector Adapter
N6100157
Charcoal Trap
N6100275
Charcoal Trap for PPC Version**
N6100331
Split Vent Tube
N6100159
Column Nut 1/16 in. Long length
09903392
for reversed ferrule (pkg. 5)

Each ()
21
96
202
96
421
9
21
37
4

22
34
31
29
109
236
331
306
9
55
84
43
30
105
242
553
42
27

* For more septa, see page 159.


** Not shown.

Gas Chromatography

Miscellaneous Accessories

150

Each ()

Description

Part No.

2 oz. Replacement Charcoal (30/60 mesh)


5 g. Quartz Wool (Untreated)
Column Ferrule Graphite/Vespel
Liner Removal Tool
Merlin Microseal Adapter Kit
Includes: 2 Merlin Microseal septa,
1 nut, and 1 injection port adapter
Merlin Microseal Septa
Zero Dilution Liner (Inner)
Zero Dilution Liner (Outer)

03300904
N6102354
09920105
N6100102
N9303344

20
26
84
125
434

N9303345
N1011446
N1011445

181
41
74

Injectors
Capillary Injectors
Split/Splitless Injector Add-On Kits
Capillary Injector with PPC
Kit includes split/splitless injector with programmable
pneumatic control for carrier gas, split vent, heater, sensor,
and heater block. The AutoSystem XL must be PPC ready.
If not, a PPC upgrade kit (N6120146) is required. (See page
166 for more information.) Installation by PerkinElmer
Service is required, but not included.
Voltage

Part No.

120 V
240 V

N6120138
N6120139

Each ()
3128

Complete Capillary Injector Add-On Kits

Injectors

Kit includes split/splitless injector in module with heater


and sensor, 0-60 psig pressure regulator, and transducer for
pressure readout. For manual gas control.
Voltage

Part No.

120 V AutoSystem
240 V AutoSystem
120 V Clarus
230 V Clarus

N6120009
N6120022
N6520012
N6520013

Each ()
3329
1916

Dual Capillary Column Adapter Kit


Kit includes all necessary hardware to install two capillary
columns to a capillary injector. Note: Kit does not include
appropriate 1/8 in. 2-hole ferrule. (See page 94) For manual
gas control.
Voltage

Part No.

120 V

N6120050

Each ()
122

Split/Splitless Injector Starter Kit


for Manual Gas Control
Includes: 2 mm i.d. quartz liner, 4 mm i.d. quartz liner,
silicone O-Rings (10), Thermogreen septa (50), 0.5 mm
graphite ferrules (10), 0.8 mm graphite ferrules (10), 1/16 in.
stainless steel nuts (5), untreated quartz wool, packing rod,
and wafer scribes (10).
Part No.
Each ()
N6120101

574

Gas Chromatography

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

151

Injectors
Packed Column Injector
Add-On Kits

Injector Replacement Parts

Packed Column Injector Kit with Manual Pneumatics


Includes: complete injector assembly with heater and sensor,
0-100 mL flow controller, and column head pressure gauge
for installation into the AutoSystem.
Voltage

Part No.

120 V*
240 V*

N6120007
N6120023

1
2
3
4

Each ()
5
2245

Description

Part No.

Septum Cap
Septa Thermogreen (pkg. 50)**
Needle Guide
Glass Liner
Quartz Liner
Packed Injector Assembly

N6100153
N6621028
N6101050
N6101048
N6121000
N6100048

** For more septa see page 159.

Packed Column Injector Kit with PPC

Injectors

The kit includes complete injector assembly with


programmable pneumatic control, heater, sensor, and
heater block. The GC must be PPC ready. If not, a PPC
upgrade kit (N6120146) is required. (See page 166 for
more information.)
Voltage

Part No.

120 V*
240 V*

N6120136
N6120137

Each ()

2288
3

Packed Column Injector Kit


with Screen Readout and Manual Pneumatics
Includes: complete injector assembly with heater and sensor,
0-100 mL flow controller and column head pressure gauge,
and transducer for screen readout of column carrier flow.
Voltage

Part No.

120 V* AutoSystem
240 V* AutoSystem
120 V* Clarus
230 V* Clarus

N6120008
N6120025
N6520010
N6520011

Each ()
4
2729
1398

Packed Column Injector Kit AutoSystem XL and Clarus


The kit includes complete injector, heater, sensor,
and heater block. (Does not include pneumatics.)
Voltage

Part No.

120 V*
240 V*

N6120071
N6120072

Each ()
1824

Packed Column Injector Starter Kit

Gas Chromatography

Includes glass liner, needle guide,


Thermogreen septa (50), untreated
quartz wool, and packing rod.

Part No.
N6120100

Each ()
389

Packed On-Column Injector for 1/4 in.


(Long-Legged) Glass Columns
For use with 1/4 in. (long-legged) on-column glass column.
Includes: complete injector, heater, and sensor and heater
block. Does NOT include pneumatics.
Voltage

Part No.

120 V*
240 V*

N6520016
N6520017

* Service installation required.

152

Each ()
1970

Each ()
96
202
48
57
124
536

Injectors
Packed Column Injector
Miscellaneous Accessories
Injector/Detector Adapter 1/4 in.
Adapter fits on injector and detector
outlet (inside oven) for use with
1/4 in. columns.

Part No.
00080100

Liner Removal Tool


Part No.

Allows easy removal of glass


liners from injector port.

N6100102

Quartz Wool

Part No.
N6102354

Silanized Glass Wool

Part No.

Packing for wide-bore glass liners.


(2 oz.)

03300905

172

Each ()
125

Each ()
26

Injectors

Quartz wool (untreated) for


packing glass liners. (5 g.)

Each ()

Each ()
34

Silanized Glass Wool


Part No. 03300905

Wide-Bore Adapter Kit


0.53 Capillary Column Adapter Kit
The AutoSystem Wide-Bore Adapter Kit allows conversion
of the packed inlet for 0.53 mm capillary column operation.
The kit includes 0-20 mL flow control element, wide-bore
adapter with 1/16 in. fitting, wide-bore glass liner, and
column support hanger. Can be used in both on-column
and off-column modes of operation.
Part No.
Each ()
N6120001

523

Gas Chromatography

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

153

Injectors
POC Injector
POC Replacement Parts

1
2
3
4
5

Programmed-Temperature
On-Column Injector System

Components

Part No.

Septum Cap
Septa (pkg. 50)**
Needle Guide
Liner/Hour Glass
Body Assembly

N6100153
N6621028
N6101702
N6101703
N6100256

** For more septa see page 159.

Each ()
96
202
66
37
555

The Programmed-Temperature On-Column (POC) Inlet is


designed to be used with fused-silica capillary columns.
The sample is injected onto the column while the inlet is
cool.After the injection, the inlet begins to heat. This delay
in heating avoids the flash vaporization associated with a
normal injection. This explosive vaporization can cause
thermal breakdown and/or discrimination of certain
analytes, which can be avoided by using the POC.
The POC Injector is best used to achieve recovery of compounds
of greater than C60 (e.g., polywaxes). The POC utilizes flow
control, producing the best recovery out to C100 or greater.

Injectors

POC Injector with Manual Flow Controller


and Head Pressure Gauge
2

Kit includes all necessary hardware to install injector into


AutoSystem Series or Clarus Series.
Voltage
120 V*
240 V*

Part No.
N6120076
N6120077

Each ()
2436

POC Injector with Manual Flow Controller and Head


Pressure Gauge with Flow Readout on Screen

Kit includes all necessary hardware to install injector into


AutoSystem Series or Clarus Series.

Voltage
120 V*
240 V*

Part No.
N6120082
N6120083

Each ()
3354

POC Injector with PPC Add-On Kit


Kit includes injector with programmable pneumatic control,
heater, sensor, and heater block. The AutoSystem XL or Clarus
GC must be PPCTM ready. If not, a PPC upgrade kit (N6120146)
is required. (See page 166 for more information.) Installation
by PerkinElmer Service is required, but not included.
Voltage
120 V*
240 V*

Part No.
N6120142
N6120143

Each ()
3219

Gas Chromatography

POC Injector Starter Kit


Includes: needle guides (5), universal connectors (5),
0.53 mm i.d. deactivated fused silica (5 m), 1/16 in.
stainless steel nuts (5), 0.8 mm graphite ferrules (10),
Thermogreen septa (50),
Part No.
Each ()
and wafer scribes (10).
N6120098
* Service installation suggested. AutoSystem firmware revision 1.7
or higher. Operators manual (09938559) revision F or greater.

154

625

Injectors
PSS Injector
PSS Replacement Parts

Programmed-Temperature
Split/Splitless Injector System
PSS Injector Add-On Kits with Manual Pneumatics
The programmed-temperature split/splitless (PSS) inlet
allows accurate sample delivery to a capillary column.
The PSS allows the analysis of thermally labile compounds,
while eliminating the discrimination of high-boiling
compounds. One of the major advantages of the PSS is
that any nonvolatile material will remain in the inlet
liner and not on the front of the column.

1
2
3
4
5
6
7

PSS with pneumatics and pressure readout on screen. Kit


includes all necessary hardware to install injector into GC.
Part No.

120 V* AutoSystem
240 V* AutoSystem
120 V* Clarus
230 V* Clarus

N6120074
N6120075
N6520014
N6520015

Each ()
4795
2076

PSS Injector with PPC


Kit includes injector with programmable pneumatic control,
heater, sensor, and heater block. The GC must be PPC
ready. If not, a PPC upgrade kit (N6120146) is required.
(See page 166 for more information.)
Voltage

Part No.

120 V*
240 V*

N6120140
N6120141

9
10
11
12
13
14

Part No.

Each ()

Septum Cap
Injector Cover
Septa** (pkg. 50)
Trap, Charcoal non PPC version
PPC version (not shown)
Nut
Septum Purge
O-Ring Viton (pkg. 10) max. temp
250 C, recommended for use with
mass spec. Shipped with instrument.
O-Ring KALREZ (pkg. 1)
max. temp. 450 C
O-Ring Graphite (pkg. 5)
max. temp. 450 C
Quartz Liner, 2 mm Split Mode
Shipped with instrument.
Quartz Liner, 1 mm Splitless Mode
On-column liner
Body Assembly
Ferrule 1/8 in. x 1/16 in. (pkg. 10)
Nut 1/8 in.
Split Vent Line
Purge Restrictor
Nut

N6100153
N6101482
N6621028
N6100275
N6100331
N6101715
N6100260
N6101747

96
21
202
242
553
179
548
11

09921004

33

N6101751

23

N6121004

17

N6121006
N6101539
N6100261
09920301
09903128
N6100159
N6101034
09903392

108
47
765
84
1
42
55
27

Injectors

Voltage

Description

** For more septa see page 159.

Each ()

3326
2

PSS Injector Starter Kit


Includes: universal connectors (5), 0.53 mm i.d. deactivated
fused-silica (5 m), 2 mm i.d. quartz liner, 1 mm i.d. quartz
liner, glass hourglass liner, 1/16 in. stainless steel nuts (5),
0.5 mm i.d. graphite ferrules (10), 0.8 mm i.d. graphite
ferrules (10), Viton O-Rings (6), graphite O-Rings (5),
untreated quartz wool, wafer scribes
Part No.
Each ()
(10), and Thermogreen septa (50).
N6120102

11

10
4

12
5

956
6

13

Zero Dilution Liners

Description

Part No.

Inner Liner
Outer Liner

N1011446
N1011447

Each ()

Gas Chromatography

Used together as set.


8

41
90

* Service installation suggested.


9

Manual Pneumatic Control (non-PPC)

14

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

155

Injectors
PreVent
PreVent

Enhanced Large Volume Injection


Allows the use of chlorinated solvents with
an electron capture detector.

Isolation Mode
Eliminates downtime during routine injector
maintenance. Can provide approximately 100 extra
analytical hours of productivity per system per year.
ELVI Mode
Facilitates manual injection volumes up to 150 L
and automatic injection volumes up to 50 L
without solvent reaching the column or detector.

