AT&T Hall Ridge Work Plan 03-07-2016

CB&I
500 Penn Center Blvd.

Suite 1000
Pittsburgh, PA 15235
Tel: 412.372.7701
Fax: 412.380.4091
www.CBI.com
March7,2016
ProjectNo.156319
Mr.GeoffreyBrown
EmergencyResponseProgram
OregonDepartmentofEnvironmentalQuality
WesternRegionEugene
165E7thAve,Suite100
Eugene,OR974013049
Re:
PathtoClosureWorkPlan
AT&THallRidgeCellTower
NationalResponseCenterReportNo.1140291
OregonEmergencyResponseSystemReportNo.20160374
Detroit,MarionCounty,Oregon
DearMr.Brown:
CB&IonthebehalfofAT&T,ispleasedtopresentthisPathtoClosureWorkPlanforthepostexcavation
and characterization activities at the AT&Ts Hall Ridge, Detroit, Oregon, cell tower (Site). The
emergencyresponseteam,whichconsistedofCB&I,NRC,NWFF,andSMAF,havecompletedtheinitial
phase of the emergency response including the removal of impacted soil in the release area,
containmentofthedownslopemigrationoffuel,characterizationoftheimpactedsoil,snowremoval,
andinitialroadrepairs.
OnFebruary11,2016,BarryWilliams(AT&T)receivednotificationofareleaseofdieselatthesubject
site.Theinitialinvestigationestimatedtheamountoffuelreleasedfromthetanksystemat550gallons.
It appeared the fuel was pumped from the 800gallon main tank to the 220gallon day tank, which
discharged from the vent located on the roof. Mr. Williams notified the National Response Center to
reportthespillat1740EasternStandardTime(EST).TheNationalResponseCenterassignedReportNo.
1140291tothespill.Mr.WilliamsalsonotifiedtheOregonEmergencyResponseSystemat1750ESTto
reportthespillandwasassignedReportNo.20160374.
ThisWorkPlanwasdevelopedtoprovideguidancefortheimplementationofbiostimulationtreatment
activitiesandpostexcavationandcharacterizationmonitoring.
Mr.GeoffreyBrown
March7,2016
Background
The site and surrounding area are located on the U.S. Geological Survey 7.5minute Detroit, Oregon,
topographic quadrangle map. The site is located at approximately 444309.7 north latitude,
1221303.6 west longitude. A review of the quadrangle map shows the site at an elevation of
approximately 4,400 feet above mean sea level (msl). The nearest surface water to the site is an
unnamed tributary, which is approximately 600 feet northeast of the site. A site vicinity map is
presentedasFigure1.
AccordingtotheUnitedStatesGeologicalSurveysNationalGeologicMapDatabase,thesiteislocated
ontheeasternflankoftheSardineSynclineandtheBreitenbushAnticlineislocatedtotheeast.Bedrock
dips at a shallow angle to the west. Bedrock listed is the Sardine Series, which consists of series of
Miocene age rhyolite, andesite, basalt, tuff, and breccia exposed on Sardine Mountain northwest of
Detroit.
EmergencyResponseTasksCompleted
Thefollowingtaskshavebeencompletedunderthisemergencyresponse:
OnFebruary12,2016,crewsweremobilizedtoinspectthesite.Theimpactedareawas
assessedandabsorbentboomsandpadsplacedinstrategicareastocapturethefreephase
diesel.
FromFebruary13throughFebruary19,2016Roadclearingcontinuedwithadditionalsnow
fall.Severalimpactedareaswerehandexcavated.Absorbentpadsinspectedandreplaced.
Wastewascontainerizedandstagedfordisposal.
OnFebruary22,2016,theORDEQandUSFSprovisionallyapprovedtheSamplingandAnalysis
Plan.
OnFebruary23,2016,theUSFSlocatedandauthorizedNRCtocollectwaterfromasourcenear
thesiteforthepercolationtest.
OnFebruary2425,2016,thepercolationtestcommencedoveratwodayperiodusing
fluorescentdye(BrightDyesFLTYellowGreenPowder)torecreatetheflowpathsofdieselfuel
throughbedrock.
OnFebruary26,2016,soilsampleswerecollectedona20footgridtodelineatetheextentof
thedieselintheshallowsoildownslopefromtherelease.
OnFridayFebruary19,2016,SundayFebruary21,2016,andSundayFebruary28,2016,four
surfacewatersampleswerecollectedfromtheunnamedtributaries(SW01,SW02,SW03,and
SW04)andSW05onThursdayFebruary25,2016.Dailyinspectionsoccuratthefivesurface
waterlocations.
Mr.GeoffreyBrown
March7,2016
DiscussionofSoilSampleResults
On February 26, 2016, soil samples were taken from 21 locations at the release area excavation and
downslope areas. Sample locations were identified using an established downslope grid and biased
wheredieselfuelwasvisuallyobserved(Figure3).Soilsampleswereanalyzedfordieselrangeorganics
byNWTPHDx,RBDMVOCsbyEPA8260B,andPAHsbyEPA8270DSIM.Thelaboratoryanalyticalresults
havebeentabulatedandpresentedinTable1.
The soil sample results were compared against ORDEQ riskbased concentrations (RBCs) for two
exposure pathways: soil ingestion, dermal contact, and inhalation (RBCSS), and soil leaching to
groundwater(RBCSW).ThreesamplelocationsshowedNWTPHDxconcentrationsthatexceedRBCsvia
eitherexposurepathway.Thesethreehotspotlocations(0C,1C,and2C)followthecenterlineofthe
downslopegrid,adjacenttothereleaseareaexcavation.
At sample location 0C, laboratory results show RBC exceedances for NWTPHDx (9,430 milligrams per
kilogram[mg/kg]),Benzene(0.161mg/kg),Ethylbenzene(3.70mg/kg),Naphthalene(2.15mg/kg),and
1,2,4Trimethylbenzene(19.9mg/kg).Atsamplelocation1C,resultsshowRBCexceedanceforNWTPH
Dx(66,400mg/kg).Atsamplelocation2C,resultsshowRBCexceedanceforNWTPHDx(96,800mg/kg).
NWTPHDx concentrations were also observed at sample locations EWSIDEWALLE (184 mg/kg), 0B
(1,090 mg/kg), 1B (44.6 mg/kg), 2B (70.2 mg/kg), and 3A (29.1 mg/kg). These locations are directly
adjacent to the hot spot locations, with the exception of 3A. The NWTPHDx concentrations at all
othersamplelocationswerenondetect.ThelaboratoryanalyticalresultsarepresentedinAppendixA.
OutcropSourceRemoval
Dieselhasaccumulatedontopofabedrockoutcroplocatedapproximately40feetdownslopefromthe
releaseareaasindicatedbysoilanalyticaldata,PIDreadingsandsiteobservation.Impactedsoilontop
of the rock outcrop will be excavated to provide mass removal and eliminate known potential source
areasforfutureleachingofdiesel.Thelimitsoftheexcavationwillextendapproximately4feetupslope
from the rock outcrop, approximately 10 feet across the width of the rock outcrop, and extend
approximately1footdeeptobedrock.Thelimitsoftheexcavationwillbedeterminedinthefieldusing
aPIDandfieldobservations.Duetotheextremesiteconditions,theimpactedsoilwillbeexcavatedby
hand.
Confirmationsoilsampleswillbecollectedonthesidewallsoftheexcavation,estimatedattwosamples
alongthetopwallandonesampleoneachsidewallsoftheexcavation.Theflooranddownslopewall
of the excavation are anticipated to be bedrock; therefore, soil samples are not anticipated at these
locations. Soil samples will be analyzed for diesel range organics by NWTPHDx, RBDM VOCs by EPA
8260B,andPAHsbyEPA8270DSIM.
Mr.GeoffreyBrown
March7,2016
Biostimulation
AT&T proposes to use a combination of two biostimulation products to naturally degrade residual
dieselattheSite.TheseproductsincludeOilSpillEatersInternationalCorporationsproprietaryOSEII
and MicroBlaze NonFormulated. MicroBlaze NonFormulated is a consortium of hydrocarbon
degrading bacteria that will be applied to the individual release areas in a 10% solution following the
application of OSE II. MicroBlaze NonFormulated contains no surfactants or nutrients, just a
consortiumofknownhydrocarbondegradingbacteria.
AT&T proposes to use Oil Spill Eaters International Corporations proprietary OSE II amendment to
breakdown residual diesel LNAPL in the subsurface. OSE II is a biocatalyst that contains enzymes and
nutrients designed to enhance the emulsification of LNAPL and stimulate hydrocarbon consuming
bacteriatodegradehydrocarbonsreleasedintheenvironment.NutrientswithinOSEIIwillincreasethe
rate of biodegradation of the dieselconsuming bacteria present beneath the Site to remove the
dissolveddiesel.OSEIIhasbeenevaluatedbytheEnvironmentalProtectionAgencyandislistedasan
accepted remedial response technology for hydrocarbon releases (Environmental Protection Agency,
2009).TheCaliforniaDepartmentofWildlife(formerlyDepartmentofFishandGame)haslicensedOSE
IIforoilspilltreatmentinCalifornia.DocumentationoftheOSEIIisprovidedinAppendixB.
The application of the OSE II and MicroBlaze NonFormulated is proposed in three areas. The first
application will be applied to a small trench excavated on the upgradient side of the AT&T
communicationbuilding.Thiswillbeconductedtotreatresidualdieselinthebasecoursebeneaththe
building foundation. The second application will be in the release area excavation to introduce these
solutionsintothesubsurfacefollowingasimilarpathwayastheoriginalrelease.Thethirdapplication
willbeasurfaceapplicationofthesesolutionswithinthelimitsofthedownslopeexcavationfollowing
theremovalofimpactedsoilontopoftherockoutcropandthesurfaceapplicationofthesoilbetween
the release area and rock outcrop. Documentation of MicroBlaze NonFormulated is provided in
AppendixB.Eachoftheseapplicationsisdiscussedbelow.
BuildingFoundationApplication
OSE II/MicroBlaze NonFormulated will be applied hydraulically upgradient of the AT&T
Communicationbuildinginanattempttotreatresidualdieselresidinginthebasecoursebeneaththe
building foundation. A small trench will be excavated along the north footing of the building for the
application of the OSE II. The trench will be approximately 1 foot wide and 6 inches deep. Excavated
materialwillbeplacedalongtheoutsideextentofthetrenchtoformaberm.Alicensedarcheologist
willbeonsiteduringallgrounddisturbanceactivities.Approximately300gallonsoftheOSEIIsolution
will be gravity fed into the trench at such a rate as to not overflow the trench, while maintaining a
constantheadinthetrench.Absorbentpadswillbeplacedadjacenttotheexposedbasecoursealong
thesouthsideofthebuildingtocapturedieselthatmaybedisplacedduringthisprocedure.
Mr.GeoffreyBrown
5
March7,2016
ReleaseAreaApplication
OSEIIwillbeappliedwithinthelimitsofthereleaseareainanefforttofollowthesamepathwayasthe
dieselduringtheoriginalrelease.Approximately900gallonsofOSEIIsolutionwillbeappliedontopof
theexposedbedrockinthereleaseareaexcavation.Theapplicationratewillbeconsistentwiththedye
test conducted on February 23, 2016 to evaluate flow pathways and maintained at a rate as to not
overflow the excavation. Absorbent pads located downslope of the excavation will be monitored and
replacedasnecessaryduringthistask.
OutcropExcavationOSEIIApplication
OSEIIwillbeappliedtothesurfaceofthedownslopeoutcropexcavationadjacenttotherockoutcrop
andsurroundingsoil.Approximately100gallonsofOSEIIsolutionwillbeappliedontopofthesoilinthe
areaextendingfromthereleaseareatotherockoutcropusingahose.Thesoilinthisareaispotentially
impactedbasedonsoilanalyticaldataandsiteobservations.Theapplicationrateshouldbemonitored
to prevent surface runoff, but sufficient to promote infiltration and near saturation. If the soil in the
treatment area becomes saturated to the point surface runoff occurs, the application rate will be
reduced. If surface water runoff continues to occur, the remaining volume of OSE II solution will be
applied to the release area. Absorbent pads located downslope of the impacted soil area will be
monitoredandreplacedasnecessaryduringthistask.
MixingProcedure
MicroBlaze NonFormulated will be mixed to a 10% solution using 5 gallons of MicroBlaze to 50
gallonsofwater.Thewaterwillbecollectedfromthesamplesourceusedinthedyetest,pendingUSFS
approval.
The OSE II application system will consist of a bulk mixing tank, one 55 gallon drum of OSE II, a
circulationpump,andassociatedhoses,valves,andfittings.Theapplicationsystemwillbepoweredby
anexistingonsitegenerator.SurfacewaterfromanearbystreamwillbeusedtoblendwiththeOSEIIto
makethe25:1solutionofwatertoOSEII,pendingUSFSapproval.Approximately1,375gallonsofthe
OSE II/surface water solution will be applied in and around the release area. It is anticipated that the
OSE II/surface water solution will be prepared in 300gallon batches for application; therefore, 12
gallonsofOSEIIwillbemixedwith300gallonsofwatertopreparethe25:1solution.
SurfaceWaterSampling
Currently, CB&I performs a daily visual inspection of five unnamed tributaries (SW01, SW02, SW03,
SW04,andSW05)andcollectsweeklysurfacewatersamplesfromtheselocationsonaweeklybasis.
These surface water samples are analyzed for RBDM VOCs by EPA Method 8260B and PAHs by EPA
Method8270DSIM.NoVOCsorPAHshavebeendetectedinanyofthesurfacewatersamplescollected
from the identified streams. The laboratory analytical results have been tabulated and presented in
Table2.SurfacewatersamplelocationsarepresentedinFigure4.
Mr.GeoffreyBrown
6
March7,2016
Surfacewatersampleswillbecollected30days,90days,and180daysfollowingtheapplicationofOSE
II to monitor potential impact to the adjacent surface water streams. Surface water sampling will be
discontinued following the 180 day sampling event if the analytical results remain below laboratory
detectionlimits.ApprovalwillberequestedfromORDEQandUSFStodiscontinuethesamplingprogram
if no VOCs or PAHs have been detected in the surface water following the 180 days of post bio
stimulationsampling.
In the event that any RBDM VOCs and PAHs are detected in the surface water samples above the
applicablestandards,thenthesurfacewatersamplingplanwillbeamendedtocollectsamplesfurther
downstream and/or at the reservoir discharge locations. The new surface water locations and the
numberofcollectedsampleswillbeapprovedbyORDEQandUSFS.
DatafromthesamplingwillbesubmittedtotheORDEQandUSFSinstatusreports.Thestatusreports
