a r t i c l e
i n f o
Article history:
Received 1 November 2010
Received in revised form 15 March 2011
Accepted 11 April 2011
Available online 4 May 2011
Keywords:
Self-compacting lightweight concrete
Expanded polystyrene aggregate
Hauling time
Workability
Nano-SiO2
a b s t r a c t
This paper presents the fresh properties of structural self-compacted lightweight concrete (SCLC) containing expanded polystyrene (EPS) assessed by means of slump ow, T50, V-funnel and L-box tests. Fifteen mixes including different water/binder (W/B) ratios, nano-SiO2 contents and EPS percentages (10%,
15%, 22.5% and 30% by volume) were designed. The change in slump ow by hauling time was also evaluated and was predicted with multiple regression equations.
The results indicate that mixtures with density higher than 1900 kg/m3 (up to 22.5% EPS) generally satisfy the self-compactibility criteria of SCLC containing EPS. The nano-SiO2 addition has some negative
effects on the fresh self-compacted concrete (SCC), but this is to be less for EPS mixtures. While, the
slump ow of SCLC containing EPS decreased up to 6% by reducing the given W/B ratio, T50 and V-funnel
times increased in the ranges of 2329% and 1848%, respectively. EPS inclusion in SCC shows an increase
in the slump ow retention up to 17%. Additionally, by using nonlinear multiple regression, the slump
ow with hauling time can be accurately predicted.
2011 Elsevier Ltd. All rights reserved.
1. Introduction
The traditional vibrated concrete produces differential compaction and hence differential durability. This aspect coupled with
shortage of skilled workmen and noisy nature of vibrated concrete
were the factors which forced to develop a new type of high performance concrete, namely self-compacted concrete (SCC). The main
requirements of fresh SCC are lling ability, passing ability and
very high segregation resistance. SCC contains powder material
as constituent in addition to the traditional concrete materials.
Therefore, in general, the density of SCC seems to be higher than
the density of normal concrete [1,2].
Use of lightweight aggregates in the production of concrete can
decrease the self-weight of structures. This can result in reduced
members sections and, therefore, it will save on overall construction costs. Lightweight aggregates are generally classied either as
natural or articial. Expanded polystyrene (EPS) beads are a type of
articial ultra-lightweight non-absorbent aggregate [3]. Polystyrene is a thermoplastic polymeric material initially in the solid
form and it can be expanded by the use of steam and expansive
agents transform to EPS beads. EPS aggregates are commercially
available worldwide and have a closed cell structure consisting
essentially of 98% air.
3722
and Babu [4,6]. Regarding to extremely lightweight and hydrophobic nature of EPS aggregates, it tends to oat. This can result in a
poor mix distribution and segregation, necessitating the use of
bonding additives [12]. Chen and Liu [9] showed that incorporating
ne silica fume, instead of bonding additives can improve the dispersion of EPS in the matrix and the interfacial bonding strength.
Furthermore, an experimental investigation and modeling were
conducted by Miled et al. [13] to evaluate the effect of particle sizes
on the compressive strength of EPS concrete. The compressive
strength of lightweight concrete containing EPS has been reported
to be higher than those obtained for vermiculite or perlite concrete
[14], but still its strength gain is a main objective which must be
considered for structural lightweight concrete. This weakness of
EPS aggregates can be compensated either by reducing W/B ratio
or using advanced nanotechnology development such as nanoSiO2 considered in this study. These procedures which increase
the compressive strength, can mainly affect the workability of
the cement matrix. So, the secondary objective of this study is to
nd the effect of these two procedures on the workability of SCLC
containing EPS aggregates.
Nano-SiO2 is recently receiving special attention because of its
better performance when compared with traditional mineral additions. Qing et al. [15] reported that the compressive strength of
hardened cement paste and bond strength of pasteaggregate
interface containing nano-SiO2 were remarkably higher than those
obtained for mixtures containing silica fume, especially at early
ages. Jo et al. [16] reported that the addition of nano-SiO2 behaves
as an activator to promote pozzolanic reaction. Li [17] found that
nano-SiO2 can enhance both short-term and long-term strengths
of high-strength concrete containing high-volume y ash. Ji [18]
indicated that with nano-SiO2 addition, the water permeability
resistant capacity of concrete can be improved. At the fresh-state
point of view, Senff et al. [19] reported that nano-SiO2 addition
leads to lower fresh apparent density. Their results also concluded
that nano-SiO2 addition reduces the setting time and the beginning
of the acceleration period of cement hydration. Diamantonis et al.