2 l of 20 pg/l Pesticide Solution in n-Hexane

Time-Saver Mode
Prevents unwanted, high molecular weight material
from reaching the detector. Shortens analysis time,
facilitates isothermal chromatography and protects
the detector from contamination.
ProTect Mode
Eliminates contamination by preventing heavy
components in the sample from reaching the
expensive and retentive chromatographic column.
Allows backflushing during chromatographic run.

Injectors

50 l of 20 pg/l Solution in Methylene Chloride

PreVent Time-Saver Mode

PreVent Add-On Kit

Conventional
C5
100 C4 C6
0
Analyze
Cleanup
Equilibrate

10

30

50

70

PreVent

Kit includes all necessary hardware to add PreVent capability


to an existing PSS injector with PPC or to a capillary
injector with PPC. Includes restrictor
Part No.
Each ()
and mid-point PPC module.
N6120144

PreVent Hourglass Guide

100

Part No.
N6103082

10

30

50

Analyze
Cleanup
Equilibrate

70

2093
Each ()
63

PreVent Restrictor
Description

Part No.

0.06 mm i.d., 108 mm Length


0.06 to 0.25 mm i.d., 104 mm Length

N6103080
N6100342

PreVent Spacer

Part No.
N6103079

Three Successive Injections of Diesel Oil

Each ()
23
7
Each ()
103

ProTect Add-On Kit


Includes all the necessary parts to add
a ProTect accessory to a Clarus GC.
Includes one ProTect column.

Part No.

ProTect Replacement Column

Part No.

N6120163

Each ()
650

Gas Chromatography

Normal Injection

N6103196

Each ()
254

Septum changed and liner inspected during run

MSVent Add-On Kit for the Clarus 500 GC/MS


Includes all the necessary parts to
add an MSVent accessory to a
Clarus GC/MS.*

Part No.
N6120179

Normal Injection

* Requires a PreVent option (N6120144) to be already installed


in the Clarus 500 GC gas chromatograph.

156

Each ()
714

Injector Supplies
Injector Liners
Glass Inlet Liners
Inlet liners for split injection have mixing chambers with tortuous flow paths to allow full vaporization of the sample.
Deactivating the surface of these liners prevents active compounds from degrading. Packing the liner with wool will trap
non-volatile residue and prevent column contamination when analyzing dirty samples.
Inlet liners for splitless injection are generally designed as straight tubes, although new designs such as the gooseneck will
help contain the sample in the injector. Packing these liners with wool will also help trap non-volatile residue and prevent
column contamination.

Capillary Split/Splitless Injector Liners


ID
mm

Length
mm

Pk
Size Part No.

86.2

N6502001

251

6.2

92.1

N6121020

236

92.1

N6502009

131

92.1

N6502010

203

92.1

N6502011

267

92.1

N6502012

254

6.2

92.1

N6121022

331

6.2

92.1

N6502006

164

6.2

92.1

N6121002

22

6.2

92.1

N6101372

31

6.2

92.1

N6121021

109

6.2

92.1

N6502004

177

6.2

92.1

N6121001

34

6.2

92.1

N6101052

29

6.2

92.1

N6502003

134

6.2

92.1

N6502005

246

6.3

90

N1011445

74

6.3

90

N1011446

41

Each ()

Column installs at
left side of image.

Gas Chromatography

NEW! PSS Splitless Glass Liner Siltek Deactivated Surface Liner (with wool)
2
General purpose use, ideal for chlorinated pesticides analyses
Split Glass Liner Siltek Deactivated Surface Liner (with wool) Universal liner for general 4
purpose analyses. Surface provides inertness over a wide sample pH range. Wool can
be adsorptive if fibers are broken
NEW! Split Glass Liner (with wool)
4
Universal liner for general purpose analyses
NEW! Split Siltek Deactivated Glass Liner (with wool) Universal liner for general purpose 4
analyses. Deactivated surface provides minimal bleed and inertness over a wide
sample pH range
NEW! Clarus Cup Split Glass Liner Good for both high and low molecular weight
4
compounds. Sample vaporization is aided by tortuous flow path and minimizes
molecular weight discrimination. Difficult to clean
NEW! Clarus Cyclosplitter Glass Liner Patented cylindrical design for dirty samples,
4
easy to clean and allows many injections before cleaning is required. Not recommended
for large volume injections
Uniliner Deactivated Glass Liner (with wool)
4
Universal liner for general purpose analyses
NEW! Clarus Splitless Glass Liner Low volume sample analyses, beneficial with
1
headspace and purge/trap
Quartz Liner for Splitless Operation (ships with instrument)
2
Standard injector liner
Glass Liner for Splitless Operation
2
Universal liner for general purpose analyses
Deactivated Glass Liner for Splitless Operation (with wool)
2
Good for analyses of trace samples
NEW! Siltek Deactivated Liner (with wool) for Splitless Operation Optimum sample
2
dispertion for active samples. Surface provides inertness over a wide sample pH range.
Wool can be adsorptive if fibers are broken
Quartz Liner for Split Operation
4
Good for large volume injection samples
Glass Liner for Split Operation
4
Universal liner for general purpose analyses
NEW! Siltek Deactivated Double Gooseneck Glass Liner (with wool) Optimum sample
4
dispertion for active samples. Decreases breakdown of active compounds such as
endrin and DDT. Chamber contains sample vaporization cloud. Not suitable for PPC systems
NEW! Cyclo Double Gooseneck Liner for Split Operation Cylindrical design for large
4
volume and trace dirty samples. Decreases injection port discrimination. Cannot be
packed with wool and more difficult to clean
Zero Dilution Glass Outer Liner Ideal for trace HS work.
2
Use in conjunction with N1011446
Zero Dilution Glass Inner Liner Ideal for trace HS work.
2
Use in conjunction with N1011445

OD
mm

Injector Supplies

Description

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

157

Injector Supplies
Injector Liners
Programmed Temperature Split/Splitless (PSS) Injector Liners
Column installs at
left side of image.

ID
mm

OD
mm

Length
mm

Pk
Size

Part No.

86.2

N6121006

108

86.2

N6502000

343

86.2

N6121004

17

86.2

N6502001

251

86.2

N6502002

216

2.8

83

N1011447

90

73

N1011446

41

2.4
2.4

4
4

86.2
19.05

1
1

N6101539
N6101703

47
37

ID
mm

OD
mm

Length
mm

Pk
Size

Part No.

Drilled Uniliner (hole on top) Excellent liner for high sample


recovery and linearity, recommended for aqueous injections.
Good for PPC equipped GCs

6.2

92.1

N6121022

331

NEW! Drilled Uniliner (hole on bottom) Recommended for analysis


in which compounds of interest could be affected by a tailing
solvent peak. Good for PPC equipped GCs
NEW! Gooseneck Drilled Uniliner (hole on top) Use for trace, active
samples, high recovery and linearity
NEW! Gooseneck Drilled Uniliner (hole on bottom) Use for trace,
active samples, high recovery and linearity
NEW! Open Top Uniliner (with wool) Packed with fused silica wool,
highly recommended for high molecular weight active samples.
The fused silica wool traps dirt and sample residue
NEW! Cyclo Uniliner Cylindrical design for high molecular weight
samples provides an excellent vaporization surface. Spiral traps
dirt reducing further residue sample interaction
Wide-Bore Column Glass Liner
Wide-Bore Column On/Off Quartz Liner

6.2

92.1

N6502013

471

6.2

92.1

N6502014

407

6.2

92.1

N6502015

407

6.2

92.1

N6502016

241

6.2

92.1

N6502017

305

6
6

4
4

92.1
92.1

1
1

N6101375
N6121003

29
32

Description

Injector Supplies

Quartz Liner for Splitless operation (ships with instrument)


Excellent liner for low volume analyses
NEW! Siltek Deactivated Glass PSS Liner
Used for low volume trace sample analyses
Quartz Liner for Split operation (ships with instrument)
Approved PerkinElmer standard injector liner
NEW! Siltek Deactivated Glass Liner for Split operation
(with wool) Maximum inertness and packed with wool gives
optimum sample dispersion. Surface provides inertness over wide
sample pH range. Wool can be adsorptive if fibers are broken
NEW! Siltek Deactivated Glass Liner for Split operation Max.
inertness gives optimum sample dispersion. Deactivated surface
provides minimal bleed and inertness over a wide sample pH range
Zero Dilution Outer Liner
Use in conjunction with N1011446
Zero Dilution Inner Liner
Use in conjunction with N1011447
On-column Glass Liner
Liner/Hour Glass for POC Injector

Each ()

Packed Column Injector Liners

Gas Chromatography

Column installs at
left side of image.

158

Description

Each ()

Injector Supplies
Injector Septa
Merlin MicroSeal
Merlin MicroSeal Septum Cut-Away View

Merlin MicroSeal Adapter Kit

Septum nut aligns needle

Syringe needle
Increase lifetime with over 2000 injections
2 Step sealing system

Syringe needle wiper

Temperature ranges up to 325 C

O-rings seal needle


during injection

Pressure ranges 40 to 100 psi


Low bleed, long life alternative for injector port septa

Injector Supplies

Microseal septum

Quick and easy installation


The Merlin MicroSeal Septa is a unique replacement
septa employing a two-step sealing system and an advanced
elastomer material. Because the syringe needle does not
pierce the septa, there is no debris and ghost peaks are
greatly reduced. The MicroSeal Septa also reduces the
incidence of bent syringe needles and liner contamination.
Usable in either manual or autosampler applications, this
septa can improve your productivity and run reliability.
Designed to be used with 23 gauge straight needle syringes.
Pressure ranges from 4 to 100 psi and injection port
temperatures up to 325 C. Easy installation on most
PerkinElmer chromatographs.

Duckbill opens easily, seals reliably

Spring
Septum cup

BTOTM (Bleed Temperature Optimized) Injector Septa


Maximum recommended operating temperature 300 C.
Low bleed, high temperature. 11 mm diameter.

Merlin MicroSeal Nut

Merlin MicroSeal
Adaptor

Merlin MicroSeal
Septum

High Pressure Merlin MicroSeal Kit:

Description

Part No.

Package of 50

N9302972

Each ()
103

Thermogreen Injector Septa


Maximum recommended operating temperature 350 C.
Low bleed, high temperature. 11 mm diameter.

Part No.

Includes: 2 Merlin MicroSeal septa,


1 nut, and 1 injection port adapter.

N9303344

Merlin MicroSeal Septum

Part No.

Merlin MicroSeal Septa. (pkg 1)

N9303345

Each ()
434

Description

Part No.

Package of 50

N6621028

Each ()
202

Low Bleed Injector Septa


Each ()
181

Description

Part No.

Package of 50

N9303343

Each ()
81

PTFE-Silicone Injector Septa

Silicone Injector Septa

Maximum recommended operating temperature 300 C.


11 mm diameter.

Maximum recommended operating temperature 250 C.


11 mm diameter.

Description

Part No.

Package of 12
Package of 50

00091357
00090652

Each ()
14
58

Description

Part No.

Package of 50

54019985

Gas Chromatography

Septa for Use with All Injectors

Maximum recommended operating temperature 320 C.


11 mm diameter.

Each ()
36

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

159

Injector Supplies
Subambient Accessories
PerkinElmer offers subambient systems which are
microprocessor controlled. This control allows precise
injection of coolant for the greatest accuracy. Our design
assures you of minimum thermal gradients, thereby
eliminating the peak splitting often found in
other systems.
NOTE: All of the subambient systems require, but do not include,
PerkinElmer Service installation.

