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SPILL/RELEASE REPORT

2016-0374
1 - GENERAL INFORMATION
OERS No. ____________
AT&T Services, Inc.
a. Company/Individual Name: ________________________________
308 South Akard Street, Room 1700
b. Address: _________________________________________________
Dallas, Texas 75202
_________________________________________________
Lauren Plunk
c. Company Contact Person: ___________________________________
214-202-5420
d. Phone Number(s): _________________________________________
e. Specific on-site location of the release (and address if different from above):
Halls Ridge Cell Tower: French Creek Road, Marion County, Detroit, Oregon
___________________________________________________________________________
44.71940278 -122.2176472
___________________________________________________________________________
___________________________________________________________________________
Please provide a map of the site showing area(s) where the release occurred, any sample
collection locations, location of roads/ditches/surface water bodies, etc.

2 - RELEASE INFORMATION
2/11/16 @ 1700
Discovered 2/11/16 @ 1700 Date/Time stopped:_________________
a. Date/Time Release started:__________________
b. Release was reported to (specify Date/Time/Name of Person contacted where applicable):
2/11/16 5:50PM; Called Oregon Emergency Response System to report spill (report # 2016-0374).
ODEQ _________________________________________________
2/11/16 1750 EST, Report # 2016-0374
OERS
_________________________________________________
2/11/16 1740 EST, Report # 1140291
NRC
_________________________________________________
2/12/16 USFS Penny Keen
Other (describe):___________________________________________
Barry Williams (AT&T)
c. Person(s) reporting release:________________________________________
d. Name, quantity and physical state (gas, liquid, solid or semi-solid) of material(s) released:
Diesel Fuel, 550 gallons (liquid)
___________________________________________________________________________
___________________________________________________________________________
Please attach copies of material safety data sheets (MSDS) or constituent profiles for
released material(s).
X
e. The release affected: ____Air ____Groundwater ____Surface Water ____Soil
____Sediment
f. Name and distance to nearest surface water body(s), even if unaffected (include locations of
creeks, streams, rivers and ditches that discharge to surface water on maps):
Unaffected unnamed tributary approximately 600 feet southeast from cell tower (see Figure 1)
___________________________________________________________________________
X
Has the release reached the surface water identified above?: ____Yes ____No
X
Could the release potentially reach the surface water identified above? ____Yes ____No
Location and distance from the release; field observation and analytical results.
Explain:____________________________________________________________________
___________________________________________________________________________
Unknown
g. Depth to nearest aquifer/groundwater:_____________
Is nearest aquifer/groundwater potable (drinkable)? ____Yes ____No
Has the release reached the nearest aquifer/groundwater? ____Yes ____No
Not Applicable - Nearest aquifer/groundwater depths are unknown.
Explain:____________________________________________________________________
___________________________________________________________________________

X
h. Release or potential release to the air occurred? ____Yes ____No
Explain:____________________________________________________________________
___________________________________________________________________________
X
i. Was there a threat to public safety? ____Yes ____No
X
j. Is there potential for future releases? ____Yes ____No
Prior to placing the fueling system back on-line at the site, AT&T is preparing to make fuel system modifications.
Explain:____________________________________________________________________
The planned fuel system modifications are tentatively scheduled for the week of 3/21 (ODEQ and USFS have been notified).
___________________________________________________________________________
k. Describe other effects/impacts from release (emergency evacuation, fish kills, etc.):
No additional impact to the environment to report.
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
l. Describe how the release occurred. Include details such as the release source, cause,
contributing weather factors, activities occurring prior to or during the release, dates and
times of various activities, first responders involved in containment activities, etc.:
The amount of fuel released from the tank system is approximately 550 gallons. AT&T is investigating the likely cause of
___________________________________________________________________________
the release. Our preliminary evaluation indicates excess fuel was pumped from from the 850 gallon main tank to the
___________________________________________________________________________
145 gallon day tank which then overflowed out the emergency vent. Upon completion of the evaluation, AT&T will notify
___________________________________________________________________________
the ORDEQ of its findings.
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________

3 - SITE INFORMATION
a. Adjacent land uses include (check all that apply and depict on site maps):
____Residential ____Commercial ____Light Industrial ____Heavy Industrial
X
United State Forest Service
____Agricultural ____Other
(describe):_________________________________________
Unknown
b. What is the population density surrounding the site:_______________
X
c. Is the site and/or release area secured by fencing or other means? ____Yes ____No
X
d. Soil types (check all that apply): ____alluvial ____
bedrock ____ clay ____sandy
X
____silt ____ silty loam ____artificial surface (cement/asphalt/etc.)
e. Describe site topography:______________________________________________________
A review of the quadrangle map shows the site at an elevation of approximately 4,400 feet above mean sea level (msl). The
___________________________________________________________________________
nearest surface water to the site is an unnamed tributary, which is approximately 600 feet northeast of the site. (see Figure 1).
___________________________________________________________________________

4 - CLEANUP INFORMATION
X
a. Was site cleanup performed? ____Yes
____No
If No, explain:_______________________________________________________________
___________________________________________________________________________
b. Who performed the site cleanup?
NWFF Environmental (on behalf of CB&I)
Company Name: ____________________________
106 S 11th St
Address: ____________________________________
Philomath, OR 97370
____________________________________
Anthony True
Cleanup Supervisor: _________________________
541-929-4884
Phone Number(s): ____________________________
X
c. Has all contamination been removed from the site? ____Yes ____No
Crews are managing absorbent while the ORDEQ-approved Path to
If No, explain:______________________________________________________________
Closure Work Plan is being implemented (anticipated start date 3/21/2016).
___________________________________________________________________________
41 cu yds
d. Estimated volume of contaminated soil removed:______________
e. Estimated volume of contaminated soil left in place:______________
X
f. Was a hazardous waste determination made for cleanup materials? ____Yes ____No
g. Based on the determination, are the cleanup materials hazardous wastes?
X
____Yes ____No
If Yes, list all waste codes:__________________________________
X
h. Was contaminated soil or water disposed of at an off-site location? ____Yes
____No
If yes, attach copies of receipts/manifests/etc., and provide the following information:
Waste Management River Bend Landfill
Facility Name: _______________________________
13469 SW Highway 18
Address: _____________________________________
McMinnville, OR 97128
_____________________________________
Facility Contact: ________________________________
503-472-8788
Phone Number(s): _____________________________
X
i. Is contaminated soil or water being stored and/or treated on-site? ____Yes ____No
If yes, please describe the material(s), storage and/or treatment area, and methods utilized
(attach additional sheets if necessary):
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
j. Describe cleanup activities including what actions were taken, dates and times actions were
initiated and completed, volumes of contaminated materials that were removed, etc. (attach
additional sheets or contractor reports if necessary or more convenient):
See Appendix A (Daily Activity Updates)
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________
___________________________________________________________________________

5 - SAMPLING INFORMATION
Attach copies of all sample data and indicate locations of sample collection on maps.
X
a. Were samples of contaminated soil collected? ____Yes
____No ____N/A
X
b. Were samples of contaminated water collected? ____Yes ____No ____N/A
c. Were samples collected to show that all contamination had been removed?
X
____Yes ____No ____N/A
d. Describe sampling activities, results and discuss rationale for sampling methods:
On February 26, 2016 a total of 21 soil samples were collected to identify the areas of impact and the lateral extent.
___________________________________________________________________________
A sampling grid included rows of five sample points parallel to the excavation area, on 20-foot centers, with the middle sample
___________________________________________________________________________
point of each row being on the centerline of the excavation (Figure 2). The rows were placed on 20-foot centers in the uphill___________________________________________________________________________
downhill direction. Soil from each sample location will be screened with a PID. Any soil sample with a PID reading greater than
___________________________________________________________________________
50 ppm an obvious diesel fuel impact will only be sampled for NWTPH-DX. If soil samples have PID readings greater
___________________________________________________________________________
than zero but less than 50 ppm then these samples will be analyzed for RBDM VOCs, NWTPH-DX and PAHs.
___________________________________________________________________________
Tabulated soil analytical results are provided in Table 1. See Appendix B (Apex Laboratory Reports).
___________________________________________________________________________

6 - ADDITIONAL INFORMATION
a. Provide a description or plan outlining the list of actions to be taken to prevent future
releases from occurring.
AT&T will contact the ORDEQ and USFS following the completion of their investigation to discuss corrective actions.
___________________________________________________________________________
Surface water samples were collected from five unnamed tributaries. Analytical results were non-detect for the samples.
___________________________________________________________________________
Tabulated surface water analytical results are provided in Table 2 and sample locations are presented on Figure 1.
___________________________________________________________________________
See Appendix B (Apex Laboratory Reports).
___________________________________________________________________________
7 - SPILL REPORT CHECKLIST
To ensure that you have gathered all the information requested by the Department in this
Spill/Release Report, please complete the following checklist:
X
____
Map(s), pre and post cleanup photos of the site showing buildings, roads, surface water
bodies, ditches, waterways, point of the release, extent of contamination, areas of
excavation and sample collection locations attached.
NA
____
Material Safety Data Sheet (MSDS), or constituent profiles for released material(s)
attached. Note: an MSDS is not required for motor fuels.

X
____
Sampling data/analytical results attached.
X
____
Receipts/manifests (if any) for disposal of cleanup materials attached.

X
____
Contractor reports (if any) attached.

If you would like to submit your report by e-mail it can be submitted electronically to:
DOSPILLS@deq.state.or.us

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw 1 RBCss 2
Contaminant
PID Reading (ppm)
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

(mg/kg) (mg/kg)
----9,500
4,600
> Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
No Std. No Std.
5.6
2,000
110
3,500
0.00056
9
0.013
200

1A
02/26/16
(mg/kg)
5.4
ND (< 28.6)
123
ND (< 0.0217)
ND (< 0.108)
ND (< 0.0542)
ND (< 0.163)
ND (< 0.217)
ND (< 0.108)
ND (< 0.108)
ND (< 0.0542)
ND (< 0.108)
ND (< 0.108)
ND (< 0.0542)
ND (< 0.0542)

1B
02/26/16
(mg/kg)
6.4
44.6
159
ND (< 0.0272)
ND (< 0.136)
ND (< 0.0680)
ND (< 0.204)
ND (< 0.272)
ND (< 0.136)
ND (< 0.136)
ND (< 0.0680)
ND (< 0.136)
ND (< 0.136)
ND (< 0.0680)
ND (< 0.0680)

1C
02/26/16
(mg/kg)
397
66,400
ND (< 4,080)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

Page 1 of 7

2A
02/26/16
(mg/kg)
2.7
ND (< 26.1)
ND (< 52.2)
ND (< 0.162)
ND (< 0.812)
ND (< 0.0406)
ND (< 0.122)
ND (< 0.162)
ND (< 0.0812)
ND (< 0.0812)
ND (< 0.0406)
ND (< 0.0812)
ND (< 0.0812)
ND (< 0.0406)
ND (< 0.0406)

2B
02/26/16
(mg/kg)
1.9
70.2
312
ND (< 0.0353)
ND (< 0.177)
ND (< 0.0883)
ND (< 0.265)
ND (< 0.353)
ND (< 0.177)
ND (< 0.177)
ND (< 0.0883)
ND (< 0.177)
ND (< 0.177)
ND (< 0.0883)
ND (< 0.0883)

2C
02/26/16
(mg/kg)
183
96,800
ND (<4,970)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

2D
02/26/16
(mg/kg)
33.8
ND (< 180)
606
0.0449
0.887
0.832
4.74
ND (<0.391)
ND (<0.195)
ND (<0.195)
0.642
3.53
1.04
ND (<0.0976)
ND (<0.0976)

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw 1 RBCss 2
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

(mg/kg) (mg/kg)
--21,000
No Std. No Std.
--110,000
2.3
24
1.9
2.4
--24
--240
No Std. No Std.
--2,400
--2.4
No Std. No Std.
--10,000
--14,000
--24
No Std. No Std.
No Std. No Std.
0.37
580
No Std. No Std.
--7,500

1A
02/26/16
(mg/kg)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)
ND (< 0.0143)

1B
02/26/16
(mg/kg)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)
ND (< 0.0161)

1C
02/26/16
(mg/kg)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

Page 2 of 7

2A
02/26/16
(mg/kg)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)
ND (<0.0130)

2B
02/26/16
(mg/kg)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)

2C
02/26/16
(mg/kg)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

2D
02/26/16
(mg/kg)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
ND (<0.0198)
ND (<0.0180)
0.0249
ND (<0.0180)
ND (<0.0180)
ND (<0.0207)
ND (<0.0180)
ND (<0.0180)
ND (<0.0180)
0.0229
ND (<0.0180)
0.0284
0.0433
0.0502
0.0229
ND (<0.0180)

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw 1 RBCss 2
Contaminant
PID Reading (ppm)
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

(mg/kg) (mg/kg)
----9,500
4,600
> Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
No Std. No Std.
5.6
2,000
110
3,500
0.00056
9
0.013
200

3A
02/26/16
(mg/kg)
3.3
29.1
116
ND (< 0.0216)
ND (< 0.108)
ND (< 0.0539)
ND (< 0.162)
ND (< 0.216)
ND (< 0.108)
ND (< 0.108)
ND (< 0.0539)
ND (< 0.108)
ND (< 0.108)
ND (< 0.0539)
ND (< 0.0539)

3B
02/26/16
(mg/kg)
2.0
ND (< 25.7)
ND (< 51.5)
ND (< 0.0160)
ND (< 0.0801)
ND (< 0.0400)
ND (< 0.120)
ND (< 0.160)
ND (< 0.0801)
ND (< 0.0801)
ND (< 0.0400)
ND (< 0.0801)
ND (< 0.0801)
ND (< 0.0400)
ND (< 0.0400)

3C
02/26/16
(mg/kg)
3.3
ND (< 27.0)
98.7
ND (< 0.0156)
ND (< 0.0782)
ND (< 0.0391)
ND (< 0.177)
ND (< 0.156)
ND (< 0.0782)
ND (< 0.0782)
ND (< 0.0391)
ND (< 0.0782)
ND (< 0.0782)
ND (< 0.0391)
ND (< 0.0391)

Page 3 of 7

3D
02/26/16
(mg/kg)
1.7
ND (< 27.6)
ND (< 55.3)
ND (< 0.0199)
ND (< 0.0994)
ND (< 0.0497)
ND (< 0.149)
ND (< 0.199)
ND (< 0.0944)
ND (< 0.0944)
ND (< 0.0497)
ND (< 0.0994)
ND (< 0.0994)
ND (< 0.0497)
ND (< 0.0497)

4A
02/26/16
(mg/kg)
3.4
ND (< 29.8)
117
ND (< 0.0205)
ND (< 0.103)
ND (< 0.0513)
ND (< 0.154)
ND (< 0.205)
ND (< 0.103)
ND (< 0.103)
ND (< 0.0513)
ND (< 0.103)
ND (< 0.103)
ND (< 0.0513)
ND (< 0.0513)

4B
02/26/16
(mg/kg)
4.8
ND (< 25.0)
ND (< 50.0)
ND (< 0.0162)
ND (< 0.0809)
ND (< 0.0404)
ND (< 0.121)
ND (< 0.162)
ND (< 0.0809)
ND (< 0.0809)
ND (< 0.0404)
ND (< 0.0809)
ND (< 0.0809)
ND (< 0.0404)
ND (< 0.0404)

4C
02/26/16
(mg/kg)
1.1
ND (< 28.9)
87.2
ND (< 0.0140)
ND (< 0.0702)
ND (< 0.0351)
ND (< 0.105)
ND (< 0.140)
ND (< 0.0702)
ND (< 0.0702)
ND (< 0.0351)
ND (< 0.0702)
ND (< 0.0702)
ND (< 0.0351)
ND (< 0.0351)

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw 1 RBCss 2
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

(mg/kg) (mg/kg)
--21,000
No Std. No Std.
--110,000
2.3
24
1.9
2.4
--24
--240
No Std. No Std.
--2,400
--2.4
No Std. No Std.
--10,000
--14,000
--24
No Std. No Std.
No Std. No Std.
0.37
580
No Std. No Std.
--7,500

3A
02/26/16
(mg/kg)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)
ND (< 0.0136)

3B
02/26/16
(mg/kg)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)
ND (< 0.0129)

3C
02/26/16
(mg/kg)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)
ND (<0.0135)

Page 4 of 7

3D
02/26/16
(mg/kg)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)
ND (< 0.0138)

4A
02/26/16
(mg/kg)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)
ND (<0.0149)

4B
02/26/16
(mg/kg)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)
ND (< 0.0123)

4C
02/26/16
(mg/kg)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)
ND (< 0.0144)

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw
Contaminant
PID Reading (ppm)
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

RBCss

(mg/kg) (mg/kg)
----9,500
4,600
> Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
No Std. No Std.
5.6
2,000
110
3,500
0.00056
9
0.013
200

4D
02/26/16
(mg/kg)
1.2
ND (< 25.0)
ND (< 50.0)
ND (< 0.00983)
ND (< 0.0491)
ND (< 0.0246)
ND (< 0.0737)
ND (< 0.0983)
ND (< 0.0491)
ND (< 0.0491)
ND (< 0.0246)
ND (< 0.0491)
ND (< 0.0491)
ND (< 0.0246)
ND (< 0.0246)

0A
02/26/16
(mg/kg)
0.9
ND (< 34.5)
ND (< 69.1)
ND (< 0.0324)
ND (< 0.162)
ND (< 0.0810)
ND (< 0.243)
ND (< 0.324)
ND (< 0.162)
ND (< 0.162)
ND (< 0.0810)
ND (< 0.162)
ND (< 0.162)
ND (< 0.0810)
ND (< 0.0810)

0B
02/26/16
(mg/kg)
10.5
1,090
ND (< 66.8)
ND (< 0.0272)
0.224
0.200
1.04
ND (< 0.272)
ND (< 0.136)
ND (< 0.136)
0.162
0.755
0.264
ND (< 0.0680)
ND (< 0.0680)

Page 5 of 7

0C
02/26/16
(mg/kg)
36.8
9,430
ND (< 372)
0.161
2.93
3.70
20.6
2.15
ND (<0.168)
1.03
3.82
19.9
6.59
ND (<0.0840)
ND (<0.0840)

Ex Sidewall
S
02/26/16
(mg/kg)
5.0
ND (< 25.0)
ND (< 50.0)
ND (< 0.00773)
ND (< 0.0386)
ND (< 0.0193)
ND (< 0.0580)
ND (< 0.0773)
ND (< 0.0386)
ND (< 0.0386)
ND (< 0.0193)
ND (< 0.0386)
ND (< 0.0386)
ND (< 0.0193)
ND (< 0.0193)

Ex Sidewall
W
02/26/16
(mg/kg)
1.8
ND (<26.7)
ND (< 53.5)
ND (< 0.0119)
ND (< 0.0594)
ND (< 0.0297)
ND (< 0.0890)
ND (< 0.119)
ND (< 0.0594)
ND (< 0.0594)
ND (< 0.0297)
ND (< 0.0594)
ND (< 0.0594)
ND (< 0.0297)
ND (< 0.0297)

Ex Sidewall
E
02/26/16
(mg/kg)
6.0
184
ND (< 50.0)
ND (< 0.00717)
ND (< 0.0358)
ND (< 0.0179)
ND (< 0.0538)
ND (< 0.0717)
ND (< 0.0358)
ND (< 0.0358)
ND (< 0.0179)
ND (< 0.0358)
ND (< 0.0358)
ND (< 0.0179)
ND (< 0.0179)

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

RBCss

(mg/kg) (mg/kg)
--21,000
No Std. No Std.
--110,000
2.3
24
1.9
2.4
--24
--240
No Std. No Std.
--2,400
--2.4
No Std. No Std.
--10,000
--14,000
--24
No Std. No Std.
No Std. No Std.
0.37
580
No Std. No Std.
--7,500

4D
02/26/16
(mg/kg)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)
ND (<0.0120)

0A
02/26/16
(mg/kg)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)
ND (< 0.0173)

0B
02/26/16
(mg/kg)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
ND (< 0.0167)
0.0620
ND (< 0.0167)
ND (< 0.0401)
ND (< 0.0167)
0.114
0.155
ND (< 0.0301)
0.0489
0.0411

Page 6 of 7

0C
02/26/16
(mg/kg)
ND (< 0.208)
ND (< 0.0763)
ND (< 0.104)
ND (< 0.0242)
ND (< 0.0186)
ND (< 0.0186)
ND (< 0.0186)
ND (< 0.0186)
ND (< 0.0260)
ND (<0.0186)
0.376
ND (< 0.0186)
0.454
ND (< 0.0186)
3.29
5.58
2.08
0.740
0.389

Ex Sidewall
S
02/26/16
(mg/kg)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)
ND (< 0.0107)

Ex Sidewall
W
02/26/16
(mg/kg)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)
ND (< 0.0134)

Ex Sidewall
E
02/26/16
(mg/kg)
ND (< 0.0105)
0.0181
0.0526
0.635
0.219
0.603
0.206
0.0799
0.947
0.0306
ND (< 0.0105)
1.86
ND (< 0.0105)
0.116
ND (< 0.0105)
0.0135
ND (< 0.0105)
0.0119
1.60

Table 1
Soil Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
Soil Sample Analytical Results

RBCsw 1 RBCss 2
Contaminant
PID Reading (ppm)
NWTPH-Dx: Diesel
NWTPH-Dx: Oil

(mg/kg) (mg/kg)
----9,500
4,600
> Max
11,000

Foundation-S
03/06/16
(mg/kg)
94.0
27,600
ND (< 1,070)

----

----

----

----

----

----

Notes:
1

Risk-Based Concentrations For Individual Chemicals (State of Oregon Department of Environmental Quality), Soils Leaching to Groundwater (RBCsw), Urban Residential dated November 1, 2015.

Risk-Based Concentrations For Individual Chemicals (State of Oregon Department of Environmental Quality), Soils Leaching to Soil Ingestion, Dermal Contact, and Inhalation (RBCss), Construction Worker dated
November 1, 2015.
Bold = Soil Sample analytical results exceeded applicable standard.
Analytical Results were compared to the Oregon standards for the Soils Leaching to Groundwater (RCBsw) Urban Residential and the Soil Leaching to Soil Ingestion, Dermal Contact and Inhulation (RCBss) Construction
Worker. The lowere of the two values was selected for comparison to the analytic results for soils.
mg/kg = milligrams per kilogram.
> Max = The constituent RBC for this pathway is calculated as greater than 1,000,000 mg/kg or 1,000,000 mg/L. Therefore, this substance is deemed not to pose risks in this scenario.
MTBE = Methyl tert-butyl ether
No Std. = No standard listed in Risk Based Concentrations for Individual Chemicals State of Oregon Department of Environmental Quality dated November 1, 2015.
PID = Photoionization detector readings are reported in parts per million (ppm).
ND = Concentration not detected at the laboratory method detection limit.
NA = Not Analyzed
--- = All RBC values for indirect pathways that exceed a limit (Csat, S, or Pv) are removed from the Risk-Based Concentrations For Individual Chemicals Table.