[20] evaluated the effect of nano-SiO2 as additives on the viscosity
of SCC. This study focused on the performance of nano-SiO2 on
SCLC containing EPS as the available information is not adequate
in this area.
To attain the scopes of this study, the characterization of SCLC
containing EPS was evaluated at fresh-state. Several tests such as
slump ow, T50, visual segregation index (VSI), V-funnel and
L-box were conducted to assess the workability of the matrix. To
simulate the real-world applications, the slump ow values were
measured at different hauling times. Furthermore, linear and nonlinear regression analysis has been carried out to predict how
slump ow changes with hauling time.
2. Experimental plan
2.1. Materials
Type I ordinary Portland cement complying with the requirement of ASTM C
150 was used. Silica fume was used to improve segregation resistance. Nano-SiO2
with 1.3 g/cm3 density has been used in this study. The chemical compositions
and physical properties of cement, silica fume and nano-SiO2 are given in Table 1.
Two types of commercial spherical EPS were used as replacement of ne and coarse
aggregates equally at required volume percentages. River sand with neness modulus of 2.83 and crushed gravel were used as natural aggregates. Fine and coarse
aggregate properties are shown in Table 2. Polycarboxylic ether based high range
water reducer (HRWR) namely Glenium51 with density between 1.06 and 1.08 g/
cm3 (at 20 C) was used to enhance the owability of the mixtures.
2.2. Mixture proportion
The SCLC mixtures were designed in three groups which dened as G1, G2 and
G3. In the rst concrete group (G1), the W/B ratio was 0.44 and no nano-SiO2 was
employed. To keep slump ow in a desired range, HRWR dosage was adjusted from
Table 1
Chemical composition and physical properties of ordinary Portland cement, silica
fume and nano-SiO2.
Cement
Silica fume
Nano-SiO2
21.46
5.55
3.46
63.95
1.86
1.42
0.54
0.26
91.7
1
0.9
1.68
1.8
0.87
0.1
2
99.9
0.1
Physical properties
Specic gravity
Specic surface (m2/g)
Particle size
3.15
0.33
13 (lm)
2.12
20
0.1 (lm)
160
15 (nm)
2.5 to 4 kg/m3. The natural aggregates were partially replaced with EPS aggregates
with 10%, 15%, 22.5% and 30% by volume in order to produce structural SCLC having
compressive strength above 17 MPa. This range was established to meet these
requirements on the basis of preliminary studies. In the case of second concrete
group (G2), the W/B ratio was 0.44 and nano-SiO2 was replaced 2.7% by weight
of the total cementitious materials. To assess the effect of nano-SiO2 on the fresh
SCLC, the HRWR and EPS contents were considered to be the same as the rst concrete group. In the third concrete group (G3), the W/B ratio was 0.38 and no nanoSiO2 was employed. The W/B ratio was adjusted to obtain a similar strength compared to G2 group. The HRWR and EPS contents were the same as that used for
G1 group.
Considering the above groups, totally fteen mixes were presented in Table 3 in
which silica fume was replaced 10% by weight of the total cementitious materials.
Silica fume was considered as additive in order to improve the bonding between
EPS and the cement paste and to ensure proper resistance to segregation.
For mix preparation, similar procedure established by Khayat et al. [21] for SCC
was used in this study. In this way, natural coarse and ne aggregates followed by
EPS aggregates were homogenized for 30 s at normal mixing speed (about 18 rpm).
Thereafter, adding about half of the mixing water into the mixer while mixing goes
on for 1 min. The mixture was rested for 1 min so that the aggregates could absorb
the water in the mixer. Then, binder materials including cement and silica fume
were added and mixed for one more minute. The remaining water and HRWR were
introduced to the wet mixture, while mixing was going on for 3 min. Finally, after
2 min resting, mixing sequence resumed for additional 2 min. This optimum time is
necessary to disperse HRWR and stabilize viscosity. It should be emphasized that
for mixes containing nano-SiO2 (G2), the HRWR was dissolved in water and then
nano-SiO2 was added and stirred at a high speed for 2 min and subsequently were
introduced to the mixtures.