willprovideabriefsummaryoftheanalyticalresultsandconfirmthefuturesamplingfrequency.
AbsorbentandWeirMaintenance
Afterexcavationofthesourcearea,crewsestablishedadownslopecatchmentsystemincludingaweir
and trenches containing absorbent booms, and absorbent pads interweaved across the exposed
bedrock seepage areas. Crews are monitoring the absorbents daily and replacing them as needed.
SaturatedabsorbentsarecontainerizedinSuperSacsandremovedoffsitetoalandfill.
FollowingapplicationoftheOSEIItreatment,crewswillcontinuetochangeoutabsorbentpadsand/or
booms along the downslope hillside on a weekly basis. In the event that no color change in the
absorbents is observed for 30 days, then crews will remove absorbents and booms from the site and
backfill the weir, trenches, and potholes. Crews will restore the site as close as possible to pre
disturbancedrainageconditions.
SiteRestoration
Releasearea
The release area excavation and adjacent area will be restored to preexcavation conditions following
thebiostimulationapplication.Approximately4inchlayerofpeatmosswillbeappliedadjacenttothe
exposed building footing and over the exposed bedrock with previously observed contact with diesel.
The diesel readily binds with peat moss until it naturally biodegrades, preventing any residual diesel
frommigratingoffsite.Sufficientgravelwillbeplacedoverthepeatmosstorestorethesitetonearpre
excavation grade. Clean gravel that was excavated during the initial response and temporarily
stockpiled adjacent to the excavation will be used as fill material. Additional gravel from an offsite
sourceconsistingof3/4inchminuswillbeappliedtotheexcavationtorestoretheareatotheoriginal
grade.Fillmaterialwillbeappliedin6inchliftsandcompactedbydrivingoverthefillmaterialwiththe
equipment.Theareawillbegradedtopromotepositivedrainageawayfromthebuilding.
Mr.GeoffreyBrown
7
March7,2016
OutcropExcavation
The outcrop excavation and adjacent area will be restored to preexcavation conditions following the
biostimulation application. Approximately 4inch layer of peat moss will be applied adjacent to the
exposed bedrock with previously observed contact with diesel. Top soil will be applied on top of the
peatmossin6inchliftsandhandcompacteduntiltheelevationofthefillmaterialisconsistentwiththe
surroundingtopography.Grassmattingwillbeappliedoverthetopsoiltominimizeerosion.
Recommendation
Please provide your written approval if this Work Plan is acceptable or let us know if you have any
questions,comments,orrevisions.Ifnecessary,theWorkPlanwillberevisedandresubmittedforyour
approval.Thankyouforyourtimeduringouronsitemeetingsandforyourresponsivenessinworking
withustodevelopthisPlan.
Pleasecontacteitheroftheundersignedifyouhaveanyquestionsconcerningthisreport.
Sincerely:
RonaldMalec,P.G.
IncidentCommander,UnitChief
4123804484
Ron.Malec@CBI.com
MF:KR:RM:lmk
Attachments
cc:LaurenPlunk(AT&T)
BrynThoms(ORDEQ)
GregAitken(ORDEQ)
GradyMcMahan(USFS)
DarrinNeff(USFS)
JamieSheahanAlonso(USFS)
PennyKeen(USFS)
MarkFinney(CB&I)
BryanHolmes(CB&I)
KentRoberts
SeniorOperationsManager
3215431194
Kent.Roberts@cbi.com
Tables
Table1
SoilSampleAnalyticalResults
AT&THallRidge
WillametteNationalForest
Detroit,Oregon
RBCsw
Contaminant
PIDReading(ppm)
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)
RBCss
(mg/kg) (mg/kg)
9,500
4,600
>Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
NoStd. NoStd.
5.6
2,000
110
3,500
0.00056
9
0.013
200
1A
(mg/kg)
5.4
ND
123
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1B
(mg/kg)
6.4
44.6
159
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page1of7
1C
(mg/kg)
397
66,400
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2A
(mg/kg)
2.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2B
(mg/kg)
1.9
70.2
312
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2C
(mg/kg)
183
96,800
ND
0.0449
0.887
0.832
4.74
ND
ND
ND
0.642
3.53
1.04
ND
ND
2D
(mg/kg)
33.8
ND
606
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Table1
AT&THallRidge
Detroit,Oregon
RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCss
(mg/kg) (mg/kg)
21,000
NoStd. NoStd.
110,000
2.3
24
1.9
2.4
24
240
NoStd. NoStd.
2,400
2.4
NoStd. NoStd.
10,000
14,000
24
NoStd. NoStd.
NoStd. NoStd.
0.37
580
NoStd. NoStd.
7,500
1A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page2of7
1C
(mg/kg)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2C
(mg/kg)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2D
(mg/kg)
ND
ND
ND
ND
ND
0.0249
ND
ND
ND
ND
ND
ND
0.0229
ND
0.0284
0.0433
0.0502
0.0229
ND
Table1
AT&THallRidge
Detroit,Oregon
RBCsw
Contaminant
PIDReading(ppm)
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
RBCss
(mg/kg) (mg/kg)
9,500
4,600
>Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
NoStd. NoStd.
5.6
2,000
110
3,500
0.00056
9
0.013
200
3A
(mg/kg)
3.3
29.1
116
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3B
(mg/kg)
2.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page3of7
3C
(mg/kg)
3.3
ND
98.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3D
(mg/kg)
1.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4A
(mg/kg)
3.4
ND
117
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4B
(mg/kg)
4.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4C
(mg/kg)
1.1
ND
87.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Table1
AT&THallRidge
Detroit,Oregon
RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCss
(mg/kg) (mg/kg)
21,000
NoStd. NoStd.
110,000
2.3
24
1.9
2.4
24
240
NoStd. NoStd.
2,400
2.4
NoStd. NoStd.
10,000
14,000
24
NoStd. NoStd.
NoStd. NoStd.
0.37
580
NoStd. NoStd.
7,500
3A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page4of7
3C
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3D
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4C
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Table1
AT&THallRidge
Detroit,Oregon
RBCsw
Contaminant
PIDReading(ppm)
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
RBCss
(mg/kg) (mg/kg)
9,500
4,600
>Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
NoStd. NoStd.
5.6
2,000
110
3,500
0.00056
9
0.013
200
4D
(mg/kg)
1.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0A
(mg/kg)
0.9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page5of7
0B
(mg/kg)
10.5
1,090
ND
ND
0.224
0.200
1.04
ND
ND
ND
0.162
0.755
0.264
ND
ND
0C
(mg/kg)
36.8
9,430
ND
0.161
2.93
3.70
20.6
2.15
ND
1.03
3.82
19.9
6.59
ND
ND
ExSidewall
S
(mg/kg)
5.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ExSidewall
W
(mg/kg)
1.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ExSidewall
E
(mg/kg)
6.0
184
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Table1
AT&THallRidge
Detroit,Oregon
RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCss
(mg/kg) (mg/kg)
21,000
NoStd. NoStd.
110,000
2.3
24
1.9
2.4
24
240
NoStd. NoStd.
2,400
2.4
NoStd. NoStd.
10,000
14,000
24
NoStd. NoStd.
NoStd. NoStd.
0.37
580
NoStd. NoStd.
7,500
4D
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page6of7
0B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0620
ND
ND
ND
0.114
0.155
ND
0.0489
0.0411
0C
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.376
ND
0.454
ND
3.29
5.58
2.08
0.740
0.389
ExSidewall
S
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ExSidewall
W
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ExSidewall
E
(mg/kg)
ND
0.0181
0.0526
0.635
0.219
0.603
0.206
0.0799
0.947
0.0306
ND
1.86
ND
0.116
ND
0.0135
ND
0.0119
1.60
Table1
AT&THallRidge
Detroit,Oregon
Notes:
1
RiskBasedConcentrationsForIndividualChemicals(StateofOregonDepartmentofEnvironmentalQuality),SoilsLeachingtoGroundwater(RBCsw),UrbanResidential
datedNovember1,2015.
2
RiskBasedConcentrationsForIndividualChemicals(StateofOregonDepartmentofEnvironmentalQuality),SoilsLeachingtoSoilIngestion,DermalContact,and
Inhalation(RBCss),ConstructionWorkerdatedNovember1,2015.
Bold=SoilSampleanalyticalresultsexceededapplicablestandard.
AnalyticalResultswerecomparedtotheOregonstandardsfortheSoilsLeachingtoGroundwater(RCBsw)UrbanResidentialandtheSoilLeachingtoSoilIngestion,
DermalContactandInhulation(RCBss)ConstructionWorker.Thelowereofthetwovalueswasselectedforcomparisontotheanalyticresultsforsoils.
mg/kg=milligramsperkilogram.
>Max=TheconstituentRBCforthispathwayiscalculatedasgreaterthan1,000,000mg/kgor1,000,000mg/L.Therefore,thissubstanceisdeemednottoposerisksin
thisscenario.
MTBE=Methyltertbutylether
NoStd.=NostandardlistedinRiskBasedConcentrationsforIndividualChemicalsStateofOregonDepartmentofEnvironmentalQualitydatedNovember1,2015.
PID=Photoionizationdetectorreadingsarereportedinpartspermillion(ppm).
SoilsampleswerecollectedonFebruary26,2016.
ND=Concentrationnotdetectedatthelaboratorymethoddetectionlimit.
NA=NotAnalyzed
=AllRBCvaluesforindirectpathwaysthatexceedalimit(Csat,S,orPv)areremovedfromtheRiskBasedConcentrationsForIndividualChemicalsTable.
Page7of7
Table2
WaterSampleAnalyticalResults
AT&THallRidge
Detroit,Oregon
SW01
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1
RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78
SW01
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW01
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW01
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page1of11
SW01
SW01
SW01
SW01
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW01
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCtw
(g/L)
2,400
NoStd.
0.043
0.011
0.11
NoStd.
0.011
NoStd.
1,400
0.11
NoStd.
NoStd.
0.78
NoStd.
SW01
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW01
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW01
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page2of11
SW01
SW01
SW01
SW01
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW02
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78
SW02
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW02
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW02
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page3of11
SW02
SW02
SW02
SW02
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW02
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCtw
(g/L)
2,400
NoStd.
0.043
0.011
0.11
NoStd.
0.011
NoStd.
1,400
0.11
NoStd.
NoStd.
0.78
NoStd.
SW02
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW02
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW02
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page4of11
SW02
SW02
SW02
SW02
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW03
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78
SW03
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW03
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW03
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page5of11
SW03
SW03
SW03
SW03
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW03
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCtw
(g/L)
2,400
NoStd.
0.043
0.011
0.11
NoStd.
0.011
NoStd.
1,400
0.11
NoStd.
NoStd.
0.78
NoStd.
SW03
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW03
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW03
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page6of11
SW03
SW03
SW03
SW03
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW04
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78
SW04
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW04
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW04
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page7of11
SW04
SW04
SW04
SW04
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW04
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCtw
(g/L)
2,400
NoStd.
0.043
0.011
0.11
NoStd.
0.011
NoStd.
1,400
0.11
NoStd.
NoStd.
0.78
NoStd.
SW04
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW04
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW04
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page8of11
SW04
SW04
SW04
SW04
(g/L)
(g/L)
(g/L)
(g/L)
Table2
AT&THallRidge
Detroit,Oregon
SW05
UnnamedTributary
Contaminant
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
RBCtw
(g/L)
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78
SW05
02/25/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW05
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW05
SW05
SW05
SW05
SW05
(g/L)
(g/L)
(g/L)
(g/L)
(g/L)
Page9of11
Table2
AT&THallRidge
Detroit,Oregon
SW05
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Chrysene
Dibenzofuran
Fluoranthene
Fluorene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
RBCtw
(g/L)
2,400
NoStd.
0.043
0.011
0.11
NoStd.
0.011
NoStd.
1,400
0.11
NoStd.
NoStd.
0.78
NoStd.
SW05
02/25/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW05
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SW05
SW05
SW05
SW05
SW05
(g/L)
(g/L)
(g/L)
(g/L)
(g/L)
Page10of11
Table2
AT&THallRidge
Detroit,Oregon
Notes:
1
RiskBasedConcentrationsForIndividualChemicals(StateofOregonDepartmentofEnvironmentalQuality),GroundwaterIngestion&InhalationfromTapwater
(RBCtw),UrbanResidentialdatedNovember1,2015.
(g/L)=microgramsperliter.
MTBE=Methyltertbutylether
NoStd.=NoStandardListed
ND=Concentrationnotdetectedatthelaboratoryreportinglimit.
NA=NotAnalyzed
=AllRBCvaluesforindirectpathwaysthatexceedalimit(Csat,S,orPv)areremovedfromtheRiskBasedConcentrationsForIndividualChemicalsTable.
Page11of11
Figures
AppendixA
DraftLaboratoryAnalyticalResults
Apex Labs
12232 S.W. Garden Place