Subambient Accessories
Liquid Carbon Dioxide (CO2) Subambient Accessory
Contains all the necessary hardware to add subambient
capability to AutoSystem XL or Clarus GC. Operating
temperature range down to -50 C.
Part No.
Each ()
Installation by PerkinElmer Service
is required, but not included.
N6120159
1231

Pressure Ratings

Injector Supplies

LN2 20 30 psi
CO2 50 70 psi

Liquid Nitrogen (LN2) Subambient Accessory

AutoSystem
Subambient Accessories
Liquid Carbon Dioxide (CO2) Subambient Accessory
Contains all of the necessary hardware to add subambient
capability. Capable of operating down to -50 C. Installation
by PerkinElmer Service is required, but not included.
Part No.

Each ()

N6120017

1977

Liquid Nitrogen (LN2) Subambient Accessory


Contains all of the necessary hardware to add subambient
capability. Capable of operating down to -99 C. Installation
by PerkinElmer Service is required, but not included.
Part No.

Each ()

N6120016

1671

Liquid Nitrogen (LN2) Subambient Accessory


for Temperature Programmable Injectors
Contains all of the necessary hardware to add subambient
capability to two temperature programmable injectors
(PSS/Program Split Splitless, POC/Program On-Column)
on one Gas Chromatograph. Capable of operation down to
-99 C. Requires but does not include oven LN2 subambient.
Installation by PerkinElmer Service
Part No.
Each ()
is required, but not included.

Gas Chromatography

N6120078

160

727

Contains all the necessary hardware to add subambient


capability to AutoSystem XL or Clarus GC. Operating
temperature range down to -99 C.
Part No.
Each ()
Installation by PerkinElmer Service
is required, but not included.
N6120158
1352

Injector Supplies
Syringes
Autosampler Syringes

Volume/o.d.

Low injection volume analysis.


Plunger type: metal plunger in needle.

0.5 L/0.63

N6101252

210

Routine analysis. Shipped with instrument.

5 L/0.63

N6101390

110

0.53 capillary column on-column injection.


Plunger type: metal plunger in barrel.

5 L/0.47

N6101380

113

Low injection volume. 0.53 capillary on-column injection.


Plunger type: metal plunger in needle.

5 L/0.47

N6101253

210

Routine analysis, plunger type: metal plunger in barrel.

5 L/0.63

N6101251

110

Metal plunger in barrel type

50 L/0.47
50 L/0.63

N9302799
N6101760

223
200

Each ()

Replacement
Needle
Part No.
Each ()
N6101469

74

N6101470

74

Injector Supplies

Description

Syringe
Part No.

Plunger metal plunger in barrel with Teflon-tipped seal.

Needle Syringes
Why a 7 cm Needle?

Fixed Needle Syringes

All PerkinElmer injectors have been tested and optimized


for use with a 7 cm needle. A 7 cm needle is critical to be
sure your sample is deposited in the optimal zone.

Syringe
Capacity

P.S. #2
Part No.

Point Style 2

10 L
10 L*
25 L
50 L
100 L

00230113
00230523
N9302202
N9302203
N9302204

General-purpose point style designed for septum penetration


in all chromatographic techniques. The needle has a 22
bevel with the tip slightly bent to minimize coring and
needle plugging.

Each ()
47
47
52
61
61

P.S. #3
Part No.

Each ()

09904823
09904941
09904822

52
60
62

Fixed Needle Syringe Six Pack


Contains six syringes (10 L, fixed
needle, point style #2, 00230523).
Fitted with 7 cm needle.

Part No.
N9302230

Each ()
236

Removable Needle Syringes (RN)


Point Style 3

P.S. #2
Part No.

10 L*
25 L
50 L
100 L
250 L
500 L

N9302210
N9302211
N9302212
N9302213
N9302214
N9302215

Each ()
71
78
83
94
110
123

Gas Chromatography

Needle has a 90 bevel. Point style 3 is recommended


when the syringe is used for accurate pipetting of liquids.
Excellent for mixing standards of very small volume.

Syringe
Capacity

* Standard syringe but fitted with 7 cm needle for PerkinElmer injectors.

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

161

Injector Supplies
Syringes

Injector Supplies

Replacement Needles
for Removable Needle Syringes (RN)

Ultramicro Volume Syringes

Syringe
Capacity

Gauge

Length

Qty.

P.S. #2
Part No.

10 L**
10 L
25 L
50 L
100 L

26S
26S
22S
22S
22S

7 cm
2 in.
2 in.
2 in.
2 in.

pkg. 3
pkg. 3
pkg. 3
pkg. 3
pkg. 3

N9302220
N9302222
N9302224
N9302224
N9302226

Each ()
35
35
35
35
35

Replacement Needles for RN Syringes


Needle Gauge

Volume

Part No.

26S
22S
22S

10 L
25, 50, 100 L
250 L

N9302222
N9302224
N9302226

Each ()

Recommended for liquid sample injections of less than


5 L for gas chromatography. Syringes come standard with
needle length of 7 cm optimum for PerkinElmer injectors.
Syringe
Capacity

Needle
Gauge

Syringe
Part No.

0.5 L
1.0 L
1.0 L
2.0 L
2.0 L
5.0 L

25
26*
22
25
23
24

N9302231
00230111
00230177
N9302235
N9302237
00230178

* Recommended for PerkinElmer Wide-Bore Capillary Adapter.


35
35
35

P.S. = Point Style


** Recommended for PerkinElmer injectors.

Syringes Gas Tight


Syringe
Capacity

Fixed
Needle (N)
Part No.
Each ()

Removable
Needle (RN)
Part No.
Each ()

10 L
25 L
50 L
100 L
250 L
500 L
1.0 mL
2.5 mL
5.0 mL
10 mL

N9302240
N9302242
N9302244
N9302247
N9302250
N9302253
N9302256
N9302259
N9302262
N9302265

N9302241
N9302243
N9302245

83
75
94

N9302251
N9302254
N9302257

94
94
111

N9302266

140

61
59
71
75
78
78
99
75
94
120

Gas Chromatography

10 mL Gas Tight Syringe Part No. N9302266

162

Each ()
134
106
106
123
143
123

Laboratory Supplies
Gas Sampling Supplies
Filters and Traps
Carrier Gas Filter for GC/MS

Part No.

21 in. long with 1/8 in. fitting.

N6471025

Each ()
293

Gas In-line Filter

Description

Part No.

Base-Mount Filter
In-line Gas Filter
Packing Refill Kit (sufficient for two refills)

N9301177
N9301178
N9301176

Each ()
299
200
29

Hydrocarbon Trap
Use our activated charcoal
in-line trap to remove
gaseous hydrocarbons
from carrier gas supply.
This trap will remove all hydrocarbons at room temperature
except methane. Essential for purge- and-trap systems, or
high-sensitivity FID operation when contamination is a
problem. Maximum pressure 1000 psig. Frits at the end
prevent any particles from entering the gas stream. Trap is
purged with nitrogen and should be purged with the gas you
plan to use. Approximate dimensions:
Part No.
Each ()
2 x 14 in. with 1/8 in. fittings.
N9301192

High efficiency oxygen


trap has a capacity of 2.5
liters at room temperature.
It is also effective for removing sulfur compounds such as
hydrogen sulfide and mercaptans. This oxygen trap is for use
with nonoxidizing gases such as; He, Ar, N2, and CH4. Oxygen
removal to below 70 ppb using normal GC flow rates. The
catalyst is a copper-based material that forms copper oxide
in the presence of oxygen; no gas is produced from this
reaction. This trap is intended for use with gases containing
less than 1% oxygen. The trap is delivered active purged
with nitrogen. (Purging with the gas you will be using is
recommended.) Maximum pressure 1000 psig. Approximate
dimensions: 2 x 14 in. including
Part No.
Each ()
fitting end; fittings are 1/8 in.
N9301179

Laboratory Supplies

This in-line filter


removes moisture,
oil, and particulate
from gas supplies. Large capacity filter requires fewer filter
changes, and improves baseline stability and chromatographic
results. Free-standing model also available. Maximum
pressure 100 psig. Trap packing can be refilled. Approximate
dimensions: 2 1/4 x 17 in. with 1/8 in. fittings.

Oxygen Trap

262

Safe Glass Moisture Trap


In-line moisture trap.
Drierite indicating agent
and Molecular Sieve 5A
are packed in glass which is enclosed in a safety plastic tube
in the event the glass breaks. Unique loading design allows
operation in any orientation without channeling. For use with
pressures up to 100 psig. Designed for use with GC detectors
that require high-purity gases. Recommended for ELCD and
ECD systems in which moisture and contamination are a
problem. Trap is shipped active and purged with nitrogen.
It is recommended that you purge the trap with the gas you
plan to use. Approximate dimensions:
Part No.
Each ()
1 3/8 x 10 1/4 in. with 1/8 in. end fittings.
N9301193

147

159

Recommended Filters

Indicating Oxygen Trap

Indicating Oxygen Filter

Detector Carrier Gas

H2

Air

ECD

Moisture Trap
and Oxygen Trap

ELCD

Hydrocarbon Trap*

Hydrocarbon Trap

FID

Hydrocarbon Trap*

Moisture Trap

Moisture Trap

FPD

Hydrocarbon Trap*

Moisture Trap

Moisture Trap

MS

Indicating Oxygen Trap

NPD

Hydrocarbon Trap*

Moisture Trap

Moisture Trap

PID

Hydrocarbon Trap*

TCD

Hydrocarbon Trap*

Gas Chromatography

Indicating trap has a


capacity of 40 cc of
pure oxygen. The trap
has a maximum pressure of 100 psig. The trap is shipped in
the active state purged with hydrogen. It is recommended
that you purge the trap with the gas you will be using.
Approximate dimensions: 1 3/8 x 10 1/4 in. Includes
1/8 in. fittings. It is recommended that
Part No.
Each ()
the indicating trap be used downstream
of the high-capacity oxygen trap.
N9301191
159

* Oxygen Trap if capillary columns are used.


Gas Flow

High-Capacity
Oxygen Filter

Indicating
Packing

Gas Flow
Note: All gases MUST have a minimum purity of 99.995%.
Gases for either ELCD or mass spectrometer MUST have a
minimum purity of 99.999%.

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

163

Laboratory Supplies
Gas Sampling Supplies

Laboratory Supplies

Gas Purification Systems

Three-Cartridge Gas Purification System


All-In-One Gas Purification System
The trace contaminant removal available from the
three-cartridge Gas Purification System is now available
in a single-cartridge system. The purifier consists of a
manifold head and an all-welded steel cartridge with a
multiple-layer adsorbent bed to sequentially remove
water, oxygen, sulfur compounds, and hydrocarbons.
The All-In-One Gas Purification System has a capacity for
oxygen of at least 450 cc, enough to purify eight 292 cu. ft.
tanks of 99.995% pure helium. Water capacity is at least
1.7 g, while capacity for hydrocarbons (as n-butane) is
5.2 g. The system comes ready to wall mount, but may be
bench-mounted by removing from the bracket and attaching
to a bench-mount base (included). It is shipped fully
activated and filled with high-purity helium.
Product

Part No.

Gas Purification System with Trap, 1.8 in. Fittings N9306050


Replacement Cartridge
N9306051

345
206

Gas Chromatography

Including hardware to hook up three gas supplies to gas


chromatograph. Kit includes: (1) safety gas flow restrictor
for hydrogen (00090038), (1) restrictor warning tag
(00091216), (1) restrictor tag (00091360), (50 ft.) 1/8 in.
refrigeration grade copper tubing (N9300077), (6) 1/8 in.
Swagelok nut (09903128), (6) 1/8 in. brass front ferrules
(09903129), (6) 1/8 in. brass rear ferrules (09903130),
(3) 1/8 in. Swagelok brass 3-way tee (09903170), (3) 1/4 in.
NPT x 1/8 in. Swagelok adapter (09903795), and (1) 1/4 in.
NPT x 1/8 in. NPT reducer female (09903212).

N6500123

164

Cartridges are easy to replace


High capacity
Wall bracket gets the system up and out of the way

Each ()

Gas Supply Installation Kit

Part No.