3723
Fine aggregates
Sieve opening
Gradation
1/2 in. (12.5 mm)
3/8 in. (9.5 mm)
No. 4 (4.75 mm)
No. 8 (2.36 mm)
No. 16 (1.18 mm)
No. 30 (600 lm)
No. 50 (300 lm)
No. 100 (150 lm)
Maximum nominal size (mm)
Specic gravity
Bulk density (kg/m3)
Water absorption (%)
Coarse aggregates
River sand
EPS (type I)
Crushed gravel
96
82.4
68.2
42.5
20.7
6.9
4.75
2.65
1567
1.3
96
4
0
0
0
0
4.75
0.025
13.6
92.5
54.8
2.7
12.5
2.75
1638
0.78
100
100
0
0
0
0
0
0
9.5
0.018
10.4
Table 3
Mix details of EPS concrete.
Mix group
Mix ID
Cement
(kg/m3)
SF
(kg/m3)
G1
SCCM
SCLCM10
SCLCM15
SCLCM22.5
SCLCM30
400
400
400
400
400
44
44
44
44
44
G2
SCCN
SCLCN10
SCLCN15
SCLCN22.5
SCLCN30
388
388
388
388
388
G3
SCCH
SCLCH10
SCLCH15
SCLCH22.5
SCLCH30
434
434
434
434
434
Nano-SiO2
(kg/m3)
Water
(kg/m3)
Total aggregates
(kg/m3)
Gravel
(kg/m3)
Sand
(kg/m3)
EPS volume
(%)
HRWR
(kg/m3)
196
196
196
196
196
1715
1445
1310
1108
904
800
662
594
491
387
915
783
716
617
517
0
10
15
22.5
30
4.0
3.5
3.2
2.8
2.5
44
44
44
44
44
12
12
12
12
12
196
196
196
196
196
1715
1445
1310
1108
904
800
662
594
491
387
915
783
716
617
517
0
10
15
22.5
30
4.0
3.5
3.2
2.8
2.5
48
48
48
48
48
183
183
183
183
183
1715
1445
1310
1108
904
800
662
594
491
387
915
783
716
617
517
0
10
15
22.5
30
4.0
3.5
3.2
2.8
2.5
Table 4
Slump ow, viscosity and passing ability classes with respect to EFNARC [22].
Class
Slump ow (mm)
Slump ow classes
SF1
SF2
SF3
550650
660750
760850
Class
Viscosity classes
VS1/VF1
VS2/VF2
Passing ability classes
PA1
PA2
T50 (s)
62
>2
68
925
tom gate is opened. The time takes by fresh concrete to ow out of the funnel was
measured and recorded as the V-funnel time. On the basis of EFNARC [22], there are
two viscosity classes which determined by V-funnel and T50 ow times (Table 4).
The V-funnel test was also used to describe the stability of SCC as well as viscosity
assessment.
The L-box test is utilized to determine passing ability of SCC when owing
through conned or reinforced areas. The L-box test consists of an L-shaped apparatus in which the vertical part is lled with 12 L of concrete without any compaction. A gate between the horizontal and vertical parts of the L-box is lifted up and
the concrete passed through three 12 mm-diameter steel bars separated by 40 mm
clear spacing. The ratio of the height of concrete remaining at the leading edge in
the horizontal section to that in the vertical section h2/h1 is an indication of the
passing ability of concrete through obstacles. The passing ability classications
according to EFNARC [22] were presented in Table 4.
To assess the 28-days compressive strength development, mixtures were cast in
the 100 mm cubic molds. The specimens were demolded after 24 h of casting and
standard water curing regime were applied until the testing day.
3724
Table 5
Workability test results after mixing.
Mix group
Mix ID
Slump ow (mm)
T50 (s)
V-funnel (s)
Eyes observation
G1
SCCM
SCLCM10
SCLCM15
SCLCM22.5
SCLCM30
0
10
15
22.5
30
2424
2185
2040
1896
1712
645
650
645
660
680
2.0
2.1
2.2
2.3
2.4
6.2
8.0
9.5
11.8
13.6
0.92
0.95
0.90
0.90
0.83
No segregation
No segregation
No segregation
No segregation
Slight segregation
G2
SCCN
SCLCN10
SCLCN15
SCLCN22.5
SCLCN30
0
10
15
22.5
30
2392
2187
2105
1898
1701
620
615
625
640
660
2.5
2.5
2.5
2.6
2.8
8.2
10.7
12.2
14.2
15.7
0.89
0.93
0.88
0.87
0.81
No
No
No
No
No
segregation
segregation
segregation
segregation
segregation
G3
SCCH
SCLCH10
SCLCH15
SCLCH22.5
SCLCH30
0
10
15
22.5
30
2518
2235
2077
1919
1748
600
610
615
630
640
2.6
2.6
2.7
2.9
3.1
10.9
11.7
14.1
14.9
16.1
0.87
0.89
0.88
0.81
0.78
No
No
No
No
No
segregation
segregation
segregation
segregation
segregation
700
4.5
Slump flow (G1,W/B=0.44,NS=0)
Slump flow (G2,W/B=0.44,NS=12)
680
3.5
640
620
2.5
600
10%
15%
22.50%
660
HRWR (kg/m )
HRWR
2
30%
EPS in vol.