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Sunday, February 28, 2016

Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
RE: AT&T Hall Ridge / 156319

Enclosed are the results of analyses for work order A6B0900, which was received by the laboratory on
2/27/2016 at 9:15:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.
DRAFT REPORT
DRAFT REPORT, DATA SUBJECT TO CHANGE
The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory
Page 1 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
Project: AT&T Hall Ridge
NRC-CB&I
6211 N Ensign St
Project Number: 156319
Portland, OR 97217
Project Manager: Ron Malec
Reported:
02/28/16 12:19
ANALYTICAL REPORT FOR SAMPLES

SAMPLE INFORMATION
Sample ID
Laboratory ID
Matrix
1A
A6B0900-01
A6B0900-02
A6B0900-03
A6B0900-04
A6B0900-05
A6B0900-06
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
1B
1C
2A
2B
2C
2D
3A
3B
3C
3D
4A
4B
4C
4D
0A
0B
0C
Ex Sidewall S
Ex Sidewall W
Ex Sidewall E
DRAFT REPORT
Date Sampled
Date Received
02/26/16 09:40
02/26/16 09:50
02/26/16 10:00
02/26/16 10:55
02/26/16 11:00
02/26/16 10:10
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
Page 2 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19
ANALYTICAL SAMPLE RESULTS

Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte
Result
MDL
1A (A6B0900-01)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Diesel
ND
---
28.6
mg/kg dry
02/27/16 13:53
NWTPH-Dx
Oil
123
---
57.2
"
"
"
"
"
"
"
Surrogate: o-Terphenyl (Surr)
Recovery: 88 %
1B (A6B0900-02)
Notes
Batch: 6020836
Limits: 50-150 %
Matrix: Soil
F-17
Batch: 6020836
Diesel
44.6
---
32.2
mg/kg dry
02/27/16 14:33
NWTPH-Dx
F-17
Oil
159
---
64.3
"
"
"
"
F-17
"
"
"
Recovery: 90 %
1C (A6B0900-03)
Diesel
Oil
Limits: 50-150 %
Matrix: Soil
Batch: 6020835
66400
---
2040
mg/kg dry
50
02/27/16 13:53
NWTPH-Dx
ND
---
4080
"
"
"
"
"
"
"
Recovery: %
2A (A6B0900-04)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
ND
---
26.1
mg/kg dry
02/27/16 15:12
NWTPH-Dx
Oil
ND
---
52.2
"
"
"
"
"
"
"
Recovery: 90 %
2B (A6B0900-05)
S-01
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
70.2
---
35.9
mg/kg dry
02/27/16 15:32
NWTPH-Dx
F-17
Oil
312
---
71.8
"
"
"
"
F-17
"
"
"
Recovery: 83 %
2C (A6B0900-06)
Diesel
Oil
Limits: 50-150 %
Matrix: Soil
Batch: 6020835
96800
---
2490
mg/kg dry
50
02/27/16 14:33
NWTPH-Dx
ND
---
4970
"
"
"
"
"
"
"
Recovery: %
2D (A6B0900-07)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
ND
---
180
mg/kg dry
02/27/16 16:12
NWTPH-Dx
Oil
606
---
360
"
"
"
"
"
"
"
Recovery: 84 %
3A (A6B0900-08)
S-01
Limits: 50-150 %
Matrix: Soil
F-17
Batch: 6020836
Diesel
29.1
---
27.2
mg/kg dry
02/27/16 16:32
NWTPH-Dx
F-17
Oil
116
---
54.4
"
"
"
"
F-17
"
"
"
DRAFT REPORT
Recovery: 90 %
Limits: 50-150 %
Page 3 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
MDL
3B (A6B0900-09)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Diesel
ND
---
25.7
mg/kg dry
02/27/16 17:12
NWTPH-Dx
Oil
ND
---
51.5
"
"
"
"
"
"
"
Recovery: 92 %
3C (A6B0900-10)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
ND
---
27.0
mg/kg dry
02/27/16 17:31
NWTPH-Dx
Oil
98.7
---
54.0
"
"
"
"
"
"
"
Recovery: 90 %
3D (A6B0900-11)
Limits: 50-150 %
Matrix: Soil
ND
---
27.6
mg/kg dry
02/27/16 17:12
NWTPH-Dx
Oil
ND
---
55.3
"
"
"
"
"
"
"
Recovery: 90 %
4A (A6B0900-12)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
ND
---
29.8
mg/kg dry
02/27/16 17:31
NWTPH-Dx
Oil
117
---
59.6
"
"
"
"
"
"
"
Recovery: 91 %
4B (A6B0900-13)
Limits: 50-150 %
Matrix: Soil
ND
---
25.0
mg/kg dry
02/27/16 14:52
NWTPH-Dx
Oil
ND
---
50.0
"
"
"
"
"
"
"
Recovery: 94 %
4C (A6B0900-14RE1)
Diesel
Oil
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
ND
---
28.9
mg/kg dry
02/27/16 15:12
NWTPH-Dx
87.2
---
57.7
"
"
"
"
"
"
"
Recovery: 95 %
4D (A6B0900-15)
Limits: 50-150 %
Matrix: Soil
ND
---
25.0
mg/kg dry
02/27/16 15:32
NWTPH-Dx
Oil
ND
---
50.0
"
"
"
"
"
"
"
Recovery: 94 %
0A (A6B0900-16)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
ND
---
34.5
mg/kg dry
02/27/16 12:29
NWTPH-Dx
Oil
ND
---
69.1
"
"
"
"
"
"
"
DRAFT REPORT
Recovery: 90 %
F-17
Batch: 6020836
Diesel
F-17
Batch: 6020836
Diesel
F-17
Batch: 6020836
Diesel
Notes
Batch: 6020836
Limits: 50-150 %
Page 4 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
MDL
0B (A6B0900-17)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Diesel
1090
---
33.4
mg/kg dry
02/27/16 15:52
NWTPH-Dx
Oil
ND
---
66.8
"
"
"
"
"
"
"
Recovery: 99 %
0C (A6B0900-18)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
9430
---
186
mg/kg dry
02/27/16 16:32
NWTPH-Dx
Oil
ND
---
372
"
"
"
"
"
"
"
Recovery: 137 %
Ex Sidewall S (A6B0900-19)
Limits: 50-150 %
Matrix: Soil
ND
---
25.0
mg/kg dry
02/27/16 12:49
NWTPH-Dx
Oil
ND
---
50.0
"
"
"
"
"
"
"
Recovery: 95 %
Ex Sidewall W (A6B0900-20)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
ND
---
26.7
mg/kg dry
02/27/16 12:49
NWTPH-Dx
Oil
ND
---
53.5
"
"
"
"
"
"
"
Recovery: 95 %
Ex Sidewall E (A6B0900-21)
Limits: 50-150 %
Matrix: Soil
Batch: 6020836
Diesel
184
---
25.0
mg/kg dry
02/27/16 16:52
NWTPH-Dx
Oil
ND
---
50.0
"
"
"
"
"
"
"
DRAFT REPORT
Recovery: 94 %
S-05
Batch: 6020836
Diesel
Notes
Batch: 6020836
Limits: 50-150 %
Page 5 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