Page 7 of 7

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-01
Unnamed Tributary
Contaminant
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

Water Sample Analytical Results

RBCtw 1
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
No Std.
54
500
0.034
0.78

SW-01
02/19/16
(g/L)
ND (< 208)
ND (< 417)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-01
02/21/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-01
02/28/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

Page 1 of 11

SW-01
03/06/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-01

SW-01

SW-01

(g/L)
---------------

(g/L)
---------------

(g/L)
---------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-01
Unnamed Tributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

Water Sample Analytical Results

RBCtw
(g/L)
2,400
No Std.
--0.043
0.011
0.11
--No Std.
--0.011
No Std.
--1,400
0.11
No Std.
No Std.
0.78
No Std.
---

SW-01
02/19/16
(g/L)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0833)
ND (< 0.0833)
ND (< 0.0833)
ND (< 0.0417)
ND (< 0.0417)

SW-01
02/21/16
(g/L)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0784)
ND (< 0.0784)
ND (< 0.0784)
ND (< 0.0392)
ND (< 0.0392)

SW-01
02/28/16
(g/L)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0784)
ND (< 0.0784)
ND (< 0.0784)
ND (< 0.0392)
ND (< 0.0392)

Page 2 of 11

SW-01
03/06/16
(g/L)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0777)
ND (<0.0777)
ND (<0.0777)
ND (<0.0388)
ND (<0.0388)

SW-01

SW-01

SW-01

(g/L)
--------------------

(g/L)
--------------------

(g/L)
--------------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-02
Unnamed Tributary
Contaminant
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

Water Sample Analytical Results

RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
No Std.
54
500
0.034
0.78

SW-02
02/19/16
(g/L)
ND (< 208)
ND (< 417)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-02
02/21/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-02
02/28/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

Page 3 of 11

SW-02
03/06/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-02

SW-02

SW-02

(g/L)
---------------

(g/L)
---------------

(g/L)
---------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-02
Unnamed Tributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

Water Sample Analytical Results

RBCtw
(g/L)
2,400
No Std.
--0.043
0.011
0.11
--No Std.
--0.011
No Std.
--1,400
0.11
No Std.
No Std.
0.78
No Std.
---

SW-02
02/19/16
(g/L)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0833)
ND (< 0.0833)
ND (< 0.0833)
ND (< 0.0417)
ND (< 0.0417)

SW-02
02/21/16
(g/L)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0417)
ND (< 0.0833)
ND (< 0.0833)
ND (< 0.0833)
ND (< 0.0417)
ND (< 0.0417)

SW-02
02/28/16
(g/L)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0404)
ND (< 0.0808)
ND (< 0.0808)
ND (< 0.0808)
ND (< 0.0404)
ND (< 0.0404)

Page 4 of 11

SW-02
03/06/16
(g/L)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0388)
ND (<0.0777)
ND (<0.0777)
ND (<0.0777)
ND (<0.0388)
ND (<0.0388)

SW-02

SW-02

SW-02

(g/L)
--------------------

(g/L)
--------------------

(g/L)
--------------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-03
Unnamed Tributary
Contaminant
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

Water Sample Analytical Results

RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
No Std.
54
500
0.034
0.78

SW-03
02/19/16
(g/L)
ND (< 200)
ND (< 400)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-03
02/21/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-03
02/28/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

Page 5 of 11

SW-03
03/06/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-03

SW-03

SW-03

(g/L)
---------------

(g/L)
---------------

(g/L)
---------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-03
Unnamed Tributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

Water Sample Analytical Results

RBCtw
(g/L)
2,400
No Std.
--0.043
0.011
0.11
--No Std.
--0.011
No Std.
--1,400
0.11
No Std.
No Std.
0.78
No Std.
---

SW-03
02/19/16
(g/L)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND (< 0.0400)
ND ( < 0.0800)
ND ( < 0.0800)
ND ( < 0.0800)
ND (< 0.0400)
ND (< 0.0400)

SW-03
02/21/16
(g/L)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0412)
ND (< 0.0825)
ND (< 0.0825)
ND (< 0.0825)
ND (< 0.0412)
ND (< 0.0412)

SW-03
02/28/16
(g/L)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0421)
ND (<0.0842)
ND (<0.0842)
ND (<0.0842)
ND (<0.0421)
ND (<0.0421)

Page 6 of 11

SW-03
03/06/16
(g/L)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0396)
ND (<0.0792)
ND (<0.0792)
ND (<0.0792)
ND (<0.0396)
ND (<0.0396)

SW-03

SW-03

SW-03

(g/L)
--------------------

(g/L)
--------------------

(g/L)
--------------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-04
Unnamed Tributary
Contaminant
NWTPH-Dx: Diesel
NWTPH-Dx: Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

Water Sample Analytical Results

RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
No Std.
54
500
0.034
0.78

SW-04
02/19/16
(g/L)
ND (< 194)
ND (< 388)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-04
02/21/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-04
02/28/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

Page 7 of 11

SW-04
03/06/16
(g/L)
NA
NA
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-04

SW-04

SW-04

(g/L)
---------------

(g/L)
---------------

(g/L)
---------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-04
Unnamed Tributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

Water Sample Analytical Results

RBCtw
(g/L)
2,400
No Std.
--0.043
0.011
0.11
--No Std.
--0.011
No Std.
--1,400
0.11
No Std.
No Std.
0.78
No Std.
---

SW-04
02/19/16
(g/L)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (< 0.0388)
ND (<0.0777)
ND (<0.0777)
ND (<0.0777)
ND (< 0.0388)
ND (< 0.0388)

SW-04
02/21/16
(g/L)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0396)
ND (< 0.0792)
ND (< 0.0792)
ND (< 0.0792)
ND (< 0.0396)
ND (< 0.0396)

SW-04
02/28/16
(g/L)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0408)
ND (< 0.0816)
ND (< 0.0816)
ND (< 0.0816)
ND (< 0.0408)
ND (< 0.0408)

Page 8 of 11

SW-04
03/06/16
(g/L)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0392)
ND (< 0.0784)
ND (< 0.0784)
ND (< 0.0784)
ND (< 0.0392)
ND (< 0.0392)

SW-04

SW-04

SW-04

(g/L)
--------------------

(g/L)
--------------------

(g/L)
--------------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-05
Unnamed Tributary
Contaminant
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane (EDC)

Water Sample Analytical Results

RBCtw
(g/L)
2.0
4,400
6.7
710
0.78
64
1,800
No Std.
54
500
0.034
0.78

SW-05
02/25/16
(g/L)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-05
02/28/16
(g/L)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

SW-05
03/06/16
(g/L)
ND (< 0.200)
ND (< 1.00)
ND ( < 0.500)
ND (< 1.50)
ND (< 2.00)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 1.00)
ND (< 1.00)
ND (< 0.500)
ND (< 0.500)

Page 9 of 11

SW-05

SW-05

SW-05

SW-05

(g/L)
-------------

(g/L)
-------------

(g/L)
-------------

(g/L)
-------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon
SW-05
Unnamed Tributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

Water Sample Analytical Results

RBCtw
(g/L)
2,400
No Std.
--0.043
0.011
0.11
--No Std.
--0.011
No Std.
--1,400
0.11
No Std.
No Std.
0.78
No Std.
---

SW-05
02/25/16
(g/L)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0879)
ND (< 0.0879)
ND (< 0.0879)
ND (< 0.0440)
ND (< 0.0440)

SW-05
02/28/16
(g/L)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0440)
ND (< 0.0879)
ND (< 0.0879)
ND (< 0.0879)
ND (< 0.0440)
ND (< 0.0440)

SW-05
03/06/16
(g/L)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (< 0.0385)
ND (<0.0769)
ND (<0.0769)
ND (<0.0769)
ND (< 0.0385)
ND (< 0.0385)

Page 10 of 11

SW-05

SW-05

SW-05

SW-05

(g/L)
--------------------

(g/L)
--

(g/L)
--------------------

(g/L)
--------------------

------------------

Table 2
Water Sample Analytical Results
AT&T Hall Ridge
Oregon Emergency Response System Report No. 2016-0374
Willamette National Forest
Detroit, Oregon

Notes:
1

Risk-Based Concentrations For Individual Chemicals (State of Oregon Department of Environmental Quality), Groundwater Ingestion & Inhalation from Tapwater (RBCtw),
Urban Residential dated November 1, 2015.
(g/L) = micrograms per liter.
MTBE = Methyl tert-butyl ether
No Std. = No Standard Listed
ND = Concentration not detected at the laboratory reporting limit.
NA = Not Analyzed
--- = All RBC values for indirect pathways that exceed a limit (Csat, S, or Pv) are removed from the Risk-Based Concentrations For Individual Chemicals Table.

Page 11 of 11

OFFICE

DRAWING
NUMBER 156319-D1

LEGEND:
STREAM SAMPLE LOCATIONS

SW-1

SITE
SW-5

SW-2

SW-3

DETROIT LAKE

SW-4

REV

TY
UN
CO
TY
RI
UN
MA
CO
N
LI N
ON

DESCRIPTION / ISSUE

DATE

APPROVED

CB&I
500 Penn Center Boulevard, Suite 1000
Pittsburgh, Pennsylvania 15235
DESIGNED BY:

AT&T HALL RIDGE CELL TOWER


DRAWN BY:

FIGURE 1
STREAM SAMPLE LOCATION MAP

CHECKED BY:

APPROVED BY:

FRENCH CREEK ROAD


MARION COUNTY, OREGON
DATE:

SCALE:

DRAWING NO.

SHEET NO.

DRAWING
NUMBER 156319-D1

LEGEND:
GROUND SURFACE CONTOUR
(20 FT INTERVAL)

CELL TOWER

EXCAVATION AREA

1A

SOIL SAMPLE LOCATION

5A

POTHOLE LOCATION - NOT


SAMPLED

OFFICE

WOODED

WOODED

6A

4A

2A
1A

3A
5A

2B

0A

4B

1B

FOUNDATION-S

3B

0B

5B

1C
0C

6B

DOWN SLOPE TO
DETROIT LAKE

2C

EX-SIDEWALL-W
EX-SIDEWALL-S

4C

3C

1D

EX-SIDEWALL-E

2D

5C
6C

3D
4D
5D
6D
3E

4E

5E
REV

DESCRIPTION / ISSUE

DATE

APPROVED

ACCESS

ROAD

6E

CB&I
500 Penn Center Boulevard, Suite 1000
Pittsburgh, Pennsylvania 15235

WOODED

DESIGNED BY:

AT&T HALL RIDGE CELL TOWER


DRAWN BY:

FIGURE 2
SOIL SAMPLE LOCATIONS

CHECKED BY:

APPROVED BY:

FRENCH CREEK ROAD


MARION COUNTY, OREGON
DATE:

SCALE:

DRAWING NO.

SHEET NO.

Photographic Documentation
Client: AT&T Services
Location: Halls Ridge Cell Tower

Prepared by: CB&I


Project No: 156319.02323210

Direction: South
Date: 02/12/2016
Photographer: NWFF

Description:
Impacted snow with diesel.
Snow was removed and
placed in lined super sacks
for disposal.

Direction: South
Date:02/12/16
Photographer: NWFF

Description:
Impacted snow with diesel.
Snow was removed and
placed in lined super sacks
for disposal.

Page 1 of 6

Photographic Documentation
Client: AT&T Services
Location: Halls Ridge Cell Tower

Prepared by: CB&I


Project No: 156319.02323210

Direction: South
Date:02/17/16
Photographer: R. Malec

Description:
NWFF employees
managing absorbent pads
at downslope rock outcrop.

Direction: South
Date: 02/28/16
Photographer: R. Malec

Description:
Absorbent pads applied
and managed at
downslope rock outcrop.

Page 2 of 6

Photographic Documentation
Client: AT&T Services
Location: Halls Ridge Cell Tower

Prepared by: CB&I


Project No: 156319.02323210

Direction:
Date: 02/28/16
Photographer: R. Malec

Description:
Downslope interception
trench and weir.

Direction: North
Date: 02/22/16
Photographer: P. Bauer

Description:
Excavating source material
on the eastern side of the
building.

Page 3 of 6

Photographic Documentation
Client: AT&T Services
Location: Halls Ridge Cell Tower

Prepared by: CB&I


Project No: 156319.02323210

Direction: South
Date: 02/22/16
Photographer: P. Bauer

Description:
Excavating source material
on the eastern side of the
building.

Direction: Northwest
Date: 02/24/16
Photographer: P. Bauer

Description:
Excavation on the eastern
side of the building after
source removal.

Page 4 of 6

Photographic Documentation
Client: AT&T Services
Location: Halls Ridge Cell Tower

Prepared by: CB&I


Project No: 156319.02323210

Direction: West
Date: 02/24/16
Photographer: P.Bauer

Description:
Impacted gravel and soils
removed from eastern side
of building.

Direction: South
Date:02/24/16
Photographer: P. Bauer

Description:
Start of dye test (5 gpm).

Page 5 of 6

Photographic Documentation
Client: AT&T Services
Location: Halls Ridge Cell Tower

Prepared by: CB&I


Project No: 156319.02323210

Direction: Northwest
Date: 02/24/16
Photographer: R. Malec

Description:
Dye test (5 gpm).

Direction: West
Date: 02/24/16
Photographer: R. Malec

Description:
Dye observed at downslope
soil sample location (1C)
mimic flow path of diesel.

Page 6 of 6

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Sunday, February 28, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0900, which was received by the laboratory on
2/27/2016 at 9:15:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

1A

A6B0900-01
A6B0900-02
A6B0900-03
A6B0900-04
A6B0900-05
A6B0900-06
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

1B
1C
2A
2B
2C
2D
3A
3B
3C
3D
4A
4B
4C
4D
0A
0B
0C
Ex Sidewall S
Ex Sidewall W
Ex Sidewall E

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Date Sampled

Date Received

02/26/16 09:40
02/26/16 09:50
02/26/16 10:00
02/26/16 10:55
02/26/16 11:00
02/26/16 10:10
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

1A (A6B0900-01)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Diesel

ND

---

28.6

mg/kg dry

02/27/16 13:53

NWTPH-Dx

Oil

123

---

57.2

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 88 %

1B (A6B0900-02)

Notes

Batch: 6020836

Limits: 50-150 %

Matrix: Soil

F-17

Batch: 6020836

Diesel

44.6

---

32.2

mg/kg dry

02/27/16 14:33

NWTPH-Dx

F-17

Oil

159

---

64.3

"

"

"

"

F-17

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 90 %

1C (A6B0900-03)

Diesel

Oil

Limits: 50-150 %

Matrix: Soil

Batch: 6020835

66400

---

2040

mg/kg dry

50

02/27/16 13:53

NWTPH-Dx

ND

---

4080

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: %

2A (A6B0900-04)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

26.1

mg/kg dry

02/27/16 15:12

NWTPH-Dx

Oil

ND

---

52.2

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 90 %

2B (A6B0900-05)

S-01

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

70.2

---

35.9

mg/kg dry

02/27/16 15:32

NWTPH-Dx

F-17

Oil

312

---

71.8

"

"

"

"

F-17

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 83 %

2C (A6B0900-06)

Diesel

Oil

Limits: 50-150 %

Matrix: Soil

Batch: 6020835

96800

---

2490

mg/kg dry

50

02/27/16 14:33

NWTPH-Dx

ND

---

4970

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: %

2D (A6B0900-07)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

180

mg/kg dry

02/27/16 16:12

NWTPH-Dx

Oil

606

---

360

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 84 %

3A (A6B0900-08)

S-01

Limits: 50-150 %

Matrix: Soil

F-17

Batch: 6020836

Diesel

29.1

---

27.2

mg/kg dry

02/27/16 16:32

NWTPH-Dx

F-17

Oil

116

---

54.4

"

"

"

"

F-17

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 90 %

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

3B (A6B0900-09)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Diesel

ND

---

25.7

mg/kg dry

02/27/16 17:12

NWTPH-Dx

Oil

ND

---

51.5

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 92 %

3C (A6B0900-10)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

27.0

mg/kg dry

02/27/16 17:31

NWTPH-Dx

Oil

98.7

---

54.0

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 90 %

3D (A6B0900-11)

Limits: 50-150 %

Matrix: Soil

ND

---

27.6

mg/kg dry

02/27/16 17:12

NWTPH-Dx

Oil

ND

---

55.3

"

"

"

"

"

"

"

Recovery: 90 %

4A (A6B0900-12)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

29.8

mg/kg dry

02/27/16 17:31

NWTPH-Dx

Oil

117

---

59.6

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 91 %

4B (A6B0900-13)

Limits: 50-150 %

Matrix: Soil

ND

---

25.0

mg/kg dry

02/27/16 14:52

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Recovery: 94 %

4C (A6B0900-14RE1)

Diesel
Oil

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

ND

---

28.9

mg/kg dry

02/27/16 15:12

NWTPH-Dx

87.2

---

57.7

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 95 %

4D (A6B0900-15)

Limits: 50-150 %

Matrix: Soil

ND

---

25.0

mg/kg dry

02/27/16 15:32

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Recovery: 94 %

0A (A6B0900-16)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

34.5

mg/kg dry

02/27/16 12:29

NWTPH-Dx

Oil

ND

---

69.1

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 90 %

F-17

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

F-17

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

F-17

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

Notes

Batch: 6020836

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

0B (A6B0900-17)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Diesel

1090

---

33.4

mg/kg dry

02/27/16 15:52

NWTPH-Dx

Oil

ND

---

66.8

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 99 %

0C (A6B0900-18)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

9430

---

186

mg/kg dry

02/27/16 16:32

NWTPH-Dx

Oil

ND

---

372

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 137 %

Ex Sidewall S (A6B0900-19)

Limits: 50-150 %

Matrix: Soil

ND

---

25.0

mg/kg dry

02/27/16 12:49

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Recovery: 95 %

Ex Sidewall W (A6B0900-20)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

26.7

mg/kg dry

02/27/16 12:49

NWTPH-Dx

Oil

ND

---

53.5

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 95 %

Ex Sidewall E (A6B0900-21)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

184

---

25.0

mg/kg dry

02/27/16 16:52

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 94 %

S-05

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

Notes

Batch: 6020836

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

1A (A6B0900-01)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Benzene

ND

---

0.0217

mg/kg dry

50

02/27/16 13:54

5035/8260B

Toluene

ND

---

0.108

"

"

"

"

Ethylbenzene

ND

---

0.0542

"

"

"

"

Xylenes, total

ND

---

0.163

"

"

"

"

Naphthalene

ND

---

0.217

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.108

"

"

"

"

Isopropylbenzene

ND

---

0.108

"

"

"

"

n-Propylbenzene

ND

---

0.0542

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0542

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0542

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 106 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

1B (A6B0900-02)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0272

mg/kg dry

50

02/27/16 14:51

5035/8260B

Toluene

ND

---

0.136

"

"

"

"

Ethylbenzene

ND

---

0.0680

"

"

"

"

Xylenes, total

ND

---

0.204

"

"

"

"

Naphthalene

ND

---

0.272

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.136

"

"

"

"

Isopropylbenzene

ND

---

0.136

"

"

"

"

n-Propylbenzene

ND

---

0.0680

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.136

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.136

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0680

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0680

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

98 %

Limits: 70-130 %

"

"

"

02/27/16 15:20

5035/8260B

4-Bromofluorobenzene (Surr)

2A (A6B0900-04)

Benzene

Matrix: Soil

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

0.0162

Notes

Batch: 6020833

Batch: 6020833

mg/kg dry

50

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

2A (A6B0900-04)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Toluene

ND

---

0.0812

mg/kg dry

50

"

5035/8260B

Ethylbenzene

ND

---

0.0406

"

"

"

"

Xylenes, total

ND

---

0.122

"

"

"

"

Naphthalene

ND

---

0.162

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0812

"

"

"

"

Isopropylbenzene

ND

---

0.0812

"

"

"

"

n-Propylbenzene

ND

---

0.0406

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0812

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0812

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0406

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0406

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 109 %

Limits: 70-130 %

"

"

104 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

2B (A6B0900-05)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0353

mg/kg dry

50

02/27/16 15:48

5035/8260B

Toluene

ND

---

0.177

"

"

"

"

Ethylbenzene

ND

---

0.0883

"

"

"

"

Xylenes, total

ND

---

0.265

"

"

"

"

Naphthalene

ND

---

0.353

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.177

"

"

"

"

Isopropylbenzene

ND

---

0.177

"

"

"

"

n-Propylbenzene

ND

---

0.0883

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.177

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.177

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0883

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0883

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 70-130 %

"

"

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

95 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

2D (A6B0900-07)

Matrix: Soil

Batch: 6020833

Benzene

0.0449

---

0.0391

mg/kg dry

50

02/27/16 16:16

5035/8260B

Toluene

0.887

---

0.195

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

2D (A6B0900-07)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Ethylbenzene

0.832

---

0.0976

mg/kg dry

50

"

5035/8260B

Xylenes, total

4.74

---

0.293

"

"

"

"

Naphthalene

ND

---

0.391

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.195

"

"

"

"

Isopropylbenzene

ND

---

0.195

"

"

"

"

n-Propylbenzene

0.642

---

0.0976

"

"

"

"

1,2,4-Trimethylbenzene

3.53

---

0.195

"

"

"

"

1,3,5-Trimethylbenzene

1.04

---

0.195

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0976

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0976

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 108 %

Limits: 70-130 %

"

"

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

93 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

3A (A6B0900-08)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0216

mg/kg dry

50

02/27/16 16:45

5035/8260B

Toluene

ND

---

0.108

"

"

"

"

Ethylbenzene

ND

---

0.0539

"

"

"

"

Xylenes, total

ND

---

0.162

"

"

"

"

Naphthalene

ND

---

0.216

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.108

"

"

"

"

Isopropylbenzene

ND

---

0.108

"

"

"

"

n-Propylbenzene

ND

---

0.0539

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0539

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0539

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

3B (A6B0900-09)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0160

mg/kg dry

50

02/27/16 17:13

5035/8260B

Toluene

ND

---

0.0801

"

"

"

"

Ethylbenzene

ND

---

0.0400

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

3B (A6B0900-09)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Xylenes, total

ND

---

0.120

mg/kg dry

50

"

5035/8260B

Naphthalene

ND

---

0.160

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0801

"

"

"

"

Isopropylbenzene

ND

---

0.0801

"

"

"

"

n-Propylbenzene

ND

---

0.0400

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0801

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0801

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0400

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

"

"

"

Recovery: 108 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

93 %

Limits: 70-130 %

"

"

"

Surrogate: Dibromofluoromethane (Surr)

4-Bromofluorobenzene (Surr)

3C (A6B0900-10)

0.0400

"

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0156

mg/kg dry

50

02/27/16 17:41

5035/8260B

Toluene

ND

---

0.0782

"

"

"

"

Ethylbenzene

ND

---

0.0391

"

"

"

"

Xylenes, total

ND

---

0.117

"

"

"

"

Naphthalene

ND

---

0.156

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0782

"

"

"

"

Isopropylbenzene

ND

---

0.0782

"

"

"

"

n-Propylbenzene

ND

---

0.0391

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0782

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0782

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0391

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0391

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 106 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 70-130 %

"

"

"

93 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

3D (A6B0900-11)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0199

mg/kg dry

50

02/27/16 18:10

5035/8260B

Toluene

ND

---

0.0994

"

"

"

"

Ethylbenzene

ND

---

0.0497

"

"

"

"

Xylenes, total

ND

---

0.149

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

3D (A6B0900-11)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Naphthalene

ND

---

0.199

mg/kg dry

50

"

5035/8260B

Methyl tert-butyl ether (MTBE)

ND

---

0.0994

"

"

"

"

Isopropylbenzene

ND

---

0.0994

"

"

"

"

n-Propylbenzene

ND

---

0.0497

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0994

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0994

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0497

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0497

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 70-130 %

"

"

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

95 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

4A (A6B0900-12)

Matrix: Soil

Benzene

ND

---

Toluene

ND

Ethylbenzene

ND

Xylenes, total

Batch: 6020833

0.0205

mg/kg dry

50

02/27/16 18:38

5035/8260B

---

0.103

"

"

"

"

---

0.0513

"

"

"

"

ND

---

0.154

"

"

"

"

Naphthalene

ND

---

0.205

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.103

"

"

"

"

Isopropylbenzene

ND

---

0.103

"

"

"

"

n-Propylbenzene

ND

---

0.0513

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.103

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.103

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0513

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0513

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 70-130 %

"

"

"

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

4B (A6B0900-13)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0162

mg/kg dry

50

02/27/16 19:07

5035/8260B

Toluene

ND

---

0.0809

"

"

"

"

Ethylbenzene

ND

---

0.0404

"