Fig. 2. Variation of slump ow and HRWR vs. EPS volume for different concrete groups.
decreasing the free water. Therefore, there is a higher internal friction which resulted in decreasing the owability. However, the
same pattern was not reported by Maghsoudi and Arabpour [27].
Nevertheless, this reduction was found to be lower for mixes containing EPS.
For similar EPS content, the slump ow of mixes increased with
increasing W/B ratio, as seen in Fig. 2. This may be due to the increase in the lubrication between the ne particles which resulted
in reducing the yielding stress and better owability.
In Fig. 3, the relative slump ow vs. EPS content is presented for
all groups. Although the slump ow for G2 and G3 groups are lower than G1group, it is clearly shown that the inuence of W/B ratio
to be more detrimental than the addition of nano-SiO2 on slump
ow reduction.
3.2. Slump ow retention
The elapsed time from the rst contact of water and cement to
the time when concrete is placed is described as hauling time
[28]. The slump ow changes were measured at four hauling times
of 15, 25, 35 and 45 min. The results were compared with slump
3725
108
G1
G2
G3
104
100
96
92
88
84
10%
15%
22.50%
30%
EPS in vol.
Fig. 3. Relative slump ow vs. EPS in vol.
700
w/b=0.44, NS=0
w/b=0.44, NS=12
w/b=0.38, NS=0
650
600
550
500
450
400
10
15
20
25
30
35
40
45
50
700
650
600
550
500
450
SCCM
400
10
SCLCM10
15
SCLCM15
20
25
SCLCM22.5
30
35
SCLCM30
40
45
50
3726
700
650
600
550
500
450
400
SCCN
SCLCN10
10
15
SCLCN15
20
25
SCLCN22.5
SCLCN30
30
40
35
45
50
700
650
600
550
500
450
400
SCCH
SCLCH10
10
15
SCLCH15
20
25
SCLCH22.5
30
35
SCLCH30
40
45
50
700
SF = 838.68T
650
-0.1368
R = 0.6305
600
550
500
450
400
10
15
20
25
30
35
40
45
50
3727
mixtures with lower W/B ratio (G3 group) indicate a higher plastic
viscosity.
1:681 EPS
R2
LMRT
Training
Testing
0.909
0.901
2.71
2.86
5.84
9.05
NLMRT
Training
Testing
0.947
0.914
1.99
2.73
4.27
5.22
For each concrete mixture, segregation and bleeding were visually inspected during the slump ow test. Generally, after mixing, a
VSI of 0 or 1 (stable matrix) were attained for all mixes except for
SCLCM30 in G1 group. For this mix, segregation of EPS due to buoyancy was detected on the surface of concrete (Fig. 11). In addition,
due to low plastic viscosity of this mix, EPS segregation was also
detected near the edges of the spread-out concrete. This segregation can be reduced either by applying nano-SiO2 or by lowering
W/B ratio.
3.5. V-funnel test
The effect of EPS on slump ow and V-funnel time are illustrated in Figs. 1214. From these gures, it can be seen that the
V-funnel time for different concrete groups were in the range of
6.216.1 s. For all concrete groups, the greater EPS volume, the
longer V-funnel time was recorded. For instance, SCCM had a Vfunnel time of 6.2 s which increased to 13.6 s as EPS introduced
up to 30% by volume. By increasing the EPS percentage, the unit
weight will decrease. Hence, the self-compactibility of concrete
cannot be achieved completely by its dead weight which will be resulted a higher V-funnel time [36]. A similar conclusion was also
observed by other researchers. Kim et al. [24] reported that the
V-funnel time was mostly increased to some extent when natural
coarse aggregates were replaced by lightweight aggregates. Choi
et al. [25] also showed that the V-funnel times increased with
increasing the proportion of lightweight ne aggregates. As evident
from Figs. 12 and 13, the incorporation of nano-SiO2 increased the
V-funnel times of the SCLC containing EPS. Regarding the effect of
W/B ratio, the V-funnel times of G3 mixes group (W/B = 0.38) are
about 1848% higher than that of G1 group (W/B = 0.44) depending
on the EPS content. Similar tendency has been reported by Felekoglu et al. [23] for SCC.
