INTERNATIONAL STANDARD
INTERNATIONAL ORGANIZATION FOR STANDARDIZATION .MElKJl.YHAPOJlHA.II
oprAHW3All.J.lR
no
713
CTAHJlAPTJ.l3All.J.lJ.I.ORGANISATION
INTERNATIONALE DE NORMALISATION
determination
lead, cadmium,
polarographic
analysis.
713-75
FOREWORD
Belgium
Brazil
Canada
Chile
Czechoslovakia
Egypt, Arab Rep. of
France
Germany
Hungary
India
Ireland
Italy
Japan
Korea, Rep. of
Korea, D.P. Rep. of
New Zealand
Norway
South Africa, Rep. of
The Member
Body of the following
Recommendation
on technical grounds:
country
Spain
Swjtzerland
Thailand
Turkey
United Kingdom
U.S.A.
U.S.S.R.
Yugoslavia
expressed
disapproval
of
the
Australia
disapproved
Spain
International
Printed
Organization
in Switzerland
for Standardization,
1975
the transformation
of
4851903 0070445 5
II
INTERNATIONAL
713-75
STANDARD
0070446
7 ~
4851903
REFERENCES
and preparation
PRINCIPLE
REAGENTS
4.2 Hydrochloric
cadmium.
acid, pl,19g/ml,
free from
lead and
2)
of
zinc
do
not
normally
contain
any
portion
with
4.3
4.4
4.5
Hydroxylammonium
4.6 Nickel
chloride
NiCI2. 6H20 per litre.
100 ml
of
thallium
chloride.
solution
containing
2g
of
1) Although
these types
determination.
test
4.7
4.2.4 Attack
the third
hydrochloric acid (4.2).
of
4.8
or
indium,
these two
elements, if
in this
713-75
4.9
I 4851903
0070447
4.10
7.3 Determination
200 mg of
Verify that the step heights are less than those produced by
adding 0,5 ml of the standard lead and cadmium solution
No.3 (4.9) to 25 ml of the solution of zinc chloride.
This test determines whether 25 ml of the solution of zinc
chloride contains less than 0,005 mg of lead and less than
0,005 mg of cadmium.
5 APPARATUS
6 SAMPLING
with the
7 PROCEDURE
8 EXPRESSION OF RESULTS
Read from the calibration curve the values corresponding to
the step heights obtained.
9 TEST REPORT
The test report shall mention the method used and the
results obtained. It shall also mention all operational details
not provided for in this International Standard or any
optional details, as well as any circumstances which could
have influenced the results.
The test report shall include all details required for
. complete identification of the sample