"

"

"

Xylenes, total

ND

---

0.121

"

"

"

"

Naphthalene

ND

---

0.162

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

4B (A6B0900-13)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Methyl tert-butyl ether (MTBE)

ND

---

0.0809

mg/kg dry

50

"

5035/8260B

Isopropylbenzene

ND

---

0.0809

"

"

"

"

n-Propylbenzene

ND

---

0.0404

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0809

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0809

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0404

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0404

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 107 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

98 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

4C (A6B0900-14)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.0140

mg/kg dry

50

02/27/16 14:15

5035/8260B

Toluene

ND

---

0.0702

"

"

"

"

Ethylbenzene

ND

---

0.0351

"

"

"

"

Xylenes, total

ND

---

0.105

"

"

"

"

Naphthalene

ND

---

0.140

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0702

"

"

"

"

Isopropylbenzene

ND

---

0.0702

"

"

"

"

n-Propylbenzene

ND

---

0.0351

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0702

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0702

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0351

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

"

"

"

Recovery: 97 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

93 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 70-130 %

"

"

"

Surrogate: Dibromofluoromethane (Surr)

4D (A6B0900-15)

0.0351

"

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.00983

mg/kg dry

50

02/27/16 14:41

5035/8260B

Toluene

ND

---

0.0491

"

"

"

"

Ethylbenzene

ND

---

0.0246

"

"

"

"

Xylenes, total

ND

---

0.0737

"

"

"

"

Naphthalene

ND

---

0.0983

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0491

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

4D (A6B0900-15)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Isopropylbenzene

ND

---

0.0491

mg/kg dry

50

"

5035/8260B

n-Propylbenzene

ND

---

0.0246

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0491

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0491

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0246

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0246

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 96 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

92 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 70-130 %

"

"

"

0A (A6B0900-16)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.0324

mg/kg dry

50

02/27/16 15:08

5035/8260B

Toluene

ND

---

0.162

"

"

"

"

Ethylbenzene

ND

---

0.0810

"

"

"

"

Xylenes, total

ND

---

0.243

"

"

"

"

Naphthalene

ND

---

0.324

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.162

"

"

"

"

Isopropylbenzene

ND

---

0.162

"

"

"

"

n-Propylbenzene

ND

---

0.0810

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.162

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.162

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0810

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0810

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 97 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

92 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

02/27/16 15:35

5035/8260B

0B (A6B0900-17)

Benzene

Matrix: Soil

ND

---

Batch: 6020834

0.0272

mg/kg dry

50

Toluene

0.224

---

0.136

"

"

"

"

Ethylbenzene

0.200

---

0.0680

"

"

"

"

Xylenes, total

1.04

---

0.204

"

"

"

"

Naphthalene

ND

---

0.272

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.136

"

"

"

"

Isopropylbenzene

ND

---

0.136

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

0B (A6B0900-17)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

n-Propylbenzene

0.162

---

0.0680

mg/kg dry

50

"

1,2,4-Trimethylbenzene

0.755

---

0.136

"

"

"

"

1,3,5-Trimethylbenzene

0.264

---

0.136

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0680

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0680

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

5035/8260B

Recovery: 94 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

91 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

0C (A6B0900-18)

Matrix: Soil

Batch: 6020834

Benzene

0.161

---

0.0336

mg/kg dry

50

02/27/16 16:29

5035/8260B

Toluene

2.93

---

0.168

"

"

"

"

Ethylbenzene

3.70

---

0.0840

"

"

"

"

Xylenes, total

20.6

---

0.252

"

"

"

"

Naphthalene

2.15

---

0.336

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.168

"

"

"

"

Isopropylbenzene

1.03

---

0.168

"

"

"

"

n-Propylbenzene

3.82

---

0.0840

"

"

"

"

1,2,4-Trimethylbenzene

19.9

---

0.168

"

"

"

"

1,3,5-Trimethylbenzene

6.59

---

0.168

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0840

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0840

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Ex Sidewall S (A6B0900-19)

Recovery: 97 %

Limits: 70-130 %

"

"

93 %

Limits: 70-130 %

"

"

"

101 %

Limits: 70-130 %

"

"

"

98 %

Limits: 70-130 %

"

"

"

Matrix: Soil

ND

---

0.00773

mg/kg dry

50

02/27/16 16:56

5035/8260B

Toluene

ND

---

0.0386

"

"

"

"

Ethylbenzene

ND

---

0.0193

"

"

"

"

Xylenes, total

ND

---

0.0580

"

"

"

"

Naphthalene

ND

---

0.0773

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0386

"

"

"

"

Isopropylbenzene

ND

---

0.0386

"

"

"

"

n-Propylbenzene

ND

---

0.0193

"

"

"

"

DRAFT REPORT, DATA SUBJECT TO CHANGE

M-04

Batch: 6020834

Benzene

DRAFT REPORT

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

Ex Sidewall S (A6B0900-19)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

1,2,4-Trimethylbenzene

ND

---

0.0386

mg/kg dry

50

"

5035/8260B

1,3,5-Trimethylbenzene

ND

---

0.0386

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0193

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0193

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 94 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

91 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 70-130 %

"

"

"

Ex Sidewall W (A6B0900-20)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.0119

mg/kg dry

50

02/27/16 17:22

5035/8260B

Toluene

ND

---

0.0594

"

"

"

"

Ethylbenzene

ND

---

0.0297

"

"

"

"

Xylenes, total

ND

---

0.0890

"

"

"

"

Naphthalene

ND

---

0.119

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0594

"

"

"

"

Isopropylbenzene

ND

---

0.0594

"

"

"

"

n-Propylbenzene

ND

---

0.0297

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0594

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0594

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0297

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0297

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 94 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

92 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

Ex Sidewall E (A6B0900-21)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.00717

mg/kg dry

50

02/27/16 17:49

5035/8260B

Toluene

ND

---

0.0358

"

"

"

"

Ethylbenzene

ND

---

0.0179

"

"

"

"

Xylenes, total

ND

---

0.0538

"

"

"

"

Naphthalene

ND

---

0.0717

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0358

"

"

"

"

Isopropylbenzene

ND

---

0.0358

"

"

"

"

n-Propylbenzene

ND

---

0.0179

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0358

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

Ex Sidewall E (A6B0900-21)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

1,3,5-Trimethylbenzene

ND

---

0.0358

mg/kg dry

50

"

5035/8260B

1,2-Dibromoethane (EDB)

ND

---

0.0179

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0179

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 93 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

91 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

1A (A6B0900-01)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0143

mg/kg dry

02/27/16 14:05

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0143

"

"

"

"

Anthracene

ND

---

0.0143

"

"

"

"

Benz(a)anthracene

ND

---

0.0143

"

"

"

"

Benzo(a)pyrene

ND

---

0.0143

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0143

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0143

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0143

"

"

"

"

Chrysene

ND

---

0.0143

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0143

"

"

"

"

Dibenzofuran

ND

---

0.0143

"

"

"

"

Fluoranthene

ND

---

0.0143

"

"

"

"

Fluorene

ND

---

0.0143

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0143

"

"

"

"

1-Methylnaphthalene

ND

---

0.0143

"

"

"

"

2-Methylnaphthalene

ND

---

0.0143

"

"

"

"

Naphthalene

ND

---

0.0143

"

"

"

"

Phenanthrene

ND

---

0.0143

"

"

"

"

Pyrene

ND

---

0.0143

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 87 %

Limits: 44-115 %

"

"

"

105 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

1B (A6B0900-02)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0161

mg/kg dry

02/27/16 14:59

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0161

"

"

"

"

Anthracene

ND

---

0.0161

"

"

"

"

Benz(a)anthracene

ND

---

0.0161

"

"

"

"

Benzo(a)pyrene

ND

---

0.0161

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0161

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0161

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0161

"

"

"

"

Chrysene

ND

---

0.0161

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0161

"

"

"

"

Dibenzofuran

ND

---

0.0161

"

"

"

"

Fluoranthene

ND

---

0.0161

"

"

"

"

Fluorene

ND

---

0.0161

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0161

"

"

"

"

1-Methylnaphthalene

ND

---

0.0161

"

"

"

"

2-Methylnaphthalene

ND

---

0.0161

"

"

"

"

Naphthalene

ND

---

0.0161

"

"

"

"

Phenanthrene

ND

---

0.0161

"

"

"

"

Pyrene

ND

---

0.0161

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 89 %

Limits: 44-115 %

"

"

"

107 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

2A (A6B0900-04)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0130

mg/kg dry

02/27/16 15:27

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0130

"

"

"

"

Anthracene

ND

---

0.0130

"

"

"

"

Benz(a)anthracene

ND

---

0.0130

"

"

"

"

Benzo(a)pyrene

ND

---

0.0130

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0130

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0130

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0130

"

"

"

"

Chrysene

ND

---

0.0130

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0130

"

"

"

"

Dibenzofuran

ND

---

0.0130

"

"

"

"

Fluoranthene

ND

---

0.0130

"

"

"

"

Fluorene

ND

---

0.0130

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0130

"

"

"

"

1-Methylnaphthalene

ND

---

0.0130

"

"

"

"

2-Methylnaphthalene

ND

---

0.0130

"

"

"

"

Naphthalene

ND

---

0.0130

"

"

"

"

Phenanthrene

ND

---

0.0130

"

"

"

"

Pyrene

ND

---

0.0130

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 86 %

Limits: 44-115 %

"

"

"

102 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

2B (A6B0900-05)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0180

mg/kg dry

02/27/16 15:54

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0180

"

"

"

"

Anthracene

ND

---

0.0180

"

"

"

"

Benz(a)anthracene

ND

---

0.0180

"

"

"

"

Benzo(a)pyrene

ND

---

0.0180

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0180

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0180

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0180

"

"

"

"

Chrysene

ND

---

0.0180

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0180

"

"

"

"

Dibenzofuran

ND

---

0.0180

"

"

"

"

Fluoranthene

ND

---

0.0180

"

"

"

"

Fluorene

ND

---

0.0180

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0180

"

"

"

"

1-Methylnaphthalene

ND

---

0.0180

"

"

"

"

2-Methylnaphthalene

ND

---

0.0180

"

"

"

"

Naphthalene

ND

---

0.0180

"

"

"

"

Phenanthrene

ND

---

0.0180

"

"

"

"

Pyrene

ND

---

0.0180

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 80 %

Limits: 44-115 %

"

"

"

98 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 19 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

2D (A6B0900-07)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0180

mg/kg dry

02/27/16 13:37

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0180

"

"

"

"

Anthracene

ND

---

0.0180

"

"

"

"

Benz(a)anthracene

ND

---

0.0198

"

"

"

"

Benzo(a)pyrene

ND

---

0.0180

"

"

"

"

Benzo(b)fluoranthene

0.0249

---

0.0180

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0180

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0180

"

"

"

"

Chrysene

ND

---

0.0207

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0180

"

"

"

"

Dibenzofuran

ND

---

0.0180

"

"

"

"

Fluoranthene

ND

---

0.0180

"

"

"

"

0.0229

---

0.0180

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0180

"

"

"

"

1-Methylnaphthalene

0.0284

---

0.0180

"

"

"

"

2-Methylnaphthalene

0.0433

---

0.0180

"

"

"

"

Naphthalene

0.0502

---

0.0180

"

"

"

"

Phenanthrene

0.0229

---

0.0180

"

"

"

"

ND

---

0.0180

"

"

"

"

Fluorene

Pyrene
Surrogate: 2-Fluorobiphenyl (Surr)
p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 84 %

Limits: 44-115 %

"

"

"

102 %

Limits: 54-127 %

"

"

"

R-02
M-02

R-02

M-02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 20 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3A (A6B0900-08)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0136

mg/kg dry

02/27/16 16:21

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0136

"

"

"

"

Anthracene

ND

---

0.0136

"

"

"

"

Benz(a)anthracene

ND

---

0.0136

"

"

"

"

Benzo(a)pyrene

ND

---

0.0136

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0136

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0136

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0136

"

"

"

"

Chrysene

ND

---

0.0136

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0136

"

"

"

"

Dibenzofuran

ND

---

0.0136

"

"

"

"

Fluoranthene

ND

---

0.0136

"

"

"

"

Fluorene

ND

---

0.0136

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0136

"

"

"

"

1-Methylnaphthalene

ND

---

0.0136

"

"

"

"

2-Methylnaphthalene

ND

---

0.0136

"

"

"

"

Naphthalene

ND

---

0.0136

"

"

"

"

Phenanthrene

ND

---

0.0136

"

"

"

"

Pyrene

ND

---

0.0136

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 87 %

Limits: 44-115 %

"

"

"

107 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 21 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3B (A6B0900-09)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0129

mg/kg dry

02/27/16 16:48

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0129

"

"

"

"

Anthracene

ND

---

0.0129

"

"

"

"

Benz(a)anthracene

ND

---

0.0129

"

"

"

"

Benzo(a)pyrene

ND

---

0.0129

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0129

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0129

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0129

"

"

"

"

Chrysene

ND

---

0.0129

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0129

"

"

"

"

Dibenzofuran

ND

---

0.0129

"

"

"

"

Fluoranthene

ND

---

0.0129

"

"

"

"

Fluorene

ND

---

0.0129

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0129

"

"

"

"

1-Methylnaphthalene

ND

---

0.0129

"

"

"

"

2-Methylnaphthalene

ND

---

0.0129

"

"

"

"

Naphthalene

ND

---

0.0129

"

"

"

"

Phenanthrene

ND

---

0.0129

"

"

"

"

Pyrene

ND

---

0.0129

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 92 %

Limits: 44-115 %

"

"

"

109 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 22 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3C (A6B0900-10)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0135

mg/kg dry

02/27/16 17:15

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0135

"

"

"

"

Anthracene

ND

---

0.0135

"

"

"

"

Benz(a)anthracene

ND

---

0.0135

"

"

"

"

Benzo(a)pyrene

ND

---

0.0135

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0135

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0135

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0135

"

"

"

"

Chrysene

ND

---

0.0135

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0135

"

"

"

"

Dibenzofuran

ND

---

0.0135

"

"

"

"

Fluoranthene

ND

---

0.0135

"

"

"

"

Fluorene

ND

---

0.0135

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0135

"

"

"

"

1-Methylnaphthalene

ND

---

0.0135

"

"

"

"

2-Methylnaphthalene

ND

---

0.0135

"

"

"

"

Naphthalene

ND

---

0.0135

"

"

"

"

Phenanthrene

ND

---

0.0135

"

"

"

"

Pyrene

ND

---

0.0135

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 89 %

Limits: 44-115 %

"

"

"

109 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 23 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3D (A6B0900-11)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0138

mg/kg dry

02/27/16 18:09

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0138

"

"

"

"

Anthracene

ND

---

0.0138

"

"

"

"

Benz(a)anthracene

ND

---

0.0138

"

"

"

"

Benzo(a)pyrene

ND

---

0.0138

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0138

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0138

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0138

"

"

"

"

Chrysene

ND

---

0.0138

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0138

"

"

"

"

Dibenzofuran

ND

---

0.0138

"

"

"

"

Fluoranthene

ND

---

0.0138

"

"

"

"

Fluorene

ND

---

0.0138

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0138

"

"

"

"

1-Methylnaphthalene

ND

---

0.0138

"

"

"

"

2-Methylnaphthalene

ND

---

0.0138

"

"

"

"

Naphthalene

ND

---

0.0138

"

"

"

"

Phenanthrene

ND

---

0.0138

"

"

"

"

Pyrene

ND

---

0.0138

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 86 %

Limits: 44-115 %

"

"

"

100 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 24 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4A (A6B0900-12)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0149

mg/kg dry

02/27/16 18:36

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0149

"

"

"

"

Anthracene

ND

---

0.0149

"

"

"

"

Benz(a)anthracene

ND

---

0.0149

"

"

"

"

Benzo(a)pyrene

ND

---

0.0149

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0149

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0149

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0149

"

"

"

"

Chrysene

ND

---

0.0149

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0149

"

"

"

"

Dibenzofuran

ND

---

0.0149

"

"

"

"

Fluoranthene

ND

---

0.0149

"

"

"

"

Fluorene

ND

---

0.0149

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0149

"

"

"

"

1-Methylnaphthalene

ND

---

0.0149

"

"

"

"

2-Methylnaphthalene

ND

---

0.0149

"

"

"

"

Naphthalene

ND

---

0.0149

"

"

"

"

Phenanthrene

ND

---

0.0149

"

"

"

"

Pyrene

ND

---

0.0149

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 86 %

Limits: 44-115 %

"

"

"

102 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 25 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4B (A6B0900-13)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0123

mg/kg dry

02/27/16 19:02

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0123

"

"

"

"

Anthracene

ND

---

0.0123

"

"

"

"

Benz(a)anthracene

ND

---

0.0123

"

"

"

"

Benzo(a)pyrene

ND

---

0.0123

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0123

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0123

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0123

"

"

"

"

Chrysene

ND

---

0.0123

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0123

"

"

"

"

Dibenzofuran

ND

---

0.0123

"

"

"

"

Fluoranthene

ND

---

0.0123

"

"

"

"

Fluorene

ND

---

0.0123

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0123

"

"

"

"

1-Methylnaphthalene

ND

---

0.0123

"

"

"

"

2-Methylnaphthalene

ND

---

0.0123

"

"

"

"

Naphthalene

ND

---

0.0123

"

"

"

"

Phenanthrene

ND

---

0.0123

"

"

"

"

Pyrene

ND

---

0.0123

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 95 %

Limits: 44-115 %

"

"

"

119 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 26 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4C (A6B0900-14)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0144

mg/kg dry

02/27/16 19:29

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0144

"

"

"

"

Anthracene

ND

---

0.0144

"

"

"

"

Benz(a)anthracene

ND

---

0.0144

"

"

"

"

Benzo(a)pyrene

ND

---

0.0144

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0144

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0144

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0144

"

"

"

"

Chrysene

ND

---

0.0144

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0144

"

"

"

"

Dibenzofuran

ND

---

0.0144

"

"

"

"

Fluoranthene

ND

---

0.0144

"

"

"

"

Fluorene

ND

---

0.0144

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0144

"

"

"

"

1-Methylnaphthalene

ND

---

0.0144

"

"

"

"

2-Methylnaphthalene

ND

---

0.0144

"

"

"

"

Naphthalene

ND

---

0.0144

"

"

"

"

Phenanthrene

ND

---

0.0144

"

"

"

"

Pyrene

ND

---

0.0144

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 91 %

Limits: 44-115 %

"

"

"

115 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 27 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4D (A6B0900-15)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0120

mg/kg dry

02/27/16 19:56

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0120

"

"

"

"

Anthracene

ND

---

0.0120

"

"

"

"

Benz(a)anthracene

ND

---

0.0120

"

"

"

"

Benzo(a)pyrene

ND

---

0.0120

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0120

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0120

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0120

"

"

"

"

Chrysene

ND

---

0.0120

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0120

"

"

"

"

Dibenzofuran

ND

---

0.0120

"

"

"

"

Fluoranthene

ND

---

0.0120

"

"

"

"

Fluorene

ND

---

0.0120

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0120

"

"

"

"

1-Methylnaphthalene

ND

---

0.0120

"

"

"

"

2-Methylnaphthalene

ND

---

0.0120

"

"

"

"

Naphthalene

ND

---

0.0120

"

"

"

"

Phenanthrene

ND

---

0.0120

"

"

"

"

Pyrene

ND

---

0.0120

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 92 %

Limits: 44-115 %

"

"

"

115 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 28 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

0A (A6B0900-16)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0173

mg/kg dry

02/27/16 20:23

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0173

"

"

"

"

Anthracene

ND

---

0.0173

"

"

"

"

Benz(a)anthracene

ND

---

0.0173

"

"

"

"

Benzo(a)pyrene

ND

---

0.0173

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0173

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0173

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0173

"

"

"

"

Chrysene

ND

---

0.0173

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0173

"

"

"

"

Dibenzofuran

ND

---

0.0173

"

"

"

"

Fluoranthene

ND

---

0.0173

"

"

"

"

Fluorene

ND

---

0.0173

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0173

"

"

"

"

1-Methylnaphthalene

ND

---

0.0173

"

"

"

"

2-Methylnaphthalene

ND

---

0.0173

"

"

"

"

Naphthalene

ND

---

0.0173

"

"

"

"

Phenanthrene

ND

---

0.0173

"

"

"

"

Pyrene

ND

---

0.0173

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 91 %

Limits: 44-115 %

"

"

"

111 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 29 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

0B (A6B0900-17)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0167

mg/kg dry

02/27/16 20:49

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0167

"

"

"

"

Anthracene

ND

---

0.0167

"

"

"

"

Benz(a)anthracene

ND

---

0.0167

"

"

"

"

Benzo(a)pyrene

ND

---

0.0167

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0167

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0167

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0167

"

"

"

"

Chrysene

ND

---

0.0167

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0167

"

"

"

"

Dibenzofuran

0.0620

---

0.0167

"

"

"

"

Fluoranthene

ND

---

0.0167

"

"

"

"

Fluorene

ND

---

0.0401

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0167

"

"

"

"

1-Methylnaphthalene

0.114

---

0.0167

"

"

"

"

2-Methylnaphthalene

0.155

---

0.0167

"

"

"

"

ND

---

0.0301

"

"

"

"

Phenanthrene

0.0489

---

0.0167

"

"

"

"

Pyrene

0.0411

---

0.0167

"

"

"

"

Naphthalene

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 100 %

Limits: 44-115 %

"

"

"

118 %

Limits: 54-127 %

"

"

"

R-02

R-02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 30 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

0C (A6B0900-18)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Notes

Batch: 6020836

Acenaphthene

ND

---

0.208

mg/kg dry

02/27/16 21:16

EPA 8270D (SIM)

R-02

Acenaphthylene

ND

---

0.0763

"

"

"

"

R-02

Anthracene

ND

---

0.104

"

"

"

"

R-02

Benz(a)anthracene

ND

---

0.0242

"

"

"

"

R-02

Benzo(a)pyrene

ND

---

0.0186

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0186

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0186

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0186

"

"

"

"

Chrysene

ND

---

0.0260

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0186

"

"

"

"

Dibenzofuran

0.376

---

0.0186

"

"

"

"

Fluoranthene

ND

---

0.0186

"

"

"

"

0.454

---

0.0186

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0186

"

"

"

"

Fluorene
1-Methylnaphthalene

3.29

---

0.0186

"

"

"

"

2-Methylnaphthalene

5.58

---

0.0186

"

"

"

"

Naphthalene

2.08

---

0.0186

"

"

"

"

Phenanthrene

0.740

---

0.0186

"

"

"

"

Pyrene

0.389

---

0.0186

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 78 %

Limits: 44-115 %

"

"

"

112 %

Limits: 54-127 %

"

"

"

R-02

M-04

M-02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 31 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

Ex Sidewall S (A6B0900-19)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0107

mg/kg dry

02/27/16 21:43

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0107

"

"

"

"

Anthracene

ND

---

0.0107

"

"

"

"

Benz(a)anthracene

ND

---

0.0107

"

"

"

"

Benzo(a)pyrene

ND

---

0.0107

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0107

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0107

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0107

"

"

"

"

Chrysene

ND

---

0.0107

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0107

"

"

"

"

Dibenzofuran

ND

---

0.0107

"

"

"

"

Fluoranthene

ND

---

0.0107

"

"

"

"

Fluorene

ND

---

0.0107

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0107

"

"

"

"

1-Methylnaphthalene

ND

---

0.0107

"

"

"

"

2-Methylnaphthalene

ND

---

0.0107

"

"

"

"

Naphthalene

ND

---

0.0107

"

"

"

"

Phenanthrene

ND

---

0.0107

"

"

"

"

Pyrene

ND

---

0.0107

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 97 %

Limits: 44-115 %

"

"

"

123 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 32 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

