Environmental
2.00
2
True
CERTIFICATE OF ANALYSIS
Work Order
Amendment
ES1503241
:2
Page
: 1 of 10
Client
Laboratory
Contact
: AARON HORNE
Contact
: Client Services
Address
: DUNHAVEN CIRCUIT
Address
: sydney@alsglobal.com
Telephone
: +61-2-8784 8555
Facsimile
: +61-2-8784 8500
QC Level
: 11-FEB-2015
Issue Date
: 20-FEB-2015
ST MARYS
SYDNEY NSW 2001
-------------------------
Telephone
Facsimile
Project
Order number
C-O-C number
Sampler
Site
Quote number
: ----
:1
:1
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for
release.
This Certificate of Analysis contains the following information:
l General Comments
l Analytical Results
l Surrogate Control Limits
NATA Accredited Laboratory 825
Accredited for compliance with
ISO/IEC 17025.
Signatories
This document has been electronically signed by the authorized signatories indicated below. Electronic signing has been
carried out in compliance with procedures specified in 21 CFR Part 11.
Signatories
Position
Accreditation Category
Pabi Subba
Sydney Organics
Address 277-289 Woodpark Road Smithfield NSW Australia 2164 | PHONE +61-2-8784 8555 | Facsimile +61-2-8784 8500
Environmental Division Sydney ABN 84 009 936 029 Part of the ALS Group An ALS Limited Company
Page
Work Order
Client
Project
:
:
:
:
2 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
General Comments
The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA,
developed procedures are employed in the absence of documented standards or by client request.
Where moisture determination has been performed, results are reported on a dry weight basis.
Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.
Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.
When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing purposes.
Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.
Key :
CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.
LOR = Limit of reporting
^ = This result is computed from individual analyte detections at or above the level of reporting
Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to
Benzo(a)pyrene. TEF values are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0),
Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0), Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero.
EP075: 'Sum of PAH' is the sum of the USEPA 16 priority PAHs
Page
Work Order
Client
Project
:
:
:
:
3 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
Compound
08-FEB-2015 15:00
----
----
----
----
LOR
Unit
ES1503241-001
----
----
----
----
71-43-2
g/L
<1
----
----
----
----
108-88-3
g/L
----
----
----
----
100-41-4
g/L
<2
----
----
----
----
108-38-3 106-42-3
g/L
<2
----
----
----
----
CAS Number
100-42-5
g/L
<5
----
----
----
----
ortho-Xylene
95-47-6
g/L
<2
----
----
----
----
Isopropylbenzene
98-82-8
g/L
<5
----
----
----
----
n-Propylbenzene
103-65-1
g/L
<5
----
----
----
----
1.3.5-Trimethylbenzene
108-67-8
g/L
<5
----
----
----
----
sec-Butylbenzene
135-98-8
g/L
<5
----
----
----
----
1.2.4-Trimethylbenzene
95-63-6
g/L
<5
----
----
----
----
tert-Butylbenzene
98-06-6
g/L
<5
----
----
----
----
p-Isopropyltoluene
99-87-6
g/L
<5
----
----
----
----
104-51-8
g/L
<5
----
----
----
----
108-05-4
50
g/L
<50
----
----
----
----
g/L
<50
----
----
----
----
Styrene
n-Butylbenzene
78-93-3
50
4-Methyl-2-pentanone (MIBK)
108-10-1
50
g/L
<50
----
----
----
----
2-Hexanone (MBK)
591-78-6
50
g/L
<50
----
----
----
----
75-15-0