RBDM Compounds (BTEX+) by EPA 8260B
Result
Analyte
MDL
1A (A6B0900-01)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Benzene
ND
---
0.0217
mg/kg dry
50
02/27/16 13:54
5035/8260B
Toluene
ND
---
0.108
"
"
"
"
Ethylbenzene
ND
---
0.0542
"
"
"
"
Xylenes, total
ND
---
0.163
"
"
"
"
Naphthalene
ND
---
0.217
"
"
"
"
Methyl tert-butyl ether (MTBE)
ND
---
0.108
"
"
"
"
Isopropylbenzene
ND
---
0.108
"
"
"
"
n-Propylbenzene
ND
---
0.0542
"
"
"
"
1,2,4-Trimethylbenzene
ND
---
0.108
"
"
"
"
ND
---
0.108
"
"
"
"
1,2-Dibromoethane (EDB)
ND
---
0.0542
"
"
"
"
1,2-Dichloroethane (EDC)
ND
---
0.0542
"
"
"
"
Surrogate: Dibromofluoromethane (Surr)
Recovery: 106 %
Limits: 70-130 %
"
"
1,4-Difluorobenzene (Surr)
103 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
100 %
Limits: 70-130 %
"
"
"
97 %
Limits: 70-130 %
"
"
"
4-Bromofluorobenzene (Surr)
1B (A6B0900-02)
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0272
mg/kg dry
50
02/27/16 14:51
5035/8260B
Toluene
ND
---
0.136
"
"
"
"
Ethylbenzene
ND
---
0.0680
"
"
"
"
Xylenes, total
ND
---
0.204
"
"
"
"
Naphthalene
ND
---
0.272
"
"
"
"
ND
---
0.136
"
"
"
"
Isopropylbenzene
ND
---
0.136
"
"
"
"
n-Propylbenzene
ND
---
0.0680
"
"
"
"
ND
---
0.136
"
"
"
"
ND
---
0.136
"
"
"
"
ND
---
0.0680
"
"
"
"
ND
---
0.0680
"
"
"
"
Recovery: 104 %
Limits: 70-130 %
"
"
102 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
100 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
02/27/16 15:20
5035/8260B
2A (A6B0900-04)
Benzene
Matrix: Soil
ND
DRAFT REPORT
---
0.0162
Notes
Batch: 6020833
Batch: 6020833
mg/kg dry
50
Page 6 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
2A (A6B0900-04)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Toluene
ND
---
0.0812
mg/kg dry
50
"
5035/8260B
Ethylbenzene
ND
---
0.0406
"
"
"
"
Xylenes, total
ND
---
0.122
"
"
"
"
Naphthalene
ND
---
0.162
"
"
"
"
ND
---
0.0812
"
"
"
"
Isopropylbenzene
ND
---
0.0812
"
"
"
"
n-Propylbenzene
ND
---
0.0406
"
"
"
"
ND
---
0.0812
"
"
"
"
ND
---
0.0812
"
"
"
"
ND
---
0.0406
"
"
"
"
ND
---
0.0406
"
"
"
"
Recovery: 109 %
Limits: 70-130 %
"
"
104 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
99 %
Limits: 70-130 %
"
"
"
96 %
Limits: 70-130 %
"
"
"
2B (A6B0900-05)
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0353
mg/kg dry
50
02/27/16 15:48
5035/8260B
Toluene
ND
---
0.177
"
"
"
"
Ethylbenzene
ND
---
0.0883
"
"
"
"
Xylenes, total
ND
---
0.265
"
"
"
"
Naphthalene
ND
---
0.353
"
"
"
"
ND
---
0.177
"
"
"
"
Isopropylbenzene
ND
---
0.177
"
"
"
"
n-Propylbenzene
ND
---
0.0883
"
"
"
"
ND
---
0.177
"
"
"
"
ND
---
0.177
"
"
"
"
ND
---
0.0883
"
"
"
"
ND
---
0.0883
"
"
"
"
Recovery: 105 %
Limits: 70-130 %
"
"
102 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
99 %
Limits: 70-130 %
"
"
"
95 %
Limits: 70-130 %
"
"
"
2D (A6B0900-07)
Matrix: Soil
Batch: 6020833
Benzene
0.0449
---
0.0391
mg/kg dry
50
02/27/16 16:16
5035/8260B
Toluene
0.887
---
0.195
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020833
Page 7 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
2D (A6B0900-07)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Ethylbenzene
0.832
---
0.0976
mg/kg dry
50
"
Xylenes, total
4.74
---
0.293
"
"
"
"
Naphthalene
ND
---
0.391
"
"
"
"
ND
---
0.195
"
"
"
"
Isopropylbenzene
ND
---
0.195
"
"
"
"
n-Propylbenzene
0.642
---
0.0976
"
"
"
"
3.53
---
0.195
"
"
"
"
5035/8260B
1.04
---
0.195
"
"
"
"
ND
---
0.0976
"
"
"
"
ND
---
0.0976
"
"
"
"
Recovery: 108 %
Limits: 70-130 %
"
"
103 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
93 %
Limits: 70-130 %
"
"
"
96 %
Limits: 70-130 %
"
"
"
3A (A6B0900-08)
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0216
mg/kg dry
50
02/27/16 16:45
5035/8260B
Toluene
ND
---
0.108
"
"
"
"
Ethylbenzene
ND
---
0.0539
"
"
"
"
Xylenes, total
ND
---
0.162
"
"
"
"
Naphthalene
ND
---
0.216
"
"
"
"
ND
---
0.108
"
"
"
"
Isopropylbenzene
ND
---
0.108
"
"
"
"
n-Propylbenzene
ND
---
0.0539
"
"
"
"
ND
---
0.108
"
"
"
"
ND
---
0.108
"
"
"
"
ND
---
0.0539
"
"
"
"
ND
---
0.0539
"
"
"
"
Recovery: 105 %
Limits: 70-130 %
"
"
102 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
100 %
Limits: 70-130 %
"
"
"
97 %
Limits: 70-130 %
"
"
"
3B (A6B0900-09)
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0160
mg/kg dry
50
02/27/16 17:13
5035/8260B
Toluene
ND
---
0.0801
"
"
"
"
Ethylbenzene
ND
---
0.0400
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020833
Page 8 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
3B (A6B0900-09)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Xylenes, total
ND
---
0.120
mg/kg dry
50
"
5035/8260B
Naphthalene
ND
---
0.160
"
"
"
"
ND
---
0.0801
"
"
"
"
Isopropylbenzene
ND
---
0.0801
"
"
"
"
n-Propylbenzene
ND
---
0.0400
"
"
"
"
ND
---
0.0801
"
"
"
"
ND
---
0.0801
"
"
"
"
ND
---
0.0400
"
"
"
"
ND
---
"
"
"
Recovery: 108 %
Limits: 70-130 %
"
"
103 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
100 %
Limits: 70-130 %
"
"
"
93 %
Limits: 70-130 %
"
"
"
3C (A6B0900-10)
0.0400
"
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0156
mg/kg dry
50
02/27/16 17:41
5035/8260B
Toluene
ND
---
0.0782
"
"
"
"
Ethylbenzene
ND
---
0.0391
"
"
"
"
Xylenes, total
ND
---
0.117
"
"
"
"
Naphthalene
ND
---
0.156
"
"
"
"
ND
---
0.0782
"
"
"
"
Isopropylbenzene
ND
---
0.0782
"
"
"
"
n-Propylbenzene
ND
---
0.0391
"
"
"
"
ND
---
0.0782
"
"
"
"
ND
---
0.0782
"
"
"
"
ND
---
0.0391
"
"
"
"
ND
---
0.0391
"
"
"
"
Recovery: 106 %
Limits: 70-130 %
"
"
103 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
101 %
Limits: 70-130 %
"
"
"
93 %
Limits: 70-130 %
"
"
"
3D (A6B0900-11)
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0199
mg/kg dry
50
02/27/16 18:10
5035/8260B
Toluene
ND
---
0.0994
"
"
"
"
Ethylbenzene
ND
---
0.0497
"
"
"
"
Xylenes, total
ND
---
0.149
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020833
Page 9 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
3D (A6B0900-11)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Naphthalene
ND
---
0.199
mg/kg dry
50
"
5035/8260B
ND
---
0.0994
"
"
"
"
Isopropylbenzene
ND
---
0.0994
"
"
"
"
n-Propylbenzene
ND
---
0.0497
"
"
"
"
ND
---
0.0994
"
"
"
"
ND
---
0.0994
"
"
"
"
ND
---
0.0497
"
"
"
"
ND
---
0.0497
"
"
"
"
Recovery: 104 %
Limits: 70-130 %
"
"
102 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
99 %
Limits: 70-130 %
"
"
"
95 %
Limits: 70-130 %
"
"
"
4A (A6B0900-12)
Matrix: Soil
Benzene
ND
---
Toluene
ND
Ethylbenzene
ND
Xylenes, total
Batch: 6020833
0.0205
mg/kg dry
50
02/27/16 18:38
5035/8260B
---
0.103
"
"
"
"
---
0.0513
"
"
"
"
ND
---
0.154
"
"
"
"
Naphthalene
ND
---
0.205
"
"
"
"
ND
---
0.103
"
"
"
"
Isopropylbenzene
ND
---
0.103
"
"
"
"
n-Propylbenzene
ND
---
0.0513
"
"
"
"
ND
---
0.103
"
"
"
"
ND
---
0.103
"
"
"
"
ND
---
0.0513
"
"
"
"
ND
---
0.0513
"
"
"
"
Recovery: 105 %
Limits: 70-130 %
"
"
102 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
101 %
Limits: 70-130 %
"
"
"
96 %
Limits: 70-130 %
"
"
"
4B (A6B0900-13)
Matrix: Soil
Batch: 6020833
Benzene
ND
---
0.0162
mg/kg dry
50
02/27/16 19:07
5035/8260B
Toluene
ND
---
0.0809
"
"
"
"
Ethylbenzene
ND
---
0.0404
"
"
"
"
Xylenes, total
ND
---
0.121
"
"
"
"
Naphthalene
ND
---
0.162
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020833
Page 10 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
4B (A6B0900-13)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
ND
---
0.0809
mg/kg dry
50
"
5035/8260B
Isopropylbenzene
ND
---
0.0809
"
"
"
"
n-Propylbenzene
ND
---
0.0404
"
"
"
"
ND
---
0.0809
"
"
"
"
ND
---
0.0809
"
"
"
"
ND
---
0.0404
"
"
"
"
ND
---
0.0404
"
"
"
"
Recovery: 107 %
Limits: 70-130 %
"
"
102 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
100 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
4C (A6B0900-14)
Matrix: Soil
Batch: 6020834
Benzene
ND
---
0.0140
mg/kg dry
50
02/27/16 14:15
5035/8260B
Toluene
ND
---
0.0702
"
"
"
"
Ethylbenzene
ND
---
0.0351
"
"
"
"
Xylenes, total
ND
---
0.105
"
"
"
"
Naphthalene
ND
---
0.140
"
"
"
"
ND
---
0.0702
"
"
"
"
Isopropylbenzene
ND
---
0.0702
"
"
"
"
n-Propylbenzene
ND
---
0.0351
"
"
"
"
ND
---
0.0702
"
"
"
"
ND
---
0.0702
"
"
"
"
ND
---
0.0351
"
"
"
"
ND
---
"
"
"
Recovery: 97 %
Limits: 70-130 %
"
"
93 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
97 %
Limits: 70-130 %
"
"
"
97 %
Limits: 70-130 %
"
"
"
4D (A6B0900-15)
0.0351
"
Matrix: Soil
Batch: 6020834
Benzene
ND
---
0.00983
mg/kg dry
50
02/27/16 14:41
5035/8260B
Toluene
ND
---
0.0491
"
"
"
"
Ethylbenzene
ND
---
0.0246
"
"
"
"
Xylenes, total
ND
---
0.0737
"
"
"
"
Naphthalene
ND
---
0.0983
"
"
"
"
ND
---
0.0491
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020833
Page 11 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
4D (A6B0900-15)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Isopropylbenzene
ND
---
0.0491
mg/kg dry
50
"
5035/8260B
n-Propylbenzene
ND
---
0.0246
"
"
"
"
ND
---
0.0491
"
"
"
"
ND
---
0.0491
"
"
"
"
ND
---
0.0246
"
"
"
"
ND
---
0.0246
"
"
"
"
Recovery: 96 %
Limits: 70-130 %
"
"
92 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
97 %
Limits: 70-130 %
"
"
"
97 %
Limits: 70-130 %
"
"
"
0A (A6B0900-16)
Matrix: Soil
Batch: 6020834
Benzene
ND
---
0.0324
mg/kg dry
50
02/27/16 15:08
5035/8260B
Toluene
ND
---
0.162
"
"
"
"
Ethylbenzene
ND
---
0.0810
"
"
"
"
Xylenes, total
ND
---
0.243
"
"
"
"
Naphthalene
ND
---
0.324
"
"
"
"
ND
---
0.162
"
"
"
"
Isopropylbenzene
ND
---
0.162
"
"
"
"
n-Propylbenzene
ND
---
0.0810
"
"
"
"
ND
---
0.162
"
"
"
"
ND
---
0.162
"
"
"
"
ND
---
0.0810
"
"
"
"
ND
---
0.0810
"
"
"
"
Recovery: 97 %
Limits: 70-130 %
"
"
92 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
96 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
02/27/16 15:35
5035/8260B
0B (A6B0900-17)
Benzene
Matrix: Soil
ND
---
0.0272
Batch: 6020834
mg/kg dry
50
Toluene
0.224
---
0.136
"
"
"
"
Ethylbenzene
0.200
---
0.0680
"
"
"
"
Xylenes, total
1.04
---
0.204
"
"
"
"
Naphthalene
ND
---
0.272
"
"
"
"
ND
---
0.136
"
"
"
"
Isopropylbenzene
ND
---
0.136
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020834
Page 12 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
0B (A6B0900-17)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
n-Propylbenzene
0.162
---
0.0680
mg/kg dry
50
"
0.755
---
0.136
"
"
"
"
0.264
---
0.136
"
"
"
"
ND
---
0.0680
"
"
"
"
ND
---
0.0680
"
"
"
"
5035/8260B
Recovery: 94 %
Limits: 70-130 %
"
"
91 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
96 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
5035/8260B
0C (A6B0900-18)
Matrix: Soil
Batch: 6020834
Benzene
0.161
---
0.0336
mg/kg dry
50
02/27/16 16:29
Toluene
2.93
---
0.168
"
"
"
"
Ethylbenzene
3.70
---
0.0840
"
"
"
"
Xylenes, total
20.6
---
0.252
"
"
"
"
Naphthalene
2.15
---
0.336
"
"
"
"
ND
---
0.168
"
"
"
"
Isopropylbenzene
1.03
---
0.168
"
"
"
"
n-Propylbenzene
3.82
---
0.0840
"
"
"
"
19.9
---
0.168
"
"
"
"
6.59
---
0.168
"
"
"
"
ND
---
0.0840
"
"
"
"
ND
---
0.0840
"
"
"
"

Toluene-d8 (Surr)
Recovery: 97 %
Limits: 70-130 %
"
"
93 %
Limits: 70-130 %
"
"
"
101 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
Matrix: Soil
ND
---
0.00773
mg/kg dry
50
02/27/16 16:56
5035/8260B
Toluene
ND
---
0.0386
"
"
"
"
Ethylbenzene
ND
---
0.0193
"
"
"
"
Xylenes, total
ND
---
0.0580
"
"
"
"
Naphthalene
ND
---
0.0773
"
"
"
"
ND
---
0.0386
"
"
"
"
Isopropylbenzene
ND
---
0.0386
"
"
"
"
n-Propylbenzene
ND
---
0.0193
"
"
"
"
M-04
Batch: 6020834
Benzene
DRAFT REPORT
Notes
Batch: 6020834
Page 13 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
ND
---
0.0386
mg/kg dry
50
"
5035/8260B
ND
---
0.0386
"
"
"
"
ND
---
0.0193
"
"
"
"
ND
---
0.0193
"
"
"
"
Recovery: 94 %
Limits: 70-130 %
"
"
91 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
96 %
Limits: 70-130 %
"
"
"
97 %
Limits: 70-130 %
"
"
"
Matrix: Soil
Batch: 6020834
Benzene
ND
---
0.0119
mg/kg dry
50
02/27/16 17:22
5035/8260B
Toluene
ND
---
0.0594
"
"
"
"
Ethylbenzene
ND
---
0.0297
"
"
"
"
Xylenes, total
ND
---
0.0890
"
"
"
"
Naphthalene
ND
---
0.119
"
"
"
"
ND
---
0.0594
"
"
"
"
Isopropylbenzene
ND
---
0.0594
"
"
"
"
n-Propylbenzene
ND
---
0.0297
"
"
"
"
ND
---
0.0594
"
"
"
"
ND
---
0.0594
"
"
"
"
ND
---
0.0297
"
"
"
"
ND
---
0.0297
"
"
"
"
Recovery: 94 %
Limits: 70-130 %
"
"
92 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
96 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
Matrix: Soil
Batch: 6020834
Benzene
ND
---
0.00717
mg/kg dry
50
02/27/16 17:49
5035/8260B
Toluene
ND
---
0.0358
"
"
"
"
Ethylbenzene
ND
---
0.0179
"
"
"
"
Xylenes, total
ND
---
0.0538
"
"
"
"
Naphthalene
ND
---
0.0717
"
"
"
"
ND
---
0.0358
"
"
"
"
Isopropylbenzene
ND
---
0.0358
"
"
"
"
n-Propylbenzene
ND
---
0.0179
"
"
"
"
ND
---
0.0358
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020834
Page 14 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
ND
---
0.0358
mg/kg dry
50
"
5035/8260B
ND
---
0.0179
"
"
"
"
ND
---
0.0179
"
"
"
"
Recovery: 93 %
Limits: 70-130 %
"
"
91 %
Limits: 70-130 %
"
"
"
Toluene-d8 (Surr)
97 %
Limits: 70-130 %
"
"
"
98 %
Limits: 70-130 %
"
"
"
DRAFT REPORT
Notes
Batch: 6020834
Page 15 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result
Analyte
MDL
1A (A6B0900-01)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0143
mg/kg dry
02/27/16 14:05
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0143
"
"
"
"
Anthracene
ND
---
0.0143
"
"
"
"
Benz(a)anthracene
ND
---
0.0143
"
"
"
"
Benzo(a)pyrene
ND
---
0.0143
"
"
"
"
ND
---
0.0143
"
"
"
"
ND
---
0.0143
"
"
"
"
ND
---
0.0143
"
"
"
"
Chrysene
ND
---
0.0143
"
"
"
"
ND
---
0.0143
"
"
"
"
Dibenzofuran
ND
---
0.0143
"
"
"
"
Fluoranthene
ND
---
0.0143
"
"
"
"
Fluorene
ND
---
0.0143
"
"
"
"
Indeno(1,2,3-cd)pyrene
ND
---
0.0143
"
"
"
"
1-Methylnaphthalene
ND
---
0.0143
"
"
"
"
2-Methylnaphthalene
ND
---
0.0143
"
"
"
"
Naphthalene
ND
---
0.0143
"
"
"
"
Phenanthrene
ND
---
0.0143
"
"
"
"
Pyrene
ND
---
0.0143
"
"
"
"
Surrogate: 2-Fluorobiphenyl (Surr)