This system will provide in-line contaminant removal for


your GC gases. This system has convenient replaceable
cartridges with a visual indicator. The PerkinElmer Gas
system consists of three cartridges in series to reduce
column damaging impurities. The first cartridge in the
system will remove residual hydrocarbons and water from
the carrier gas stream. The second cartridge provides
high-capacity oxygen removal (capacity is at least 1000 cc
of pure oxygen); the third cartridge contains an inorganic
indicator that changes from light green to gray to provide
warning when the high-capacity oxygen trap is depleted.
All systems are helium leak tested after assembly.
Approximate dimensions: 33 cm W x 33 cm H x 8 cm D;
weight 4 kg.

Each ()
211

Product

Part No.

Each ()

Gas Purification System, 1/8 in. fittings


complete system (includes all three traps)
Hydrocarbon Moisture Replacement Cartridge
High Capacity Oxygen Replacement Cartridge
Indicating Oxygen Replacement Cartridge
Replacement Cartridge Set, one each
hydrocarbon/moisture, high-capacity oxygen
and indicating oxygen
Bypass Accessory, allows operation of system
when installed in place of cartridge
Bench Mount Adapter

N9306002

689

N9306003
N9306004
N9306005
N9306048

185
204
182
573

N9306006

75

N9306014

48

Laboratory Supplies
Gas Sampling Supplies
High Purity Brass Regulators
Barstock body construction

PerkinElmer regulators are constructed of high-purity


brass barstock and have stainless steel diaphragms and
metal-to-metal seals. They are suitable for use with
high-purity (>99.995% pure) non-corrosive gases.
Regulators terminate in a 1/4 in. NPT Swagelok fitting.

Stainless steel diaphragms


Metal-to-metal seals
Use with high-purity carrier gas

Laboratory Supplies

High-purity Brass Regulators (Dual Stage)


CGA
Fitting

Delivery
Pressure Use

Delivery
Pressure
Range (psig)

Cylinder
Pressure
Gauge (psig)

Gauge
(psig)

Part No.

CGA-350

H2 and Ar/CH4 mixes

4-100

0-250

0-3000

09907128

763

CGA-580

He, Ar

4-100

0-250

0-3000

09907127

763

Each ()
High-Purity Brass Regulator Part No. 09907128

High-purity Brass Regulators (Single Stage)

Safety Straps

CGA
Fitting

Delivery
Pressure Use

Delivery
Pressure
Range (psig)

Cylinder
Pressure
Gauge (psig)

Gauge
(psig)

Part No.

CGA-350

H2 and Ar/CH4 mixes

3-80

0-100

0-3000

00230091

381

CGA-580

He, Ar

10-180

0-250

0-3000

00230253

381

CGA-590*

Air

5-180

0-250

0-3000

00230090

381

Each ()

Nylon adjustable cylinder safety


straps hold tanks securely to
bench top or wall.
Model/Component

Part No.

Wall Mount
Bench Mount

N9301298
N9301299

Each ()
101
101

* Supplied with 590-580 Adapter.

PG-H2 Pure Gas Hydrogen Generators


The PG-H2 series Hydrogen Generators employ the newest
membrane technology available for the safe production
of pure hydrogen gas.
The patented DBS PG-H2 series of Hydrogen Pure Gas
Generators is ideal for operation with gas analyzers, as fuel
gas for flame tools, or as a source of pure hydrogen. Electrolytic
membrane technology is preferred over alternative hydrogen
generating techniques because it is clean, requires less
maintenance, and there is no need to store chemicals
to maintain operation. Only pure water, either distilled
or deionized, is required to provide trouble-free,
long-term operation.
Features and Benefits:
LCD display shows set points, operating conditions and status
Visual operating status lights

Gas Chromatography

Continuous or intermittent operation

PG-H2 Series
Hydrogen Generator

Alarm conditions
Flow indicator informs the operator at a glance that hydrogen
gas is flowing at the specified rate

Model/Component

Part No.

Bi-directional RS232 interface

Deionizer Bag
Desiccant Cartridge, Fitting, and Refill Kit
Desiccant Refill (pkg. 3)
PG-H2 100 Hydrogen Generator 100 mL/min.
PG-H2 160 Hydrogen Generator 160 mL/min.
PG-H2 250 Hydrogen Generator 250 mL/min.
PG-H2 500 Hydrogen Generator 500 mL/min.

N9306066
N9306064
N9306065
N9306058
N9306059
N9306060
N9306061

Selectable auto start


Remote control (optional)
Cascading of 2 or more units (optional)
PC-Control capability

Each ()
75
279
101
4322
5200
6000
8000

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

165

Laboratory Supplies
Instrument Pneumatics Accessories
PPC Upgrade Kit

Manual Pneumatics
0-20 mL/min. Flow Accessory
For use when converting a flow
controller for low flow applications.

Part No.

Each ()

N6101377

261

Kit includes the main control board and hardware to add


PPC capability to an existing AutoSystem XL or Clarus Gas
Chromatograph. Installation by PerkinElmer Service is
required, but not included.
Part No.
Each ()
N6120146

Laboratory Supplies

Auxiliary Gas Pneumatics Box


For use with carrier or combustion gas. 0-100 psig gauge.
This compact unit comes in either wall or bench mount,
with or without toggle valve for quick shutoff. Design
allows several units to be installed together. 1/8 in.
Swagelok fittings for gas inlet/outlet. Mounting screws
included. Dimensions: 15 x 2 x 7 in. (D x W x H).
Description

Part No.

With Toggle Valve


Without Toggle Valve

N9302146
N9302145

1354

Preset Pressure Regulator


Consists of a preset (30 psig) nonadjustable pressure regulator
for use with manual detector gas controls. Recommended for
use on hydrogen and air for FID.
Part No.
Each ()

Each ()

N6101473

249

784
746

Pressure Regulator with Screen Readout


Flow Controller and Gauge with Screen Readout
Includes: flow controller, gauge, and
transducer for mounting into an
empty instrument pneumatic panel.

Part No.
N6120004

Each ()

Includes pressure regulator (0-60 psig)


and transducer for mounting into an
empty instrument panel.

Part No.
N6120005

Each ()
434

670

PPC Frits
PPC Detector Control Pneumatics Add-On Kit
Kit includes parts to add one channel of PPC control for
detector gas to an existing detector. For use with hydrogen
or air on FID, NPD, and FPD; makeup on ECD and PID. The
GC must be PPC ready. If not, a PPC upgrade kit (N6120146)
is required. Requires, but does not include, appropriate
PPC frit (see table).
Note: Do not use for ELCD or TCD makeup. These require special kits with
tees. The AutoSystem XL must be PPC ready. If not, a PPC upgrade kit
(N6120146) is required. Installation by PerkinElmer Service is required,
but not included.
Part No.
Each ()
N6120148

1192

PPC Flow Control Pneumatics Add-On Kit


for Packed or POC Injector

Gas Chromatography

Kit includes parts to add PPC flow control for carrier gas
to an existing packed or POC injector. Requires but does
not include appropriate PPC frit (see table). The GC must
be PPC ready. If not, a PPC upgrade kit (N6120146) is
required. Installation by PerkinElmer Service is required,
but not included.
Part No.
Each ()
N6120149

166

2130

Injector/
Detector
ECD

Gas

Frit No.

Argon/
4
Methane
or Nitrogen
FID
Air
6
FID
Hydrogen
4
FPD
Air
5
FPD
Hydrogen
4
NPD
Air
5
NPD
Hydrogen
1
Packed
Carrier
4
POC
Carrier
3
POC
Carrier Use
2
for Low Flows
(i.e., <3 mL/min.)
Split/Splitless Carrier
6
or PSS
TCD
Helium
4
TCD
Hydrogen
3

Color

Part No.

Each ()

Black

N6120155

84

Blue
Black
Green
Black
Green
Silver
Black
Yellow
Red

N6120157
N6120155
N6120156
N6120155
N6120156
N6120152
N6120155
N6120154
N6120153

84
84
84
84
84
84
84
84
84

Blue

N6120157

84

Black
Yellow

N6120155
N6120154

84
84

Laboratory Supplies
Maintenance Supplies
Flow Meters

Tools

Digital Flow Meter

Adjustable Wrench

The PerkinElmer Model 570 meets ISO 9000 and Good


Laboratory Practice (GLP) requirements. The flow meter
comes with a Certificate of Calibration that states all of
the traceability information needed for ISO-9000
compliance. The Model 570 is uniquely indentified by
serial number, internal instrument number, and date(s) of
calibration. It is also capable of periodic recalibration.

Adjustable 12 in. steel wrench for cylinder pressure


regulators. Wrench opens out to 1 3/4 in.
Part No.
Each ()
Fits all regulators listed in this catalog.

Part No.

Digital Flow Meter


Replacement Glass for Digital Flow Meter

N9302974
N9303429

Each ()
1016
80

Basic Tool Kit


Tools come in tool box for easy storage and use. Kit includes:
open-end wrench set (6 pc.), screwdriver set (6 pc.), adjustable
wrench (6 in.), chain nose pliers (narrow), wire cutters, and
wire strippers.
Part No.
Each ()
N9301327

PerkinElmer Electronic Flowmeter 1000


Flow range 0.1-1000 mL/min.

55

Laboratory Supplies

Product

N9301324

242

Deluxe Tool Kit

Operating Temperature 0 to 45 C
Traceable to NIST Primary Standard
Split Ratio Mode
Accuracy +/- -3%
LCD Alphanumeric Display
The PerkinElmer Flowmeter 1000 allows for rapid real-time
flow measurements. Flow rates measured in mL/min.
(volumetric flow). The PerkinElmer Flowmeter 1000 can
quickly calculate split ratios. Ratios are displayed in real
time. Flowmeter not compatible with corrosive or
flammable gases. Portable operation.
Part No.
Each ()
(9 V battery included).
N9307029

842

Soap Bubble Flow Meters


The glass soap bubble flow meters are calibrated in 1 and
10 mL two-stage or 1, 10, and 100 mL three-stage for easy
flow reading. Bubble meters come complete with liquid
soap, rubber squeeze bulb, miscellaneous-sized plastic tube
pieces to adapt to various fittings, and instructions (stand
required, but not included N9303314).
Part No.

Two-stage
Three-stage
Stand

00230522
N9300081
N9303314

Each ()
101
218
74

N9301328

306

6-Piece, Open-End Wrench Set


Six
1/4
3/8
1/2

sizes. Includes:
x 5/16 in. 5/16 x 3/8 in.
x 1/16 in. 7/16 x 1/2 in.
x 9/16 in. 9/16 x 5/8 in.

Part No.
N9301325

Each ()
69

Tubing
Description

Qty.

Part No.

Precleaned Copper Tubing


Teflon Tubing, 1/8 in. o.d.
Teflon Tubing, 1/16 in. o.d. Hall Solvent Lines
Tygon Tubing, 1/4 in. i.d., 3/8 in. o.d. for
Water and Air (not for carrier gas)

50 ft.
1 ft.
1 ft.
1 ft.

N9300077
02506483
09985708
02506518

Each ()

Gas Chromatography

Product

Great for use on all lab


instruments! Kit includes
the following tools: openend wrench set (6 pc.),
screwdriver set (6 pc.),
adjustable wrench (6 in.),
chain nose pliers (narrow),
wire cutters, wire strippers,
slip-joint pliers (6 in.), long
nose No. 5 stainless steel
tweezers (4 3/8 in.), needle file set (6 pc.), Allen key set
(11 pc. imperial sizes), and Allen key set (9 pc. metric sizes).
Shipped in a plastic tool box for
Part No.
Each ()
convenient storage.

120
3
7
3

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

167

Laboratory Supplies
Valves
Valves

Laboratory Supplies

There are two types of valves offered. Internal Volume


sample size is determined by an etched rotor inside the
valve. External Volume sample size is determined by a
sample loop outside the valve. External valves are used
primarily for sample injection and/or switching applications.
A valve used for just switching requires another valve
for sample injection. Valves include nuts and ferrules,
but not loops.
8-Port Valve
Part No. N9302819

3-Port Valve
Requires 90 actuator and standoff for automatic operation.