g/L
<5
----
----
----
----
2.2-Dichloropropane
594-20-7
g/L
<5
----
----
----
----
1.2-Dichloropropane
78-87-5
g/L
<5
----
----
----
----
cis-1.3-Dichloropropylene
10061-01-5
g/L
<5
----
----
----
----
trans-1.3-Dichloropropylene
10061-02-6
g/L
<5
----
----
----
----
106-93-4
g/L
<5
----
----
----
----
Dichlorodifluoromethane
75-71-8
50
g/L
<50
----
----
----
----
Chloromethane
74-87-3
50
g/L
<50
----
----
----
----
Vinyl chloride
75-01-4
50
g/L
<50
----
----
----
----
Bromomethane
74-83-9
50
g/L
<50
----
----
----
----
Chloroethane
75-00-3
50
g/L
<50
----
----
----
----
2-Butanone (MEK)
EP074D: Fumigants
1.2-Dibromoethane (EDB)
Page
Work Order
Client
Project
:
:
:
:
4 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
Compound
08-FEB-2015 15:00
----
----
----
----
LOR
Unit
ES1503241-001
----
----
----
----
75-69-4
50
g/L
<50
----
----
----
----
75-35-4
g/L
<5
----
----
----
----
74-88-4
g/L
<5
----
----
----
----
156-60-5
g/L
<5
----
----
----
----
CAS Number
75-34-3
g/L
<5
----
----
----
----
156-59-2
g/L
<5
----
----
----
----
1.1.1-Trichloroethane
71-55-6
g/L
<5
----
----
----
----
1.1-Dichloropropylene
563-58-6
g/L
<5
----
----
----
----
Carbon Tetrachloride
56-23-5
g/L
<5
----
----
----
----
107-06-2
g/L
<5
----
----
----
----
Trichloroethene
79-01-6
g/L
<5
----
----
----
----
Dibromomethane
74-95-3
g/L
<5
----
----
----
----
1.1.2-Trichloroethane
79-00-5
g/L
<5
----
----
----
----
1.3-Dichloropropane
142-28-9
g/L
<5
----
----
----
----
Tetrachloroethene
127-18-4
g/L
<5
----
----
----
----
1.1.1.2-Tetrachloroethane
630-20-6
g/L
<5
----
----
----
----
110-57-6
g/L
<5
----
----
----
----
1476-11-5
g/L
<5
----
----
----
----
79-34-5
g/L
<5
----
----
----
----
1.2.3-Trichloropropane
96-18-4
g/L
<5
----
----
----
----
Pentachloroethane
76-01-7
g/L
<5
----
----
----
----
1.2-Dibromo-3-chloropropane
96-12-8
g/L
<5
----
----
----
----
1.1-Dichloroethane
cis-1.2-Dichloroethene
1.2-Dichloroethane
trans-1.4-Dichloro-2-butene
cis-1.4-Dichloro-2-butene
1.1.2.2-Tetrachloroethane
108-90-7
g/L
<5
----
----
----
----
Bromobenzene
108-86-1
g/L
<5
----
----
----
----
2-Chlorotoluene
95-49-8
g/L
<5
----
----
----
----
4-Chlorotoluene
106-43-4
g/L
<5
----
----
----
----
87-61-6
g/L
<5
----
----
----
----
67-66-3
g/L
<5
----
----
----
----
75-27-4
g/L
<5
----
----
----
----
124-48-1
g/L
<5
----
----
----
----
75-25-2
g/L
<5
----
----
----
----
1.2.3-Trichlorobenzene
EP074G: Trihalomethanes
Chloroform
Bromodichloromethane
Dibromochloromethane
Bromoform
Page
Work Order
Client
Project
:
:
:
:
5 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
08-FEB-2015 15:00
----
----
----
----
ES1503241-001
----
----
----
----
Compound
LOR
Unit
108-95-2
g/L
<2
----
----
----
----
95-57-8
g/L
<2
----
----
----
----
95-48-7
g/L
<2
----
----
----
----
1319-77-3
g/L
14
----
----
----
----
CAS Number
88-75-5
g/L
<2
----
----
----
----
2.4-Dimethylphenol
105-67-9
g/L
<2
----
----
----
----
2.4-Dichlorophenol
120-83-2
g/L
<2
----
----
----
----
2.6-Dichlorophenol
87-65-0
g/L
<2
----
----
----
----
4-Chloro-3-methylphenol
59-50-7
g/L
<2
----
----
----
----
2.4.6-Trichlorophenol
88-06-2
g/L
<2
----
----
----
----
2.4.5-Trichlorophenol
95-95-4
g/L
<2
----
----
----
----
Pentachlorophenol
87-86-5
g/L
<4
----
----
----
----
91-20-3
g/L
<2
----
----
----
----
91-57-6
g/L
<2
----
----
----
----
91-58-7
g/L
<2
----
----
----
----
g/L
<2
----
----
----
----
2-Nitrophenol
208-96-8
