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MAPA INSTITUTE OF TECHNOLOGY

SCHOOL OF CHEMICAL ENGINEERING AND CHEMISTRY (INTRAMUROS)


VISION
Mapa shall be an international center of excellence in technology education by:
The Mapa Institute of Technology shall be a global center of excellence in education by providing instructions that are current in
content and state-of-the-art in delivery; by engaging in cutting-edge, high-impact research; and by aggressively taking on
present-day global concerns.
MISSION
The Mapa Institute of Technology disseminates, generates, preserves and applies knowledge in various fields of study.
The Institute, using the most effective and efficient means, provides its students with highly relevant professional and advanced
education in preparation for and furtherance of global practice.
The Institute engages in research with high socio-economic impact and reports on the results of such inquiries.
The Institute brings to bear humanitys vast store of knowledge on the problems of industry and community in order to make the
Philippines and the world a better place.

a.
b.
c.
d.

PROGRAM EDUCATIONAL OBJECTIVES


1.
2.

MISSION
b
c

To enable our graduates to practice as successful engineers for the advancement


of society.
To promote professionalism in engineering practice.

COURSE SYLLABUS
1.

Course Code:

CHM111-1L

2.

Course Title:

ANALYTICAL CHEMISTRY LABORATORY 1

3.

Pre-requisite:

CHM12-2, CHM12-2L

4.

Co-requisite:

CHM111-1

5.

Credit:

6.

Course Description:
This laboratory component of CHM111-1 covers experiments and exercises to enhance the students
understanding of basic tools and operations of analytical chemistry, data handling, measurements and
calibration, gravimetric analysis and calculations, standardization techniques, acid-base titration using
double indicator and EDTA, redox titration, and potentiometric titration.
Credit
: 1 units
Prerequisites : CHM13-2P, CHM13L or CHM12-2, CHM12-2L
Corequisite : CHM111-1

7.

Student Outcomes and Relationship to Program Educational Objectives


Program
Educational
Objectives
1
2

Student Outcomes
(a)

An ability to apply knowledge of mathematics,


science, and applied sciences.

Course Title:
ANALYTICAL CHEMISTRY LABORATORY
1

Date
Effectivity:
1st Quarter
SY 20122013

Date
Revised:
4th Quarter
SY 20112012

Prepared By:

Approved By:

Marilen M. Martin
Dean
Luz L.Lozano

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(b)
(c)
(d)
(e)
(f)
(g)
(h)
(i)
(j)
(k)

8.

An ability to design and conduct experiments, as


well as to analyze and interpret data.
An ability to formulate or design a system, process,
or program to meet desired needs.
An ability to function on multidisciplinary teams
An ability to identify and solve applied science
problems.
An understanding of professional and ethical
responsibility.
An ability to communicate effectively.
The broad education necessary to understand the
impact of solutions in a global and societal context.
A recognition of the need for and an ability to
engage in life-long learning.
A knowledge of contemporary issues.
An ability to use the techniques, skills, and modern
scientific and technical tools necessary for
professional practice.

Course Outcomes (COs) and Relationship to Student Outcomes

Course Outcomes
After completing the course, the student must be able to:
1. Apply quantitative skills and techniques require to perform
chemical analyses in the laboratory (data handling).
2. Develop analytical techniques employed in gravimetric
analysis.
3. Demonstrate the techniques on handling volumetric
(titrimetric) titration.
4. Acquire basic knowledge on the operation of analytical
instruments (UV-Vis, AAS and FTIR)
* Level: I- Introduced, R- Reinforced, D- Demonstrated
9.

Student Outcomes*
d e f g h i

Course Coverage
Week
1

COURSE
OUTCOMES
CO1

TOPIC

TLA

Vision and Mission of the School,


Introduction to the course
Mapas Vision and Mision, Departments
Specific Objectives, Course Policies and
Guidelines
Borrowing of apparatus
Discussion on Chemicals, Apparatus and
Unit Operations of Analytical Chemistry &
Data Handling in Analytical Chemistry

AT

Rounds (giving
turns to
individual
students to talk)
(Start the discussion
(involve the students)
on chemicals,
apparatus and unit
operations of analytical
chemistry)

Group
discussion
(Orientation on course
policies and grading
system)

Problem solving
(Give practical
exercises on the topics
introduce.)