Ex Sidewall W (A6B0900-20)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0134

mg/kg dry

02/27/16 22:10

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0134

"

"

"

"

Anthracene

ND

---

0.0134

"

"

"

"

Benz(a)anthracene

ND

---

0.0134

"

"

"

"

Benzo(a)pyrene

ND

---

0.0134

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0134

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0134

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0134

"

"

"

"

Chrysene

ND

---

0.0134

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0134

"

"

"

"

Dibenzofuran

ND

---

0.0134

"

"

"

"

Fluoranthene

ND

---

0.0134

"

"

"

"

Fluorene

ND

---

0.0134

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0134

"

"

"

"

1-Methylnaphthalene

ND

---

0.0134

"

"

"

"

2-Methylnaphthalene

ND

---

0.0134

"

"

"

"

Naphthalene

ND

---

0.0134

"

"

"

"

Phenanthrene

ND

---

0.0134

"

"

"

"

Pyrene

ND

---

0.0134

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 93 %

Limits: 44-115 %

"

"

"

114 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 33 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

Ex Sidewall E (A6B0900-21)

Acenaphthene

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Notes

Batch: 6020836

ND

---

0.0105

mg/kg dry

02/27/16 22:36

EPA 8270D (SIM)

Acenaphthylene

0.0181

---

0.0105

"

"

"

"

Anthracene

0.0526

---

0.0105

"

"

"

"

Benz(a)anthracene

0.635

---

0.0105

"

"

"

"

Benzo(a)pyrene

0.219

---

0.0105

"

"

"

"

Benzo(b)fluoranthene

0.603

---

0.0105

"

"

"

"

M-02, Q-42

Benzo(k)fluoranthene

0.206

---

0.0105

"

"

"

"

M-02

Benzo(g,h,i)perylene

0.0799

---

0.0105

"

"

"

"

Chrysene

0.947

---

0.0105

"

"

"

"

Dibenz(a,h)anthracene

0.0306

---

0.0105

"

"

"

"

Dibenzofuran

ND

---

0.0105

"

"

"

"

Fluoranthene

1.86

---

0.0105

"

"

"

"

Fluorene

ND

---

0.0105

"

"

"

"

0.116

---

0.0105

"

"

"

"

Indeno(1,2,3-cd)pyrene

1-Methylnaphthalene

ND

---

0.0105

"

"

"

"

2-Methylnaphthalene

0.0135

---

0.0105

"

"

"

"

ND

---

0.0105

"

"

"

"

0.0119

---

0.0105

"

"

"

"

1.60

---

0.0105

"

"

"

"

Naphthalene
Phenanthrene
Pyrene
Surrogate: 2-Fluorobiphenyl (Surr)
p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 95 %

Limits: 44-115 %

"

"

"

121 %

Limits: 54-127 %

"

"

"

Q-42

Q-42

Q-42

Q-42

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 34 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

1A (A6B0900-01)

% Solids

Matrix: Soil

65.4

---

57.4

---

44.8

---

72.9

---

1B (A6B0900-02)

% Solids

49.6

---

36.0

---

53.9

---

68.4

---

75.0

---

67.6

---

63.3

---

64.6

---

74.8

---

67.9

---

76.7

---

49.2

---

1.00
Matrix: Soil

0A (A6B0900-16)

% Solids

1.00
Matrix: Soil

4D (A6B0900-15)

% Solids

1.00
Matrix: Soil

4C (A6B0900-14)

% Solids

1.00
Matrix: Soil

4B (A6B0900-13)

% Solids

1.00
Matrix: Soil

4A (A6B0900-12)

% Solids

1.00
Matrix: Soil

3D (A6B0900-11)

% Solids

1.00
Matrix: Soil

3C (A6B0900-10)

% Solids

1.00
Matrix: Soil

3B (A6B0900-09)

% Solids

1.00
Matrix: Soil

3A (A6B0900-08)

% Solids

1.00
Matrix: Soil

2D (A6B0900-07)

% Solids

1.00
Matrix: Soil

2C (A6B0900-06)

% Solids

1.00
Matrix: Soil

2B (A6B0900-05)

% Solids

1.00
Matrix: Soil

2A (A6B0900-04)

% Solids

1.00
Matrix: Soil

1C (A6B0900-03)

% Solids

Reporting
Limit

1.00
Matrix: Soil

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1.00

Dilution

Units

Date Analyzed

Method

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

Notes

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 35 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

55.4

---

0B (A6B0900-17)

% Solids

Matrix: Soil

0C (A6B0900-18)

% Solids

51.2

---

91.7

---

71.1

---

82.9

---

1.00
Matrix: Soil

Ex Sidewall E (A6B0900-21)

% Solids

1.00
Matrix: Soil

Ex Sidewall W (A6B0900-20)

% Solids

1.00
Matrix: Soil

Ex Sidewall S (A6B0900-19)

% Solids

Reporting
Limit

1.00
Matrix: Soil

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1.00

Dilution

Units

Date Analyzed

Method

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

Notes

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 36 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020835 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:01 Analyzed: 02/27/16 13:13

Blank (6020835-BLK1)
NWTPH-Dx

Diesel

ND

---

25.0

mg/kg wet

---

---

---

---

---

---

Oil

ND

---

50.0

"

"

---

---

---

---

---

---

---

---

Surr: o-Terphenyl (Surr)

Recovery: 97 %

Limits: 50-150 %

Dilution: 1x

Prepared: 02/27/16 10:01 Analyzed: 02/27/16 13:33

LCS (6020835-BS1)
NWTPH-Dx

Diesel

119

---

Surr: o-Terphenyl (Surr)

25.0
Recovery: 98 %

mg/kg wet

125

Limits: 50-150 %

---

95

76-115%

Dilution: 1x

Prepared: 02/27/16 10:01 Analyzed: 02/27/16 14:13

Duplicate (6020835-DUP1)
QC Source Sample: 1C (A6B0900-03)
NWTPH-Dx

Diesel
Oil

54200

---

2010

mg/kg dry

50

---

66400

---

---

20

30%

ND

---

4030

"

"

---

ND

---

---

---

30%

Surr: o-Terphenyl (Surr)

Recovery: %

Limits: 50-150 %

Dilution: 50x

S-01

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:13

Blank (6020836-BLK1)
NWTPH-Dx

Diesel

ND

---

25.0

mg/kg wet

---

---

---

---

---

---

Oil

ND

---

50.0

"

"

---

---

---

---

---

---

---

---

34

30%

Surr: o-Terphenyl (Surr)

Recovery: 92 %

Limits: 50-150 %

Dilution: 1x

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:33

LCS (6020836-BS1)
NWTPH-Dx

Diesel

120

---

Surr: o-Terphenyl (Surr)

25.0
Recovery: 88 %

mg/kg wet

125

Limits: 50-150 %

---

96

76-115%

Dilution: 1x

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:13

Duplicate (6020836-DUP1)
QC Source Sample: 1A (A6B0900-01)
NWTPH-Dx

Diesel

33.9

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

26.9

mg/kg dry

---

24.2

---

---

F-17, Q-05

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 37 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

42

30%

F-17, Q-05

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:13

Duplicate (6020836-DUP1)
QC Source Sample: 1A (A6B0900-01)

Oil

188

---

Surr: o-Terphenyl (Surr)

53.7
Recovery: 89 %

mg/kg dry

"

---

Limits: 50-150 %

123

---

---

Dilution: 1x

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 17:52

Duplicate (6020836-DUP2)
QC Source Sample: 3C (A6B0900-10)
NWTPH-Dx

Diesel

34.3

---

27.3

mg/kg dry

---

23.7

---

---

36

30%

F-17, Q-05

Oil

122

---

54.6

"

"

---

98.7

---

---

21

30%

F-17

Surr: o-Terphenyl (Surr)

Recovery: 88 %

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Limits: 50-150 %

Dilution: 1x

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 38 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020833 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 13:26

Blank (6020833-BLK1)
5035/8260B

Benzene

ND

---

0.00667

mg/kg wet

50

---

---

---

---

---

---

Toluene

ND

---

0.0333

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

0.0500

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0667

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

ND

---

0.0333

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.0167

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 107 %

Limits: 70-130 %

Dilution: 1x

103 %

70-130 %

"

Toluene-d8 (Surr)

98 %

70-130 %

"

4-Bromofluorobenzene (Surr)

97 %

70-130 %

"

1,4-Difluorobenzene (Surr)

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:01

LCS (6020833-BS1)
5035/8260B

Benzene

1.08

---

0.0100

mg/kg wet

50

1.00

---

108

65-135%

Toluene

1.02

---

0.0500

"

"

"

---

102

"

---

---

Ethylbenzene

0.979

---

0.0250

"

"

"

---

98

"

---

---

Xylenes, total

2.85

---

0.0750

"

"

3.00

---

95

"

---

---

Naphthalene

0.948

---

0.100

"

"

1.00

---

95

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

1.01

---

0.0500

"

"

"

---

101

"

---

---

0.982

---

0.0500

"

"

"

---

98

"

---

---

n-Propylbenzene

0.991

---

0.0250

"

"

"

---

99

"

---

---

1,2,4-Trimethylbenzene

0.983

---

0.0500

"

"

"

---

98

"

---

---

1,3,5-Trimethylbenzene

0.996

---

0.0500

"

"

"

---

100

"

---

---

1,2-Dibromoethane (EDB)

1.08

---

0.0250

"

"

"

---

108

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 39 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020833 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:01

LCS (6020833-BS1)

1,2-Dichloroethane (EDC)

Source
Result

0.986

Surr: Dibromofluoromethane (Surr)

---

0.0250

mg/kg wet

"

"

---

Recovery: 102 %

Limits: 70-130 %

Dilution: 1x

102 %

70-130 %

"

Toluene-d8 (Surr)

97 %

70-130 %

"

4-Bromofluorobenzene (Surr)

97 %

70-130 %

"

1,4-Difluorobenzene (Surr)

99

"

---

---

Prepared: 02/26/16 09:40 Analyzed: 02/27/16 14:23

Duplicate (6020833-DUP1)
QC Source Sample: 1A (A6B0900-01)
5035/8260B

Benzene

ND

---

0.0198

mg/kg dry

50

---

ND

---

---

---

30%

Toluene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

Ethylbenzene

ND

---

0.0494

"

"

---

ND

---

---

---

30%

Xylenes, total

ND

---

0.148

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

0.198

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

ND

---

0.0988

"

"

---

ND

---

---

---

30%

n-Propylbenzene

ND

---

0.0494

"

"

---

ND

---

---

---

30%

1,2,4-Trimethylbenzene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

1,3,5-Trimethylbenzene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

1,2-Dibromoethane (EDB)

ND

---

0.0494

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.0494

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 70-130 %

Dilution: 1x

101 %

70-130 %

"

Toluene-d8 (Surr)

99 %

70-130 %

"

4-Bromofluorobenzene (Surr)

93 %

70-130 %

"

1,4-Difluorobenzene (Surr)

Prepared: 02/26/16 10:30 Analyzed: 02/27/16 19:35

Matrix Spike (6020833-MS1)


QC Source Sample: 4B (A6B0900-13)
5035/8260B

Benzene

1.75

---

0.0162

mg/kg dry

50

1.62

ND

108

65-135%

---

---

Toluene

1.64

---

0.0809

"

"

"

ND

101

"

---

---

Ethylbenzene

1.59

---

0.0404

"

"

"

ND

98

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 40 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020833 - EPA 5035A

Prepared: 02/26/16 10:30 Analyzed: 02/27/16 19:35

Matrix Spike (6020833-MS1)


QC Source Sample: 4B (A6B0900-13)

Xylenes, total

4.58

---

0.121

mg/kg dry

"

4.86

ND

94

"

---

---

Naphthalene

1.39

---

0.162

"

"

1.62

ND

86

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

1.63

---

0.0809

"

"

"

ND

101

"

---

---

1.57

---

0.0809

"

"

"

ND

97

"

---

---

n-Propylbenzene

1.55

---

0.0404

"

"

"

ND

96

"

---

---

1,2,4-Trimethylbenzene

1.51

---

0.0809

"

"

"

ND

93

"

---

---

1,3,5-Trimethylbenzene

1.55

---

0.0809

"

"

"

ND

96

"

---

---

1,2-Dibromoethane (EDB)

1.67

---

0.0404

"

"

"

ND

103

"

---

---

1,2-Dichloroethane (EDC)

1.67

---

0.0404

"

"

"

ND

103

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

99 %

70-130 %

"

Toluene-d8 (Surr)

98 %

70-130 %

"

4-Bromofluorobenzene (Surr)

93 %

70-130 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 41 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020834 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 13:48

Blank (6020834-BLK1)
5035/8260B

Benzene

ND

---

0.00667

mg/kg wet

50

---

---

---

---

---

---

Toluene

ND

---

0.0333

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

0.0500

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0667

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

ND

---

0.0333

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.0167

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 96 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

92 %

70-130 %

"

Toluene-d8 (Surr)

97 %

70-130 %

"

4-Bromofluorobenzene (Surr)

98 %

70-130 %

"

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:54

LCS (6020834-BS1)
5035/8260B

Benzene

0.878

---

0.0100

mg/kg wet

50

1.00

---

88

65-135%

Toluene

0.924

---

0.0500

"

"

"

---

92

"

---

---

Ethylbenzene

0.981

---

0.0250

"

"

"

---

98

"

---

---

Xylenes, total

2.96

---

0.0750

"

"

3.00

---

99

"

---

---

Naphthalene

0.940

---

0.100

"

"

1.00

---

94

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

0.876

---

0.0500

"

"

"

---

88

"

---

---

1.05

---

0.0500

"

"

"

---

105

"

---

---

n-Propylbenzene

0.898

---

0.0250

"

"

"

---

90

"

---

---

1,2,4-Trimethylbenzene

0.988

---

0.0500

"

"

"

---

99

"

---

---

1,3,5-Trimethylbenzene

0.998

---

0.0500

"

"

"

---

100

"

---

---

1,2-Dibromoethane (EDB)

1.00

---

0.0250

"

"

"

---

100

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 42 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020834 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:54

LCS (6020834-BS1)

1,2-Dichloroethane (EDC)

Source
Result

0.848

---

Surr: Dibromofluoromethane (Surr)

0.0250

mg/kg wet

"

"

---

Recovery: 97 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

92 %

70-130 %

"

Toluene-d8 (Surr)

95 %

70-130 %

"

4-Bromofluorobenzene (Surr)

99 %

70-130 %

"

85

"

---

---

Prepared: 02/26/16 12:05 Analyzed: 02/27/16 16:02

Duplicate (6020834-DUP1)
QC Source Sample: 0B (A6B0900-17)
5035/8260B

Benzene

ND

---

0.0288

mg/kg dry

50

---

0.0177

---

---

***

30%

Toluene

0.247

Ethylbenzene

0.220

---

0.144

"

"

---

0.224

---

---

10

30%

---

0.0719

"

"

---

0.200

---

---

10

30%

Xylenes, total
Naphthalene

1.16

---

0.216

"

"

---

1.04

---

---

11

30%

ND

---

0.288

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.144

"

"

---

ND

---

---

---

30%

ND

---

0.144

"

"

---

ND

---

---

---

30%

n-Propylbenzene

0.167

---

0.0719

"

"

---

0.162

---

---

30%

1,2,4-Trimethylbenzene

0.698

---

0.144

"

"

---

0.755

---

---

30%

1,3,5-Trimethylbenzene

0.262

---

0.144

"

"

---

0.264

---

---

0.7

30%

1,2-Dibromoethane (EDB)

ND

---

0.0719

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.0719

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 93 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

91 %

70-130 %

"

Toluene-d8 (Surr)

95 %

70-130 %

"

100 %

70-130 %

"

4-Bromofluorobenzene (Surr)

Prepared: 02/26/16 12:40 Analyzed: 02/27/16 18:16

Matrix Spike (6020834-MS1)


QC Source Sample: Ex Sidewall E (A6B0900-21)
5035/8260B

Benzene

0.642

---

0.00717

mg/kg dry

50

0.710

ND

90

65-135%

---

---

Toluene

0.680

---

0.0358

"

"

"

ND

96

"

---

---

Ethylbenzene

0.718

---

0.0179

"

"

"

ND

101

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 43 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020834 - EPA 5035A

Prepared: 02/26/16 12:40 Analyzed: 02/27/16 18:16

Matrix Spike (6020834-MS1)


QC Source Sample: Ex Sidewall E (A6B0900-21)

Xylenes, total

2.16

---

0.0538

mg/kg dry

"

2.13

ND

102

"

---

---

Naphthalene

0.697

---

0.0717

"

"

0.710

ND

98

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

0.644

---

0.0358

"

"

"

ND

91

"

---

---

0.775

---

0.0358

"

"

"

ND

109

"

---

---

n-Propylbenzene

0.652

---

0.0179

"

"

"

ND

92

"

---

---

1,2,4-Trimethylbenzene

0.721

---

0.0358

"

"

"

ND

102

"

---

---

1,3,5-Trimethylbenzene

0.738

---

0.0358

"

"

"

ND

104

"

---

---

1,2-Dibromoethane (EDB)

0.746

---

0.0179

"

"

"

ND

105

"

---

---

1,2-Dichloroethane (EDC)

0.616

---

0.0179

"

"

"

ND

87

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 96 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

91 %

70-130 %

"

Toluene-d8 (Surr)

96 %

70-130 %

"

4-Bromofluorobenzene (Surr)

99 %

70-130 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 44 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 12:43

Blank (6020836-BLK2)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.00833

mg/kg wet

---

---

---

---

---

---

Acenaphthylene

ND

---

0.00833

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.00833

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.00833

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.00833

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.00833

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.00833

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.00833

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.00833

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.00833

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.00833

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.00833

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.00833

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.00833

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 91 %

Limits: 44-115 %

Dilution: 1x

104 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:10

LCS (6020836-BS2)
EPA 8270D (SIM)

Acenaphthene

0.718

---

0.0100

mg/kg wet

0.800

---

90

40-122%

---

Acenaphthylene

0.709

---

0.0100

"

"

"

---

89

32-132%

---

---

Anthracene

0.771

---

0.0100

"

"

"

---

96

47-123%

---

---

Benz(a)anthracene

0.701

---

0.0100

"

"

"

---

88

49-126%

---

---

Benzo(a)pyrene

0.727

---

0.0100

"

"

"

---

91

45-129%

---

---

Benzo(b)fluoranthene

0.729

---

0.0100

"

"

"

---

91

45-132%

---

---

Benzo(k)fluoranthene

0.731

---

0.0100

"

"

"

---

91

47-132%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 45 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:10

LCS (6020836-BS2)

Benzo(g,h,i)perylene

Source
Result

0.657

---

0.0100

"

"

"

---

82

43-134%

---

---

Chrysene

0.698

---

0.0100

"

"

"

---

87

50-124%

---

---

Dibenz(a,h)anthracene

0.691

---

0.0100

"

"

"

---

86

45-134%

---

---

Dibenzofuran

0.721

---

0.0100

"

"

"

---

90

44-120%

---

---

Fluoranthene

0.708

---

0.0100

"

"

"

---

89

50-127%

---

---

Fluorene

0.719

---

0.0100

"

"

"

---

90

43-125%

---

---

Indeno(1,2,3-cd)pyrene

0.653

---

0.0100

"

"

"

---

82

45-133%

---

---

1-Methylnaphthalene

0.677

---

0.0100

"

"

"

---

85

40-120%

---

---

2-Methylnaphthalene

0.715

---

0.0100

"

"

"

---

89

38-122%

---

---

Naphthalene

0.697

---

0.0100

"

"

"

---

87

35-123%

---

---

Phenanthrene

0.722

---

0.0100

"

"

"

---

90

50-121%

---

---

Pyrene

0.719

---

0.0100

"

"

"

---

90

47-127%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 92 %

Limits: 44-115 %

Dilution: 1x

101 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:32

Duplicate (6020836-DUP3)
QC Source Sample: 1A (A6B0900-01)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0134

mg/kg dry

---

ND

---

---

---

30%

Acenaphthylene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Anthracene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benz(a)anthracene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(a)pyrene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(b)fluoranthene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(k)fluoranthene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(g,h,i)perylene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Chrysene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Dibenz(a,h)anthracene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Dibenzofuran

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Fluoranthene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Fluorene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Indeno(1,2,3-cd)pyrene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 46 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:32

Duplicate (6020836-DUP3)
QC Source Sample: 1A (A6B0900-01)

1-Methylnaphthalene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

2-Methylnaphthalene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Phenanthrene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Pyrene

ND

---

"

"

---

ND

---

---

---

30%

Surr: 2-Fluorobiphenyl (Surr)

0.0134
Recovery: 88 %

Limits: 44-115 %

Dilution: 1x

106 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 17:43

Duplicate (6020836-DUP4)
QC Source Sample: 3C (A6B0900-10)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0137

mg/kg dry

---

ND

---

---

---

30%

Acenaphthylene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Anthracene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benz(a)anthracene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(a)pyrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(b)fluoranthene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(k)fluoranthene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(g,h,i)perylene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Chrysene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Dibenz(a,h)anthracene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Dibenzofuran

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Fluoranthene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Fluorene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Indeno(1,2,3-cd)pyrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

1-Methylnaphthalene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

2-Methylnaphthalene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Phenanthrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Pyrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 47 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 17:43

Duplicate (6020836-DUP4)
QC Source Sample: 3C (A6B0900-10)
Surr: 2-Fluorobiphenyl (Surr)

Recovery: 88 %

Limits: 44-115 %

Dilution: 1x

108 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 23:03

Matrix Spike (6020836-MS1)


QC Source Sample: Ex Sidewall E (A6B0900-21)
EPA 8270D (SIM)

Acenaphthene

0.751

---

0.0107

mg/kg dry

0.852

ND

88

40-122%

---

---

Acenaphthylene

0.758

---

0.0107

"

"

"

0.0181

87

32-132%

---

---

Anthracene

0.774

---

0.0107

"

"

"

0.0526

85

47-123%

---

---

Benz(a)anthracene

0.752

---

0.0107

"

"

"

0.635

14

49-126%

---

---

Benzo(a)pyrene

0.779

---

0.0107

"

"

"

0.219

66

45-129%

---

---

Benzo(b)fluoranthene

0.795

---

0.0107

"

"

"

0.603

22

45-132%

---

---

Benzo(k)fluoranthene

0.782

---

0.0107

"

"

"

0.206

68

47-132%

---

---

Benzo(g,h,i)perylene

0.580

---

0.0107

"

"

"

0.0799

59

43-134%

---

---

Chrysene

0.753

---

0.0107

"

"

"

0.947

-23

50-124%

---

---

Dibenz(a,h)anthracene

0.665

---

0.0107

"

"

"

0.0306

74

45-134%

---

---

Dibenzofuran

0.777

---

0.0107

"

"

"

0.00750

90

44-120%

---

---

Fluoranthene

0.792

---

0.0107

"

"

"

1.86

-125

50-127%

---

---

Fluorene

0.768

---

0.0107

"

"

"

ND

90

43-125%

---

---

Indeno(1,2,3-cd)pyrene

0.625

---

0.0107

"

"

"

0.116

60

45-133%

---

---

1-Methylnaphthalene

0.727

---

0.0107

"

"

"

0.00568

85

40-120%

---

---

2-Methylnaphthalene

0.765

---

0.0107

"

"

"

0.0135

88

38-122%

---

---

Naphthalene

0.724

---

0.0107

"

"

"

ND

85

35-123%

---

---

Phenanthrene

0.775

---

0.0107

"

"

"

0.0119

90

50-121%

---

---

Pyrene

0.784

---

0.0107

"

"

"

1.60

-96

47-127%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 92 %

Limits: 44-115 %

Dilution: 1x

112 %

54-127 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Q-04

Q-04

Q-04

Q-04

Q-04

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 48 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020837 - Total Solids (Dry Weight)

Prepared: 02/27/16 10:49 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP1)
QC Source Sample: 1A (A6B0900-01)
EPA 8000C