p-Terphenyl-d14 (Surr)
DRAFT REPORT
Notes
Batch: 6020836
Recovery: 87 %
Limits: 44-115 %
"
"
"
105 %
Limits: 54-127 %
"
"
"
Page 16 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
1B (A6B0900-02)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0161
mg/kg dry
02/27/16 14:59
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0161
"
"
"
"
Anthracene
ND
---
0.0161
"
"
"
"
Benz(a)anthracene
ND
---
0.0161
"
"
"
"
Benzo(a)pyrene
ND
---
0.0161
"
"
"
"
ND
---
0.0161
"
"
"
"
ND
---
0.0161
"
"
"
"
ND
---
0.0161
"
"
"
"
Chrysene
ND
---
0.0161
"
"
"
"
ND
---
0.0161
"
"
"
"
Dibenzofuran
ND
---
0.0161
"
"
"
"
Fluoranthene
ND
---
0.0161
"
"
"
"
Fluorene
ND
---
0.0161
"
"
"
"
ND
---
0.0161
"
"
"
"
1-Methylnaphthalene
ND
---
0.0161
"
"
"
"
2-Methylnaphthalene
ND
---
0.0161
"
"
"
"
Naphthalene
ND
---
0.0161
"
"
"
"
Phenanthrene
ND
---
0.0161
"
"
"
"
Pyrene
ND
---
0.0161
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 89 %
Limits: 44-115 %
"
"
"
107 %
Limits: 54-127 %
"
"
"
Page 17 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
2A (A6B0900-04)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0130
mg/kg dry
02/27/16 15:27
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0130
"
"
"
"
Anthracene
ND
---
0.0130
"
"
"
"
Benz(a)anthracene
ND
---
0.0130
"
"
"
"
Benzo(a)pyrene
ND
---
0.0130
"
"
"
"
ND
---
0.0130
"
"
"
"
ND
---
0.0130
"
"
"
"
ND
---
0.0130
"
"
"
"
Chrysene
ND
---
0.0130
"
"
"
"
ND
---
0.0130
"
"
"
"
Dibenzofuran
ND
---
0.0130
"
"
"
"
Fluoranthene
ND
---
0.0130
"
"
"
"
Fluorene
ND
---
0.0130
"
"
"
"
ND
---
0.0130
"
"
"
"
1-Methylnaphthalene
ND
---
0.0130
"
"
"
"
2-Methylnaphthalene
ND
---
0.0130
"
"
"
"
Naphthalene
ND
---
0.0130
"
"
"
"
Phenanthrene
ND
---
0.0130
"
"
"
"
Pyrene
ND
---
0.0130
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 86 %
Limits: 44-115 %
"
"
"
102 %
Limits: 54-127 %
"
"
"
Page 18 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
2B (A6B0900-05)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0180
mg/kg dry
02/27/16 15:54
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0180
"
"
"
"
Anthracene
ND
---
0.0180
"
"
"
"
Benz(a)anthracene
ND
---
0.0180
"
"
"
"
Benzo(a)pyrene
ND
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
Chrysene
ND
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
Dibenzofuran
ND
---
0.0180
"
"
"
"
Fluoranthene
ND
---
0.0180
"
"
"
"
Fluorene
ND
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
1-Methylnaphthalene
ND
---
0.0180
"
"
"
"
2-Methylnaphthalene
ND
---
0.0180
"
"
"
"
Naphthalene
ND
---
0.0180
"
"
"
"
Phenanthrene
ND
---
0.0180
"
"
"
"
Pyrene
ND
---
0.0180
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 80 %
Limits: 44-115 %
"
"
"
98 %
Limits: 54-127 %
"
"
"
Page 19 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
2D (A6B0900-07)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0180
mg/kg dry
02/27/16 13:37
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0180
"
"
"
"
Anthracene
ND
---
0.0180
"
"
"
"
Benz(a)anthracene
ND
---
0.0198
"
"
"
"
Benzo(a)pyrene
ND
---
0.0180
"
"
"
"
0.0249
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
Chrysene
ND
---
0.0207
"
"
"
"
ND
---
0.0180
"
"
"
"
Dibenzofuran
ND
---
0.0180
"
"
"
"
Fluoranthene
ND
---
0.0180
"
"
"
"
0.0229
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
1-Methylnaphthalene
0.0284
---
0.0180
"
"
"
"
2-Methylnaphthalene
0.0433
---
0.0180
"
"
"
"
Naphthalene
0.0502
---
0.0180
"
"
"
"
Phenanthrene
0.0229
---
0.0180
"
"
"
"
ND
---
0.0180
"
"
"
"
Fluorene
Pyrene
DRAFT REPORT
Notes
Batch: 6020836
Recovery: 84 %
Limits: 44-115 %
"
"
"
102 %
Limits: 54-127 %
"
"
"
R-02
M-02
R-02
M-02
Page 20 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
3A (A6B0900-08)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0136
mg/kg dry
02/27/16 16:21
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0136
"
"
"
"
Anthracene
ND
---
0.0136
"
"
"
"
Benz(a)anthracene
ND
---
0.0136
"
"
"
"
Benzo(a)pyrene
ND
---
0.0136
"
"
"
"
ND
---
0.0136
"
"
"
"
ND
---
0.0136
"
"
"
"
ND
---
0.0136
"
"
"
"
Chrysene
ND
---
0.0136
"
"
"
"
ND
---
0.0136
"
"
"
"
Dibenzofuran
ND
---
0.0136
"
"
"
"
Fluoranthene
ND
---
0.0136
"
"
"
"
Fluorene
ND
---
0.0136
"
"
"
"
ND
---
0.0136
"
"
"
"
1-Methylnaphthalene
ND
---
0.0136
"
"
"
"
2-Methylnaphthalene
ND
---
0.0136
"
"
"
"
Naphthalene
ND
---
0.0136
"
"
"
"
Phenanthrene
ND
---
0.0136
"
"
"
"
Pyrene
ND
---
0.0136
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 87 %
Limits: 44-115 %
"
"
"
107 %
Limits: 54-127 %
"
"
"
Page 21 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
3B (A6B0900-09)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0129
mg/kg dry
02/27/16 16:48
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0129
"
"
"
"
Anthracene
ND
---
0.0129
"
"
"
"
Benz(a)anthracene
ND
---
0.0129
"
"
"
"
Benzo(a)pyrene
ND
---
0.0129
"
"
"
"
ND
---
0.0129
"
"
"
"
ND
---
0.0129
"
"
"
"
ND
---
0.0129
"
"
"
"
Chrysene
ND
---
0.0129
"
"
"
"
ND
---
0.0129
"
"
"
"
Dibenzofuran
ND
---
0.0129
"
"
"
"
Fluoranthene
ND
---
0.0129
"
"
"
"
Fluorene
ND
---
0.0129
"
"
"
"
ND
---
0.0129
"
"
"
"
1-Methylnaphthalene
ND
---
0.0129
"
"
"
"
2-Methylnaphthalene
ND
---
0.0129
"
"
"
"
Naphthalene
ND
---
0.0129
"
"
"
"
Phenanthrene
ND
---
0.0129
"
"
"
"
Pyrene
ND
---
0.0129
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 92 %
Limits: 44-115 %
"
"
"
109 %
Limits: 54-127 %
"
"
"
Page 22 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
3C (A6B0900-10)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0135
mg/kg dry
02/27/16 17:15
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0135
"
"
"
"
Anthracene
ND
---
0.0135
"
"
"
"
Benz(a)anthracene
ND
---
0.0135
"
"
"
"
Benzo(a)pyrene
ND
---
0.0135
"
"
"
"
ND
---
0.0135
"
"
"
"
ND
---
0.0135
"
"
"
"
ND
---
0.0135
"
"
"
"
Chrysene
ND
---
0.0135
"
"
"
"
ND
---
0.0135
"
"
"
"
Dibenzofuran
ND
---
0.0135
"
"
"
"
Fluoranthene
ND
---
0.0135
"
"
"
"
Fluorene
ND
---
0.0135
"
"
"
"
ND
---
0.0135
"
"
"
"
1-Methylnaphthalene
ND
---
0.0135
"
"
"
"
2-Methylnaphthalene
ND
---
0.0135
"
"
"
"
Naphthalene
ND
---
0.0135
"
"
"
"
Phenanthrene
ND
---
0.0135
"
"
"
"
Pyrene
ND
---
0.0135
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 89 %
Limits: 44-115 %
"
"
"
109 %
Limits: 54-127 %
"
"
"
Page 23 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
3D (A6B0900-11)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0138
mg/kg dry
02/27/16 18:09
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0138
"
"
"
"
Anthracene
ND
---
0.0138
"
"
"
"
Benz(a)anthracene
ND
---
0.0138
"
"
"
"
Benzo(a)pyrene
ND
---
0.0138
"
"
"
"
ND
---
0.0138
"
"
"
"
ND
---
0.0138
"
"
"
"
ND
---
0.0138
"
"
"
"
Chrysene
ND
---
0.0138
"
"
"
"
ND
---
0.0138
"
"
"
"
Dibenzofuran
ND
---
0.0138
"
"
"
"
Fluoranthene
ND
---
0.0138
"
"
"
"
Fluorene
ND
---
0.0138
"
"
"
"
ND
---
0.0138
"
"
"
"
1-Methylnaphthalene
ND
---
0.0138
"
"
"
"
2-Methylnaphthalene
ND
---
0.0138
"
"
"
"
Naphthalene
ND
---
0.0138
"
"
"
"
Phenanthrene
ND
---
0.0138
"
"
"
"
Pyrene
ND
---
0.0138
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 86 %
Limits: 44-115 %
"
"
"
100 %
Limits: 54-127 %
"
"
"
Page 24 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
4A (A6B0900-12)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0149
mg/kg dry
02/27/16 18:36
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0149
"
"
"
"
Anthracene
ND
---
0.0149
"
"
"
"
Benz(a)anthracene
ND
---
0.0149
"
"
"
"
Benzo(a)pyrene
ND
---
0.0149
"
"
"
"
ND
---
0.0149
"
"
"
"
ND
---
0.0149
"
"
"
"
ND
---
0.0149
"
"
"
"
Chrysene
ND
---
0.0149
"
"
"
"
ND
---
0.0149
"
"
"
"
Dibenzofuran
ND
---
0.0149
"
"
"
"
Fluoranthene
ND
---
0.0149
"
"
"
"
Fluorene
ND
---
0.0149
"
"
"
"
ND
---
0.0149
"
"
"
"
1-Methylnaphthalene
ND
---
0.0149
"
"
"
"
2-Methylnaphthalene
ND
---
0.0149
"
"
"
"
Naphthalene
ND
---
0.0149
"
"
"
"
Phenanthrene
ND
---
0.0149
"
"
"
"
Pyrene
ND
---
0.0149
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 86 %
Limits: 44-115 %
"
"
"
102 %
Limits: 54-127 %
"
"
"
Page 25 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
4B (A6B0900-13)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0123
mg/kg dry
02/27/16 19:02
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0123
"
"
"
"
Anthracene
ND
---
0.0123
"
"
"
"
Benz(a)anthracene
ND
---
0.0123
"
"
"
"
Benzo(a)pyrene
ND
---
0.0123
"
"
"
"
ND
---
0.0123
"
"
"
"
ND
---
0.0123
"
"
"
"
ND
---
0.0123
"
"
"
"
Chrysene
ND
---
0.0123
"
"
"
"
ND
---
0.0123
"
"
"
"
Dibenzofuran
ND
---
0.0123
"
"
"
"
Fluoranthene
ND
---
0.0123
"
"
"
"
Fluorene
ND
---
0.0123
"
"
"
"
ND
---
0.0123
"
"
"
"
1-Methylnaphthalene
ND
---
0.0123
"
"
"
"
2-Methylnaphthalene
ND
---
0.0123
"
"
"
"
Naphthalene
ND
---
0.0123
"
"
"
"
Phenanthrene
ND
---
0.0123
"
"
"
"
Pyrene
ND
---
0.0123
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 95 %
Limits: 44-115 %
"
"
"
119 %
Limits: 54-127 %
"
"
"
Page 26 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
4C (A6B0900-14)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0144
mg/kg dry
02/27/16 19:29
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0144
"
"
"
"
Anthracene
ND
---
0.0144
"
"
"
"
Benz(a)anthracene
ND
---
0.0144
"
"
"
"
Benzo(a)pyrene
ND
---
0.0144
"
"
"
"
ND
---
0.0144
"
"
"
"
ND
---
0.0144
"
"
"
"
ND
---
0.0144
"
"
"
"
Chrysene
ND
---
0.0144
"
"
"
"
ND
---
0.0144
"
"
"
"
Dibenzofuran
ND
---
0.0144
"
"
"
"
Fluoranthene
ND
---
0.0144
"
"
"
"
Fluorene
ND
---
0.0144
"
"
"
"
ND
---
0.0144
"
"
"
"
1-Methylnaphthalene
ND
---
0.0144
"
"
"
"
2-Methylnaphthalene
ND
---
0.0144
"
"
"
"
Naphthalene
ND
---
0.0144
"
"
"
"
Phenanthrene
ND
---
0.0144
"
"
"
"
Pyrene
ND
---
0.0144
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 91 %
Limits: 44-115 %
"
"
"
115 %
Limits: 54-127 %
"
"
"
Page 27 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
4D (A6B0900-15)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0120
mg/kg dry
02/27/16 19:56
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0120
"
"
"
"
Anthracene
ND
---
0.0120
"
"
"
"
Benz(a)anthracene
ND
---
0.0120
"
"
"
"
Benzo(a)pyrene
ND
---
0.0120
"
"
"
"
ND
---
0.0120
"
"
"
"
ND
---
0.0120
"
"
"
"
ND
---
0.0120
"
"
"
"
Chrysene
ND
---
0.0120
"
"
"
"
ND
---
0.0120
"
"
"
"
Dibenzofuran
ND
---
0.0120
"
"
"
"
Fluoranthene
ND
---
0.0120
"
"
"
"
Fluorene
ND
---
0.0120
"
"
"
"
ND
---
0.0120
"
"
"
"
1-Methylnaphthalene
ND
---
0.0120
"
"
"
"
2-Methylnaphthalene
ND
---
0.0120
"
"
"
"
Naphthalene
ND
---
0.0120
"
"
"
"
Phenanthrene
ND
---
0.0120
"
"
"
"
Pyrene
ND
---
0.0120
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 92 %
Limits: 44-115 %
"
"
"
115 %
Limits: 54-127 %
"
"
"
Page 28 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
0A (A6B0900-16)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0173
mg/kg dry
02/27/16 20:23
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0173
"
"
"
"
Anthracene
ND
---
0.0173
"
"
"
"
Benz(a)anthracene
ND
---
0.0173
"
"
"
"
Benzo(a)pyrene
ND
---
0.0173
"
"
"
"
ND
---
0.0173
"
"
"
"
ND
---
0.0173
"
"
"
"
ND
---
0.0173
"
"
"
"
Chrysene
ND
---
0.0173
"
"
"
"
ND
---
0.0173
"
"
"
"
Dibenzofuran
ND
---
0.0173
"
"
"
"
Fluoranthene
ND
---
0.0173
"
"
"
"
Fluorene
ND
---
0.0173
"
"
"
"
ND
---
0.0173
"
"
"
"
1-Methylnaphthalene
ND
---
0.0173
"
"
"
"
2-Methylnaphthalene
ND
---
0.0173
"
"
"
"
Naphthalene
ND
---
0.0173
"
"
"
"
Phenanthrene
ND
---
0.0173
"
"
"
"
Pyrene
ND
---
0.0173
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 91 %
Limits: 44-115 %
"
"
"
111 %
Limits: 54-127 %
"
"
"
Page 29 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
0B (A6B0900-17)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0167
mg/kg dry
02/27/16 20:49
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0167
"
"
"
"
Anthracene
ND
---
0.0167
"
"
"
"
Benz(a)anthracene
ND
---
0.0167
"
"
"
"
Benzo(a)pyrene
ND
---
0.0167
"
"
"
"
ND
---
0.0167
"
"
"
"
ND
---
0.0167
"
"
"
"
ND
---
0.0167
"
"
"
"
Chrysene
ND
---
0.0167
"
"
"
"
ND
---
0.0167
"
"
"
"
Dibenzofuran
0.0620
---
0.0167
"
"
"
"
Fluoranthene
ND
---
0.0167
"
"
"
"
Fluorene
ND
---
0.0401
"
"
"
"
ND
---
0.0167
"
"
"
"
1-Methylnaphthalene
0.114
---
0.0167
"
"
"
"
2-Methylnaphthalene
0.155
---
0.0167
"
"
"
"
ND
---
0.0301
"
"
"
"
Phenanthrene
0.0489
---
0.0167
"
"
"
"
Pyrene
0.0411
---
0.0167
"
"
"
"
Naphthalene