Rotation

Max.
Temp.

Max.
Pressure

Fitting (in.)

90

330 C

300 psi

1/16

Coating

Valve
Part No.

Each ()

N9302885

548

Replacement
Rotor
Part No.
Each ()

4-Port Valve
Requires 60 actuator and standoff for automatic operation.
90

175 C

400 psi

1/16

N9302809

721

90

350 C

300 psi

1/16

N9302813

740

90

330 C

300 psi

1/8

N9302817

568

6-Port Valve
Requires 60 actuator and standoff for automatic operation.
60

175 C

400 psi

1/16

N9302810

810

N9302897

107

60

350 C

300 psi

1/16

N9302814

823

N9302901

107

60

330 C

300 psi

1/8

N9302818

644

N9302905

107

8-Port Valve

Gas Chromatography

Requires 45 actuator and standoff for automatic operation.


45

175 C

400 psi

1/16

N9302811

899

45

350 C

300 psi

1/16

N9302815

905

45

330 C

300 psi

1/8

N9302819

740

899

N9302899

107

N9302903

107

10-Port Valve
Requires 36 actuator and standoff for automatic operation.
36

175 C

400 psi

1/16

N9302812

36

350 C

300 psi

1/16

N9302816

905

36

330 C

300 psi

1/8

N9302820*

765

* Special 4 1/8 in. standoff included.

168

Laboratory Supplies
Valves/Loops

4-Port Internal Valve and Rotor for Liquid Sample Injection


Replacement
Rotor
Part No.
Each ()

Fitting Size

Port Diameter

0.06

1/16 in.

0.016

N9302800

810

0.2

1/16 in.

0.016

N9302802

810

N9302889

107

0.5

1/16 in.

0.016

N9302803

810

N9302890

107

2.0

1/8 in.

0.030

N9302808

810

Each ()

Laboratory Supplies

Fixed Volume (L)

Valve
Part No.

Max. Temp. = 75 C, Max. Pressure = 500 psi, Fitting Size = 1/16 in.
These valves require a 90 actuator and standoff for automatic operation.

Sample Loops

4-Port Internal Valve and Rotor

Sample Loops
Volume

Size

6-Port
Part No.

100 L

1/16 in.

N9302851

29

100 L

1/8 in.

N9302860

29

250 L

1/16 in.

N9302852

29

250 L

1/8 in.

500 L

1/16 in.

N9302853

500 L

1/8 in.

N9302862

1 mL

1/16 in.

N9302950

48

1 mL

1/8 in.

2 mL

1/16 in.

N9302951

48

N9302957

48

2 mL

1/8 in.

N9302960

48

N9302966

29

5 mL

1/16 in.

N9302952

48

N9302958

48

5 mL

1/8 in.

N9302961

48

N9302967

30

Each ()

8-Port
Part No.
N9302854

Each ()

Each ()

N9302857

29

N9302866

29

N9302858

29

N9302867

29

29

N9302859

29

29

N9302868

29

N9302855

29

10-Port
Part No.

29

48

N9302956

48

N9302962

26

N9302965

28

N9302954

48

Gas Chromatography

N9302953

1/8 in. fitting loop for valves with 0.030 in. standard port diameter. 1/16 in. fitting loop for valves with 0.016 in. standard port diameter.

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

169

Laboratory Supplies
Valve Accessories
Adapters
Fused-Silica Adapters
These adapters allow connection of fused-silica to unions, valve ports, and reducers.

Laboratory Supplies

Description

i.d.

Colum i.d.

Fitting

Part No.

0.5 mm

0.18 mm - 0.35 mm

1/16 in.

N9302846

Each ()
49

0.6 - 0.8 mm

0.53 mm

1/16 in.

N9302847

49

Any

1/16 in.

N9302850

0.5 mm

0.18 mm - 0.35 mm

1/16 in.

N9302848

28

0.6 - 0.8 mm

0.53 mm

1/16 in.

N9302849

28

Any

1/16 in.

N9302886

Fused-Silica Tubing
Stainless Steel Nut
Removable Polyimide Liner

Polyimide
Ferrule
Rotor

Slot
Standard Port Diameter

Valve Body

Air Actuators
For Use With

Degree Rotation

Part No.

3- and 4-port valves


6-port valves
8-port valves
10-port valves

90
60
45
36

N9302882
N9302881
N9302825
N9302827

Each ()
293
293
293
293

Angle Bracket
General purpose bracket for
mounting standoff and actuators.

Part No.

Each ()

N9300090

27

Closemount Assembly
Allows close mounting of actuator and valve. Primarily used
for mounting valve outside oven. (Not
Each ()
to be used with manual actuator knobs) Part No.
N9302908

42

Gas Chromatography

Restrictor
Actuator Knob
Part No. N9302913

Angle Bracket
Part No. N9300090

Closemount
Part No. N9302908

Actuator Knob
Manual knob allows manual switching of valves. Can be used
with any valve or standoff listed,
Part No.
Each ()
except closemount assembly.
N9302913

18

Air Actuator Extension Kit


Extension screw allows easy tightening of
the air actuator to the standoff. Required
on AutoSystem Series/Clarus GC.

Part No.
N9300088

Each ()
18

At ambient conditions, flows range


from 2-200 mL/min. (inlet at 15 psi).
Includes: stainless steel lines (18 in.
long, 1/16 in. o.d., 0.020 in. i.d.) and
inlet filter.
Part No.
Each ()
N9302823

Rotor Removal Tool


Magnet end allows easy removal
of rotor from valves.
Part No.
N9302914

170

210

Each ()
7

Laboratory Supplies
Valve Accessories
Special Standoff for 10-Port Valve

Starter Kit

This standoff will allow connection


of a 10-port 1/8 in. valve to the
AutoSystem Series/Clarus GC.

Part No.

Part No.
N9302821

Each ()

N9302781

Each ()
427

54

Standoffs

Length

Part No.

2 in.

N9302909

51

3 1/4 in.

N9302910

51

4 1/8 in.

N9302911

51

6 in.

N9302912

Each ()

51

Kits
Sample Loop

Sample Valve

Air Actuator

Fitting
Solenoid

Column

Mounting Bracket

Description

Qty.

Part No.

2u Screen Filter for use with


Replacement Filters for N9302879
Filter Union 1/16 in. with Removable
Screen for use with Gas Line Filter
Reducer 1/8 in. Swagelok to 1/16 in.
Valco for Packed Column Adapter
Reducer 1/8 in. Swagelok Male Nut
to 1/16 in. Valco
for Injector/Detector Adapter
Stainless Steel Tubing, 50 cm,
1/16 in. o.d. to 0.02 in. i.d.
for Carrier to detector
Stainless Steel Tubing, 125 cm,
1/16 in. o.d. to 0.02 in. i.d.
for Sample Input/Output
Valco Ferrule 1/16 in.
Valco Nut 1/16 in.*

N9302880

N9302879

N9302917

N9302844

N9302922

N9300087

10
6

N9302835
N9302832

Tubing Kits
Particulate contamination is the leading cause of valve
failure. This tubing has been washed and precleaned, with
solvent and microfiltered steam from deionized water to
remove organic and ionic particulate contamination.
Each kit contains two pieces of 1/16 in. o.d. S/S tubing.

395

Solenoid Kit
Kit is required for each air actuator. Solenoid Kit allows
precise pulse of air needed to drive air actuator. Kit
includes instructions. For use with
Part No.
Each ()
AutoSystem Series/Clarus GC only.

Length

0.02 in.
Part No.

20 cm
30 cm
50 cm
125 cm

N9302871
N9302872
N9302922
N9300087

Gas Chromatography

Kit includes all necessary hardware to install valves on


AutoSystem Series/Clarus GC. Each kit is capable of
mounting up to two gas valves inside the oven. Includes
detailed instructions that show how to use gas valves,
set up timed events, and configure
Part No.
Each ()
the AutoSystem GC software.

N6120032

Kit includes:

* Cannot be used with fused-silica adapters (N9302846 or N9302847).

Mounting Kit

N6120033

Laboratory Supplies

A standoff supports both the actuator and the valve.


The standoff places the valve at the specific distance
from the actuator. A 4 1/8 in. standoff is recommended
for mounting valves in PerkinElmer GC ovens. Standoff
and actuator sold separately.

Each ()
11
10
17
114

287

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

171

Laboratory Supplies
Valve Fittings
Gas Sampling Valve Fittings

Laboratory Supplies

Ferrules
Each ()

Description

Qty.

Part No.

1/16 in. stainless steel

pkg. 1

N9302835

1/8 in. stainless steel

pkg. 1

N9302836

Description

Qty.

Part No.

1/16 in. plug

pkg. 1

N9302918

1/8 in. plug

pkg. 1

N9302919

Plugs and Caps


Each ()

1/16 in. cap

pkg. 1

N9302920

10

1/8 in. cap

pkg. 1

N9302921

10

Qty.

Part No.

1/8 in. Swagelok to 1/16 in. Valco

pkg. 1

N9302917

24

1/16 in. adapter for 1/16 in. port

pkg. 1

N9302843

14

Description

Qty.

Part No.

1/16 in.

pkg. 1

N9302832

1/8 in.

pkg. 1

N9302833

Description

Qty.

Part No.

1/16 in. to 1/32 in. reducing union

pkg. 1

N9302838

60

1/16 in. union

pkg. 1

N9302839

36

1/8 in. to 1/16 in. reducing union

pkg. 1

N9302840

36

1/8 in. union

pkg. 1

N9302841

17

Reducers
Description
TM

Each ()

3/8 in. HEX

1/4 in. HEX

Standard Nuts
Each ()

Unions
Each ()

Gas Chromatography

1/4 in. HEX

1/4 in. HEX

7/16 in. HEX

7/16 in. HEX

172

Software
TotalChrom Data Handling Systems

TotalChrom
Chromatography Data Systems
A proven solution with leading edge productivity.
Streamlining Your Laboratory Workflow
The entire process, from setting up an analytical method
to the final approval of reports, is a streamlined series of
operations in TotalChrom.
TotalChrom features TC Publisher, a powerful application
that extends report capabilities beyond the standard
templates by providing a sophisticated laboratory report
generator using standardized tools. Unique features let
you graphically format the exact report as needed without
extensive training or special commands. It ensures that
the stages of chromatographic analysis, report generation
and distribution are quick, easy, and complete.

low resolution image


TotalChrom Navigator Screen

PerkinElmers TotalChrom Chromatography Data System is


designed to provide laboratories with the total answer to
chromatography data-handling needs.
Acquiring, processing, reporting, reviewing, and approving
data is a streamlined series of operations in PerkinElmers
TotalChrom Chromatography Data Systems (CDS), software
designed to fit your laboratory workflow and maximize
productivity. With its scalable architecture, 21 CFR Part
11 compliance features and proven algorithms, TotalChrom
offers a computing strategy to manage your chromatography
data quickly and securely in both regulated and
non-regulated environments.
When configured with a PerkinElmer Clarus 500 Gas
Chromatograph or a PerkinElmer Series 200 Liquid
Chromatograph, the TotalChrom Data System is the
controller and data manager for the overall system. In addition,
TotalChrom can also control selected instruments from other
vendors and can acquire data from
any chromatographic system
through A/D interface.

TCPublisher
Replicate Injections Report

TotalChrom Client/Server (TC


C/S) Data System is the solution
in multi-user environments. TC
C/S systems can easily integrate
all existing chromatographs into a
single networked system supporting
an unlimited number of users
and an unlimited number
of chromatographs.

Report templates can perform calculations between different


peaks in the same sample or even between samples, as
well as automate statistical determination for replicate
injections, with full control over the output format.