Acenaphthene
83-32-9
g/L
<2
----
----
----
----
Fluorene
86-73-7
g/L
<2
----
----
----
----
Phenanthrene
85-01-8
g/L
<2
----
----
----
----
Anthracene
120-12-7
g/L
<2
----
----
----
----
Fluoranthene
206-44-0
g/L
<2
----
----
----
----
Pyrene
129-00-0
g/L
<2
----
----
----
----
N-2-Fluorenyl Acetamide
53-96-3
g/L
<2
----
----
----
----
Benz(a)anthracene
56-55-3
g/L
<2
----
----
----
----
218-01-9
g/L
<2
----
----
----
----
205-99-2 207-08-9
g/L
<4
----
----
----
----
7.12-Dimethylbenz(a)anthracene
57-97-6
g/L
<2
----
----
----
----
Benzo(a)pyrene
50-32-8
g/L
<2
----
----
----
----
3-Methylcholanthrene
56-49-5
g/L
<2
----
----
----
----
Indeno(1.2.3.cd)pyrene
193-39-5
g/L
<2
----
----
----
----
Dibenz(a.h)anthracene
53-70-3
g/L
<2
----
----
----
----
191-24-2
g/L
<2
----
----
----
----
Acenaphthylene
Chrysene
Benzo(b+j) &
Benzo(k)fluoranthene
Benzo(g.h.i)perylene
Page
Work Order
Client
Project
:
:
:
:
6 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
08-FEB-2015 15:00
----
----
----
----
ES1503241-001
----
----
----
----
Compound
CAS Number
LOR
Unit
----
g/L
<2
----
----
----
----
----
g/L
<2
----
----
----
----
g/L
<2
----
----
----
----
Diethyl phthalate
84-66-2
g/L
<2
----
----
----
----
Di-n-butyl phthalate
84-74-2
g/L
<2
----
----
----
----
85-68-7
g/L
<2
----
----
----
----
117-81-7
10
g/L
<10
----
----
----
----
117-84-0
g/L
<2
----
----
----
----
10595-95-6
g/L
<2
----
----
----
----
55-18-5
g/L
<2
----
----
----
----
N-Nitrosopyrrolidine
930-55-2
g/L
<4
----
----
----
----
N-Nitrosomorpholine
59-89-2
g/L
<2
----
----
----
----
N-Nitrosodi-n-propylamine
621-64-7
g/L
<2
----
----
----
----
N-Nitrosopiperidine
100-75-4
g/L
<2
----
----
----
----
N-Nitrosodibutylamine
924-16-3
g/L
<2
----
----
----
----
86-30-6 122-39-4
g/L
<4
----
----
----
----
91-80-5
g/L
<2
----
----
----
----
Dimethyl phthalate
bis(2-ethylhexyl) phthalate
Di-n-octylphthalate
EP075D: Nitrosamines
N-Nitrosomethylethylamine
N-Nitrosodiethylamine
N-Nitrosodiphenyl &
Diphenylamine
Methapyrilene
g/L
<2
----
----
----
----
Acetophenone
98-86-2
g/L
<2
----
----
----
----
Nitrobenzene
98-95-3
g/L
<2
----
----
----
----
Isophorone
78-59-1
g/L
<2
----
----
----
----
2.6-Dinitrotoluene
606-20-2
g/L
<4
----
----
----
----
2.4-Dinitrotoluene
121-14-2
g/L
<4
----
----
----
----
134-32-7
g/L
<2
----
----
----
----
56-57-5
g/L
<2
----
----
----
----
99-55-8
g/L
<2
----
----
----
----
103-33-3
g/L
<2
----
----
----
----
1.3.5-Trinitrobenzene
99-35-4
g/L
<2
----
----
----
----
Phenacetin
62-44-2
g/L
<2
----
----
----
----
2-Picoline
1-Naphthylamine
4-Nitroquinoline-N-oxide
5-Nitro-o-toluidine
Azobenzene
Page
Work Order
Client
Project
:
:
:
:
7 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
08-FEB-2015 15:00
----
----
----
----
ES1503241-001
----
----
----
----
Compound
LOR
Unit
92-67-1
g/L
<2
----
----
----
----
82-68-8
g/L
<2
----
----
----
----
23950-58-5
g/L
<2
----
----
----
----
60-11-7
g/L
<2
----
----
----
----
510-15-6
g/L
<2
----
----
----
----
CAS Number
EP075F: Haloethers
Bis(2-chloroethyl) ether
111-44-4
g/L
<2
----
----
----
----
Bis(2-chloroethoxy) methane
111-91-1
g/L
<2
----
----
----
----
7005-72-3
g/L
<2
----
----
----
----
101-55-3
g/L
<2
----
----
----
----
541-73-1
g/L
<2
----
----
----
----
106-46-7
g/L
<2
----
----
----
----
95-50-1
g/L
<2
----
----
----
----
67-72-1
g/L
<2
----
----
----
----
120-82-1
g/L
<2
----
----
----
----
Hexachloropropylene
1888-71-7
