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Experiment:

Date:

Gas Chromatography: Distillate


Name

Katheryn Soto
Purpose:

Partners

10/22/25
Drawer No.

Course / Section

CHEM
315/204

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

Katheryn Soto

Course / Section

CHEM
315/204

Approach:

References
Text
Pavia, D.L., Lampman, G.M., Kriz, G.S., Engel, .G.R., 2011, Introduction to Organic Laboratory
Techniques, A Small Scale Approach, GMU Edition, Chem 315/318, Cengage Learning: pp. 817-836
Slayden, S., Stalick, W., Roth, R, 2014, Organic Chemistry Laboratory Manual, 2nd Edition: Pearson
Custom Publishing: pp. 61-62
Web Site URL
Dr Schornicks Website: http:/mason.gmu.edu/~jschorni/gaschromatography
Unknown or Synthesized Compound
CRC Handbook of Chemistry & Physics, 84th Edition, Lide, D.R., Editor-in-chief, 2003-2004, CRC
Press, page no., item no.
Ibid.

Experiment:

Date:

Gas Chromatography: Distillate


Name

10/22/25

Partners

Drawer No.

CHEM
315/204

Katheryn Soto

Proc # 1

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Unk No.

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc # 2

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc # 3

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

10/22/25

Partners

Drawer No.

Course / Section

CHEM
315/204

Katheryn Soto

NOTE: This procedure page is to be numbered and placed in the appropriate


place in the report; normally after the computation of Moles in a Synthesis
experiment. Delete this page if not used.
Proc #

Experimental Reactions / Molar Ratio

Stoichiometric Balanced Equation (Use Structural Formulas)


Example:

Molar Ratio

: 1

Reaction Mechanism

The reaction mechanism may be hand printed in this space or you can use a
chemical drawing program to create the reaction.
http:/www.acdlabs.com

(Chemsketch 10.0 - Free Download)

http:/www.cambridgesoft.com

(ChemDraw 10.0 - Not sure of cost)

DO NOT USE the REACTION Mechanism in the WEB Notes; you must derive
you own mechanism.

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Determine Limiting Reagent


Materials

Desc:

Results

Equipment

Equation Setup:

Proc #

Compute Theoretical Yield


Materials

Desc:

Equation Setup:

Course / Section

Equipment

Results

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Theoretical Yield Summary Table

Course / Section

Results

Desc:

NOTE: If this experiment is not a Synthesis then DELETE this page


For a Synthesis Experiment, use either of the Theoretical Yield Computation Summary Tables
below for most Synthesis experiments. Delete the one not being used.

Balanced
Equation
Molecular
Weight
Mass
(grams)
Moles

Balanced
Equation
Molecular
Weight
Mass
(grams)
Moles

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Partners

10/22/25
Drawer No.

CHEM
315/204

Katheryn Soto

Proc #

Results
Materials

Desc:

Equation Setup:

Course / Section

Equipment

Experiment:

Date:

Gas Chromatography: Distillate


Name

Katheryn Soto

Summary of Results:

Partners

10/22/25
Drawer No.

Course / Section

CHEM
315/204

Experiment:

Date:

Gas Chromatography: Distillate


Name

Katheryn Soto
Analysis & Conclusions:

Partners

10/22/25
Drawer No.

Course / Section

CHEM
315/204

Experiment:

Date:

Gas Chromatography: Distillate


Name

10/22/25

Partners

Drawer No.

Course / Section

CHEM
315/204

Katheryn Soto

Literature Summary (Unknowns, Synthesized Compounds)


Unknown No.
CAS No.
Name (IUPAC)

Synonyms

Melting Point
(oC)

Lit
Exp

Lit
Exp

Lit
Exp

Lit
Exp

Boiling Point
(oC)

Lit
Exp

Lit
Exp

Lit
Exp

Lit
Exp

Refractive Index Lit


(nD20)
Exp

Lit
Exp

Lit
Exp

Lit
Exp

Solubility
(Rel to Water)

Lit
Exp

Lit
Exp

Lit
Exp

Lit
Exp

Density
Rel to Water

Lit
Exp

Lit
Exp

Lit
Exp

Lit
Exp

Molecular
Formula

Structural
Formula