Quickly and Easily Navigate,


Review, and Approve Your Data
In the paper world, reports need to be reviewed and
signed. The TotalChrom Review & Approve (R&A) feature
is a Graphical Reviewing environment that allows intuitive
navigation into data and reports, and provides for the
implementation of a data approval cycle. With TotalChrom
R&A, chromatograms, raw data, results, and reports can
be easily viewed and compared at a glance. Reviewing and
approving reports can be done electronically, with multiple
levels of authority and secure electronic signatures.
High-throughput applications have dramatically increased the
amount of information produced every day in a laboratory.
This feature streamlines tedious data review by using one
single environment to navigate into data, just like we, every
day, navigate into e-mail.

TCPublisher
Single Injection Report

www.perkinelmer.com/supplies

TCPublisher
Dual Channel Report

173

Software
Intelligent Interfaces
dotLINK

Integral LINK for Clarus GC and


TotalChrom Workstation Software

dotLINK Interfacing with ease.

Provides digital-to-digital connection between the Clarus


GC and TotalChrom Chromatography Workstation or the
Clarus 500 Mass Spectrometer. Includes Integral LINK,
TotalChrom Workstation Software,
Part No.
Each ()
AutoSystem XL IPM, and serial cable.

All totalchrom systems utilize PerkinElmer Intelligent


Interfaces to connect each chromatography system to the
data system PC. Each interface contains buffered RAM
memory to maintain data collection in the event that the PC
or PC network becomes inoperative during data acquisition.
Data from instruments is never lost and chromatograph
productivity is preserved.

Software

Analog chromatographs connect to TotalChrom through


NCI (Network Chromatograpy Interface) Series Intelligent
Interfaces. The model NCI 901 is a single-channel device,
while the model NCI 902 is a dual-channel device. Both
interface models are capable of taking analog detector data
(unipolar or bipolar) at sampling rates from 0.1 to 100 Hz.
dotLINK is a Windows CE-based interface that allows you
to connect your Clarus GC, Agilent 1100 GC, Agilent 6890 GC,
and Series 200 HPLC directly to the network. Designed to face
todays workload challenges and provide Ethernet connectivity,
dotLINK allows external buffering with a minimal need for
validation. The dotLINK box integral link has a small
footprint, providing valuable space for your laboratory.
dotLINK supports the following GC and HPLC configurations:
Maximum of 3 PerkinElmer Clarus GCs
Maximum of 1 PerkinElmer Series 200 HPLC System Stack
Maximum of 2 Agilent 6890 GCs
Maximum of 1 Agilent 1100 HPLC/UV System Stack

dotLINK
Model

Recommended
Applications

Memory

Part No.

dotLINK

1-3 Clarus 500 GCs

1 MB

N5150060

Each ()
3314

Integral Link
Integral Link for Clarus GC

Gas Chromatography

Provides a digital-to-digital connection between the Clarus


GC and TotalChrom. Requires AutoSystem XL IPM for
TotalChrom Workstation or Client/Server Software.
Also requires appropriate cable for
Part No.
Each ()
connection to TotalChrom system.
N6513010

174

887

N6513020

3756

Analog Board with Integral LINK*


Description

Part No.

Analog Board with Integral LINK


Analog Board with Integral LINK
and TotalChrom Workstation Software

N6513060
N6513070

Each ()
1153
4844

* For ARNEL Analyzers only.

NCI Intelligent Interfaces


NCI Series Intelligent Interfaces are 24 bit, either single or
dual-channel, buffered, A/D converters which have softwareselectable input voltage ranges of 10, 2, 1, and 0.1 V with 6
decade dynamic range, programmable sampling rates from
0.1 to 100 points per second selectable in TotalChrom
software, less than 1 microvolt noise (peak to peak), 0.1%
linearity, three sense input lines, and one-system READY
relay for communication with Autosamplers. Includes: a
board containing seven programmable relays and a
Rack/Vial Port (TTL voltage levels) for reading Autosampler
vial BCD information. Memory is segmentable for multiple
chromatograms. Software selectable symmetric bipolar or
unipolar mode operation. All Interfaces carry a 1-year
return to Service Depot warranty.

Model NCI 901 Intelligent Interface


with RVP/Relay Board
Single-channel A/D with 256KB RAM memory and RVP/
Relay board. Stores up to 120K data points. Unipolar/
bipolar operation modes. Requires but does not include
one IEEE or RS232 interface cable. Includes power cord.
Voltage

Part No.

120 V
240 V

S9000070
S9000075

Each ()
2671

Model NCI 902 Intelligent Interface


with RVP/Relay Board
Dual-channel A/D with 256KB RAM memory and RVP/
Relay board. Stores up to 120K data points. Unipolar/
bipolar operation modes. Requires but does not include
one IEEE or RS232 interface cable. Includes power cord.
Voltage

Part No.

120 V
240 V

S9000090
S9000095

Each ()
4010

Software
Intelligent Interfaces
Power Cords 240 V
No charge when ordered with 240 V Interface.
Country

Part No.

Each ()

UK, Cyprus, Nigeria, Zimbabwe, Singapore,


Malaysia, Zambia
Australia, New Zealand
Europe, Saudi Arabia, Egypt, South Africa, India,
Thailand, China
Denmark, Greenland
Switzerland, Liechtenstein

09991414

41

09991417
09991415

23
30

09991416
09991413

27
25

SoftLINK
SoftLINK Entry-level solution for instrument connectivity.

Software

Designed for workstation environments, SoftLINKTM provides


instrument connectivity at a glance. SoftLINK is able to
control 1 Series 200 HPLC/UV or up to 3 Clarus GC.

SoftLINK/TotalChrom Workstation Software


Includes: appropriate cable for connection of SoftLINK to
TotalChrom system, TotalChrom
Part No.
Each ()
software, and Clarus 500 GC IPM.**
N6513040

3098

SoftLINK Software Kit


Includes: appropriate cable for connection to TotalChrom
system, SoftLINK software CD,
Part No.
Each ()
utilities CD, and the install sheet.
N6520235

106

USB to Serial Adapter for SoftLINK


One serial port is required for each
Clarus 500 GC. Additional ports can
be added via this USB converter.

Part No.
09410077

Each ()
79

** SoftLINK is not available with PerkinElmer-ARNEL systems.

Gas Chromatography

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

175

Software
Interface Modules
Interface Personality Modules (IPM)

Interface Validation Modules (IVM)

IPMs are instrument-specific software programs that


interpret and translate instrument control and data
acquisition parameters between TotalChromTM and a specific
digital instrument. IPMs are downloaded from the host PC
(TotalChrom) by a configuration function to a specific port.
(Serial or Ethernet) on a dotLINK interface (internal or
external). Downloaded IPMs are stored in nonvolatile
memory in the dotLINK interface.

Model 520 Interface Validation Module, 120 V

IPM for AutoSystem, AutoSystem XL,


and Clarus GCs

Software

Provides control for the PerkinElmer AutoSystem Series


and Clarus GCs and their associated liquid Autosampler,
with simultaneous digital data acquisition from two inboard
detectors. Utilizes one serial port on a dotLINK interface and
may be configured to any port or ports on any LINK interface
or interfaces connected to a single TotalChrom acquisition
system. For TotalChrom Professional
Part No.
Each ()
users, v4.0 or higher is required, but
not included.
N5150160
494

IPM for Agilent 5890 Series II and Agilent 5890A GCs


Provides control for the Agilent Series 5890 GCs and their
associated liquid Autosamplers, with simultaneous digital
data acquisition from two inboard detectors. Utilizes one
serial port on a Model 600 LINK Series interface and a
second port for each associated Autosampler that is to be
controlled. This IPM may be configured to any port or ports
on any LINK interface or interfaces connected to a single
TotalChrom acquisition system. Requires one serial cable
for each connected Agilent GC and one serial cable for
each connected Autosampler. For TotalChrom Professional
users, v4.0 or higher is required, but not included. Note:
Each Agilent 5890 and 7673 autosampler must have the
appropriate Agilent serial external
Part No.
Each ()
controller card(s) and remote start
cable installed.
N5150165
494

IPM for Agilent 6890/6890Plus

Gas Chromatography

Provides control for the Agilent Series 6890 GCs and their
associated liquid Autosampler, with simultaneous digital
data acquisition from two inboard detectors. Utilizes one
serial port on a dotLINK. This IPM may be configured to
any port or ports on any LINK interface or interfaces
connected to a single TotalChrom acquisition system. It is
recommended that no more than two Agilent 6890 GCs be
configured per workstation LINK interface. Requires one
serial cable for each connected Agilent
Part No.
Each ()
GC. Control of the Agilent 6890/
6890Plus is not available for TC Pro.
N5150166
494

176

The Model 520 IVM is a calibrated analog peak pattern


generator for use in testing/validating analog to digital
converters such as the NCI 901/902 and the Series 900/900A
Intelligent Interfaces. The module generates eight possible
analog patterns at selectable voltage ranges of 0-0.1, 0-1, 0-2,
and 0-10 volts. Factory calibration is traceable to a NIST
standard volt. Includes remote start/stop cable and analog
signal cable for connection to PerkinElmer NCI/900/900A
Series Intelligent Interfaces. Includes 1-year return to
Service Depot warranty.
Voltage

Part No.

120 V
240 V

S9000160
S9000165

Each ()
2586

TotalChrom Workstation Model 520 IVM Software


Allows user to test any NCI Series and M900A Series
Intelligent Interfaces to validate interface operations
(linearity, reproducibility, etc.). Contains special TotalChrom
interface test methods and automated validation logs to
maintain results of interface tests in software.
Requires, but does not include, a
Part No.
Each ()
Model 520 Interface Validation Module.
N5150181

314

Software
Serial Cables
IEEE Cables All TC Versions

Serial Cables

Cable Length

Part No.

1m
2m
4m
8m

65105001
65105102
65105204
65105408

External Communications Cable


Shielded DB9 Male/Female 9-pin
external RS-232 communications cable.

Part No.

Each ()
153
173
184
230

Each ()

N6500133

181

TotalChromTM WS and C/S Serial


Cables to Lantronix Terminal Server
Cable Length
7 ft.
25 ft.
50 ft.
100 ft.

Part No.

Each ()

S5010021
S5010022
S5010023
S5010024

32
38
51
64

For M950/970 Interfaces


Cable Length

Part No.

7 ft.
25 ft.
50 ft.
100 ft.

S5010017
S5010018
S5010019
S5010020

Each ()
32
38
51
64

For NCI Interfaces


Cable Length

Part No.

7 ft.
25 ft.
50 ft.
100 ft.

S5010037
S5010038
S5010039
S5010040

Each ()
63
71
64
77

TotalChrom WS and
C/S Serial Cables to PC
For dotLINK Interfaces
Cable Length

Part No.

10 ft.
25 ft.

09290144
09290145

Each ()
19
47

For M941A and M600/610 Link Interfaces


Part No.

7 ft.
25 ft.
50 ft.
100 ft.

S5010025
S5010030
S5010031
S5010032

Part No.

PerkinElmer Clarus GC to dotLINK, 10 ft.

09290146

Each ()

PerkinElmer Clarus GC to dotLINK, 25 ft.

09290147

47

PerkinElmer Clarus GC
to M600/M610 LINK, 10 ft.

65609010

223

PerkinElmer Clarus GC
to M600/M610 LINK, 25 ft.

65609025

300

M900/960/970 Series Interface to M600/M610


LINK, 6 ft. (not for M941)

S5010013

223

NCI Series Interface to dotLINK, 7 ft.

S5010037

63

NCI Series Interface to M600/M610 LINK, 6 ft.

S5010041

223

Agilent 1100 GC-Autosampler to dotLINK, 10 ft.


(Required quantity: 3)

09290144

19

Agilent 1512A Autosampler Controller


(on 5890GC) to M600/M610 LINK, 10 ft.

S5010015

223

Agilent 1512A Autosampler Controller


(on 5890GC) to M600/M610 LINK, 25 ft.

S5010016

300

Agilent 5890A/Series II GC
to M600/M610 LINK, 10 ft.

65605810

223

Agilent 6890 GC/-Agilent 6890Plus GCAutosampler to dotLINK, 10 ft.