% Solids

52.0

---

1.00

% by
Weight

---

65.4

---

---

23

10%

10%

0.7

10%

10%

Q-04

Prepared: 02/27/16 10:49 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP2)
QC Source Sample: 3C (A6B0900-10)
EPA 8000C

% Solids

64.6

---

1.00

% by
Weight

---

67.6

---

---

Prepared: 02/27/16 10:49 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP3)
QC Source Sample: Ex Sidewall E (A6B0900-21)
EPA 8000C

% Solids

83.4

---

1.00

% by
Weight

---

82.9

---

---

Prepared: 02/27/16 13:01 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP4)
QC Source Sample: 0B (A6B0900-17)
EPA 8000C

% Solids

57.3

---

1.00

% by
Weight

---

55.4

---

---

No Client related Batch QC samples analyzed for this batch. See notes page for more information.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 49 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

SAMPLE PREPARATION INFORMATION


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Prep: EPA 3546 (Fuels)
Lab Number

Matrix

Method

Sampled

Prepared

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020835

A6B0900-03
A6B0900-06

Soil
Soil

NWTPH-Dx
NWTPH-Dx

02/26/16 10:00
02/26/16 10:10

02/27/16 10:01
02/27/16 10:01

10.94g/5mL
11.18g/5mL

10g/5mL
10g/5mL

0.91
0.89

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02

10.7g/5mL
10.83g/5mL
10.51g/5mL
11.24g/5mL
10.31g/5mL
10.74g/5mL
10.36g/5mL
10.97g/5mL
11.43g/5mL
10.38g/5mL
10.86g/5mL
10.21g/5mL
10.87g/5mL
11.77g/5mL
10.8g/5mL
10.49g/5mL
10.19g/5mL
10.53g/5mL
11.5g/5mL

10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL

0.94
0.92
0.95
0.89
0.97
0.93
0.97
0.91
0.88
0.96
0.92
0.98
0.92
0.85
0.93
0.95
0.98
0.95
0.87

Batch: 6020836

A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14RE1
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

RBDM Compounds (BTEX+) by EPA 8260B


Prep: EPA 5035A
Lab Number

Matrix

Method

Sampled

Prepared

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020833

A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08

Soil
Soil
Soil
Soil
Soil
Soil

5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

4.67g/5mL
4.4g/5mL
5.47g/5mL
4.01g/5mL
3.04g/5mL
4.31g/5mL

5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL

1.07
1.14
0.91
1.25
1.64
1.16

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 50 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5035A


Lab Number

A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13

Matrix

Method

Sampled

Prepared

Soil
Soil
Soil
Soil
Soil

5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B

02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30

02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30

5.25g/5mL
6.83g/5mL
5.61g/5mL
5.14g/5mL
5.22g/5mL

5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL

0.95
0.73
0.89
0.97
0.96

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B

02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

7.9g/5mL
9.59g/5mL
4.61g/5mL
4.71g/5mL
4.05g/5mL
7.98g/5mL
9.02g/5mL
11.83g/5mL

5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL

0.63
0.52
1.08
1.06
1.23
0.63
0.55
0.42

Batch: 6020834

A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3546 (Fuels)
Lab Number

Matrix

Method

Sampled

Prepared

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05

02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020836

A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

10.7g/5mL
10.83g/5mL
10.51g/5mL
11.24g/5mL
10.31g/5mL
10.74g/5mL
10.36g/5mL
10.97g/5mL
11.43g/5mL
10.38g/5mL
10.86g/5mL
10.21g/5mL
10.87g/5mL
11.77g/5mL
10.8g/5mL

10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL

0.94
0.92
0.95
0.89
0.97
0.93
0.97
0.91
0.88
0.96
0.92
0.98
0.92
0.85
0.93

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 51 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

SAMPLE PREPARATION INFORMATION


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Prep: EPA 3546 (Fuels)
Lab Number

A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Matrix

Soil
Soil
Soil
Soil

Method

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

Sampled

Prepared

02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

10.49g/5mL
10.19g/5mL
10.53g/5mL
11.5g/5mL

10g/5mL
10g/5mL
10g/5mL
10g/5mL

0.95
0.98
0.95
0.87

Percent Dry Weight


Prep: Total Solids (Dry Weight)
Lab Number

Matrix

Method

Sampled

Prepared

02/26/16 09:40
02/26/16 09:50
02/26/16 10:00
02/26/16 10:55
02/26/16 11:00
02/26/16 10:10
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020837

A6B0900-01
A6B0900-02
A6B0900-03
A6B0900-04
A6B0900-05
A6B0900-06
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A

1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A

NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 52 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

Notes and Definitions


Qualifiers:
F-17

No fuel pattern detected. The Diesel result represents carbon range C12 to C24, and the Oil result represents >C24 to C40.

M-02

Due to matrix interference, this analyte cannot be accurately quantified. The reported result is estimated.

M-04

Due to matrix interference, this analyte cannot be accurately quantified. The reported result may contain a high bias.

Q-04

Spike recovery and/or RPD is outside control limits due to a non-homogeneous sample matrix.

Q-05

Analyses are not controlled on RPD values from sample and duplicate concentrations are below 5 times the reporting level.

Q-42

Matrix Spike and/or Duplicate analysis was performed on this sample. % Recovery or RPD for this analyte is outside laboratory control
limits. (Refer to the QC Section of Analytical Report.)

R-02

The Reporting Limit for this analyte has been raised to account for interference from coeluting organic compounds present in the sample.

S-01

Surrogate recovery for this sample is not available due to sample dilution required from high analyte concentration and/or matrix
interference.

S-05

Surrogate recovery is estimated due to sample dilution required for high analyte concentration and/or matrix interference.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 53 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

***

Reported:

02/28/16 12:19

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 54 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/28/16 12:19

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 55 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/28/16 12:19

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 56 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/28/16 12:19

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 57 of 57

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Tuesday, March 8, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6C0227, which was received by the laboratory on
3/7/2016 at 6:38:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6C0227-01
A6C0227-02
A6C0227-03
A6C0227-04
A6C0227-05
A6C0227-06

Water
Water
Water
Water
Water
Soil

03/06/16 08:13
03/06/16 08:40
03/06/16 08:50
03/06/16 09:00
03/06/16 09:50
03/06/16 10:37

03/07/16 06:38
03/07/16 06:38
03/07/16 06:38
03/07/16 06:38
03/07/16 06:38
03/07/16 06:38

SW-02
SW-03
SW-04
SW-05
Foundation-S

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

Foundation-S (A6C0227-06RE1)

Diesel

Oil

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

27600

---

537

mg/kg dry

20

03/07/16 15:21

NWTPH-Dx

ND

---

1070

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: %

Notes

Batch: 6030186

Limits: 50-150 %

Q-42

S-01

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6C0227-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

---

0.200

ug/L

03/07/16 18:24

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 80-120 %

"

"

"

101 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-02 (A6C0227-02)

Matrix: Water

Batch: 6030189

Benzene

ND

---

0.200

ug/L

03/07/16 19:22

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 80-120 %

"

"

"

03/07/16 19:51

EPA 8260B

1,4-Difluorobenzene (Surr)

SW-03 (A6C0227-03)

Benzene

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

0.200

Notes

Batch: 6030189

Batch: 6030189

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6C0227-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

---

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-04 (A6C0227-04)

Matrix: Water

Batch: 6030189

Benzene

ND

---

0.200

ug/L

03/07/16 20:19

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 106 %

Limits: 80-120 %

"

"

"

103 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-05 (A6C0227-05)

Matrix: Water

Batch: 6030189

Benzene

ND

---

0.200

ug/L

03/07/16 20:48

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030189

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-05 (A6C0227-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Ethylbenzene

ND

---

0.500

ug/L

"

EPA 8260B

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030189

Recovery: 105 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

96 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6C0227-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0388

ug/L

03/07/16 15:20

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0388

"

"

"

"

Anthracene

ND

---

0.0388

"

"

"

"

Benz(a)anthracene

ND

---

0.0388

"

"

"

"

Benzo(a)pyrene

ND

---

0.0388

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0388

"

"

"

"

Chrysene

ND

---

0.0388

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0388

"

"

"

"

Dibenzofuran

ND

---

0.0388

"

"

"

"

Fluoranthene

ND

---

0.0388

"

"

"

"

Fluorene

ND

---

0.0388

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0388

"

"

"

"

1-Methylnaphthalene

ND

---

0.0777

"

"

"

"

2-Methylnaphthalene

ND

---

0.0777

"

"

"

"

Naphthalene

ND

---

0.0777

"

"

"

"

Phenanthrene

ND

---

0.0388

"

"

"

"

Pyrene

ND

---

0.0388

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 85 %

Limits: 44-120 %

"

"

"

101 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6C0227-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0388

ug/L

03/07/16 15:47

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0388

"

"

"

"

Anthracene

ND

---

0.0388

"

"

"

"

Benz(a)anthracene

ND

---

0.0388

"

"

"

"

Benzo(a)pyrene

ND

---

0.0388

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0388

"

"

"

"

Chrysene

ND

---

0.0388

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0388

"

"

"

"

Dibenzofuran

ND

---

0.0388

"

"

"

"

Fluoranthene

ND

---

0.0388

"

"

"

"

Fluorene

ND

---

0.0388

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0388

"

"

"

"

1-Methylnaphthalene

ND

---

0.0777

"

"

"

"

2-Methylnaphthalene

ND

---

0.0777

"

"

"

"

Naphthalene

ND

---

0.0777

"

"

"

"

Phenanthrene

ND

---

0.0388

"

"

"

"

Pyrene

ND

---

0.0388

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 85 %

Limits: 44-120 %

"

"

"

98 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6C0227-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0396

ug/L

03/07/16 16:14

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0396

"

"

"

"

Anthracene

ND

---

0.0396

"

"

"

"

Benz(a)anthracene

ND

---

0.0396

"

"

"

"

Benzo(a)pyrene

ND

---

0.0396

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0396

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0396

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0396

"

"

"

"

Chrysene

ND

---

0.0396

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0396

"

"

"

"

Dibenzofuran

ND

---

0.0396

"

"

"

"

Fluoranthene

ND

---

0.0396

"

"

"

"

Fluorene

ND

---

0.0396

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0396

"

"

"

"

1-Methylnaphthalene

ND

---

0.0792

"

"

"

"

2-Methylnaphthalene

ND

---

0.0792

"

"

"

"

Naphthalene

ND

---

0.0792

"

"

"

"

Phenanthrene

ND

---

0.0396

"

"

"

"

Pyrene

ND

---

0.0396

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 66 %

Limits: 44-120 %

"

"

"

92 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6C0227-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0392

ug/L

03/07/16 16:41

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0392

"

"

"

"

Anthracene

ND

---

0.0392

"

"

"

"

Benz(a)anthracene

ND

---

0.0392

"

"

"

"

Benzo(a)pyrene

ND

---

0.0392

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0392

"

"

"

"

Chrysene

ND

---

0.0392

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0392

"

"

"

"

Dibenzofuran

ND

---

0.0392

"

"

"

"

Fluoranthene

ND

---

0.0392

"

"

"

"

Fluorene

ND

---

0.0392

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0392

"

"

"

"

1-Methylnaphthalene

ND

---

0.0784

"

"

"

"

2-Methylnaphthalene

ND

---

0.0784

"

"

"

"

Naphthalene

ND

---

0.0784

"

"

"

"

Phenanthrene

ND

---

0.0392

"

"

"

"

Pyrene

ND

---

0.0392

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 85 %

Limits: 44-120 %

"

"

"

96 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-05 (A6C0227-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0385

ug/L

03/07/16 17:07

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0385

"

"

"

"

Anthracene

ND

---

0.0385

"

"

"

"

Benz(a)anthracene

ND

---

0.0385

"

"

"

"

Benzo(a)pyrene

ND

---

0.0385

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0385

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0385

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0385

"

"

"

"

Chrysene

ND

---

0.0385

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0385

"

"

"

"

Dibenzofuran

ND

---

0.0385

"

"

"

"

Fluoranthene

ND

---

0.0385

"

"

"

"

Fluorene

ND

---

0.0385

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0385

"

"

"

"

1-Methylnaphthalene

ND

---

0.0769

"

"

"

"

2-Methylnaphthalene

ND

---

0.0769

"

"

"

"

Naphthalene

ND

---

0.0769

"

"

"

"

Phenanthrene

ND

---

0.0385

"

"

"

"

Pyrene

ND

---

0.0385

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 82 %

Limits: 44-120 %

"

"

"

97 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

Foundation-S (A6C0227-06)

% Solids

Reporting
Limit
Matrix: Soil

70.8

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

1.00

Dilution

Units

Date Analyzed

Method

03/07/16 13:09

EPA 8000C

Notes

Batch: 6030191

% by Weight

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6030186 - EPA 3546 (Fuels)

Prepared: 03/07/16 10:04 Analyzed: 03/07/16 14:11

Blank (6030186-BLK1)
NWTPH-Dx

Diesel

ND

---

25.0

mg/kg wet

---

---

---

---

---

---

Oil

ND

---

50.0

"

"

---

---

---

---

---

---

---

---

Surr: o-Terphenyl (Surr)

Recovery: 93 %

Limits: 50-150 %

Dilution: 1x

Prepared: 03/07/16 10:04 Analyzed: 03/07/16 14:31

LCS (6030186-BS1)
NWTPH-Dx

Diesel

107

---

Surr: o-Terphenyl (Surr)

25.0
Recovery: 98 %

mg/kg wet

125

Limits: 50-150 %

---

86

76-115%

Dilution: 1x

Prepared: 03/07/16 10:04 Analyzed: 03/07/16 15:41

Duplicate (6030186-DUP1)
QC Source Sample: Foundation-S (A6C0227-06RE1)
NWTPH-Dx

Diesel
Oil
Surr: o-Terphenyl (Surr)

42900

---

538

mg/kg dry

20

---

27600

---

---

43

30%

ND

---

1080

"

"

---

ND

---

---

---

30%

Recovery: %

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Limits: 50-150 %

Dilution: 20x

Q-04

S-01

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030189 - EPA 5030B

Prepared: 03/07/16 15:32 Analyzed: 03/07/16 17:56

Blank (6030189-BLK1)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

---

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

---

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

ND

---

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 80-120 %

Dilution: 1x

102 %

80-120 %

"

96 %

80-120 %

"

100 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 03/07/16 15:32 Analyzed: 03/07/16 16:58

LCS (6030189-BS1)
EPA 8260B

Benzene

20.5

---

0.200

ug/L

20.0

---

102

70-130%

Toluene

20.0

---

1.00

"

"

"

---

100

"

---

---

Ethylbenzene

20.6

---

0.500

"

"

"

---

103

"

---

---

Xylenes, total

62.8

---

1.50

"

"

60.0

---

105

"

---

---

Naphthalene

18.7

---

2.00

"

"

20.0

---

94

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

17.3

---

1.00

"

"

"

---

86

"

---

---

21.6

---

1.00

"

"

"

---

108

"

---

---

n-Propylbenzene

20.3

---

0.500

"

"

"

---

102

"

---

---

1,2,4-Trimethylbenzene

20.5

---

1.00

"

"

"

---

103

"

---

---

1,3,5-Trimethylbenzene

20.5

---

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.8

---

0.500

"

"

"

---

104

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030189 - EPA 5030B

Prepared: 03/07/16 15:32 Analyzed: 03/07/16 16:58

LCS (6030189-BS1)

1,2-Dichloroethane (EDC)

Source
Result

19.2

Surr: Dibromofluoromethane (Surr)

---

0.500

ug/L

"

"

---

Recovery: 100 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

99 %

80-120 %

"

Toluene-d8 (Surr)

96 %

80-120 %

"

4-Bromofluorobenzene (Surr)

99 %

80-120 %

"

96

"

---

---

Prepared: 03/07/16 12:42 Analyzed: 03/07/16 18:53

Duplicate (6030189-DUP1)
QC Source Sample: SW-01 (A6C0227-01)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

ND

---

---

---

30%

Toluene

ND

Ethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

---

0.500

"

"

---

ND

---

---

---

30%

Xylenes, total
Naphthalene

ND

---

1.50

"

"

---

ND

---

---

---

30%

ND

---

2.00

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

ND

---

1.00

"

"

---

ND

---

---

---

30%

n-Propylbenzene

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 80-120 %

Dilution: 1x

102 %

80-120 %

"

Toluene-d8 (Surr)

96 %

80-120 %

"

4-Bromofluorobenzene (Surr)

99 %

80-120 %

"

1,4-Difluorobenzene (Surr)

Prepared: 03/07/16 12:42 Analyzed: 03/07/16 21:16

Matrix Spike (6030189-MS1)


QC Source Sample: SW-05 (A6C0227-05)
EPA 8260B

Benzene

20.9

---

0.200

ug/L

20.0

ND

104

70-130%

---

---

Toluene

20.5

---

1.00

"

"

"

ND

103

"

---

---

Ethylbenzene

21.2

---

0.500

"

"

"

ND

106

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030189 - EPA 5030B

Prepared: 03/07/16 12:42 Analyzed: 03/07/16 21:16

Matrix Spike (6030189-MS1)


QC Source Sample: SW-05 (A6C0227-05)

Xylenes, total

64.3

---

1.50

ug/L

"

60.0

ND

107

"

---

---

Naphthalene

17.3

---

2.00

"

"

20.0

ND

86

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

17.2

---

1.00

"

"

"

ND

86

"

---

---

22.2

---

1.00

"

"

"

ND

111

"

---

---

n-Propylbenzene

20.6

---

0.500

"

"

"

ND

103

"

---

---

1,2,4-Trimethylbenzene

20.7

---

1.00

"

"

"

ND

104

"

---

---

1,3,5-Trimethylbenzene

21.1

---

1.00

"

"

"

ND

105

"

---

---

1,2-Dibromoethane (EDB)

20.4

---

0.500

"

"

"

ND

102

"

---

---

1,2-Dichloroethane (EDC)

19.7

---

0.500

"

"

"

ND

99

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 101 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

99 %

80-120 %

"

Toluene-d8 (Surr)

95 %

80-120 %

"

4-Bromofluorobenzene (Surr)

98 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030185 - EPA 3510C (Acid Extraction)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 13:59

Blank (6030185-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0182

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

---

0.0182

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.0182

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.0182

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.0182

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.0182

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.0182

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.0182

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.0182

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.0364

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.0364

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0364

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.0182

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.0182

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 69 %

Limits: 44-120 %

Dilution: 1x

95 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:26

LCS (6030185-BS1)
EPA 8270D (SIM)

Acenaphthene

2.94

---

0.0200

ug/L

4.00

---

74

47-122%

---

Acenaphthylene

3.01

---

0.0200

"

"

"

---

75

41-130%

---

---

Anthracene

3.65

---

0.0200

"

"

"

---

91

57-123%

---

---

Benz(a)anthracene

3.54

---

0.0200

"

"

"

---

88

58-125%

---

---

Benzo(a)pyrene

3.80

---

0.0200

"

"

"

---

95

54-128%

---

---

Benzo(b)fluoranthene

3.81

---

0.0200

"

"

"

---

95

53-131%

---

---

Benzo(k)fluoranthene

3.95

---

0.0200

"

"

"

---

99

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030185 - EPA 3510C (Acid Extraction)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:26

LCS (6030185-BS1)

Benzo(g,h,i)perylene

Source
Result

3.09

---

0.0200

"

"

"

---

77

50-134%

---

---

Chrysene

3.54

---

0.0200

"

"

"

---

88

59-123%

---

---

Dibenz(a,h)anthracene

3.65

---

0.0200

"

"

"

---

91

51-134%

---

---

Dibenzofuran

3.11

---

0.0200

"

"

"

---

78

53-120%

---

---

Fluoranthene

3.58

---

0.0200

"

"

"

---

89

57-128%

---

---

Fluorene

3.23

---

0.0200

"

"

"

---

81

52-124%

---

---

Indeno(1,2,3-cd)pyrene

3.25

---

0.0200

"

"

"

---

81

52-133%

---

---

1-Methylnaphthalene

2.42

---

0.0400

"

"

"

---

61

41-120%

---

---

2-Methylnaphthalene

2.52

---

0.0400

"

"

"

---

63

40-121%

---

---

Naphthalene

2.47

---

0.0400

"

"

"

---

62

"

---

---

Phenanthrene

3.42

---

0.0200

"

"

"

---

86

59-120%

---

---

Pyrene

3.62

---

0.0200

"

"

"

---

90

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 75 %

Limits: 44-120 %

Dilution: 1x

95 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:53

LCS Dup (6030185-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

2.56

---

0.0200

ug/L

4.00

---

64

47-122%

14

30%

Acenaphthylene

2.59

---

0.0200

"

"

"

---

65

41-130%

15

30%

Anthracene

3.37

---

0.0200

"

"

"

---

84

57-123%

30%

Benz(a)anthracene

3.45

---

0.0200

"

"

"

---

86

58-125%

30%

Benzo(a)pyrene

3.65

---

0.0200

"

"

"

---

91

54-128%

30%

Benzo(b)fluoranthene

3.77

---

0.0200

"

"

"

---

94

53-131%

30%

Benzo(k)fluoranthene

3.85

---

0.0200

"

"

"

---

96

57-129%

30%

Benzo(g,h,i)perylene

3.04

---

0.0200

"

"

"

---

76

50-134%

30%

Chrysene

3.43

---

0.0200

"

"

"

---

86

59-123%

30%

Dibenz(a,h)anthracene

3.57

---

0.0200

"

"

"

---

89

51-134%

30%

Dibenzofuran

2.70

---

0.0200

"

"

"

---

67

53-120%

14

30%

Fluoranthene

3.42

---

0.0200

"

"

"

---

86

57-128%

30%

Fluorene

2.82

---

0.0200

"

"

"

---

70

52-124%

14

30%

Indeno(1,2,3-cd)pyrene

3.18

---

0.0200

"

"

"

---

79

52-133%

30%

1-Methylnaphthalene

2.14

---

0.0400

"

"

"

---

54

41-120%

12

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

RPD
Limit

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:53

LCS Dup (6030185-BSD1)

2-Methylnaphthalene

2.22

---

0.0400

"

"

"

---

55

Naphthalene

2.16

---

0.0400

"

"

"

---

Phenanthrene

3.12

---

0.0200

"

"

"

---

Pyrene

3.46

---

"

"

"

---

0.0200
Recovery: 61 %

Limits: 44-120 %

Dilution: 1x

89 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6030185 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

%REC
Limits RPD

Q-19

40-121%

13

30%

54

"

14

30%

78

59-120%

30%

87

57-126%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 19 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6030191 - Total Solids (Dry Weight)

Prepared: 03/07/16 11:08 Analyzed: 03/07/16 13:09

Duplicate (6030191-DUP1)
QC Source Sample: Foundation-S (A6C0227-06)
EPA 8000C

% Solids

60.7

---

1.00

% by
Weight

---

70.8

---

---

15

10%

Q-17

No Client related Batch QC samples analyzed for this batch. See notes page for more information.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 20 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

SAMPLE PREPARATION INFORMATION


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 3546 (Fuels)


Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 10:37

03/07/16 10:04

Batch: 6030186

A6C0227-06RE1

NWTPH-Dx

Soil

10.53g/5mL

10g/5mL

0.95

RBDM Compounds (BTEX+) by EPA 8260B


Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 08:13
03/06/16 08:40
03/06/16 08:50
03/06/16 09:00
03/06/16 09:50

03/07/16 12:42
03/07/16 12:42
03/07/16 12:42
03/07/16 12:42
03/07/16 12:42

Batch: 6030189

A6C0227-01
A6C0227-02
A6C0227-03
A6C0227-04
A6C0227-05

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

Water
Water
Water
Water
Water

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 08:13
03/06/16 08:40
03/06/16 08:50
03/06/16 09:00
03/06/16 09:50

03/07/16 10:00
03/07/16 10:00
03/07/16 10:00
03/07/16 10:00
03/07/16 10:00

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

0.97
0.97
0.99
0.98
0.96

Batch: 6030185

A6C0227-01
A6C0227-02
A6C0227-03
A6C0227-04
A6C0227-05

Water
Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

1030mL/2mL
1030mL/2mL
1010mL/2mL
1020mL/2mL
1040mL/2mL

Percent Dry Weight


Prep: Total Solids (Dry Weight)
Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 10:37

03/07/16 11:08

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6030191

A6C0227-06

Soil

EPA 8000C

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1N/A/1N/A

1N/A/1N/A

NA

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 21 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

Notes and Definitions


Qualifiers:
Q-04

Spike recovery and/or RPD is outside control limits due to a non-homogeneous sample matrix.

