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Tabel 6.

1 Wadah dan Pengawetan Sampel Kualitas Air Yang Dianjurkan


Parameter

Wadah yang
diajurkan

Maximum
penyimpanan yang
diperbolehkan

Pengawetan

Aciditi

Polyethylene

dingin, 40 C

24 jam

Alkaliniti

Polyethylene

Aluminium

Polyethylene

dingin, 40 C
2 ml Conc HNO3/L sampel

6 bulan

Antimony

Polyethylene

2 ml Conc HNO3/L sampel

6 bulan

Arsenic

Polyethylene

6 bulan

Barium

Polyethylene

dingin, 40 C
2 ml Conc HNO3/L sampel

Berylium

Polyethylene

2 ml Conc HNO3/L sampel

6 bulan

BOD

Polyethylene

dingin, 40 C

Boron

Polyethylene

Cadmium

Polyethylene

dingin, 4 C
2 ml Conc HNO3/L sampel

Calcium

Polyethylene

Carbamat pesticides

Glass

24 jam

6 bualn
4 jam
6 bulan

6 bulan

dingin, 40 C
H2SO4 to pH < 4, 10 g Na2SO4 sampel

7 hari
segera dianalisa

Carbon, inorganic

Polyethylene

dingin, 40 C

24 jam

Carbon, organic

Polyethylene

dingin, 40 C

24 jam

Plastic petridish

dingin, 4 C

6 bulan

Carbon, particulate

Chloride

Polyethylene

saring dengan GF/C filter

Chlorinated hydrocarbon
pesticides

Polyethylene

dingin, 40 C

Chlorophyll

Polyethylene

Cholesterol

Glass

saring dengan GF/C filter; bekukan -20 C


1 ml Conc H2SO4 / L sampel

24 hari

Chromium

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

Cobalt

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

COD

Polyethylene

dingin, 40 C

24 jam

Colour(warna)

Polyethylene

24 jam

Copper (Tembaga)

Polyethylene

dingin, 40 C
2 ml Conc HNO3 / L sampel

6 bulan

Glass

1 ml Conc H2SO4 / L sampel

24 jam

1 ml 10 % NaOH /100 ml sampel

24 jam

Coprostanol
Cyanide
Dissolved oxygen winkler tit

Polyethylene
Glass

7 hari
segera dianalisa
0

7 hari

diukur di lapangan

6 jam

Flouride

Polyethylene

dingin, 40 C

7 hari

Hardness(kesadahan)

Polyethylene

dingin, 40 C

24 jam

Iodida

Polyethylene

Iron(besi)

Polyethylene

dingin, 40 C
2 ml Conc HNO3 / L sampel

6 bulan

Lead(Timah Hitam)

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

Lithium

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

Magnesium

Polyethylene

7 hari

Manganese

Polyethylene

dingin, 40 C
2 ml Conc HNO3 / L sampel

6 bulan

1 ml Conc H2SO4 / L sampel ,

1 bulan

Mercury(Air Raksa)

Glass atau
Teflon

24 jam

1ml 5% K2Cr2O7 larutan / 100 ml sampel

Molybdenum

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

Nickel

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

Nitrogen

Polyethylene

Amonia

Polyethylene

dingin, 40 C, 2 ml 40 % H2SO4 / L sampel

24 jam

Kjeldahl Amonia

Polyethylene

dingin, 40 C

24 jam

Nitrate + Nitrite

Polyethylene

dingin, 40 C

24 jam

Organic Nitrogen

Polyethylene

dingin, 40 C

24 jam

Saring dengan CF/C filter, dingin, 40 C

6 bulan

Perlakukan dengan 0.5 % dari 37 %


larutan formaldehyde; filter dengan 0.45
um membran filter

24 jam

Organic particulate

Plastic petridish

NTA
Polarographic

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Polyethylene

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Parameter

Wadah yang
diajurkan

GLC

Glass

Oil & Grease

Glass

Oganophosporus pesticida

Glass

Pentachlorophenol

Glass

pH

5 ml Conc. HCl/L sampel


dingin, 40C, 5 ml 1 + 1, H2SO4 to pH < 2
dingin, 4 C,10 % HCl to pH 4.4
H2SO4 to pH < 4; 0.5 g CaSO4/L ; dingin 40
0

Maximum
penyimpanan yang
diperbolehkan
24 jam
24 jam
extraksi di lapangan
24 jam

Phenolies

Glass

None
H3PO4 to pH < 4; 1.0 g CaSO4/L ; dingin 40

Phenoxy acid hibricides

Glass

H2SO4 to pH < 4, 10 g

Phosporus

Glass

Dissolved Phospat

Glass

Saring dengan 0.45 um membrane filter

24 jam

Inorganic Phospat

Glass

dingin, 40 C

24 jam

Ortho Phospat

Glass

dingin, 40 C

24 jam

Total Phospat

Glass

dingin, 40 C

1 bulan

Pottasium(Kalium)

Polyethylene

dingin, 40 C

7 hari

Residue

Polyethylene

dingin, 4 C

7 hari

Selenium

Polyethylene

dingin, 40 C

6 bulan

Silica

Polyethylene

dingin, 40 C

7 hari

Silver

Polyethylene

0.4 gram Disodium EDTA/100 ml sampel

10 hari

Sodium (Natrium)

Polyethylene

dingin, 40 C

7 hari

Specific conductance

Polyethylene

Strontium

Polyethylene

dingin, 4 C
2 ml Conc HNO3 / L sampel

6 bulan

Glass

dingin, 40 C

24 jam

Sulphate

Polyethylene

dingin, 40 C

7 hari

Turbidity

Polyethylene

Vanadium

Polyethylene

dingin, 40 C
2 ml Conc HNO3 / L sampel

6 bulan

Zing

Polyethylene

2 ml Conc HNO3 / L sampel

6 bulan

Sugar (gula)

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Polyethylene

Pengawetan

6 jam
24 jam
Segera di extract

24 jam

7 hari

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