09290144

19

Agilent 6890 GC/-Agilent 6890Plus GCAutosampler to dotLINK, 25 ft.

09290145

47

Agilent 6890 GC/-Agilent 6890Plus GCAutosampler to M600/M610 LINK, 10 ft.

S5010015

223

Agilent 6890 GC/-Agilent 6890Plus GCAutosampler to M600/M610 LINK, 25 ft.

S5010016

300

Agilent 7673A Autosampler Controller


(on 5890GC) to M600/M610 LINK, 10 ft.

65607610

223

Agilent 7673A Autosampler Controller


(on 5890GC) to M600/M610 LINK, 25 ft.

65607625

300

19

* Special serial cards, instrument communication kits, and IPM software


may be required to complete interfacing of a LINK interface to a digital
chromatograph. Please contact your local PerkinElmer Sales Representative
for details.

Each ()
46
52
64
77

M900 Series BCD Cables for Autosamplers


Description

Part No.

PerkinElmer HS100, HS101, ATD50, AS2000, AS8300 65204501

Gas Chromatography

Cable Length

Description

Software

For M941/M600 LINK Interfaces

Serial Cables* for Instrument Interface

Each ()
230

For NCI Interfaces


Cable Length

Part No.

7 ft.
25 ft.
50 ft.
100 ft.

S5010033
S5010034
S5010035
S5010036

Each ()
46
52
64
77

Agilent 6890 HS40/ATD400 Ready/Run Cables


Description

Part No.

Cable Kit, HS40/ATD400 to Agilent 6890


N6100410
Cable Kit, M950/970 Series Interface to Agilent 6890 N6100411

Each ()
149
159

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

177

Software
Software Kits
Serial Communications
Cards for TurboChrom

TotalChrom Workstation
SI/DI Upgrade Kits

Agilent 5890A/Series II GC

v6.x Workstation Migration to v6.3.x Workstation

Description

Part No.

Serial Card

S2000203

Each ()
2360

Agilent 7673A Controller


Description

Part No.

Remote Start Cable


Serial Card and Control Board
Serial Card and EPROM

S2000206
S2000205
S2000204

Migrates an existing TurboChromTM Workstation


v4.x or v6.x acquisition system, and associated RPO
systems, to TotalChrom Workstation v6.3.x software.
Requires verification of ownership of TurboChrom
v6.x software. Software supplied on
Part No.
Each ()
CD-ROM media v4.x or v6.x.

Each ()

N5150349

1140

102
2928
638

Software

v6.2.x Workstation Migration to v6.3.x Workstation

TotalChrom Workstation Manuals


Application Managers Guide
Application Managers Guide covering
installation and system management
of TotalChrom Workstation software.

Part No.
N5156025

Each ()

Migrates an existing TotalChrom Workstation v6.2.x


acquisition system, and associated RPO systems, to
TotalChrom Workstation v6.3.x software. Requires
verification of ownership of TotalChrom v6.2.x software.
Software supplied on CD-ROM media.
Part No.
Each ()

128

N5150715

855

Manual Set
Complete manual set including Users
Guide (volumes 1 and 2), Application
Managers Guide, and Tutorial.

Part No.
N5150512

Each ()
383

TotalChrom Tutorial
Software tutorial that teaches basic data acquisition, method
development, optimization techniques,
Part No.
Each ()
sequence development, and calibration.
N5156021

70

Users Guide (Volumes 1 and 2)

Gas Chromatography

Users manual covering instrument


configuration and basic operation
of TotalChromTM Workstation software.

178

Part No.
N5150518

Each ()
255

TotalChrom Workstation Software


Description

Part No.

Multi-Instrument Software Kit


Reprocess-Only Software Kit

N5150103
N5150100

Each ()
3704
542

Thermal Desorbers
TurboMatrix Thermal Desorbers

TurboMatrix
Thermal Desorbers for GC
... driving unrivaled Performance
through Innovation.
Thermal desorption is a technique that simplifies and speeds a wide range of gas
chromatography (GC) applications, including indoor and outdoor air monitoring, analysis
of outgassing from semiconductor materials, polymers, upholstery and furnishings,
packaging, pharmaceuticals, and analysis of flavors and fragrances.
As the undisputed market leader in GC sample handling, we took the next step to offer you
even more benefits for your lab. PerkinElmer offers a family of five different TurboMatrixTM
Thermal Desorber (TD) models in both single-tube and automated 50-tube configurations:
TurboMatrix 100 TD single-tube and manual pneumatics
TurboMatrix 150 ATD 50-tube autosampler and manual pneumatics
TurboMatrix 300 TD single-tube and programmable pneumatic control
TurboMatrix 350 ATD 50-tube autosampler and programmable pneumatic control
TurboMatrix 650 ATD 50-tube autosampler, programmable pneumatic control

and a variety of other accessories for a wide range of applications

This broad offering allows you to match technology


to your laboratory and applications needs.

Confirmatory Analysis

Reduced Cost Per Sample

The TurboMatrix 650 ATD allows samplesplit re-collection on same or different


tubes, delivering the ability to audit
samples and perform confirmatory
analysis and repeat analysis under a
different set of conditions.

The TurboMatrix Thermal Desorbers


save money and minimize laboratory
waste. After each use, all sample tubes
can be reconditioned and conveniently
reused. The system provides cryogenfree operation down to -30 C, reducing
operating costs. Unlike other techniques,
thermal desorption requires no solvents,
thus reducing cost, risk of contamination,
analyst exposure and the need for
solvent disposal.

Improved chromatography and narrow peak widths

as a result of 40 C per second trap heating rate

Integrity Testing
Sensors monitor all aspects of system
operation to ensure that the instrument
is working as it should and provide an
early indication of possible problems
with the analysis. Analytical techniques
such as tube and trap impedance testing
and the standard addition options help
ensure sample integrity. All of these
are designed to provide the user with
the highest confidence in the final
analytical results.

Higher productivity with overlapping tube

desorption and chromatography


Wider boiling range analysis and improved water

management using the backflush mode, where


multiple adsorbents can be used in series
Uncompromised narrow-bore capillary

chromatography due to rapid desorption


of the focusing trap (40 C per second)

Maximize Sample Throughput


Since the thermal desorber unit can
run simultaneously with the GC, you
can start your next desorption run as
the GC processes the previous run for
maximum productivity.

179

Thermal Desorbers
Ozone Precursor Accessories
Air Toxics Columns

Diffusion Limiting Caps

Part No.

(pkg. 5)

L4285001

Each ()
108

Methyl Silicone Column


For use with Air ToxicsTM (T014)
Analyzer System with FID/ECD
detectors. 100 m x 0.32 mm i.d. x 5 m.

Part No.

Each ()

N6300155

1836

Electrical Adapter
Allows for direct connection to wall
outlet. Also acts as a battery charger
for 12 V battery (120/240 V).

Part No.
L4280003

Each ()
453

Thermal Desorbers

Methyl Silicone Column


For use with the Air Toxics (T014) Analyzer System
with Mass Spectrometer
Part No.
Each ()
60 m x 0.32 mm i.d. x 5 m.
N9316000

993

Personal Monitoring Pump


Description

Size

Part No.

5-100 mL/min.
5-100 mL/min.

110 V
220 V

N6102351
N6102197

Each ()
2028

STS 25 Maintenance Kit

Model STS 25 Sequential


Tube Sampler

Each ()

Description

Part No.

Includes: Rotor Tube Seals (pkg. 50), Filter


Disks (pkg. 25), Diffusion Limiting Caps (pkg. 5),
and Rotor Seal (pkg. 10)
Rotor Filter Disk

N6609060

504

L4281023

Viton O-Ring
For use in diffusion limiting cap
and tube seals. (pkg. 50)

Part No.
L4275033

Each ()
147

Ozone Precursor Accessories


Alumina PLOT TM Column

Part No.

Each ()

50 m x 0.32 mm i.d.

N6301107

2729

Part No.

Each ()

ATD 400 Air Monitoring Trap

Gas Chromatography

The STS 25 is used for sequential sampling of air onto a


series of up to 24 ATD sample tubes. It is a portable unit
and can be operated either by a 12 V battery or 120/240 V.
The sampler includes cables with jack plug connectors
(for use with the monitoring pump) and a set of diffusion
limiting caps. The STS 25 requires but does not include
sample tubes and a monitoring
Part No.
Each ()
pump. Also requires a 12 V
battery or an electrical adapter.
L4280001
6600

Model STS 25 Accessories


Part No.

Waterproof, suitable for outdoor use.

L4280002

Air Monitoring Pump

Part No.

Each ()

120 V

L4271275

2810

For connecting the STS-25 to


a generic 12 V battery.

180

Part No.
L4285007

Each ()

L4275108

332

Methyl Silicone Column

Part No.

Each ()

50 m x 0.22 i.d. x 1.0 m

N6301108

1518

Nafion Dryer

Part No.

Each ()

04974414

1193

Part No.

Each ()

Particulate Filter Kit

12 V Rechargeable Battery

Cable

Low flow trap packed with carbonaceous


sorbents suitable for ozone precursor
and air toxics monitoring. (pkg. 1)

Includes disposable filter and fittings.


For use in the ozone precursor analyzer.

N6300063

255

548

Each ()
121

Restrictor Tubing
0.10 mm i.d. uncoated, deactivated,
fused-silica restrictor tubing. For
use in the ozone precursor analyzer.

Part No.
N9301355

Each ()
114

Thermal Desorbers
Sample Tubes
Caps for TurboMatrix

Sample Tubes for TurboMatrix

Brass Long-Term Storage Caps

Packed Sample Tubes for TurboMatrix

Recommended for long-term storage.


Two required per tube. Also requires
Teflon ferrule (L1003015). (pkg. 1)

Part No.

Each ()

09908851

For use with 1/4 in. Brass Long-term


Storage Cap (09908851). Two (2)
required per tube. (pkg. 1)

Part No.

Each ()

L1003015

Diffusion Caps Standard

Stainless Steel
Glass
Part No.
Each () Part No.

10** Air Toxics Tube

N9307001

871 N9307008

871

10** Carbopack B 60/80

N9307002

871 N9307009

871

10** Carbopack B 60/80


N9307000
Carbopack C 60/80
Carbosieve SIII 60/80

871 N9307007

871

10** Carbosieve SIII 60/80

871 N9307010

871

10** Chromasorb 106

N9307006

871 N9307013

871

10** NIOSH 2549 tube

N9307038

871 N9307037

871

10** Tenax GR 60/80

N9307004

871 N9307011

871

10** Tenax TA 60/80


N9307005
871 N9307012
** Shipped with brass long-term storage caps.

871

Part No.

For passive air sampling to ensure


correct diffusion path length. (pkg. 10)

Each ()

L4070207

164

Diffusion Caps with Membrane


Part No.

Same as above but with a


silicone membrane. (pkg. 10)

L4070208

Pen Clips

Part No.

For stainless steel ATD tubes. (pkg. 10)

L4071029

PFA Teflon Ferrules for


TurboMatrix Storage End Caps

Part No.

(pkg. 20)

M0413625

Each ()

N9307003

Each ()

Thermal Desorbers

Combined Teflon Ferrule

Pkg.
Qty. Sorbent

588

Each ()
31

Packed Sample Tubes


for TurboMatrix

Each ()
218

TurboMatrix Analytical Caps


Required for use on the TurboMatrix
instrument during analysis PTFE Caps
with O-Ring. (pkg. 20)

Part No.

Each ()

N6200119

280

Replacement Parts for ATD 400


Tube Seal and Tube
Description

Qty.

Packed Sample Tube(s)*


Sample Tube(s)*
Packing Retaining Gauzes
Retaining Springs
Chamfer Holder O-Ring
Tube Seal O-Ring
Grip Seal O-Ring
Nozzle Filter Disk

Part No.

100
50
1
10
50
1

Each ()

L4071034
L4071123
04973727
04972383
04970343
L4271159

114
86
2
1
15
2

* See Sample Tube product listing above.