g/L
<2
----
----
----
----
Hexachlorobutadiene
87-68-3
g/L
<2
----
----
----
----
Hexachlorocyclopentadiene
77-47-4
10
g/L
<10
----
----
----
----
Pentachlorobenzene
608-93-5
g/L
<2
----
----
----
----
Hexachlorobenzene (HCB)
118-74-1
g/L
<4
----
----
----
----
g/L
<2
----
----
----
----
106-47-8
g/L
<2
----
----
----
----
2-Nitroaniline
88-74-4
g/L
<4
----
----
----
----
3-Nitroaniline
99-09-2
g/L
<4
----
----
----
----
Dibenzofuran
132-64-9
g/L
<2
----
----
----
----
100-01-6
g/L
<2
----
----
----
----
86-74-8
g/L
<2
----
----
----
----
91-94-1
g/L
<2
----
----
----
----
alpha-BHC
319-84-6
g/L
<2
----
----
----
----
beta-BHC
319-85-7
g/L
<2
----
----
----
----
Aniline
4-Chloroaniline
4-Nitroaniline
Carbazole
3.3`-Dichlorobenzidine
Page
Work Order
Client
Project
:
:
:
:
8 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
08-FEB-2015 15:00
----
----
----
----
ES1503241-001
----
----
----
----
LOR
Unit
58-89-9
g/L
<2
----
----
----
----
319-86-8
g/L
<2
----
----
----
----
76-44-8
g/L
<2
----
----
----
----
309-00-2
g/L
<2
----
----
----
----
1024-57-3
g/L
<2
----
----
----
----
959-98-8
g/L
<2
----
----
----
----
4.4`-DDE
72-55-9
g/L
<2
----
----
----
----
Dieldrin
60-57-1
g/L
<2
----
----
----
----
Endrin
72-20-8
g/L
<2
----
----
----
----
33213-65-9
g/L
<2
----
----
----
----
72-54-8
g/L
<2
----
----
----
----
1031-07-8
g/L
<2
----
----
----
----
50-29-3
g/L
<4
----
----
----
----
309-00-2/60-57-1
g/L
<4
----
----
----
----
----
g/L
<4
----
----
----
----
62-73-7
g/L
<2
----
----
----
----
60-51-5
g/L
<2
----
----
----
----
Compound
CAS Number
beta-Endosulfan
4.4`-DDD
Endosulfan sulfate
4.4`-DDT
333-41-5
g/L
<2
----
----
----
----
5598-13-0
g/L
<2
----
----
----
----
Malathion
121-75-5
g/L
<2
----
----
----
----
Fenthion
55-38-9
g/L
<2
----
----
----
----
2921-88-2
g/L
<2
----
----
----
----
23505-41-1
g/L
<2
----
----
----
----
470-90-6
g/L
<2
----
----
----
----
34643-46-4
g/L
<2
----
----
----
----
563-12-2
g/L
<2
----
----
----
----
Diazinon
Chlorpyrifos-methyl
Chlorpyrifos
Pirimphos-ethyl
Chlorfenvinphos
Prothiofos
Ethion
17060-07-0
0.1
83.1
----
----
----
----
2037-26-5
0.1
103
----
----
----
----
460-00-4
0.1
91.8
----
----
----
----
367-12-4
0.1
36.3
----
----
----
----
Page
Work Order
Client
Project
:
:
:
:
9 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Analytical Results
Client sample ID
DUNHEVED CRT
ST MARY'S
----
----
----
----
08-FEB-2015 15:00
----
----
----
----
ES1503241-001
----
----
----
----
Compound
CAS Number
LOR
Unit
13127-88-3
0.1
24.6
----
----
----
----
93951-73-6
0.1
42.0
----
----
----
----
118-79-6
0.1
62.7
----
----
----
----
4165-60-0
0.1
47.5
----
----
----
----
1.2-Dichlorobenzene-D4
2199-69-1
0.1
44.2
----
----
----
----
2-Fluorobiphenyl
321-60-8
0.1
38.2
----
----
----
----
Anthracene-d10
1719-06-8
0.1
59.7
----
----
----
----
4-Terphenyl-d14
1718-51-0
0.1
59.1
----
----
----
----
Page
Work Order
Client
Project
:
:
:
:
10 of 10
ES1503241 Amendment 2
SOUTH CREEK COMMUNITY BASS CLUB
----
Compound
CAS Number
Low
High
17060-07-0
78.3
133.2
2037-26-5
79.1
128.9
460-00-4
80.8
123.7
116.6
10.0
Phenol-d6
13127-88-3
10.0
69.0
2-Chlorophenol-D4
93951-73-6
20.9
129.7
118-79-6
10.0
150.7
Nitrobenzene-D5
4165-60-0
29.4
141.7
1.2-Dichlorobenzene-D4
2199-69-1
23.6
120.7
2-Fluorobiphenyl
321-60-8
27.2
134.9
Anthracene-d10
1719-06-8
26.6
113
4-Terphenyl-d14
1718-51-0
21.4
123
2-Fluorophenol
2.4.6-Tribromophenol