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 100 %
Limits: 44-115 %
"
"
"
118 %
Limits: 54-127 %
"
"
"
R-02
R-02
Page 30 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
0C (A6B0900-18)
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Notes
Batch: 6020836
Acenaphthene
ND
---
0.208
mg/kg dry
02/27/16 21:16
EPA 8270D (SIM)
R-02
Acenaphthylene
ND
---
0.0763
"
"
"
"
R-02
Anthracene
ND
---
0.104
"
"
"
"
R-02
Benz(a)anthracene
ND
---
0.0242
"
"
"
"
R-02
Benzo(a)pyrene
ND
---
0.0186
"
"
"
"
ND
---
0.0186
"
"
"
"
ND
---
0.0186
"
"
"
"
ND
---
0.0186
"
"
"
"
Chrysene
ND
---
0.0260
"
"
"
"
ND
---
0.0186
"
"
"
"
Dibenzofuran
0.376
---
0.0186
"
"
"
"
Fluoranthene
ND
---
0.0186
"
"
"
"
0.454
---
0.0186
"
"
"
"
ND
---
0.0186
"
"
"
"
Fluorene
1-Methylnaphthalene
3.29
---
0.0186
"
"
"
"
2-Methylnaphthalene
5.58
---
0.0186
"
"
"
"
Naphthalene
2.08
---
0.0186
"
"
"
"
Phenanthrene
0.740
---
0.0186
"
"
"
"
Pyrene
0.389
---
0.0186
"
"
"
"

DRAFT REPORT
Recovery: 78 %
Limits: 44-115 %
"
"
"
112 %
Limits: 54-127 %
"
"
"
R-02
M-04
M-02
Page 31 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0107
mg/kg dry
02/27/16 21:43
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0107
"
"
"
"
Anthracene
ND
---
0.0107
"
"
"
"
Benz(a)anthracene
ND
---
0.0107
"
"
"
"
Benzo(a)pyrene
ND
---
0.0107
"
"
"
"
ND
---
0.0107
"
"
"
"
ND
---
0.0107
"
"
"
"
ND
---
0.0107
"
"
"
"
Chrysene
ND
---
0.0107
"
"
"
"
ND
---
0.0107
"
"
"
"
Dibenzofuran
ND
---
0.0107
"
"
"
"
Fluoranthene
ND
---
0.0107
"
"
"
"
Fluorene
ND
---
0.0107
"
"
"
"
ND
---
0.0107
"
"
"
"
1-Methylnaphthalene
ND
---
0.0107
"
"
"
"
2-Methylnaphthalene
ND
---
0.0107
"
"
"
"
Naphthalene
ND
---
0.0107
"
"
"
"
Phenanthrene
ND
---
0.0107
"
"
"
"
Pyrene
ND
---
0.0107
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 97 %
Limits: 44-115 %
"
"
"
123 %
Limits: 54-127 %
"
"
"
Page 32 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Acenaphthene
ND
---
0.0134
mg/kg dry
02/27/16 22:10
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0134
"
"
"
"
Anthracene
ND
---
0.0134
"
"
"
"
Benz(a)anthracene
ND
---
0.0134
"
"
"
"
Benzo(a)pyrene
ND
---
0.0134
"
"
"
"
ND
---
0.0134
"
"
"
"
ND
---
0.0134
"
"
"
"
ND
---
0.0134
"
"
"
"
Chrysene
ND
---
0.0134
"
"
"
"
ND
---
0.0134
"
"
"
"
Dibenzofuran
ND
---
0.0134
"
"
"
"
Fluoranthene
ND
---
0.0134
"
"
"
"
Fluorene
ND
---
0.0134
"
"
"
"
ND
---
0.0134
"
"
"
"
1-Methylnaphthalene
ND
---
0.0134
"
"
"
"
2-Methylnaphthalene
ND
---
0.0134
"
"
"
"
Naphthalene
ND
---
0.0134
"
"
"
"
Phenanthrene
ND
---
0.0134
"
"
"
"
Pyrene
ND
---
0.0134
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020836
Recovery: 93 %
Limits: 44-115 %
"
"
"
114 %
Limits: 54-127 %
"
"
"
Page 33 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Result
Analyte
MDL
Acenaphthene
Reporting
Limit
Dilution
Units
Matrix: Soil
Date Analyzed
Method
Notes
Batch: 6020836
ND
---
0.0105
mg/kg dry
02/27/16 22:36
EPA 8270D (SIM)
Acenaphthylene
0.0181
---
0.0105
"
"
"
"
Anthracene
0.0526
---
0.0105
"
"
"
"
Benz(a)anthracene
0.635
---
0.0105
"
"
"
"
Benzo(a)pyrene
0.219
---
0.0105
"
"
"
"
0.603
---
0.0105
"
"
"
"
M-02, Q-42
0.206
---
0.0105
"
"
"
"
M-02
0.0799
---
0.0105
"
"
"
"
Chrysene
0.947
---
0.0105
"
"
"
"
0.0306
---
0.0105
"
"
"
"
Dibenzofuran
ND
---
0.0105
"
"
"
"
Fluoranthene
1.86
---
0.0105
"
"
"
"
Fluorene
ND
---
0.0105
"
"
"
"
0.116
---
0.0105
"
"
"
"
1-Methylnaphthalene
ND
---
0.0105
"
"
"
"
2-Methylnaphthalene
0.0135
---
0.0105
"
"
"
"
ND
---
0.0105
"
"
"
"
0.0119
---
0.0105
"
"
"
"
1.60
---
0.0105
"
"
"
"
Naphthalene
Phenanthrene
Pyrene
DRAFT REPORT
Recovery: 95 %
Limits: 44-115 %
"
"
"
121 %
Limits: 54-127 %
"
"
"
Q-42
Q-42
Q-42
Q-42
Page 34 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Percent Dry Weight
Analyte
Result
MDL
1A (A6B0900-01)
% Solids
Matrix: Soil
65.4
---
57.4
---
44.8
---
72.9
---
1B (A6B0900-02)
% Solids
49.6
---
36.0
---
53.9
---
68.4
---
75.0
---
67.6
---
63.3
---
64.6
---
74.8
---
67.9
---
76.7
---
49.2
---
1.00
Matrix: Soil
0A (A6B0900-16)
% Solids
1.00
Matrix: Soil
4D (A6B0900-15)
% Solids
1.00
Matrix: Soil
4C (A6B0900-14)
% Solids
1.00
Matrix: Soil
4B (A6B0900-13)
% Solids
1.00
Matrix: Soil
4A (A6B0900-12)
% Solids
1.00
Matrix: Soil
3D (A6B0900-11)
% Solids
1.00
Matrix: Soil
3C (A6B0900-10)
% Solids
1.00
Matrix: Soil
3B (A6B0900-09)
% Solids
1.00
Matrix: Soil
3A (A6B0900-08)
% Solids
1.00
Matrix: Soil
2D (A6B0900-07)
% Solids
1.00
Matrix: Soil
2C (A6B0900-06)
% Solids
1.00
Matrix: Soil
2B (A6B0900-05)
% Solids
1.00
Matrix: Soil
2A (A6B0900-04)
% Solids
1.00
Matrix: Soil
1C (A6B0900-03)
% Solids
Reporting
Limit
1.00
Matrix: Soil
DRAFT REPORT
1.00
Dilution
Units
Date Analyzed
Method
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
Notes
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Page 35 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Percent Dry Weight
Analyte
Result
MDL
55.4
---
0B (A6B0900-17)
% Solids
Matrix: Soil
0C (A6B0900-18)
% Solids
51.2
---
91.7
---
71.1
---
82.9
---
1.00
Matrix: Soil
% Solids
1.00
Matrix: Soil
% Solids
1.00
Matrix: Soil
% Solids
Reporting
Limit
1.00
Matrix: Soil
DRAFT REPORT
1.00
Dilution
Units
Date Analyzed
Method
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
02/27/16 13:34
EPA 8000C
Notes
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Batch: 6020837
% by Weight
Page 36 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19
QUALITY CONTROL (QC) SAMPLE RESULTS

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020835 - EPA 3546 (Fuels)
Prepared: 02/27/16 10:01 Analyzed: 02/27/16 13:13
Blank (6020835-BLK1)
NWTPH-Dx
Diesel
ND
---
25.0
mg/kg wet
---
---
---
---
---
---
Oil
ND
---
50.0
"
"
---
---
---
---
---
---
---
---
Surr: o-Terphenyl (Surr)
Recovery: 97 %
Limits: 50-150 %
Dilution: 1x
LCS (6020835-BS1)
NWTPH-Dx
Diesel
119
---
25.0
Recovery: 98 %
mg/kg wet
125
Limits: 50-150 %
---
95
76-115%
Dilution: 1x
Duplicate (6020835-DUP1)
QC Source Sample: 1C (A6B0900-03)
NWTPH-Dx
Diesel
Oil
54200
---
2010
mg/kg dry
50
---
66400
---
---
20
30%
ND
---
4030
"
"
---
ND
---
---
---
30%
Recovery: %
Limits: 50-150 %
Dilution: 50x
S-01
Soil
NWTPH-Dx
Diesel
ND
---
25.0
mg/kg wet
---
---
---
---
---
---
Oil
ND
---
50.0
"
"
---
---
---
---
---
---
---
---
34
30%
Recovery: 92 %
Limits: 50-150 %
Dilution: 1x
LCS (6020836-BS1)
NWTPH-Dx
Diesel
120
---
25.0
Recovery: 88 %
mg/kg wet
125
Limits: 50-150 %
---
96
76-115%
Dilution: 1x
QC Source Sample: 1A (A6B0900-01)
NWTPH-Dx
Diesel
33.9
---
DRAFT REPORT
26.9
mg/kg dry
---
24.2
---
---
F-17, Q-05
Page 37 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
42
30%
F-17, Q-05
Soil
Oil
188
---
53.7
Recovery: 89 %
mg/kg dry
"
---
Limits: 50-150 %
123
---
---
Dilution: 1x
NWTPH-Dx
Diesel
34.3
---
27.3
mg/kg dry
---
23.7
---
---
36
30%
F-17, Q-05
Oil
122
---
54.6
"
"
---
98.7
---
---
21
30%
F-17
Recovery: 88 %
DRAFT REPORT
Limits: 50-150 %
Dilution: 1x
Page 38 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
MDL
Reporting
Limit
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020833 - EPA 5035A
5035/8260B
Benzene
ND
---
0.00667
mg/kg wet
50
---
---
---
---
---
---
Toluene
ND
---
0.0333
"
"
---
---
---
---
---
---
Ethylbenzene
ND
---
0.0167
"
"
---
---
---
---
---
---
Xylenes, total
ND
---
0.0500
"
"
---
---
---
---
---
---
Naphthalene
ND
---
0.0667
"
"
---
---
---
---
---
---
Methyl tert-butyl ether

(MTBE)
Isopropylbenzene
ND
---
0.0333
"
"
---
---
---
---
---
---
ND
---
0.0333
"
"
---
---
---
---
---
---
n-Propylbenzene
ND
---
0.0167
"
"
---
---
---
---
---
---
ND
---
0.0333
"
"
---
---
---
---
---
---
ND
---
0.0333
"
"
---
---
---
---
---
---
ND
---
0.0167
"
"
---
---
---
---
---
---
ND
---
0.0167
"
"
---
---
---
---
---
---
---
---
Surr: Dibromofluoromethane (Surr)
Recovery: 107 %
Limits: 70-130 %
Dilution: 1x
103 %
70-130 %
"
Toluene-d8 (Surr)
98 %
70-130 %
"
97 %
70-130 %
"
LCS (6020833-BS1)
5035/8260B
Benzene
1.08
---
0.0100
mg/kg wet
50
1.00
---
108
65-135%
Toluene
1.02
---
0.0500
"
"
"
---
102
"
---
---
Ethylbenzene
0.979
---
0.0250
"
"
"
---
98
"
---
---
Xylenes, total
2.85
---
0.0750
"
"
3.00
---
95
"
---
---
Naphthalene
0.948
---
0.100
"
"
1.00
---
95
"
---
---