Q-17

RPD between original and duplicate sample is outside of established control limits.

Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Q-42

Matrix Spike and/or Duplicate analysis was performed on this sample. % Recovery or RPD for this analyte is outside laboratory control
limits. (Refer to the QC Section of Analytical Report.)

S-01

Surrogate recovery for this sample is not available due to sample dilution required from high analyte concentration and/or matrix
interference.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 22 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

03/08/16 04:39

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 23 of 23

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Sunday, February 21, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / [none]


Enclosed are the results of analyses for work order A6B0661, which was received by the laboratory on
2/19/2016 at 9:30:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 09:30
02/19/16 09:30
02/19/16 09:30
02/19/16 09:30

SW-02
SW-03
SW-04

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

SW-01 (A6B0661-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Diesel

ND

104

208

ug/L

2.5

02/19/16 23:07

NWTPH-Dx

Oil

ND

208

417

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 84 %

SW-02 (A6B0661-02)

Limits: 50-150 %

Matrix: Water

Batch: 6020602

Diesel

ND

104

208

ug/L

2.5

02/19/16 23:29

NWTPH-Dx

Oil

ND

208

417

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 85 %

SW-03 (A6B0661-03)

Limits: 50-150 %

Matrix: Water

Diesel

ND

100

Oil

ND

200

Surrogate: o-Terphenyl (Surr)

200
400
Recovery: 83 %

SW-04 (A6B0661-04)

Batch: 6020602

ug/L

2.5

02/19/16 23:51

NWTPH-Dx

"

"

"

"

"

"

"

Limits: 50-150 %

Matrix: Water

Batch: 6020602

Diesel

ND

97.1

194

ug/L

2.5

02/20/16 00:13

NWTPH-Dx

Oil

ND

194

388

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 90 %

Notes

Batch: 6020602

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6B0661-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

0.100

0.200

ug/L

02/19/16 14:00

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

95 %

Limits: 80-120 %

"

"

"

SW-02 (A6B0661-02)

Matrix: Water

Batch: 6020583

Benzene

ND

0.100

0.200

ug/L

02/19/16 14:28

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 100 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 80-120 %

"

"

"

02/19/16 14:57

EPA 8260B

1,4-Difluorobenzene (Surr)

SW-03 (A6B0661-03)

Benzene

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

0.100

0.200

Notes

Batch: 6020583

Batch: 6020583

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6B0661-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

0.500

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

95 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 80-120 %

"

"

"

SW-04 (A6B0661-04)

Matrix: Water

Batch: 6020583

Benzene

ND

0.100

0.200

ug/L

02/19/16 15:26

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 102 %

Limits: 80-120 %

"

"

"

101 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020583

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6B0661-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0208

0.0417

ug/L

02/19/16 18:13

EPA 8270D (SIM)

Acenaphthylene

ND

0.0208

0.0417

"

"

"

"

Anthracene

ND

0.0208

0.0417

"

"

"

"

Benz(a)anthracene

ND

0.0208

0.0417

"

"

"

"

Benzo(a)pyrene

ND

0.0208

0.0417

"

"

"

"

Benzo(b)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(k)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0208

0.0417

"

"

"

"

Chrysene

ND

0.0208

0.0417

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0208

0.0417

"

"

"

"

Dibenzofuran

ND

0.0208

0.0417

"

"

"

"

Fluoranthene

ND

0.0208

0.0417

"

"

"

"

Fluorene

ND

0.0208

0.0417

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0208

0.0417

"

"

"

"

1-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

2-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

Naphthalene

ND

0.0417

0.0833

"

"

"

"

Phenanthrene

ND

0.0208

0.0417

"

"

"

"

Pyrene

ND

0.0208

0.0417

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 54 %

Limits: 44-120 %

"

"

"

96 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6B0661-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0208

0.0417

ug/L

02/19/16 18:39

EPA 8270D (SIM)

Acenaphthylene

ND

0.0208

0.0417

"

"

"

"

Anthracene

ND

0.0208

0.0417

"

"

"

"

Benz(a)anthracene

ND

0.0208

0.0417

"

"

"

"

Benzo(a)pyrene

ND

0.0208

0.0417

"

"

"

"

Benzo(b)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(k)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0208

0.0417

"

"

"

"

Chrysene

ND

0.0208

0.0417

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0208

0.0417

"

"

"

"

Dibenzofuran

ND

0.0208

0.0417

"

"

"

"

Fluoranthene

ND

0.0208

0.0417

"

"

"

"

Fluorene

ND

0.0208

0.0417

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0208

0.0417

"

"

"

"

1-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

2-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

Naphthalene

ND

0.0417

0.0833

"

"

"

"

Phenanthrene

ND

0.0208

0.0417

"

"

"

"

Pyrene

ND

0.0208

0.0417

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 61 %

Limits: 44-120 %

"

"

"

95 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6B0661-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0200

0.0400

ug/L

02/19/16 19:06

EPA 8270D (SIM)

Acenaphthylene

ND

0.0200

0.0400

"

"

"

"

Anthracene

ND

0.0200

0.0400

"

"

"

"

Benz(a)anthracene

ND

0.0200

0.0400

"

"

"

"

Benzo(a)pyrene

ND

0.0200

0.0400

"

"

"

"

Benzo(b)fluoranthene

ND

0.0200

0.0400

"

"

"

"

Benzo(k)fluoranthene

ND

0.0200

0.0400

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0200

0.0400

"

"

"

"

Chrysene

ND

0.0200

0.0400

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0200

0.0400

"

"

"

"

Dibenzofuran

ND

0.0200

0.0400

"

"

"

"

Fluoranthene

ND

0.0200

0.0400

"

"

"

"

Fluorene

ND

0.0200

0.0400

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0200

0.0400

"

"

"

"

1-Methylnaphthalene

ND

0.0400

0.0800

"

"

"

"

2-Methylnaphthalene

ND

0.0400

0.0800

"

"

"

"

Naphthalene

ND

0.0400

0.0800

"

"

"

"

Phenanthrene

ND

0.0200

0.0400

"

"

"

"

Pyrene

ND

0.0200

0.0400

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 52 %

Limits: 44-120 %

"

"

"

93 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6B0661-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0194

0.0388

ug/L

02/19/16 19:32

EPA 8270D (SIM)

Acenaphthylene

ND

0.0194

0.0388

"

"

"

"

Anthracene

ND

0.0194

0.0388

"

"

"

"

Benz(a)anthracene

ND

0.0194

0.0388

"

"

"

"

Benzo(a)pyrene

ND

0.0194

0.0388

"

"

"

"

Benzo(b)fluoranthene

ND

0.0194

0.0388

"

"

"

"

Benzo(k)fluoranthene

ND

0.0194

0.0388

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0194

0.0388

"

"

"

"

Chrysene

ND

0.0194

0.0388

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0194

0.0388

"

"

"

"

Dibenzofuran

ND

0.0194

0.0388

"

"

"

"

Fluoranthene

ND

0.0194

0.0388

"

"

"

"

Fluorene

ND

0.0194

0.0388

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0194

0.0388

"

"

"

"

1-Methylnaphthalene

ND

0.0388

0.0777

"

"

"

"

2-Methylnaphthalene

ND

0.0388

0.0777

"

"

"

"

Naphthalene

ND

0.0388

0.0777

"

"

"

"

Phenanthrene

ND

0.0194

0.0388

"

"

"

"

Pyrene

ND

0.0194

0.0388

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 81 %

Limits: 44-120 %

"

"

"

99 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 22:01

Blank (6020602-BLK2)
NWTPH-Dx

Diesel

ND

90.9

182

ug/L

2.5

---

---

---

---

---

---

Oil

ND

182

364

"

"

---

---

---

---

---

---

---

---

Surr: o-Terphenyl (Surr)

Recovery: 88 %

Limits: 50-150 %

Dilution: 2.5x

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 22:23

LCS (6020602-BS2)
NWTPH-Dx

Diesel

991

Surr: o-Terphenyl (Surr)

100

200

Recovery: 90 %

ug/L

2.5

Limits: 50-150 %

1250

---

79

58-115%

Dilution: 2.5x

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 22:45

LCS Dup (6020602-BSD2)

Q-19

NWTPH-Dx

Diesel
Surr: o-Terphenyl (Surr)

1060

100

200

Recovery: 93 %

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

ug/L

2.5

Limits: 50-150 %

1250

---

84

58-115%

20%

Dilution: 2.5x

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020583 - EPA 5030B

Prepared: 02/19/16 10:11 Analyzed: 02/19/16 12:34

Blank (6020583-BLK1)
EPA 8260B

Benzene

ND

0.100

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

0.500

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

0.750

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

1.00

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

ND

0.500

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 97 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

98 %

80-120 %

"

Toluene-d8 (Surr)

97 %

80-120 %

"

4-Bromofluorobenzene (Surr)

97 %

80-120 %

"

Prepared: 02/19/16 10:11 Analyzed: 02/19/16 11:37

LCS (6020583-BS1)
EPA 8260B

Benzene

19.6

0.100

0.200

ug/L

20.0

---

98

70-130%

Toluene

20.3

0.500

1.00

"

"

"

---

102

"

---

---

Ethylbenzene

20.7

0.250

0.500

"

"

"

---

103

"

---

---

Xylenes, total

62.4

0.750

1.50

"

"

60.0

---

104

"

---

---

Naphthalene

18.5

1.00

2.00

"

"

20.0

---

93

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.8

0.500

1.00

"

"

"

---

94

"

---

---

21.8

0.500

1.00

"

"

"

---

109

"

---

---

n-Propylbenzene

20.0

0.250

0.500

"

"

"

---

100

"

---

---

1,2,4-Trimethylbenzene

20.5

0.500

1.00

"

"

"

---

103

"

---

---

1,3,5-Trimethylbenzene

20.4

0.500

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.4

0.250

0.500

"

"

"

---

102

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC
Limits RPD

RPD
Limit

Notes

Prepared: 02/19/16 10:11 Analyzed: 02/19/16 11:37

LCS (6020583-BS1)
Surr: Dibromofluoromethane (Surr)

%REC

Water

Batch 6020583 - EPA 5030B


1,2-Dichloroethane (EDC)

Source
Result

18.4

0.250

0.500

ug/L

"

"

---

Recovery: 94 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

96 %

80-120 %

"

Toluene-d8 (Surr)

96 %

80-120 %

"

4-Bromofluorobenzene (Surr)

97 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

92

"

---

---

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 16:54

Blank (6020602-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

0.0182

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 74 %

Limits: 44-120 %

Dilution: 1x

97 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:20

LCS (6020602-BS1)
EPA 8270D (SIM)

Acenaphthene

6.61

0.0200

0.0400

ug/L

8.00

---

83

47-122%

---

Acenaphthylene

6.67

0.0200

0.0400

"

"

"

---

83

41-130%

---

---

Anthracene

7.42

0.0200

0.0400

"

"

"

---

93

57-123%

---

---

Benz(a)anthracene

7.09

0.0200

0.0400

"

"

"

---

89

58-125%

---

---

Benzo(a)pyrene

7.37

0.0200

0.0400

"

"

"

---

92

54-128%

---

---

Benzo(b)fluoranthene

7.15

0.0200

0.0400

"

"

"

---

89

53-131%

---

---

Benzo(k)fluoranthene

7.57

0.0200

0.0400

"

"

"

---

95

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:20

LCS (6020602-BS1)

Benzo(g,h,i)perylene

Source
Result

6.33

0.0200

0.0400

"

"

"

---

79

50-134%

---

---

Chrysene

7.06

0.0200

0.0400

"

"

"

---

88

59-123%

---

---

Dibenz(a,h)anthracene

7.13

0.0200

0.0400

"

"

"

---

89

51-134%

---

---

Dibenzofuran

6.82

0.0200

0.0400

"

"

"

---

85

53-120%

---

---

Fluoranthene

7.26

0.0200

0.0400

"

"

"

---

91

57-128%

---

---

Fluorene

7.07

0.0200

0.0400

"

"

"

---

88

52-124%

---

---

Indeno(1,2,3-cd)pyrene

6.17

0.0200

0.0400

"

"

"

---

77

52-133%

---

---

1-Methylnaphthalene

5.76

0.0400

0.0800

"

"

"

---

72

41-120%

---

---

2-Methylnaphthalene

5.98

0.0400

0.0800

"

"

"

---

75

40-121%

---

---

Naphthalene

5.76

0.0400

0.0800

"

"

"

---

72

"

---

---

Phenanthrene

6.99

0.0200

0.0400

"

"

"

---

87

59-120%

---

---

Pyrene

7.40

0.0200

0.0400

"

"

"

---

93

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 79 %

Limits: 44-120 %

Dilution: 1x

94 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:47

LCS Dup (6020602-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

6.83

0.0200

0.0400

ug/L

8.00

---

85

47-122%

30%

Acenaphthylene

6.79

0.0200

0.0400

"

"

"

---

85

41-130%

30%

Anthracene

7.61

0.0200

0.0400

"

"

"

---

95

57-123%

30%

Benz(a)anthracene

7.28

0.0200

0.0400

"

"

"

---

91

58-125%

30%

Benzo(a)pyrene

7.59

0.0200

0.0400

"

"

"

---

95

54-128%

30%

Benzo(b)fluoranthene

7.57

0.0200

0.0400

"

"

"

---

95

53-131%

30%

Benzo(k)fluoranthene

7.43

0.0200

0.0400

"

"

"

---

93

57-129%

30%

Benzo(g,h,i)perylene

6.45

0.0200

0.0400

"

"

"

---

81

50-134%

30%

Chrysene

7.30

0.0200

0.0400

"

"

"

---

91

59-123%

30%

Dibenz(a,h)anthracene

7.31

0.0200

0.0400

"

"

"

---

91

51-134%

30%

Dibenzofuran

7.06

0.0200

0.0400

"

"

"

---

88

53-120%

30%

Fluoranthene

7.45

0.0200

0.0400

"

"

"

---

93

57-128%

30%

Fluorene

7.21

0.0200

0.0400

"

"

"

---

90

52-124%

30%

Indeno(1,2,3-cd)pyrene

8.20

0.0200

0.0400

"

"

"

---

103

52-133%

28

30%

1-Methylnaphthalene

6.08

0.0400

0.0800

"

"

"

---

76

41-120%

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

RPD
Limit

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:47

LCS Dup (6020602-BSD1)

2-Methylnaphthalene

6.25

0.0400

0.0800

"

"

"

---

78

Naphthalene

5.97

0.0400

0.0800

"

"

"

---

Phenanthrene

7.12

0.0200

0.0400

"

"

"

---

Pyrene

7.53

0.0200

0.0400

"

"

"

---

Recovery: 81 %

Limits: 44-120 %

Dilution: 1x

94 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

%REC
Limits RPD

Q-19

40-121%

30%

75

"

30%

89

59-120%

30%

94

57-126%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

SAMPLE PREPARATION INFORMATION


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/5mL
1000mL/5mL
1000mL/5mL
1000mL/5mL

0.42
0.42
0.40
0.39

Prep: EPA 3510C (Acid Extraction)


Lab Number

Matrix

Method

Sampled

Prepared

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32

Batch: 6020602

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx

960mL/2mL
960mL/2mL
1000mL/2mL
1030mL/2mL

RBDM Compounds (BTEX+) by EPA 8260B


Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 12:34
02/19/16 12:34
02/19/16 12:34
02/19/16 12:34

Batch: 6020583

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

1.04
1.04
1.00
0.97

Batch: 6020602

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

960mL/2mL
960mL/2mL
1000mL/2mL
1030mL/2mL

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/21/16 15:02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 18

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Monday, February 22, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0703, which was received by the laboratory on
2/22/2016 at 8:30:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04

Water
Water
Water
Water

02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00

02/22/16 08:30
02/22/16 08:30
02/22/16 08:30
02/22/16 08:30

SW-02
SW-03
SW-04

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6B0703-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

0.100

0.200

ug/L

02/22/16 13:47

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 98 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

100 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-02 (A6B0703-02)

Matrix: Water

Batch: 6020629

Benzene

ND

0.100

0.200

ug/L

02/22/16 14:16

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 97 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

97 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 80-120 %

"

"

"

02/22/16 14:44

EPA 8260B

SW-03 (A6B0703-03)

Benzene

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

0.100

0.200

Notes

Batch: 6020629

Batch: 6020629

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6B0703-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

0.500

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

SW-04 (A6B0703-04)

Recovery: 99 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

Matrix: Water

Batch: 6020629

Benzene

ND

0.100

0.200

ug/L

02/22/16 15:13

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020629

Recovery: 99 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6B0703-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0196

0.0392

ug/L

02/22/16 16:34

EPA 8270D (SIM)

Acenaphthylene

ND

0.0196

0.0392

"

"

"

"

Anthracene

ND

0.0196

0.0392

"

"

"

"

Benz(a)anthracene

ND

0.0196

0.0392

"

"

"

"

Benzo(a)pyrene

ND

0.0196

0.0392

"

"

"

"

Benzo(b)fluoranthene

ND

0.0196

0.0392

"

"

"

"

Benzo(k)fluoranthene

ND

0.0196

0.0392

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0196

0.0392

"

"

"

"

Chrysene

ND

0.0196

0.0392

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0196

0.0392

"

"

"

"

Dibenzofuran

ND

0.0196

0.0392

"

"

"

"

Fluoranthene

ND

0.0196

0.0392

"

"

"

"

Fluorene

ND

0.0196

0.0392

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0196

0.0392

"

"

"

"

1-Methylnaphthalene

ND

0.0392

0.0784

"

"

"

"

2-Methylnaphthalene

ND

0.0392

0.0784

"

"

"

"

Naphthalene

ND

0.0392

0.0784

"

"

"

"

Phenanthrene

ND

0.0196

0.0392

"

"

"

"

Pyrene

ND

0.0196

0.0392

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 75 %

Limits: 44-120 %

"

"

"

106 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6B0703-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0208

0.0417

ug/L

02/22/16 17:00

EPA 8270D (SIM)

Acenaphthylene

ND

0.0208

0.0417

"

"

"

"

Anthracene

ND

0.0208

0.0417

"

"

"

"

Benz(a)anthracene

ND

0.0208

0.0417

"

"

"

"

Benzo(a)pyrene

ND

0.0208

0.0417

"

"

"

"

Benzo(b)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(k)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0208

0.0417

"

"

"

"

Chrysene

ND

0.0208

0.0417

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0208

0.0417

"

"

"

"

Dibenzofuran

ND

0.0208

0.0417

"

"

"

"

Fluoranthene

ND

0.0208

0.0417

"

"

"

"

Fluorene

ND

0.0208

0.0417

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0208

0.0417

"

"

"

"

1-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

2-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

Naphthalene

ND

0.0417

0.0833

"

"

"

"

Phenanthrene

ND

0.0208

0.0417

"

"

"

"

Pyrene

ND

0.0208

0.0417

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 70 %

Limits: 44-120 %

"

"

"

102 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6B0703-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0206

0.0412

ug/L

02/22/16 17:26

EPA 8270D (SIM)

Acenaphthylene

ND

0.0206

0.0412

"

"

"

"

Anthracene

ND

0.0206

0.0412

"

"

"

"

Benz(a)anthracene

ND

0.0206

0.0412

"

"

"

"

Benzo(a)pyrene

ND

0.0206

0.0412

"

"

"

"

Benzo(b)fluoranthene

ND

0.0206

0.0412

"

"

"

"

Benzo(k)fluoranthene

ND

0.0206

0.0412

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0206

0.0412

"

"

"

"

Chrysene

ND

0.0206

0.0412

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0206

0.0412

"

"

"

"

Dibenzofuran

ND

0.0206

0.0412

"

"

"

"

Fluoranthene

ND

0.0206

0.0412

"

"

"

"

Fluorene

ND

0.0206

0.0412

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0206

0.0412

"

"

"

"

1-Methylnaphthalene

ND

0.0412

0.0825

"

"

"

"

2-Methylnaphthalene

ND

0.0412

0.0825

"

"

"

"

Naphthalene

ND

0.0412

0.0825

"

"

"

"

Phenanthrene

ND

0.0206

0.0412

"

"

"

"

Pyrene

ND

0.0206

0.0412

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 72 %

Limits: 44-120 %

"

"

"

106 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6B0703-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0198

0.0396

ug/L

02/22/16 17:52

EPA 8270D (SIM)

Acenaphthylene

ND

0.0198

0.0396

"

"

"

"

Anthracene

ND

0.0198

0.0396

"

"

"

"

Benz(a)anthracene

ND

0.0198

0.0396

"

"

"

"

Benzo(a)pyrene

ND

0.0198

0.0396

"

"

"

"

Benzo(b)fluoranthene

ND

0.0198

0.0396

"

"

"

"

Benzo(k)fluoranthene

ND

0.0198

0.0396

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0198

0.0396

"

"

"

"

Chrysene

ND

0.0198

0.0396

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0198

0.0396

"

"

"

"

Dibenzofuran

ND

0.0198

0.0396

"

"

"

"

Fluoranthene

ND

0.0198

0.0396

"

"

"

"

Fluorene

ND

0.0198

0.0396

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0198

0.0396

"

"

"

"

1-Methylnaphthalene

ND

0.0396

0.0792

"

"

"

"

2-Methylnaphthalene

ND

0.0396

0.0792

"

"

"

"

Naphthalene

ND

0.0396

0.0792

"

"

"

"

Phenanthrene

ND

0.0198

0.0396

"

"

"

"

Pyrene

ND

0.0198

0.0396

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 78 %

Limits: 44-120 %

"

"

"

106 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020629 - EPA 5030B

Prepared: 02/22/16 10:56 Analyzed: 02/22/16 13:18

Blank (6020629-BLK1)
EPA 8260B

Benzene

ND

0.100

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

0.500

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

0.750

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

1.00

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

ND

0.500

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 98 %

Limits: 80-120 %

Dilution: 1x

98 %

80-120 %

"

100 %

80-120 %

"

97 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 02/22/16 10:56 Analyzed: 02/22/16 12:21

LCS (6020629-BS1)
EPA 8260B

Benzene

19.1

0.100

0.200

ug/L

20.0

---

95

70-130%

Toluene

20.1

0.500

1.00

"

"

"

---

100

"

---

---

Ethylbenzene

20.4

0.250

0.500

"

"

"

---

102

"

---

---

Xylenes, total

61.6

0.750

1.50

"

"

60.0

---

103

"

---

---

Naphthalene

17.8

1.00

2.00

"

"

20.0

---

89

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.3

0.500

1.00

"

"

"

---

92

"

---

---

21.5

0.500

1.00

"

"

"

---

107

"

---

---

n-Propylbenzene

19.6

0.250

0.500

"

"

"

---

98

"

---

---

1,2,4-Trimethylbenzene

20.4

0.500

1.00

"

"

"

---

102

"

---

---

1,3,5-Trimethylbenzene

20.3

0.500

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.3

0.250

0.500

"

"

"

---

102

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC
Limits RPD

RPD
Limit

Notes

Prepared: 02/22/16 10:56 Analyzed: 02/22/16 12:21

LCS (6020629-BS1)
Surr: Dibromofluoromethane (Surr)