CO1

Exercise No.1: Using the Analytical Balance


Exercise No. 2: Making Quantitative
Transfers
Exercise No. 3: Delivering an Aliquot
Exercise No. 4: Calibrating a Pipette
Exercise No. 5: Reading and Use of Burette

Course Title:
ANALYTICAL CHEMISTRY LABORATORY
1

Date
Effectivity:
1st Quarter
SY 20122013

Date
Revised:
4th Quarter
SY 20112012

Think-PairShare (An activities

Exercise 1 - 2

will be done by pair)

Prepared By:

Approved By:

Marilen M. Martin
Dean
Luz L.Lozano

Page 2 of 5

Week
3

COURSE
OUTCOMES
CO2

TOPIC

TLA
Independent
projects (A journal

Experiment No.1: Gravimetric Analysis

AT
Paper 1

report will be
prepared)

CO3

CO3

CO3

CO1, CO2

CO3

CO4

10
10.

Independent
projects (An activity

Paper 2

will be done by pair)

Independent
Paper 3
projects (the activity
will be done by pair)

Independent
Paper 4
projects (the activity
will be done by pair)

Independent
projects (The

Exam 1

activity will be done by


pair)

Independent
projects (The

Paper 5 - 6

activities will be done


by pair)

Independent
projects (The

Paper 7

activity will be done by


pair)

FINAL EXAM.

CO1, CO2,
CO3, CO4
Lifelong-Learning Opportunities

11.

Experiment No. 2: Preparation and


Standardization of Acid-Base Titrant
Solutions
Experiment No. 3: Preparation and
Standardization of Titrant Solutions
Application: Determination of Acid Content
in Commercially Available Products
Experiment No. 4: Determination of the
Components of a Base Mixture by the
Double Indicator Method
Experiment No. 5: Preparation and
Standardization of the EDTA Solution
Application: Determination of Water
Hardness using EDTA
Experiment 6: Preparation and
Standardization of the Potassium
Permanganate Solution
Application: Determination of Calcium in
Limestone
Experiment 7: Determination of Ionization
Constant of a Weak Acid by Potentiometric
Titration

The students will develop the ability to extract the best possible data from analytical instruments.
Contribution of Course to Meeting the Professional Component
Advanced Chemistry Topics - 90%
General Education - 10%

12.

Textbook
Skoog, D. A.; West, D. M.; Holler, F. J.; Crouch, S. R.; Chen, S.-C. Introduction to Analytical Chemistry,
Cengage Learning Asia Pte Ltd., 2011.

13.

Course Evaluation
Student performance will be rated based on the following:
Assessment Tasks
CO 1
CO 2
CO 3

Weight

Exam 1
Exercise 1 - 2
Exam 1
Paper 1
Paper 2

Course Title:
ANALYTICAL CHEMISTRY LABORATORY
1

Date
Effectivity:
1st Quarter
SY 20122013

5.00%
10.00%
5.00%
10.00%
10.00%
Date
Revised:
4th Quarter
SY 20112012

Minimum Average for


Satisfactory
Performance
65.00%
65.00%
65.00%
65.00%
65.00%
Prepared By:

Approved By:

Marilen M. Martin
Dean
Luz L.Lozano

Page 3 of 5

CO 4

Paper 3
Paper 4
Paper 5 - 6
Paper 7
Practical Exam 1
TOTAL

10.00%
10.00%
20.00%
10.00%
10.00%
100.00%

65.00%
65.00%
65.00%
65.00%
65.00%
65.00%

The final grades will correspond to the weighted average scores shown below
Average

Grade

Average

Grade

0 - 64.99

5.00

81.00 - 84.99

2.00

65.00 - 68.99

3.00

85.00 - 88.99

1.75

69.00 - 72.99

2.75

89.00 - 91.99

1.50

73.00 - 76.99

2.50

92.00 - 96.99

1.25

77.00 - 80.99

2.25

97.00 - 100.00

1.00

13.1.