(MTBE)
Isopropylbenzene
1.01
---
0.0500
"
"
"
---
101
"
---
---
0.982
---
0.0500
"
"
"
---
98
"
---
---
n-Propylbenzene
0.991
---
0.0250
"
"
"
---
99
"
---
---
0.983
---
0.0500
"
"
"
---
98
"
---
---
0.996
---
0.0500
"
"
"
---
100
"
---
---
1.08
---
0.0250
"
"
"
---
108
"
---
---
DRAFT REPORT
Page 39 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
MDL
Reporting
Limit
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020833 - EPA 5035A
LCS (6020833-BS1)
Source
Result
0.986
---
0.0250
mg/kg wet
"
"
---
Recovery: 102 %
Limits: 70-130 %
Dilution: 1x
102 %
70-130 %
"
Toluene-d8 (Surr)
97 %
70-130 %
"
97 %
70-130 %
"
99
"
---
---
5035/8260B
Benzene
ND
---
0.0198
mg/kg dry
50
---
ND
---
---
---
30%
Toluene
ND
---
0.0988
"
"
---
ND
---
---
---
30%
Ethylbenzene
ND
---
0.0494
"
"
---
ND
---
---
---
30%
Xylenes, total
ND
---
0.148
"
"
---
ND
---
---
---
30%
Naphthalene
ND
---
0.198
"
"
---
ND
---
---
---
30%

(MTBE)
Isopropylbenzene
ND
---
0.0988
"
"
---
ND
---
---
---
30%
ND
---
0.0988
"
"
---
ND
---
---
---
30%
n-Propylbenzene
ND
---
0.0494
"
"
---
ND
---
---
---
30%
ND
---
0.0988
"
"
---
ND
---
---
---
30%
ND
---
0.0988
"
"
---
ND
---
---
---
30%
ND
---
0.0494
"
"
---
ND
---
---
---
30%
ND
---
0.0494
"
"
---
ND
---
---
---
30%
Recovery: 104 %
Limits: 70-130 %
Dilution: 1x
101 %
70-130 %
"
Toluene-d8 (Surr)
99 %
70-130 %
"
93 %
70-130 %
"
Matrix Spike (6020833-MS1)

QC Source Sample: 4B (A6B0900-13)
5035/8260B
Benzene
1.75
---
0.0162
mg/kg dry
50
1.62
ND
108
65-135%
---
---
Toluene
1.64
---
0.0809
"
"
"
ND
101
"
---
---
Ethylbenzene
1.59
---
0.0404
"
"
"
ND
98
"
---
---
DRAFT REPORT
Page 40 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
MDL
Reporting
Limit
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020833 - EPA 5035A

Xylenes, total
4.58
---
0.121
mg/kg dry
"
4.86
ND
94
"
---
---
Naphthalene
1.39
---
0.162
"
"
1.62
ND
86
"
---
---

(MTBE)
Isopropylbenzene
1.63
---
0.0809
"
"
"
ND
101
"
---
---
1.57
---
0.0809
"
"
"
ND
97
"
---
---
n-Propylbenzene
1.55
---
0.0404
"
"
"
ND
96
"
---
---
1.51
---
0.0809
"
"
"
ND
93
"
---
---
1.55
---
0.0809
"
"
"
ND
96
"
---
---
1.67
---
0.0404
"
"
"
ND
103
"
---
---
1.67
---
0.0404
"
"
"
ND
103
"
---
---
Recovery: 103 %
Limits: 70-130 %
Dilution: 1x
99 %
70-130 %
"
Toluene-d8 (Surr)
98 %
70-130 %
"
93 %
70-130 %
"
DRAFT REPORT
Page 41 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020834 - EPA 5035A
5035/8260B
Benzene
ND
---
0.00667
mg/kg wet
50
---
---
---
---
---
---
Toluene
ND
---
0.0333
"
"
---
---
---
---
---
---
Ethylbenzene
ND
---
0.0167
"
"
---
---
---
---
---
---
Xylenes, total
ND
---
0.0500
"
"
---
---
---
---
---
---
Naphthalene
ND
---
0.0667
"
"
---
---
---
---
---
---

(MTBE)
Isopropylbenzene
ND
---
0.0333
"
"
---
---
---
---
---
---
ND
---
0.0333
"
"
---
---
---
---
---
---
n-Propylbenzene
ND
---
0.0167
"
"
---
---
---
---
---
---
ND
---
0.0333
"
"
---
---
---
---
---
---
ND
---
0.0333
"
"
---
---
---
---
---
---
ND
---
0.0167
"
"
---
---
---
---
---
---
ND
---
0.0167
"
"
---
---
---
---
---
---
---
---
Recovery: 96 %
Limits: 70-130 %
Dilution: 1x
92 %
70-130 %
"
Toluene-d8 (Surr)
97 %
70-130 %
"
98 %
70-130 %
"
LCS (6020834-BS1)
5035/8260B
Benzene
0.878
---
0.0100
mg/kg wet
50
1.00
---
88
65-135%
Toluene
0.924
---
0.0500
"
"
"
---
92
"
---
---
Ethylbenzene
0.981
---
0.0250
"
"
"
---
98
"
---
---
Xylenes, total
2.96
---
0.0750
"
"
3.00
---
99
"
---
---
Naphthalene
0.940
---
0.100
"
"
1.00
---
94
"
---
---

(MTBE)
Isopropylbenzene
0.876
---
0.0500
"
"
"
---
88
"
---
---
1.05
---
0.0500
"
"
"
---
105
"
---
---
n-Propylbenzene
0.898
---
0.0250
"
"
"
---
90
"
---
---
0.988
---
0.0500
"
"
"
---
99
"
---
---
0.998
---
0.0500
"
"
"
---
100
"
---
---
1.00
---
0.0250
"
"
"
---
100
"
---
---
DRAFT REPORT
Page 42 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020834 - EPA 5035A
LCS (6020834-BS1)
Source
Result
0.848
---
0.0250
mg/kg wet
"
"
---
Recovery: 97 %
Limits: 70-130 %
Dilution: 1x
92 %
70-130 %
"
Toluene-d8 (Surr)
95 %
70-130 %
"
99 %
70-130 %
"
85
"
---
---
5035/8260B
Benzene
ND
---
0.0288
mg/kg dry
50
---
0.0177
---
---
***
30%
Toluene
0.247
Ethylbenzene
0.220
---
0.144
"
"
---
0.224
---
---
10
30%
---
0.0719
"
"
---
0.200
---
---
10
30%
Xylenes, total
Naphthalene
1.16
---
0.216
"
"
---
1.04
---
---
11
30%
ND
---
0.288
"
"
---
ND
---
---
---
30%

(MTBE)
Isopropylbenzene
ND
---
0.144
"
"
---
ND
---
---
---
30%
ND
---
0.144
"
"
---
ND
---
---
---
30%
n-Propylbenzene
0.167
---
0.0719
"
"
---
0.162
---
---
30%
0.698
---
0.144
"
"
---
0.755
---
---
30%
0.262
---
0.144
"
"
---
0.264
---
---
0.7
30%
ND
---
0.0719
"
"
---
ND
---
---
---
30%
ND
---
0.0719
"
"
---
ND
---
---
---
30%
Recovery: 93 %
Limits: 70-130 %
Dilution: 1x
91 %
70-130 %
"
Toluene-d8 (Surr)
95 %
70-130 %
"
100 %
70-130 %
"

QC Source Sample: Ex Sidewall E (A6B0900-21)
5035/8260B
Benzene
0.642
---
0.00717
mg/kg dry
50
0.710
ND
90
65-135%
---
---
Toluene
0.680
---
0.0358
"
"
"
ND
96
"
---
---
Ethylbenzene
0.718
---
0.0179
"
"
"
ND
101
"
---
---
DRAFT REPORT
Page 43 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020834 - EPA 5035A

Xylenes, total
2.16
---
0.0538
mg/kg dry
"
2.13
ND
102
"
---
---
Naphthalene
0.697
---
0.0717
"
"
0.710
ND
98
"
---
---

(MTBE)
Isopropylbenzene
0.644
---
0.0358
"
"
"
ND
91
"
---
---
0.775
---
0.0358
"
"
"
ND
109
"
---
---
n-Propylbenzene
0.652
---
0.0179
"
"
"
ND
92
"
---
---
0.721
---
0.0358
"
"
"
ND
102
"
---
---
0.738
---
0.0358
"
"
"
ND
104
"
---
---
0.746
---
0.0179
"
"
"
ND
105
"
---
---
0.616
---
0.0179
"
"
"
ND
87
"
---
---
Recovery: 96 %
Limits: 70-130 %
Dilution: 1x
91 %
70-130 %
"
Toluene-d8 (Surr)
96 %
70-130 %
"
99 %
70-130 %
"
DRAFT REPORT
Page 44 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
EPA 8270D (SIM)
Acenaphthene
ND
---
0.00833
mg/kg wet
---
---
---
---
---
---
Acenaphthylene
ND
---
0.00833
"
"
---
---
---
---
---
---
Anthracene
ND
---
0.00833
"
"
---
---
---
---
---
---
Benz(a)anthracene
ND
---
0.00833
"
"
---
---
---
---
---
---
Benzo(a)pyrene
ND
---
0.00833
"
"
---
---
---
---
---
---
ND
---
0.00833
"
"
---
---
---
---
---
---
ND
---
0.00833
"
"
---
---
---
---
---
---
ND
---
0.00833
"
"
---
---
---
---
---
---
Chrysene
ND
---
0.00833
"
"
---
---
---
---
---
---
ND
---
0.00833
"
"
---
---
---
---
---
---
Dibenzofuran
ND
---
0.00833
"
"
---
---
---
---
---
---
Fluoranthene
ND
---
0.00833
"
"
---
---
---
---
---
---
Fluorene
ND
---
0.00833
"
"
---
---
---
---
---
---
ND
---
0.00833
"
"
---
---
---
---
---
---
1-Methylnaphthalene
ND
---
0.00833
"
"
---
---
---
---
---
---
2-Methylnaphthalene
ND
---
0.00833
"
"
---
---
---
---
---
---
Naphthalene
ND
---
0.00833
"
"
---
---
---
---
---
---
Phenanthrene
ND
---
0.00833
"
"
---
---
---
---
---
---
Pyrene
ND
---
0.00833
"
"
---
---
---
---
---
---
Surr: 2-Fluorobiphenyl (Surr)
Recovery: 91 %
Limits: 44-115 %
Dilution: 1x
104 %
54-127 %
"
LCS (6020836-BS2)
EPA 8270D (SIM)
Acenaphthene
0.718
---
0.0100
mg/kg wet
0.800
---
90
40-122%
---
---
Acenaphthylene
0.709
---
0.0100
"
"
"
---
89
32-132%
---
---
Anthracene
0.771
---
0.0100
"
"
"
---
96
47-123%
---
---
Benz(a)anthracene
0.701
---
0.0100
"
"
"
---
88
49-126%
---
---
Benzo(a)pyrene
0.727
---
0.0100
"
"
"
---
91
45-129%
---
---
0.729
---
0.0100
"
"
"
---
91
45-132%
---
---
0.731
---
0.0100
"
"
"
---
91
47-132%
---
---
DRAFT REPORT
Page 45 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
LCS (6020836-BS2)
Source
Result
0.657
---
0.0100
"
"
"
---
82
43-134%
---
---
Chrysene
0.698
---
0.0100
"
"
"
---
87
50-124%
---
---
0.691
---
0.0100
"
"
"
---
86
45-134%
---
---
Dibenzofuran
0.721
---
0.0100
"
"
"
---
90
44-120%
---
---
Fluoranthene
0.708
---
0.0100
"
"
"
---
89
50-127%
---
---
Fluorene
0.719
---
0.0100
"
"
"
---
90
43-125%
---
---
0.653
---
0.0100
"
"
"
---
82
45-133%
---
---
1-Methylnaphthalene
0.677
---
0.0100
"
"
"
---
85
40-120%
---
---
2-Methylnaphthalene
0.715
---
0.0100
"
"
"
---
89
38-122%
---
---
Naphthalene
0.697
---
0.0100
"
"
"
---
87
35-123%
---
---
Phenanthrene
0.722
---
0.0100
"
"
"
---
90
50-121%
---
---
Pyrene
0.719
---
0.0100
"
"
"
---
90
47-127%
---
---
Recovery: 92 %
Limits: 44-115 %
Dilution: 1x
101 %
54-127 %
"
EPA 8270D (SIM)
Acenaphthene
ND
---
0.0134
mg/kg dry
---
ND
---
---
---
30%
Acenaphthylene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Anthracene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Benz(a)anthracene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Benzo(a)pyrene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
ND
---
0.0134
"
"
---
ND
---
---
---
30%
ND
---
0.0134
"
"
---
ND
---
---
---
30%
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Chrysene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Dibenzofuran
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Fluoranthene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Fluorene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
ND
---
0.0134
"
"
---
ND
---
---
---
30%
DRAFT REPORT
Page 46 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
1-Methylnaphthalene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
2-Methylnaphthalene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Naphthalene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Phenanthrene
ND
---
0.0134
"
"
---
ND
---
---
---
30%
Pyrene
ND
---
"
"
---
ND
---
---
---
30%
0.0134
Recovery: 88 %
Limits: 44-115 %
Dilution: 1x
106 %
54-127 %
"
EPA 8270D (SIM)
Acenaphthene
ND
---
0.0137
mg/kg dry
---
ND
---
---
---
30%
Acenaphthylene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Anthracene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Benz(a)anthracene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Benzo(a)pyrene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
ND
---
0.0137
"
"
---
ND
---
---
---
30%
ND
---
0.0137
"
"
---
ND
---
---
---
30%
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Chrysene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Dibenzofuran
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Fluoranthene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Fluorene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
ND
---
0.0137
"
"
---
ND
---
---
---
30%
1-Methylnaphthalene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
2-Methylnaphthalene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Naphthalene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Phenanthrene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
Pyrene
ND
---
0.0137
"
"
---
ND
---
---
---
30%
DRAFT REPORT
Page 47 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Recovery: 88 %
Limits: 44-115 %
Dilution: 1x
108 %
54-127 %
"