%REC

Water

Batch 6020629 - EPA 5030B


1,2-Dichloroethane (EDC)

Source
Result

18.0

0.250

0.500

ug/L

"

"

---

Recovery: 95 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

96 %

80-120 %

"

Toluene-d8 (Surr)

99 %

80-120 %

"

4-Bromofluorobenzene (Surr)

98 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

90

"

---

---

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020635 - EPA 3510C (Acid Extraction)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 15:15

Blank (6020635-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

0.0182

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 92 %

Limits: 44-120 %

Dilution: 1x

114 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 15:41

LCS (6020635-BS1)
EPA 8270D (SIM)

Acenaphthene

7.34

0.0200

0.0400

ug/L

8.00

---

92

47-122%

---

Acenaphthylene

7.43

0.0200

0.0400

"

"

"

---

93

41-130%

---

---

Anthracene

7.74

0.0200

0.0400

"

"

"

---

97

57-123%

---

---

Benz(a)anthracene

7.61

0.0200

0.0400

"

"

"

---

95

58-125%

---

---

Benzo(a)pyrene

7.92

0.0200

0.0400

"

"

"

---

99

54-128%

---

---

Benzo(b)fluoranthene

8.27

0.0200

0.0400

"

"

"

---

103

53-131%

---

---

Benzo(k)fluoranthene

7.91

0.0200

0.0400

"

"

"

---

99

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020635 - EPA 3510C (Acid Extraction)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 15:41

LCS (6020635-BS1)

Benzo(g,h,i)perylene

Source
Result

6.86

0.0200

0.0400

"

"

"

---

86

50-134%

---

---

Chrysene

7.46

0.0200

0.0400

"

"

"

---

93

59-123%

---

---

Dibenz(a,h)anthracene

7.31

0.0200

0.0400

"

"

"

---

91

51-134%

---

---

Dibenzofuran

7.57

0.0200

0.0400

"

"

"

---

95

53-120%

---

---

Fluoranthene

8.05

0.0200

0.0400

"

"

"

---

101

57-128%

---

---

Fluorene

7.68

0.0200

0.0400

"

"

"

---

96

52-124%

---

---

Indeno(1,2,3-cd)pyrene

7.04

0.0200

0.0400

"

"

"

---

88

52-133%

---

---

1-Methylnaphthalene

6.80

0.0400

0.0800

"

"

"

---

85

41-120%

---

---

2-Methylnaphthalene

7.18

0.0400

0.0800

"

"

"

---

90

40-121%

---

---

Naphthalene

6.93

0.0400

0.0800

"

"

"

---

87

"

---

---

Phenanthrene

7.70

0.0200

0.0400

"

"

"

---

96

59-120%

---

---

Pyrene

8.13

0.0200

0.0400

"

"

"

---

102

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 91 %

Limits: 44-120 %

Dilution: 1x

104 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 16:07

LCS Dup (6020635-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

7.41

0.0200

0.0400

ug/L

8.00

---

93

47-122%

30%

Acenaphthylene

7.60

0.0200

0.0400

"

"

"

---

95

41-130%

30%

Anthracene

7.78

0.0200

0.0400

"

"

"

---

97

57-123%

0.5

30%

Benz(a)anthracene

7.63

0.0200

0.0400

"

"

"

---

95

58-125%

0.3

30%

Benzo(a)pyrene

8.00

0.0200

0.0400

"

"

"

---

100

54-128%

30%

Benzo(b)fluoranthene

8.28

0.0200

0.0400

"

"

"

---

103

53-131%

0.08

30%

Benzo(k)fluoranthene

7.87

0.0200

0.0400

"

"

"

---

98

57-129%

0.5

30%

Benzo(g,h,i)perylene

7.12

0.0200

0.0400

"

"

"

---

89

50-134%

30%

Chrysene

7.66

0.0200

0.0400

"

"

"

---

96

59-123%

30%

Dibenz(a,h)anthracene

7.62

0.0200

0.0400

"

"

"

---

95

51-134%

30%

Dibenzofuran

7.56

0.0200

0.0400

"

"

"

---

94

53-120%

0.2

30%

Fluoranthene

7.98

0.0200

0.0400

"

"

"

---

100

57-128%

0.8

30%

Fluorene

7.65

0.0200

0.0400

"

"

"

---

96

52-124%

0.4

30%

Indeno(1,2,3-cd)pyrene

7.20

0.0200

0.0400

"

"

"

---

90

52-133%

30%

1-Methylnaphthalene

6.96

0.0400

0.0800

"

"

"

---

87

41-120%

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 16:07

LCS Dup (6020635-BSD1)

Q-19

2-Methylnaphthalene

7.34

0.0400

0.0800

"

"

"

---

92

Naphthalene

7.22

0.0400

0.0800

"

"

"

---

90

Phenanthrene

7.76

0.0200

0.0400

"

"

"

---

97

Pyrene

8.10

0.0200

0.0400

"

"

"

---

101

57-126%

Recovery: 92 %

Limits: 44-120 %

Dilution: 1x

104 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020635 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

RPD
Limit

40-121%

30%

"

30%

59-120%

0.8

30%

0.4

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00

02/22/16 12:40
02/22/16 12:40
02/22/16 12:40
02/22/16 12:40

Batch: 6020629

A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04

Water
Water
Water
Water

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00

02/22/16 11:20
02/22/16 11:20
02/22/16 11:20
02/22/16 11:20

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

0.98
1.04
1.03
0.99

Batch: 6020635

A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04

Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1020mL/2mL
960mL/2mL
970mL/2mL
1010mL/2mL

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/22/16 18:29

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 16

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Friday, February 26, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0868, which was received by the laboratory on
2/26/2016 at 6:35:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-05

A6B0868-01

Water

02/25/16 13:00

02/26/16 06:35

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-05 (A6B0868-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

---

0.200

ug/L

02/26/16 13:07

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020814

Recovery: 100 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-05 (A6B0868-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0440

ug/L

02/26/16 12:14

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0440

"

"

"

"

Anthracene

ND

---

0.0440

"

"

"

"

Benz(a)anthracene

ND

---

0.0440

"

"

"

"

Benzo(a)pyrene

ND

---

0.0440

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0440

"

"

"

"

Chrysene

ND

---

0.0440

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0440

"

"

"

"

Dibenzofuran

ND

---

0.0440

"

"

"

"

Fluoranthene

ND

---

0.0440

"

"

"

"

Fluorene

ND

---

0.0440

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0440

"

"

"

"

1-Methylnaphthalene

ND

---

0.0879

"

"

"

"

2-Methylnaphthalene

ND

---

0.0879

"

"

"

"

Naphthalene

ND

---

0.0879

"

"

"

"

Phenanthrene

ND

---

0.0440

"

"

"

"

Pyrene

ND

---

0.0440

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020786

Recovery: 75 %

Limits: 44-120 %

"

"

"

112 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020814 - EPA 5030B

Prepared: 02/26/16 10:15 Analyzed: 02/26/16 12:39

Blank (6020814-BLK1)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

---

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

---

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

ND

---

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 99 %

Limits: 80-120 %

Dilution: 1x

99 %

80-120 %

"

Toluene-d8 (Surr)

101 %

80-120 %

"

4-Bromofluorobenzene (Surr)

100 %

80-120 %

"

1,4-Difluorobenzene (Surr)

Prepared: 02/26/16 10:15 Analyzed: 02/26/16 11:13

LCS (6020814-BS1)
EPA 8260B

Benzene

18.8

---

0.200

ug/L

20.0

---

94

70-130%

Toluene

20.2

---

1.00

"

"

"

---

101

"

---

---

Ethylbenzene

20.1

---

0.500

"

"

"

---

101

"

---

---

Xylenes, total

61.4

---

1.50

"

"

60.0

---

102

"

---

---

Naphthalene

17.9

---

2.00

"

"

20.0

---

90

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.2

---

1.00

"

"

"

---

91

"

---

---

20.8

---

1.00

"

"

"

---

104

"

---

---

n-Propylbenzene

19.8

---

0.500

"

"

"

---

99

"

---

---

1,2,4-Trimethylbenzene

20.4

---

1.00

"

"

"

---

102

"

---

---

1,3,5-Trimethylbenzene

20.4

---

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.5

---

0.500

"

"

"

---

102

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC
Limits RPD

RPD
Limit

Notes

Prepared: 02/26/16 10:15 Analyzed: 02/26/16 11:13

LCS (6020814-BS1)
Surr: Dibromofluoromethane (Surr)

%REC

Water

Batch 6020814 - EPA 5030B


1,2-Dichloroethane (EDC)

Source
Result

17.7

---

0.500

ug/L

"

"

---

Recovery: 96 %

Limits: 80-120 %

Dilution: 1x

95 %

80-120 %

"

Toluene-d8 (Surr)

100 %

80-120 %

"

4-Bromofluorobenzene (Surr)

101 %

80-120 %

"

1,4-Difluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

88

"

---

---

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020786 - EPA 3510C (Acid Extraction)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 10:52

Blank (6020786-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 84 %

Limits: 44-120 %

Dilution: 1x

108 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:19

LCS (6020786-BS1)
EPA 8270D (SIM)

Acenaphthene

6.55

---

0.0400

ug/L

8.00

---

82

47-122%

---

Acenaphthylene

6.52

---

0.0400

"

"

"

---

82

41-130%

---

---

Anthracene

7.27

---

0.0400

"

"

"

---

91

57-123%

---

---

Benz(a)anthracene

7.29

---

0.0400

"

"

"

---

91

58-125%

---

---

Benzo(a)pyrene

7.85

---

0.0400

"

"

"

---

98

54-128%

---

---

Benzo(b)fluoranthene

7.84

---

0.0400

"

"

"

---

98

53-131%

---

---

Benzo(k)fluoranthene

7.60

---

0.0400

"

"

"

---

95

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020786 - EPA 3510C (Acid Extraction)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:19

LCS (6020786-BS1)

Benzo(g,h,i)perylene

Source
Result

7.13

---

0.0400

"

"

"

---

89

50-134%

---

---

Chrysene

7.26

---

0.0400

"

"

"

---

91

59-123%

---

---

Dibenz(a,h)anthracene

7.46

---

0.0400

"

"

"

---

93

51-134%

---

---

Dibenzofuran

6.69

---

0.0400

"

"

"

---

84

53-120%

---

---

Fluoranthene

7.26

---

0.0400

"

"

"

---

91

57-128%

---

---

Fluorene

6.83

---

0.0400

"

"

"

---

85

52-124%

---

---

Indeno(1,2,3-cd)pyrene

7.14

---

0.0400

"

"

"

---

89

52-133%

---

---

1-Methylnaphthalene

5.60

---

0.0800

"

"

"

---

70

41-120%

---

---

2-Methylnaphthalene

5.84

---

0.0800

"

"

"

---

73

40-121%

---

---

Naphthalene

5.78

---

0.0800

"

"

"

---

72

"

---

---

Phenanthrene

7.19

---

0.0400

"

"

"

---

90

59-120%

---

---

Pyrene

7.29

---

0.0400

"

"

"

---

91

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 83 %

Limits: 44-120 %

Dilution: 1x

100 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:47

LCS Dup (6020786-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

6.86

---

0.0400

ug/L

8.00

---

86

47-122%

30%

Acenaphthylene

6.91

---

0.0400

"

"

"

---

86

41-130%

30%

Anthracene

7.76

---

0.0400

"

"

"

---

97

57-123%

30%

Benz(a)anthracene

7.26

---

0.0400

"

"

"

---

91

58-125%

0.5

30%

Benzo(a)pyrene

7.87

---

0.0400

"

"

"

---

98

54-128%

0.2

30%

Benzo(b)fluoranthene

7.58

---

0.0400

"

"

"

---

95

53-131%

30%

Benzo(k)fluoranthene

7.81

---

0.0400

"

"

"

---

98

57-129%

30%

Benzo(g,h,i)perylene

7.11

---

0.0400

"

"

"

---

89

50-134%

0.4

30%

Chrysene

7.26

---

0.0400

"

"

"

---

91

59-123%

0.05

30%

Dibenz(a,h)anthracene

7.42

---

0.0400

"

"

"

---

93

51-134%

0.5

30%

Dibenzofuran

6.91

---

0.0400

"

"

"

---

86

53-120%

30%

Fluoranthene

7.28

---

0.0400

"

"

"

---

91

57-128%

0.3

30%

Fluorene

7.03

---

0.0400

"

"

"

---

88

52-124%

30%

Indeno(1,2,3-cd)pyrene

7.07

---

0.0400

"

"

"

---

88

52-133%

30%

1-Methylnaphthalene

6.30

---

0.0800

"

"

"

---

79

41-120%

12

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:47

LCS Dup (6020786-BSD1)

Q-19

2-Methylnaphthalene

6.60

---

0.0800

"

"

"

---

82

Naphthalene

6.56

---

0.0800

"

"

"

---

82

Phenanthrene

7.24

---

0.0400

"

"

"

---

91

Pyrene

7.39

---

"

"

"

---

92

57-126%

0.0400
Recovery: 91 %

Limits: 44-120 %

Dilution: 1x

100 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020786 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

RPD
Limit

40-121%

12

30%

"

13

30%

59-120%

0.7

30%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/25/16 13:00

02/26/16 12:03

Batch: 6020814

A6B0868-01

Water

EPA 8260B

5mL/5mL

5mL/5mL

1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/25/16 13:00

02/26/16 09:16

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

910mL/2mL

1000mL/2mL

1.10

Batch: 6020786

A6B0868-01

Water

EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/26/16 16:36

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 12

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Monday, February 29, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0905, which was received by the laboratory on
2/29/2016 at 6:36:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05

Water
Water
Water
Water
Water

02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15

02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36

SW-02
SW-03
SW-04
SW-05

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6B0905-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

---

0.200

ug/L

02/29/16 12:13

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 102 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

100 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-02 (A6B0905-02)

Matrix: Water

Batch: 6020841

Benzene

ND

---

0.200

ug/L

02/29/16 13:10

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

SW-03 (A6B0905-03)

Benzene

Recovery: 102 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

02/29/16 13:39

EPA 8260B

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

0.200

Notes

Batch: 6020841

Batch: 6020841

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6B0905-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

---

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

100 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

102 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

SW-04 (A6B0905-04)

Matrix: Water

Batch: 6020841

Benzene

ND

---

0.200

ug/L

02/29/16 14:08

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

SW-05 (A6B0905-05)

Recovery: 105 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

101 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

Matrix: Water

Batch: 6020841

Benzene

ND

---

0.200

ug/L

02/29/16 14:36

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020841

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-05 (A6B0905-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Ethylbenzene

ND

---

0.500

ug/L

"

EPA 8260B

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

101 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020841

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6B0905-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0392

ug/L

02/29/16 12:57

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0392

"

"

"

"

Anthracene

ND

---

0.0392

"

"

"

"

Benz(a)anthracene

ND

---

0.0392

"

"

"

"

Benzo(a)pyrene

ND

---

0.0392

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0392

"

"

"

"

Chrysene

ND

---

0.0392

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0392

"

"

"

"

Dibenzofuran

ND

---

0.0392

"

"

"

"

Fluoranthene

ND

---

0.0392

"

"

"

"

Fluorene

ND

---

0.0392

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0392

"

"

"

"

1-Methylnaphthalene

ND

---

0.0784

"

"

"

"

2-Methylnaphthalene

ND

---

0.0784

"

"

"

"

Naphthalene

ND

---

0.0784

"

"

"

"

Phenanthrene

ND

---

0.0392

"

"

"

"

Pyrene

ND

---

0.0392

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 83 %

Limits: 44-120 %

"

"

"

114 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6B0905-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0404

ug/L

02/29/16 13:24

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0404

"

"

"

"

Anthracene

ND

---

0.0404

"

"

"

"

Benz(a)anthracene

ND

---

0.0404

"

"

"

"

Benzo(a)pyrene

ND

---

0.0404

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0404

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0404

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0404

"

"

"

"

Chrysene

ND

---

0.0404

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0404

"

"

"

"

Dibenzofuran

ND

---

0.0404

"

"

"

"

Fluoranthene

ND

---

0.0404

"

"

"

"

Fluorene

ND

---

0.0404

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0404

"

"

"

"

1-Methylnaphthalene

ND

---

0.0808

"

"

"

"

2-Methylnaphthalene

ND

---

0.0808

"

"

"

"

Naphthalene

ND

---

0.0808

"

"

"

"

Phenanthrene

ND

---

0.0404

"

"

"

"

Pyrene

ND

---

0.0404

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 82 %

Limits: 44-120 %

"

"

"

115 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6B0905-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0421

ug/L

02/29/16 13:52

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0421

"

"

"

"

Anthracene

ND

---

0.0421

"

"

"

"

Benz(a)anthracene

ND

---

0.0421

"

"

"

"

Benzo(a)pyrene

ND

---

0.0421

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0421

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0421

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0421

"

"

"

"

Chrysene

ND

---

0.0421

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0421

"

"

"

"

Dibenzofuran

ND

---

0.0421

"

"

"

"

Fluoranthene

ND

---

0.0421

"

"

"

"

Fluorene

ND

---

0.0421

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0421

"

"

"

"

1-Methylnaphthalene

ND

---

0.0842

"

"

"

"

2-Methylnaphthalene

ND

---

0.0842

"

"

"

"

Naphthalene

ND

---

0.0842

"

"

"

"

Phenanthrene

ND

---

0.0421

"

"

"

"

Pyrene

ND

---

0.0421

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 67 %

Limits: 44-120 %

"

"

"

109 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6B0905-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0408

ug/L

02/29/16 14:19

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0408

"

"

"

"

Anthracene

ND

---

0.0408

"

"

"

"

Benz(a)anthracene

ND

---

0.0408

"

"

"

"

Benzo(a)pyrene

ND

---

0.0408

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0408

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0408

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0408

"

"

"

"

Chrysene

ND

---

0.0408

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0408

"

"

"

"

Dibenzofuran

ND

---

0.0408

"

"

"

"

Fluoranthene

ND

---

0.0408

"

"

"

"

Fluorene

ND

---

0.0408

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0408

"

"

"

"

1-Methylnaphthalene

ND

---

0.0816

"

"

"

"

2-Methylnaphthalene

ND

---

0.0816

"

"

"

"

Naphthalene

ND

---

0.0816

"

"

"

"

Phenanthrene

ND

---

0.0408

"

"

"

"

Pyrene

ND

---

0.0408

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 86 %

Limits: 44-120 %

"

"

"

110 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-05 (A6B0905-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0440

ug/L

02/29/16 14:46

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0440

"

"

"

"

Anthracene

ND

---

0.0440

"

"

"

"

Benz(a)anthracene

ND

---

0.0440

"

"

"

"

Benzo(a)pyrene

ND

---

0.0440

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0440

"

"

"

"

Chrysene

ND

---

0.0440

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0440

"

"

"

"

Dibenzofuran

ND

---

0.0440

"

"

"

"

Fluoranthene

ND

---

0.0440

"

"

"

"

Fluorene

ND

---

0.0440

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0440

"

"

"

"

1-Methylnaphthalene

ND

---

0.0879

"

"

"

"

2-Methylnaphthalene

ND

---

0.0879

"

"

"

"

Naphthalene

ND

---

0.0879

"

"

"

"

Phenanthrene

ND

---

0.0440

"

"

"

"

Pyrene

ND

---

0.0440

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 78 %

Limits: 44-120 %

"

"

"

115 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020841 - EPA 5030B

Prepared: 02/29/16 09:00 Analyzed: 02/29/16 11:45

Blank (6020841-BLK1)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

---

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

---

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

ND

---

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 100 %

Limits: 80-120 %

Dilution: 1x

99 %

80-120 %

"

101 %

80-120 %

"

99 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 02/29/16 09:00 Analyzed: 02/29/16 10:19

LCS (6020841-BS1)
EPA 8260B

Benzene

18.9

---

0.200

ug/L

20.0

---

94

70-130%

Toluene

20.0

---

1.00

"

"

"

---

100

"

---

---

Ethylbenzene

20.2

---

0.500

"

"

"

---

101

"

---

---

Xylenes, total

61.0

---

1.50

"

"

60.0

---

102

"

---

---

Naphthalene

17.1

---

2.00

"

"

20.0

---

86

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.7

---

1.00

"

"

"

---

93

"

---

---

20.5

---

1.00

"

"

"

---

103

"

---

---

n-Propylbenzene

19.6

---

0.500

"

"

"

---

98

"

---

---

1,2,4-Trimethylbenzene

20.2

---

1.00

"

"

"

---

101

"

---

---

1,3,5-Trimethylbenzene

19.9

---

1.00

"

"

"

---

100

"

---

---

1,2-Dibromoethane (EDB)

20.7

---

0.500

"

"

"

---

103

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020841 - EPA 5030B

Prepared: 02/29/16 09:00 Analyzed: 02/29/16 10:19

LCS (6020841-BS1)

1,2-Dichloroethane (EDC)

Source
Result

19.0

---

Surr: Dibromofluoromethane (Surr)

0.500

ug/L

"

"

---

Recovery: 98 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

95 %

80-120 %

"

Toluene-d8 (Surr)

99 %

80-120 %

"

4-Bromofluorobenzene (Surr)

99 %

80-120 %

"

95

"

---

---

---

---

30%

Prepared: 02/29/16 11:35 Analyzed: 02/29/16 12:43

Duplicate (6020841-DUP1)
QC Source Sample: SW-01 (A6B0905-01)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

ND

---

Toluene

ND

---

1.00

"

"

---

ND

---

---

---

30%

Ethylbenzene

ND

---

0.500

"

"

---

ND

---

---

---

30%

Xylenes, total

ND

---

1.50

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

2.00

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

ND

---

1.00

"

"

---

ND

---

---

---

30%

n-Propylbenzene

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 102 %

Limits: 80-120 %

Dilution: 1x

99 %

80-120 %

"

102 %

80-120 %

"

98 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 02/29/16 11:35 Analyzed: 02/29/16 15:05

Matrix Spike (6020841-MS1)


QC Source Sample: SW-05 (A6B0905-05)
EPA 8260B

Benzene

20.8

---

0.200

ug/L

20.0

ND

104

70-130%

---

---

Toluene

21.5

---

1.00

"

"

"

ND

108

"

---

---

Ethylbenzene

21.8

---

0.500

"

"

"

ND

109

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020841 - EPA 5030B

Prepared: 02/29/16 11:35 Analyzed: 02/29/16 15:05

Matrix Spike (6020841-MS1)


QC Source Sample: SW-05 (A6B0905-05)

Xylenes, total

65.0

---

1.50

ug/L

"

60.0

ND

108

"

---

---

Naphthalene

16.8

---

2.00

"

"

20.0

ND

84

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

19.3

---

1.00

"

"

"

ND

96

"

---

---

22.2

---

1.00

"

"

"

ND

111

"

---

---

n-Propylbenzene

20.8

---

0.500

"

"

"

ND

104

"

---

---

1,2,4-Trimethylbenzene

20.8

---

1.00

"

"

"

ND

104

"

---

---

1,3,5-Trimethylbenzene

21.0

---

1.00

"

"

"

ND

105

"

---

---

1,2-Dibromoethane (EDB)

21.6

---

0.500

"

"

"

ND

108

"

---

---

1,2-Dichloroethane (EDC)

20.5

---

0.500

"

"

"

ND

102

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 100 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

97 %

80-120 %

"

Toluene-d8 (Surr)

99 %

80-120 %

"

4-Bromofluorobenzene (Surr)

97 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020838 - EPA 3510C (Acid Extraction)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 10:42

Blank (6020838-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 97 %

Limits: 44-120 %

Dilution: 1x

126 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:09

LCS (6020838-BS1)
EPA 8270D (SIM)

Acenaphthene

6.88

---

0.0400

ug/L

8.00

---

86

47-122%

---

Acenaphthylene

6.99

---

0.0400

"