Other Course Policies


a. Methodology 1
The laboratory notebook shall be checked and initialed by the instructor at the end of each
laboratory period. Analysis/Experimental results shall be graded based on accuracy, precision,
and performance. For each experiment, students are required to perform at least 4 trials for their
unknowns where they can apply a statistical treatment of their data in their analysis.
b. Methodology 2
According to CHED policy, total number of absences by the students should not be more than
20% of the total number of meetings or two meetings. Student incurring more than 2 meetings
of unexcused absences automatically gets a failing grade regardless of class standing.
c. Methodology 3
Attendance will be checked at 45th minute of each class. Anyone who is not in class at this time
will be marked absent.
d. Methodology 4
Lectures, discussions and class presentations will be in English. Written and spoken work may
receive a lower mark if it is, in the opinion of the instructor, deficient in English.
e. Methodology 5
All of us have been instructed on the Dress and Grooming Codes of the Institute. We have all
committed to obey and sustain these codes. It will be expected in this class that each of us will
honor the commitments that have made. In addition, everyone is expected to wear proper
laboratory gadgets such as laboratory gown or apron, gloves, mask, a pair of goggles, closed
shoes, hair properly tied up for ladies, and cleaning materials per group. Students that have
incomplete laboratory gadgets will not be allowed to perform the experiment.
f.

Methodology 6
Consultation schedules with the professors are posted outside the ChE-Chm Faculty room and
in the school web-page (http://che-chm.mapua.edu.ph). It is recommended that the student first
set an appointment to confirm the instructors availability.

g. Honor Codes
For this course, the Honor Code is that there will be no plagiarizing on written work and no
cheating on examinations. Proper citation must be given to authors whose works were used in
the process of developing instructional materials and learning for this course. If a student is
caught cheating on an exam, he/ she will be given a zero mark for that particular exam. If a
student is caught cheating for the second time, he/ she will be referred to the Prefect of Student
Affairs, the guidance Office and will be given a failing mark for the course.

Course Title:
ANALYTICAL CHEMISTRY LABORATORY
1

Date
Effectivity:
1st Quarter
SY 20122013

Date
Revised:
4th Quarter
SY 20112012

Prepared By:

Approved By:

Marilen M. Martin
Dean
Luz L.Lozano

Page 4 of 5

14.

Other References
14.1.

Books
Harvey, David. Modern Analytical Chemistry, International edition, McGraw-Hill International
Hargis, Larry G. Analytical Chemistry: Principles and Techniques, Prentice-Hall International, 1988;
Christian, Gary D. Analytical Chemistry, 6th edition, John Wiley and Sons, Ltd., 2004; &
Harris, Daniel. Quantitative Chemical Analysis, 5th edition.

15.

Course Materials
15.1.
15.2.
15.3.

16.

Course Syllabus
Course schedule
Laboratory Manual

Committee Members
CALDERON, EDNA (JAMORA)
CRUZ, KATHLIA (DE CASTRO)
ESPIRITU, ELIZABETH (S)
MARTIN, MARILEN (MERCADER)
MIRANDA, MARILYN (ABSULIO)
NG, JOSEPHINE (A)
SANTOS, NANETTE (D.)
SEVILLA, UREAH THEA (ANTONIO)
VELARDE, HOMER (C)

17.

CQI Remarks
The students must be able to get an average of at least 65.00% in order to pass the course.

Course Title:
ANALYTICAL CHEMISTRY LABORATORY
1

Date
Effectivity:
1st Quarter
SY 20122013

Date
Revised:
4th Quarter
SY 20112012

Prepared By:

Approved By:

Marilen M. Martin
Dean
Luz L.Lozano

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