3

Glass Lined
Pkg. Stainless Steel
Stainless Steel
Glass
Qty. Part No.
Each () Part No.
Each () Part No.
10* M0413597

739

M0413595

340 M0413598

Each ()
368

50*
M0413596 1518
* Shipped with Analytical End Caps (N6200119).

Empty Sample Tubes Without Caps

Empty Sample Tubes with Caps

Gas Chromatography

11
1
22
33
44
55
66
77

Pkg.
Qty.

Stainless Steel
Glass
Part No.
Each () Part No.

10

L4270128

100

L4270129

224 L4071594

Each ()
249

2244

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

181

Thermal Desorbers
Thermal Desorber Supplies
Cold Traps, Fittings,
and Accessories

Consumables Starter Kit


Thermal Desorber Starter Kit

ATD 400 Air Monitoring Trap


Low flow trap (L4275107) packed with carbonaceous
sorbents suitable for ozone precursor
Part No.
Each ()
and air toxics monitoring. (pkg. 1)

Thermal Desorbers

L4275108

ATD Cold Trap Nuts

Part No.

Two required per trap tube. (pkg. 1)

L4275009

Cold Trap Tube (packed)

Part No.

Standard cold trap packed


with CarbopackC.

Each ()
59

Each ()
317

Cold Trap Tube (Low Flow) Unpacked

0.7 mm

Low Flow Cold Trap

Sorbents

Part No.

Glass Fiber
Disks

Standard cold trap (L4271106)


packed with Tenax TA 60/80. (pkg. 1)

248

Description

Qty.

Part No.

Glass Wool
Tenax TA 60-80, Mesh 15 g
Packing Gauze
Retaining Spring
Stainless Steel Sample Tubes
Glass Sample Tube
PTFE Filter Discs, Large
PTFE Filter Discs
Graphite Ferrules
Trap Tube Nuts
Trap Tubes

pkg. 1
pkg. 1
pkg. 100
pkg. 50
pkg. 10
pkg. 10
pkg. 10
pkg. 10
pkg. 2
pkg. 2
pkg. 2

54120790
04978064
L4071034
L4071123
M0413595
M0413598
L1003029
L1003030
L4271187
L4275009
M0410094

Gauze Loading Supplies


Gauze Loading Rig

2.8 mm

Part No.
L4275089

4845

Includes:

Correctly positions gauze at both ends of stainless steel


sampling tubes. Highly recommended
Part No.
Each ()
when packing sample tubes.
L4070023

2168

Replacement Plastic Plunger


for Gauze Loading Device

Part No.

Each ()

(pkg. 5)

L4071151

Packing Retaining Spring

Cold Trap Tube (Tenax TA)

M0413541

Each ()

Each ()

L4275107

Quartz Wool

Part No.

332

N6200150

Cold trap with reduced bore at one


end. Allows minimum gas flow
during trap desorption. (pkg. 1)

The starter kit is recommended for all


purchasers who do not already have a
TurboMatrix Thermal Desorber.

Each ()

60

126

Interface Cables for ATD 400


Cold Trap Tube (Unpacked)
Standard cold trap tube unpacked.
(pkg. 1)

Part No.
L4271106

Each ()
92

Graphite Ferrule

Gas Chromatography

Ferrule for cold trap. Recommended


for all applications except those using
Mass Spectrometer or ECD. (pkg. 2)

Part No.
L4271187

Each ()

Note: New ferrules are required


when trap is changed.

Part No.

Also transmits BCD.

L4270034

Ready/Start Cable

Part No.

Also transmits BCD.

L4270032

210

Each ()
159

Interface Kit
Part No.
L4275110

Each ()
9

Thermal Desorber GC Interface Kit


Contains all necessary hardware for connecting the heated
transfer line to either 1/8 in. packed or
Part No.
Each ()
capillary columns inside the GC oven.
L4270026

182

Each ()

PTFE Ferrule
Ferrules for cold trap. Recommended
for use with Mass Spectrometer
or ECD. (pkg. 10)

Nelson 900 Series


Interface Box Cable

838

Thermal Desorbers
Thermal Desorber Supplies
Thermal Desorber to
Agilent 6890 GC Ready Start Cable
Connects a TurboMatrix thermal
desorber to an Agilent 6890
or Agilent 6850 GC.

TurboMatrix ATD Sample Carousel


Part No.
N6100410

Each ()
149

Manual
Part No.
M0413331

Each ()
93

Part No.

Each ()

M0413380

234

Mobile Seal Assembly


Description

Part No.

Mobile Seal O-Ring, Viton 009


Mobile Seal O-Ring, Viton 010
Nozzle Filter Disc (pkg. 1)

L1003006
04970343
L4271159

Each ()
1
15
2

Thermal Desorbers

TurboMatrix Thermal Desorber


Users Manual

Fifty (50) position tube carousel


for use on the TurboMatrix ATD.

Software

Miscellaneous Accessories

TurboMatrix TD/ATD PC Control Software Rev 1.1

Backflush Nozzle Accessory

Part No.
L4275072

Each ()
217

Graphite Vespel Ferrule


1/16 in. x 0.5 mm i.d. For connection
of 0.32 mm i.d. transfer line to ATD.
(pkg. 1)

Part No.
04972066

Each ()
7

Internal Standard Injection Accessory


To allow the introduction of a
gaseous internal standard.

Part No.

Each ()

L4270010

4056

Liquid Nitrogen Accessory


For operation of the cold trap to -100 C.
Note: Requires a pressurized Dewar with a relief valve set at 25 psig
(180 kpa). Dewar must have a 1/4 in. Swagelok TM connection. Also
requires a pressure relief valve set at 50 psig
Part No.
Each ()
(350 kpa) in pipe between Dewar and ATD 400.
L4270009

Provides full external control of a TurboMatrix thermal


desorber from a personal computer running under Windows
95, 98, or NT. Methods and sequences can be generated,
stored, edited, printed, and executed. Functions include
diagnostics, user defined access levels, run reports, and
transfer of vial identification to TotalChrom, allowing
complete data traceability. On-screen
Part No.
Each ()
interactive help function is available.
Cable included (M0417035).
M0413559
740

TurboMatrix TD/ATD Remote Control Software


Rev 1.1 (for WIN 2000)
Provides full external control of a TurboMatrix thermal
desorber from a personal computer running under Windows
95, 98, or NT. Methods and sequences can be generated,
stored, edited, printed, and executed. Functions include
diagnostics, user defined access levels, run reports, and
transfer of vial identification to TotalChrom, allowing
complete data traceability. On-screen
Part No.
Each ()
interactive help function is available.
Cable included (M0417035).
N6200210
819

1836

Regulator 0-60 psig

Trap Supplies

The standard 0-30 psig regulator can be replaced with this


0-60 psig regulator to expand the choice of column and
application range. Installation by a
Part No.
Each ()
PerkinElmer Service Engineer is
required, but not included.
N6101474
300

For use on ValcoTM valve. 1/16 in. i.d.


(pkg. 1)

Part No.
04974018

Each ()
8

Part No.

Ceramic Washer
Cold Trap O-Ring
Heat Conduction Bushing
Filter Disk (pkg. 1)
PTFE filter on either side of cold trap
Packing Disk (pkg. 20)
Glass fiber disk for separating sorbents when
packing cold trap with multiple sorbents
Packing Retaining Spring (pkg. 5)
For low flow trap
Packing Tool
Graphite Ferrule (pkg. 2)
Ferrule for cold trap. Recommended for all
applications except those using Mass Spec or ECD
Gripper Insert Replacement (pkg. 2)
Heated Transfer Line
Standard length 45 in.
Heated Transfer Line
Long length 70 in.

M0415339
09200091
M0410316
L1003030

Each ()
9
30
8
47

L4271290

16

N6301054

29

L4271203
L4271187

24
5

M0413645
M0413644

64
1314

M0413558

1454

Gas Chromatography

Valco Graphite Vespel Ferrule

Description

See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies

183

Thermal Desorbers
Thermal Desorber Supplies

Thermal Desorbers

Thermal Desorber Empty Trap (pkg. 1)


Thermal Desorber Packed Trap
Trap packed with CarbopackC
TurboMatrix Air Monitoring Trap (pkg. 1)
Trap packed with carbonaceous sorbents suitable
for ozone precurser and air toxics monitoring
TurboMatrix Thermal Desorber Packed Trap (pkg. 1)
Trap packed with TenaxTM TA
PTFE Ferrule
Ferrules for cold trap. Recommended for use with
Mass Spec or ECD. (pkg. 10)*
Trap Filter Disk
PTFE filter on either side of cold trap. (pkg.1)
Trap Heat Conduction Bushing and Ceramic Washer

M0413627
N6200150

238
317

M0413628

317

M0413535

334

L4275110

L4271160
M0410316

5
8

* New ferrules are required when trap is changed.

TurboMatrix Upgrade Kits


Internal Standard Addition/Tube Dry Purge Add-On Kit
Adds capability to introduce a known quantity of a gaseous
standard into the sample tube prior to desorption to verify
analyte recovery. Standard gas is added to the tube in the
sampling direction, allowing use of tubes packed with
multiple adsorbents.
Note: Requires, but does not include, an Options
Board when added to the entry-level thermal
desorber. Installation by PerkinElmer Service
is required, but not included.

Part No.
M0413555

5300

For operation of the cold trap to -100 C. Requires, but does


not include, the options board when added to entry-level
thermal desorber. Requires a pressurized Dewar with a relief
valve set at 25 psig (180 kpa). Dewar must have a 1/4 in.
Swagelok connection. Also requires a pressure relief
valve set at 50 psig (350 kpa) in pipe between Dewar and
TurboMatrix. Installation by
Part No.
Each ()
PerkinElmer Service is required,
but not included.
M0413557
1951

On-Line Sampling Add-On Kit

Gas Chromatography

Adds capability to perform on-line sampling of ambient


air directly to the electrically cooled trap. Overlapping
sampling and GC analysis allows collection of air for
analysis up to 50 minutes of every hour. Includes sample
valve, Nafion drier, dry air purge control, and pump.
Air Toxics trap is installed.
Note: Requires, but does not include, an Options Board when added to
entry-level thermal desorber. Allows thermal desorber to still be used for
tube desorption. Installation by PerkinElmer
Part No.
Each ()
Service is required, but not included.

184

Required for installation of the following options on an entrylevel thermal desorber Internal Standard Addition, On-Line
Sampling, or Liquid Nitrogen Cooling. Also provides output
of BCD information regarding tube position numbers and
provides relay output for timed control of external devices.
Note: This board is included as standard on the
automated thermal desorber. Installation by
PerkinElmer Service is required, but not included.

Part No.
M0413551

Each ()
988

Thermal Desorber to
Automated Thermal Desorber Upgrade Kit
Includes parts to upgrade an entry-level thermal desorber
to an automated thermal desorber for unattended analysis
of up to 50 samples. Includes BCD output communication
capabilities and timed event relays for timed control of
external devices. Installation
Part No.
Each ()
by PerkinElmer Service
is required, but not included.
M0413553 16600

TurboMatrix Upper Seal Assembly

Each ()

Liquid Nitrogen Cooling Add-On Kit

M0413556

Options Board/BCD Output Board

13200

Each ()

Description

Qty.

Part No.

Low Temp (< 225 C),


Viton 009 O-Rings
Low Temp (< 225 C),
Viton 011 O-Rings
High Temp (> 225 C),
Kalrez 011, Large Seal O-Ring
High Temp (> 225 C),
Kalrez 009, Small Seal O-Ring
Fixed Upper Seal, Graphite Ferrule

pkg. 10

L1003006

pkg. 10

L1003008

pkg. 1

M0415361

88

pkg. 1

M0415360

80

09920593

27

TurboMatrix Thermal Desorber High Temperature Kit


Contains all the necessary hardware for operation of the
valve at temperatures starting at 150 C up to 300 C.
Service is required, but not included.
Part No.
Each ()
M0413646

1212