"

"

---

87

41-130%

---

---

Anthracene

7.45

---

0.0400

"

"

"

---

93

57-123%

---

---

Benz(a)anthracene

7.32

---

0.0400

"

"

"

---

92

58-125%

---

---

Benzo(a)pyrene

7.90

---

0.0400

"

"

"

---

99

54-128%

---

---

Benzo(b)fluoranthene

7.86

---

0.0400

"

"

"

---

98

53-131%

---

---

Benzo(k)fluoranthene

8.18

---

0.0400

"

"

"

---

102

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020838 - EPA 3510C (Acid Extraction)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:09

LCS (6020838-BS1)

Benzo(g,h,i)perylene

Source
Result

6.28

---

0.0400

"

"

"

---

78

50-134%

---

---

Chrysene

7.23

---

0.0400

"

"

"

---

90

59-123%

---

---

Dibenz(a,h)anthracene

7.25

---

0.0400

"

"

"

---

91

51-134%

---

---

Dibenzofuran

7.12

---

0.0400

"

"

"

---

89

53-120%

---

---

Fluoranthene

7.07

---

0.0400

"

"

"

---

88

57-128%

---

---

Fluorene

7.17

---

0.0400

"

"

"

---

90

52-124%

---

---

Indeno(1,2,3-cd)pyrene

6.66

---

0.0400

"

"

"

---

83

52-133%

---

---

1-Methylnaphthalene

6.48

---

0.0800

"

"

"

---

81

41-120%

---

---

2-Methylnaphthalene

6.84

---

0.0800

"

"

"

---

85

40-121%

---

---

Naphthalene

6.62

---

0.0800

"

"

"

---

83

"

---

---

Phenanthrene

7.43

---

0.0400

"

"

"

---

93

59-120%

---

---

Pyrene

7.02

---

0.0400

"

"

"

---

88

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 91 %

Limits: 44-120 %

Dilution: 1x

112 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:36

LCS Dup (6020838-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

6.36

---

0.0400

ug/L

8.00

---

80

47-122%

30%

Acenaphthylene

6.48

---

0.0400

"

"

"

---

81

41-130%

30%

Anthracene

7.06

---

0.0400

"

"

"

---

88

57-123%

30%

Benz(a)anthracene

7.19

---

0.0400

"

"

"

---

90

58-125%

30%

Benzo(a)pyrene

7.78

---

0.0400

"

"

"

---

97

54-128%

30%

Benzo(b)fluoranthene

8.07

---

0.0400

"

"

"

---

101

53-131%

30%

Benzo(k)fluoranthene

7.91

---

0.0400

"

"

"

---

99

57-129%

30%

Benzo(g,h,i)perylene

6.03

---

0.0400

"

"

"

---

75

50-134%

30%

Chrysene

7.16

---

0.0400

"

"

"

---

89

59-123%

30%

Dibenz(a,h)anthracene

7.05

---

0.0400

"

"

"

---

88

51-134%

30%

Dibenzofuran

6.67

---

0.0400

"

"

"

---

83

53-120%

30%

Fluoranthene

6.63

---

0.0400

"

"

"

---

83

57-128%

30%

Fluorene

6.79

---

0.0400

"

"

"

---

85

52-124%

30%

Indeno(1,2,3-cd)pyrene

6.49

---

0.0400

"

"

"

---

81

52-133%

30%

1-Methylnaphthalene

5.81

---

0.0800

"

"

"

---

73

41-120%

11

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

RPD
Limit

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:36

LCS Dup (6020838-BSD1)

2-Methylnaphthalene

6.05

---

0.0800

"

"

"

---

76

Naphthalene

5.95

---

0.0800

"

"

"

---

Phenanthrene

7.07

---

0.0400

"

"

"

---

Pyrene

6.59

---

"

"

"

---

0.0400
Recovery: 83 %

Limits: 44-120 %

Dilution: 1x

113 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020838 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

%REC
Limits RPD

Q-19

40-121%

12

30%

74

"

11

30%

88

59-120%

30%

82

57-126%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15

02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35

Batch: 6020841

A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05

Water
Water
Water
Water
Water

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15

02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

0.98
1.01
1.05
1.02
1.10

Batch: 6020838

A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05

Water
Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1020mL/2mL
990mL/2mL
950mL/2mL
980mL/2mL
910mL/2mL

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/29/16 17:54

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 19 of 19

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Tuesday, March 8, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6C0227, which was received by the laboratory on
3/7/2016 at 6:38:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6C0227-01
A6C0227-02
A6C0227-03
A6C0227-04
A6C0227-05
A6C0227-06

Water
Water
Water
Water
Water
Soil

03/06/16 08:13
03/06/16 08:40
03/06/16 08:50
03/06/16 09:00
03/06/16 09:50
03/06/16 10:37

03/07/16 06:38
03/07/16 06:38
03/07/16 06:38
03/07/16 06:38
03/07/16 06:38
03/07/16 06:38

SW-02
SW-03
SW-04
SW-05
Foundation-S

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

Foundation-S (A6C0227-06RE1)

Diesel

Oil

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

27600

---

537

mg/kg dry

20

03/07/16 15:21

NWTPH-Dx

ND

---

1070

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: %

Notes

Batch: 6030186

Limits: 50-150 %

Q-42

S-01

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6C0227-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

---

0.200

ug/L

03/07/16 18:24

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 80-120 %

"

"

"

101 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-02 (A6C0227-02)

Matrix: Water

Batch: 6030189

Benzene

ND

---

0.200

ug/L

03/07/16 19:22

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 80-120 %

"

"

"

03/07/16 19:51

EPA 8260B

1,4-Difluorobenzene (Surr)

SW-03 (A6C0227-03)

Benzene

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

0.200

Notes

Batch: 6030189

Batch: 6030189

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6C0227-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

---

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-04 (A6C0227-04)

Matrix: Water

Batch: 6030189

Benzene

ND

---

0.200

ug/L

03/07/16 20:19

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 106 %

Limits: 80-120 %

"

"

"

103 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-05 (A6C0227-05)

Matrix: Water

Batch: 6030189

Benzene

ND

---

0.200

ug/L

03/07/16 20:48

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030189

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-05 (A6C0227-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Ethylbenzene

ND

---

0.500

ug/L

"

EPA 8260B

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030189

Recovery: 105 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

96 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6C0227-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0388

ug/L

03/07/16 15:20

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0388

"

"

"

"

Anthracene

ND

---

0.0388

"

"

"

"

Benz(a)anthracene

ND

---

0.0388

"

"

"

"

Benzo(a)pyrene

ND

---

0.0388

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0388

"

"

"

"

Chrysene

ND

---

0.0388

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0388

"

"

"

"

Dibenzofuran

ND

---

0.0388

"

"

"

"

Fluoranthene

ND

---

0.0388

"

"

"

"

Fluorene

ND

---

0.0388

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0388

"

"

"

"

1-Methylnaphthalene

ND

---

0.0777

"

"

"

"

2-Methylnaphthalene

ND

---

0.0777

"

"

"

"

Naphthalene

ND

---

0.0777

"

"

"

"

Phenanthrene

ND

---

0.0388

"

"

"

"

Pyrene

ND

---

0.0388

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 85 %

Limits: 44-120 %

"

"

"

101 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6C0227-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0388

ug/L

03/07/16 15:47

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0388

"

"

"

"

Anthracene

ND

---

0.0388

"

"

"

"

Benz(a)anthracene

ND

---

0.0388

"

"

"

"

Benzo(a)pyrene

ND

---

0.0388

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0388

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0388

"

"

"

"

Chrysene

ND

---

0.0388

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0388

"

"

"

"

Dibenzofuran

ND

---

0.0388

"

"

"

"

Fluoranthene

ND

---

0.0388

"

"

"

"

Fluorene

ND

---

0.0388

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0388

"

"

"

"

1-Methylnaphthalene

ND

---

0.0777

"

"

"

"

2-Methylnaphthalene

ND

---

0.0777

"

"

"

"

Naphthalene

ND

---

0.0777

"

"

"

"

Phenanthrene

ND

---

0.0388

"

"

"

"

Pyrene

ND

---

0.0388

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 85 %

Limits: 44-120 %

"

"

"

98 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6C0227-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0396

ug/L

03/07/16 16:14

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0396

"

"

"

"

Anthracene

ND

---

0.0396

"

"

"

"

Benz(a)anthracene

ND

---

0.0396

"

"

"

"

Benzo(a)pyrene

ND

---

0.0396

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0396

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0396

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0396

"

"

"

"

Chrysene

ND

---

0.0396

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0396

"

"

"

"

Dibenzofuran

ND

---

0.0396

"

"

"

"

Fluoranthene

ND

---

0.0396

"

"

"

"

Fluorene

ND

---

0.0396

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0396

"

"

"

"

1-Methylnaphthalene

ND

---

0.0792

"

"

"

"

2-Methylnaphthalene

ND

---

0.0792

"

"

"

"

Naphthalene

ND

---

0.0792

"

"

"

"

Phenanthrene

ND

---

0.0396

"

"

"

"

Pyrene

ND

---

0.0396

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 66 %

Limits: 44-120 %

"

"

"

92 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6C0227-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0392

ug/L

03/07/16 16:41

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0392

"

"

"

"

Anthracene

ND

---

0.0392

"

"

"

"

Benz(a)anthracene

ND

---

0.0392

"

"

"

"

Benzo(a)pyrene

ND

---

0.0392

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0392

"

"

"

"

Chrysene

ND

---

0.0392

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0392

"

"

"

"

Dibenzofuran

ND

---

0.0392

"

"

"

"

Fluoranthene

ND

---

0.0392

"

"

"

"

Fluorene

ND

---

0.0392

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0392

"

"

"

"

1-Methylnaphthalene

ND

---

0.0784

"

"

"

"

2-Methylnaphthalene

ND

---

0.0784

"

"

"

"

Naphthalene

ND

---

0.0784

"

"

"

"

Phenanthrene

ND

---

0.0392

"

"

"

"

Pyrene

ND

---

0.0392

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 85 %

Limits: 44-120 %

"

"

"

96 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-05 (A6C0227-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0385

ug/L

03/07/16 17:07

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0385

"

"

"

"

Anthracene

ND

---

0.0385

"

"

"

"

Benz(a)anthracene

ND

---

0.0385

"

"

"

"

Benzo(a)pyrene

ND

---

0.0385

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0385

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0385

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0385

"

"

"

"

Chrysene

ND

---

0.0385

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0385

"

"

"

"

Dibenzofuran

ND

---

0.0385

"

"

"

"

Fluoranthene

ND

---

0.0385

"

"

"

"

Fluorene

ND

---

0.0385

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0385

"

"

"

"

1-Methylnaphthalene

ND

---

0.0769

"

"

"

"

2-Methylnaphthalene

ND

---

0.0769

"

"

"

"

Naphthalene

ND

---

0.0769

"

"

"

"

Phenanthrene

ND

---

0.0385

"

"

"

"

Pyrene

ND

---

0.0385

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6030185

Recovery: 82 %

Limits: 44-120 %

"

"

"

97 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

ANALYTICAL SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

Foundation-S (A6C0227-06)

% Solids

Reporting
Limit
Matrix: Soil

70.8

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

1.00

Dilution

Units

Date Analyzed

Method

03/07/16 13:09

EPA 8000C

Notes

Batch: 6030191

% by Weight

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6030186 - EPA 3546 (Fuels)

Prepared: 03/07/16 10:04 Analyzed: 03/07/16 14:11

Blank (6030186-BLK1)
NWTPH-Dx

Diesel

ND

---

25.0

mg/kg wet

---

---

---

---

---

---

Oil

ND

---

50.0

"

"

---

---

---

---

---

---

---

---

Surr: o-Terphenyl (Surr)

Recovery: 93 %

Limits: 50-150 %

Dilution: 1x

Prepared: 03/07/16 10:04 Analyzed: 03/07/16 14:31

LCS (6030186-BS1)
NWTPH-Dx

Diesel

107

---

Surr: o-Terphenyl (Surr)

25.0
Recovery: 98 %

mg/kg wet

125

Limits: 50-150 %

---

86

76-115%

Dilution: 1x

Prepared: 03/07/16 10:04 Analyzed: 03/07/16 15:41

Duplicate (6030186-DUP1)
QC Source Sample: Foundation-S (A6C0227-06RE1)
NWTPH-Dx

Diesel
Oil
Surr: o-Terphenyl (Surr)

42900

---

538

mg/kg dry

20

---

27600

---

---

43

30%

ND

---

1080

"

"

---

ND

---

---

---

30%

Recovery: %

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Limits: 50-150 %

Dilution: 20x

Q-04

S-01

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030189 - EPA 5030B

Prepared: 03/07/16 15:32 Analyzed: 03/07/16 17:56

Blank (6030189-BLK1)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

---

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

---

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

ND

---

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 80-120 %

Dilution: 1x

102 %

80-120 %

"

96 %

80-120 %

"

100 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 03/07/16 15:32 Analyzed: 03/07/16 16:58

LCS (6030189-BS1)
EPA 8260B

Benzene

20.5

---

0.200

ug/L

20.0

---

102

70-130%

Toluene

20.0

---

1.00

"

"

"

---

100

"

---

---

Ethylbenzene

20.6

---

0.500

"

"

"

---

103

"

---

---

Xylenes, total

62.8

---

1.50

"

"

60.0

---

105

"

---

---

Naphthalene

18.7

---

2.00

"

"

20.0

---

94

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

17.3

---

1.00

"

"

"

---

86

"

---

---

21.6

---

1.00

"

"

"

---

108

"

---

---

n-Propylbenzene

20.3

---

0.500

"

"

"

---

102

"

---

---

1,2,4-Trimethylbenzene

20.5

---

1.00

"

"

"

---

103

"

---

---

1,3,5-Trimethylbenzene

20.5

---

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.8

---

0.500

"

"

"

---

104

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030189 - EPA 5030B

Prepared: 03/07/16 15:32 Analyzed: 03/07/16 16:58

LCS (6030189-BS1)

1,2-Dichloroethane (EDC)

Source
Result

19.2

Surr: Dibromofluoromethane (Surr)

---

0.500

ug/L

"

"

---

Recovery: 100 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

99 %

80-120 %

"

Toluene-d8 (Surr)

96 %

80-120 %

"

4-Bromofluorobenzene (Surr)

99 %

80-120 %

"

96

"

---

---

Prepared: 03/07/16 12:42 Analyzed: 03/07/16 18:53

Duplicate (6030189-DUP1)
QC Source Sample: SW-01 (A6C0227-01)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

ND

---

---

---

30%

Toluene

ND

Ethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

---

0.500

"

"

---

ND

---

---

---

30%

Xylenes, total
Naphthalene

ND

---

1.50

"

"

---

ND

---

---

---

30%

ND

---

2.00

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

ND

---

1.00

"

"

---

ND

---

---

---

30%

n-Propylbenzene

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 80-120 %

Dilution: 1x

102 %

80-120 %

"

Toluene-d8 (Surr)

96 %

80-120 %

"

4-Bromofluorobenzene (Surr)

99 %

80-120 %

"

1,4-Difluorobenzene (Surr)

Prepared: 03/07/16 12:42 Analyzed: 03/07/16 21:16

Matrix Spike (6030189-MS1)


QC Source Sample: SW-05 (A6C0227-05)
EPA 8260B

Benzene

20.9

---

0.200

ug/L

20.0

ND

104

70-130%

---

---

Toluene

20.5

---

1.00

"

"

"

ND

103

"

---

---

Ethylbenzene

21.2

---

0.500

"

"

"

ND

106

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030189 - EPA 5030B

Prepared: 03/07/16 12:42 Analyzed: 03/07/16 21:16

Matrix Spike (6030189-MS1)


QC Source Sample: SW-05 (A6C0227-05)

Xylenes, total

64.3

---

1.50

ug/L

"

60.0

ND

107

"

---

---

Naphthalene

17.3

---

2.00

"

"

20.0

ND

86

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

17.2

---

1.00

"

"

"

ND

86

"

---

---

22.2

---

1.00

"

"

"

ND

111

"

---

---

n-Propylbenzene

20.6

---

0.500

"

"

"

ND

103

"

---

---

1,2,4-Trimethylbenzene

20.7

---

1.00

"

"

"

ND

104

"

---

---

1,3,5-Trimethylbenzene

21.1

---

1.00

"

"

"

ND

105

"

---

---

1,2-Dibromoethane (EDB)

20.4

---

0.500

"

"

"

ND

102

"

---

---

1,2-Dichloroethane (EDC)

19.7

---

0.500

"

"

"

ND

99

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 101 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

99 %

80-120 %

"

Toluene-d8 (Surr)

95 %

80-120 %

"

4-Bromofluorobenzene (Surr)

98 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030185 - EPA 3510C (Acid Extraction)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 13:59

Blank (6030185-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0182

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

---

0.0182

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.0182

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.0182

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.0182

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.0182

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.0182

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.0182

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.0182

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.0182

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.0364

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.0364

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0364

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.0182

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.0182

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 69 %

Limits: 44-120 %

Dilution: 1x

95 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:26

LCS (6030185-BS1)
EPA 8270D (SIM)

Acenaphthene

2.94

---

0.0200

ug/L

4.00

---

74

47-122%

---

Acenaphthylene

3.01

---

0.0200

"

"

"

---

75

41-130%

---

---

Anthracene

3.65

---

0.0200

"

"

"

---

91

57-123%

---

---

Benz(a)anthracene

3.54

---

0.0200

"

"

"

---

88

58-125%

---

---

Benzo(a)pyrene

3.80

---

0.0200

"

"

"

---

95

54-128%

---

---

Benzo(b)fluoranthene

3.81

---

0.0200

"

"

"

---

95

53-131%

---

---

Benzo(k)fluoranthene

3.95

---

0.0200

"

"

"

---

99

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6030185 - EPA 3510C (Acid Extraction)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:26

LCS (6030185-BS1)

Benzo(g,h,i)perylene

Source
Result

3.09

---

0.0200

"

"

"

---

77

50-134%

---

---

Chrysene

3.54

---

0.0200

"

"

"

---

88

59-123%

---

---

Dibenz(a,h)anthracene

3.65

---

0.0200

"

"

"

---

91

51-134%

---

---

Dibenzofuran

3.11

---

0.0200

"

"

"

---

78

53-120%

---

---

Fluoranthene

3.58

---

0.0200

"

"

"

---

89

57-128%

---

---

Fluorene

3.23

---

0.0200

"

"

"

---

81

52-124%

---

---

Indeno(1,2,3-cd)pyrene

3.25

---

0.0200

"

"

"

---

81

52-133%

---

---

1-Methylnaphthalene

2.42

---

0.0400

"

"

"

---

61

41-120%

---

---

2-Methylnaphthalene

2.52

---

0.0400

"

"

"

---

63

40-121%

---

---

Naphthalene

2.47

---

0.0400

"

"

"

---

62

"

---

---

Phenanthrene

3.42

---

0.0200

"

"

"

---

86

59-120%

---

---

Pyrene

3.62

---

0.0200

"

"

"

---

90

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 75 %

Limits: 44-120 %

Dilution: 1x

95 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:53

LCS Dup (6030185-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

2.56

---

0.0200

ug/L

4.00

---

64

47-122%

14

30%

Acenaphthylene

2.59

---

0.0200

"

"

"

---

65

41-130%

15

30%

Anthracene

3.37

---

0.0200

"

"

"

---

84

57-123%

30%

Benz(a)anthracene

3.45

---

0.0200

"

"

"

---

86

58-125%

30%

Benzo(a)pyrene

3.65

---

0.0200

"

"

"

---

91

54-128%

30%

Benzo(b)fluoranthene

3.77

---

0.0200

"

"

"

---

94

53-131%

30%

Benzo(k)fluoranthene

3.85

---

0.0200

"

"

"

---

96

57-129%

30%

Benzo(g,h,i)perylene

3.04

---

0.0200

"

"

"

---

76

50-134%

30%

Chrysene

3.43

---

0.0200

"

"

"

---

86

59-123%

30%

Dibenz(a,h)anthracene

3.57

---

0.0200

"

"

"

---

89

51-134%

30%

Dibenzofuran

2.70

---

0.0200

"

"

"

---

67

53-120%

14

30%

Fluoranthene

3.42

---

0.0200

"

"

"

---

86

57-128%

30%

Fluorene

2.82

---

0.0200

"

"

"

---

70

52-124%

14

30%

Indeno(1,2,3-cd)pyrene

3.18

---

0.0200

"

"

"

---

79

52-133%

30%

1-Methylnaphthalene

2.14

---

0.0400

"

"

"

---

54

41-120%

12

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

RPD
Limit

Prepared: 03/07/16 10:00 Analyzed: 03/07/16 14:53

LCS Dup (6030185-BSD1)

2-Methylnaphthalene

2.22

---

0.0400

"

"

"

---

55

Naphthalene

2.16

---

0.0400

"

"

"

---

Phenanthrene

3.12

---

0.0200

"

"

"

---

Pyrene

3.46

---

"

"

"

---

0.0200
Recovery: 61 %

Limits: 44-120 %

Dilution: 1x

89 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6030185 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

%REC
Limits RPD

Q-19

40-121%

13

30%

54

"

14

30%

78

59-120%

30%

87

57-126%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 19 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

QUALITY CONTROL (QC) SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6030191 - Total Solids (Dry Weight)

Prepared: 03/07/16 11:08 Analyzed: 03/07/16 13:09

Duplicate (6030191-DUP1)
QC Source Sample: Foundation-S (A6C0227-06)
EPA 8000C

% Solids

60.7

---

1.00

% by
Weight

---

70.8

---

---

15

10%

Q-17

No Client related Batch QC samples analyzed for this batch. See notes page for more information.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 20 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

SAMPLE PREPARATION INFORMATION


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 3546 (Fuels)


Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 10:37

03/07/16 10:04

Batch: 6030186

A6C0227-06RE1

NWTPH-Dx

Soil

10.53g/5mL

10g/5mL

0.95

RBDM Compounds (BTEX+) by EPA 8260B


Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 08:13
03/06/16 08:40
03/06/16 08:50
03/06/16 09:00
03/06/16 09:50

03/07/16 12:42
03/07/16 12:42
03/07/16 12:42
03/07/16 12:42
03/07/16 12:42

Batch: 6030189

A6C0227-01
A6C0227-02
A6C0227-03
A6C0227-04
A6C0227-05

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

Water
Water
Water
Water
Water

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 08:13
03/06/16 08:40
03/06/16 08:50
03/06/16 09:00
03/06/16 09:50

03/07/16 10:00
03/07/16 10:00
03/07/16 10:00
03/07/16 10:00
03/07/16 10:00

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

0.97
0.97
0.99
0.98
0.96

Batch: 6030185

A6C0227-01
A6C0227-02
A6C0227-03
A6C0227-04
A6C0227-05

Water
Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

1030mL/2mL
1030mL/2mL
1010mL/2mL
1020mL/2mL
1040mL/2mL

Percent Dry Weight


Prep: Total Solids (Dry Weight)
Lab Number

Matrix

Method

Sampled

Prepared

03/06/16 10:37

03/07/16 11:08

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6030191

A6C0227-06

Soil

EPA 8000C

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1N/A/1N/A

1N/A/1N/A

NA

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 21 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

03/08/16 04:39

Notes and Definitions


Qualifiers:
Q-04

Spike recovery and/or RPD is outside control limits due to a non-homogeneous sample matrix.

Q-17

RPD between original and duplicate sample is outside of established control limits.

Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Q-42

Matrix Spike and/or Duplicate analysis was performed on this sample. % Recovery or RPD for this analyte is outside laboratory control
limits. (Refer to the QC Section of Analytical Report.)

S-01

Surrogate recovery for this sample is not available due to sample dilution required from high analyte concentration and/or matrix
interference.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 22 of 23

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

03/08/16 04:39

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 23 of 23

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