750
2
700
650
600
550
500
450
450
500
550
600
650
700
750
3728
750
Training data set, R2=0.947
Testing data set, R2=0.914
700
650
600
550
500
450
450
500
550
600
650
700
750
690
18
670
16
V-funnel time
14
650
12
630
10
8
610
590
6
0
10%
15%
22.50%
30%
EPS in vol.
Fig. 12. Variation of EPS vol. on slump ow and V-funnel time for G1.
Slump flow
3729
670
18
Slump flow
16
V-funnel time
14
650
12
630
10
610
590
570
6
0
10%
15%
22.50%
30%
690
EPS in vol.
Fig. 13. Variation of EPS vol. on slump ow and V-funnel time for G2.
690
16
V-funnel time
650
14
630
12
610
10
590
570
550
10%
15%
22.50%
30%
670
18
Slump flow
EPS in vol.
Fig. 14. Variation of EPS vol. on slump ow and V-funnel time for G3.
SCLCH30 (G3)
SCLCH22.5 (G3)
SCLCH15 (G3)
SCLCH10 (G3)
SCCH (G3)
SCLCN30 (G2)
SCLCN22.5 (G2)
SCLCN15 (G2)
SCLCN10 (G2)
SCCN (G2)
SCLCM30 (G1)
SCLCM22.5 (G1)
SCLCM15 (G1)
SCLCM10 (G1)
SCCM (G1)
0.7
0.75
0.8
0.85
0.9
0.95
Blocking ratio
Fig. 15. Blocking ratio of different mixes.
17 MPa) was achieved for all mixes. The increase in the EPS content
results in a signicant reduction in compressive strength for all
3730
60
50
G1
G2
G3
40
30
20
10
0
10%
15%
22.50%
30%
EPS in vol.
Fig. 16. Compressive strength of different concrete groups.
sults. But, its inuence turned out to be lower as EPS aggregate was
introduced.
3.8. Acceptance criterion of self-compactibility of SCLC containing EPS
There is yet no fully recognized standard for characterization of
fresh SCC, especially for SCLC. Nonetheless, some specications
were employed in literatures [2426]. On the basis of the authors
own experience, the following criteria for satisfactory self-compacting behavior may be adopted for SCLC with EPS.
3.8.1. Slump ow
Mixes with slump ow values between 600 and 660 mm were
accepted. These values are mostly within the EFNARC criteria class
1. Mixtures with a slump ow higher than this criterion show a
sign of segregation.
3.8.2. T50
Mixtures with a T50 time higher than 2 s can be considered as an
acceptable for SCLC design containing EPS. Most of the mixtures
fulll EFNARC VS2 specications.
3.8.3. V-funnel
In some technical literature [11,2426], the V-funnel times of
SCLC were restricted based on EFNARC or JSCE specications. However, the results of this study concluded that it was not possible to
restrict the V-funnel time into limited values to produce a selfcompactable and stable SCLC containing EPS. For instance, the Vfunnel time of 16.1 s is enough for SCLCH30 with W/B = 0.38 to attain stable mixture. While, the V-funnel time of 13.6 s for SCLCM30
with W/B = 0.44 is not enough. It should be remembered that these
results satisfy the requirements specied by EFNARC VF2 or JSCE
R2.
3.8.4. L-box
Mixtures with L-box ratios between 0.8 and 1 appear to be
acceptable. These values are within the EFNARC criteria PA2. Based
on this judgement, SCLCH30 concerning to G3 group was rejected.
In general, the mixtures with density higher than 1900 kg/m3
(up to 22.5% of EPS by vol.) satisfy the fresh-state behavior requirements related to high segregation resistance, deformability, passing and lling abilities. Moreover, by applying the nano-SiO2, all
structural SCLC containing EPS with density below 1900 kg/m3
may be accepted.
4. Conclusion
In this paper the fresh properties of SCLC containing EPS aggregates were evaluated and the following conclusions can be drawn:
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