EPA 8270D (SIM)
Acenaphthene
0.751
---
0.0107
mg/kg dry
0.852
ND
88
40-122%
---
---
Acenaphthylene
0.758
---
0.0107
"
"
"
0.0181
87
32-132%
---
---
Anthracene
0.774
---
0.0107
"
"
"
0.0526
85
47-123%
---
---
Benz(a)anthracene
0.752
---
0.0107
"
"
"
0.635
14
49-126%
---
---
Benzo(a)pyrene
0.779
---
0.0107
"
"
"
0.219
66
45-129%
---
---
0.795
---
0.0107
"
"
"
0.603
22
45-132%
---
---
0.782
---
0.0107
"
"
"
0.206
68
47-132%
---
---
0.580
---
0.0107
"
"
"
0.0799
59
43-134%
---
---
Chrysene
0.753
---
0.0107
"
"
"
0.947
-23
50-124%
---
---
0.665
---
0.0107
"
"
"
0.0306
74
45-134%
---
---
Dibenzofuran
0.777
---
0.0107
"
"
"
0.00750
90
44-120%
---
---
Fluoranthene
0.792
---
0.0107
"
"
"
1.86
-125
50-127%
---
---
Fluorene
0.768
---
0.0107
"
"
"
ND
90
43-125%
---
---
0.625
---
0.0107
"
"
"
0.116
60
45-133%
---
---
1-Methylnaphthalene
0.727
---
0.0107
"
"
"
0.00568
85
40-120%
---
---
2-Methylnaphthalene
0.765
---
0.0107
"
"
"
0.0135
88
38-122%
---
---
Naphthalene
0.724
---
0.0107
"
"
"
ND
85
35-123%
---
---
Phenanthrene
0.775
---
0.0107
"
"
"
0.0119
90
50-121%
---
---
Pyrene
0.784
---
0.0107
"
"
"
1.60
-96
47-127%
---
---
Recovery: 92 %
Limits: 44-115 %
Dilution: 1x
112 %
54-127 %
"
DRAFT REPORT
Q-04
Q-04
Q-04
Q-04
Q-04
Page 48 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Percent Dry Weight
Analyte
Result
MDL
Reporting
Limit
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Soil
Batch 6020837 - Total Solids (Dry Weight)
EPA 8000C
% Solids
52.0
---
1.00
% by
Weight
---
65.4
---
---
23
10%
10%
0.7
10%
10%
Q-04
EPA 8000C
% Solids
64.6
---
1.00
% by
Weight
---
67.6
---
---
EPA 8000C
% Solids
83.4
---
1.00
% by
Weight
---
82.9
---
---
EPA 8000C
% Solids
57.3
---
1.00
% by
Weight
---
55.4
---
---
No Client related Batch QC samples analyzed for this batch. See notes page for more information.
DRAFT REPORT
Page 49 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19
SAMPLE PREPARATION INFORMATION

Prep: EPA 3546 (Fuels)
Lab Number
Matrix
Method
Sampled
Prepared
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Batch: 6020835
A6B0900-03
A6B0900-06
Soil
Soil
NWTPH-Dx
NWTPH-Dx
02/26/16 10:00
02/26/16 10:10
02/27/16 10:01
02/27/16 10:01
10.94g/5mL
11.18g/5mL
10g/5mL
10g/5mL
0.91
0.89
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
10.7g/5mL
10.83g/5mL
10.51g/5mL
11.24g/5mL
10.31g/5mL
10.74g/5mL
10.36g/5mL
10.97g/5mL
11.43g/5mL
10.38g/5mL
10.86g/5mL
10.21g/5mL
10.87g/5mL
11.77g/5mL
10.8g/5mL
10.49g/5mL
10.19g/5mL
10.53g/5mL
11.5g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
0.94
0.92
0.95
0.89
0.97
0.93
0.97
0.91
0.88
0.96
0.92
0.98
0.92
0.85
0.93
0.95
0.98
0.95
0.87
Batch: 6020836
A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14RE1
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Prep: EPA 5035A
Lab Number
Matrix
Method
Sampled
Prepared
02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Batch: 6020833
A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
Soil
Soil
Soil
Soil
Soil
Soil
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
DRAFT REPORT
4.67g/5mL
4.4g/5mL
5.47g/5mL
4.01g/5mL
3.04g/5mL
4.31g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
1.07
1.14
0.91
1.25
1.64
1.16
Page 50 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Prep: EPA 5035A

Lab Number
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
Matrix
Method
Sampled
Prepared
Soil
Soil
Soil
Soil
Soil
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
5.25g/5mL
6.83g/5mL
5.61g/5mL
5.14g/5mL
5.22g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
0.95
0.73
0.89
0.97
0.96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40
7.9g/5mL
9.59g/5mL
4.61g/5mL
4.71g/5mL
4.05g/5mL
7.98g/5mL
9.02g/5mL
11.83g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
0.63
0.52
1.08
1.06
1.23
0.63
0.55
0.42
Batch: 6020834
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Lab Number
Matrix
Method
Sampled
Prepared
02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Batch: 6020836
A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
EPA 8270D (SIM)

EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
DRAFT REPORT
10.7g/5mL
10.83g/5mL
10.51g/5mL
11.24g/5mL
10.31g/5mL
10.74g/5mL
10.36g/5mL
10.97g/5mL
11.43g/5mL
10.38g/5mL
10.86g/5mL
10.21g/5mL
10.87g/5mL
11.77g/5mL
10.8g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
0.94
0.92
0.95
0.89
0.97
0.93
0.97
0.91
0.88
0.96
0.92
0.98
0.92
0.85
0.93
Page 51 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19

Lab Number
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21
Matrix
Soil
Soil
Soil
Soil
Method
EPA 8270D (SIM)

EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
Sampled
Prepared
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
10.49g/5mL
10.19g/5mL
10.53g/5mL
11.5g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
0.95
0.98
0.95
0.87
Percent Dry Weight

Prep: Total Solids (Dry Weight)
Lab Number
Matrix
Method
Sampled
Prepared
02/26/16 09:40
02/26/16 09:50
02/26/16 10:00
02/26/16 10:55
02/26/16 11:00
02/26/16 10:10
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Batch: 6020837
A6B0900-01
A6B0900-02
A6B0900-03
A6B0900-04
A6B0900-05
A6B0900-06
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
DRAFT REPORT
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Page 52 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/28/16 12:19
Notes and Definitions

Qualifiers:
F-17
No fuel pattern detected. The Diesel result represents carbon range C12 to C24, and the Oil result represents >C24 to C40.
M-02
Due to matrix interference, this analyte cannot be accurately quantified. The reported result is estimated.
M-04
Due to matrix interference, this analyte cannot be accurately quantified. The reported result may contain a high bias.
Q-04
Spike recovery and/or RPD is outside control limits due to a non-homogeneous sample matrix.
Q-05
Analyses are not controlled on RPD values from sample and duplicate concentrations are below 5 times the reporting level.
Q-42
Matrix Spike and/or Duplicate analysis was performed on this sample. % Recovery or RPD for this analyte is outside laboratory control
limits. (Refer to the QC Section of Analytical Report.)
R-02
The Reporting Limit for this analyte has been raised to account for interference from coeluting organic compounds present in the sample.
S-01
Surrogate recovery for this sample is not available due to sample dilution required from high analyte concentration and/or matrix
interference.
S-05
Surrogate recovery is estimated due to sample dilution required for high analyte concentration and/or matrix interference.
Notes and Conventions:

DET
Analyte DETECTED
ND
Analyte NOT DETECTED at or above the reporting limit
NR
Not Reported
dry
Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.
RPD
Relative Percent Difference
MDL
If MDL is not listed, data has been evaluated to the Method Reporting Limit only.
WMSC
Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.
Batch
QC
Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.
Blank
Policy
Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.
---
QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.
DRAFT REPORT
Page 53 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
***
Reported:
02/28/16 12:19
Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).
DRAFT REPORT
Page 54 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/28/16 12:19
Page 55 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/28/16 12:19
Page 56 of 57

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/28/16 12:19
Page 57 of 57
Apex Labs

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Sunday, February 21, 2016

Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
RE: AT&T Hall Ridge / [none]

2/19/2016 at 9:30:00AM.
DRAFT REPORT
Page 1 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Project Number: [none]
Portland, OR 97217
Reported:
02/21/16 15:02

SAMPLE INFORMATION
Sample ID
Laboratory ID
Matrix
Date Sampled
Date Received
SW-01
A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04
Water
Water
Water
Water
02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30
02/19/16 09:30
02/19/16 09:30
02/19/16 09:30
02/19/16 09:30
SW-02
SW-03
SW-04
DRAFT REPORT
Page 2 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
MDL
SW-01 (A6B0661-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Diesel
ND
104
208
ug/L
2.5
02/19/16 23:07
NWTPH-Dx
Oil
ND
208
417
"
"
"
"
"
"
"
Recovery: 84 %
SW-02 (A6B0661-02)
Limits: 50-150 %
Matrix: Water
Batch: 6020602
Diesel
ND
104
208
ug/L
2.5
02/19/16 23:29
NWTPH-Dx
Oil
ND
208
417
"
"
"
"
"
"
"
Recovery: 85 %
SW-03 (A6B0661-03)
Limits: 50-150 %
Matrix: Water
Diesel
ND
100
Oil
ND
200
200
400
Recovery: 83 %
SW-04 (A6B0661-04)
Batch: 6020602
ug/L
2.5
02/19/16 23:51
NWTPH-Dx
"
"
"
"
"
"
"
Limits: 50-150 %
Matrix: Water
Batch: 6020602
Diesel
ND
97.1
194
ug/L
2.5
02/20/16 00:13
NWTPH-Dx
Oil
ND
194
388
"
"
"
"
"
"
"
DRAFT REPORT
Recovery: 90 %
Notes
Batch: 6020602
Limits: 50-150 %
Page 3 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Result
Analyte
MDL
SW-01 (A6B0661-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Benzene
ND
0.100
0.200
ug/L
02/19/16 14:00
EPA 8260B
Toluene
ND
0.500
1.00
"
"
"
"
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"
Recovery: 99 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
97 %
Limits: 80-120 %
"
"
"
95 %
Limits: 80-120 %
"
"
"
SW-02 (A6B0661-02)
Matrix: Water
Batch: 6020583
Benzene
ND
0.100
0.200
ug/L
02/19/16 14:28
EPA 8260B
Toluene
ND
0.500
1.00
"
"
"
"
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"
Recovery: 100 %
Limits: 80-120 %
"
"
"
100 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
97 %
Limits: 80-120 %
"
"
"
96 %
Limits: 80-120 %
"
"
"
02/19/16 14:57
EPA 8260B
SW-03 (A6B0661-03)
Benzene
Matrix: Water
ND
DRAFT REPORT
0.100
0.200
Notes
Batch: 6020583
Batch: 6020583
ug/L
Page 4 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Result
Analyte
MDL
SW-03 (A6B0661-03)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Toluene
ND
0.500
1.00
ug/L
"
EPA 8260B
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"
Recovery: 99 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
95 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
SW-04 (A6B0661-04)
Matrix: Water
Batch: 6020583
Benzene
ND
0.100
0.200
ug/L
02/19/16 15:26
EPA 8260B
Toluene
ND
0.500
1.00
"
"
"
"
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"
Recovery: 102 %
Limits: 80-120 %
"
"
"
101 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
96 %
Limits: 80-120 %
"
"
"
96 %
Limits: 80-120 %
"
"
"
DRAFT REPORT
Notes
Batch: 6020583
Page 5 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Result
Analyte
MDL
SW-01 (A6B0661-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0208
0.0417
ug/L
02/19/16 18:13
EPA 8270D (SIM)
Acenaphthylene
ND
0.0208
0.0417
"
"
"
"
Anthracene
ND
0.0208
0.0417
"
"
"
"
Benz(a)anthracene
ND
0.0208
0.0417
"
"
"
"
Benzo(a)pyrene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
Chrysene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
Dibenzofuran
ND
0.0208
0.0417
"
"
"
"
Fluoranthene
ND
0.0208
0.0417
"
"
"
"
Fluorene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
1-Methylnaphthalene
ND
0.0417
0.0833
"
"
"
"
2-Methylnaphthalene
ND
0.0417
0.0833
"
"
"
"
Naphthalene
ND
0.0417
0.0833
"
"
"
"
Phenanthrene
ND
0.0208
0.0417
"
"
"
"
Pyrene
ND
0.0208
0.0417
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020602
Recovery: 54 %
Limits: 44-120 %
"
"
"
96 %
Limits: 50-133 %
"
"
"
Page 6 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Result
Analyte
MDL
SW-02 (A6B0661-02)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0208
0.0417
ug/L
02/19/16 18:39
EPA 8270D (SIM)
Acenaphthylene
ND
0.0208
0.0417
"
"
"
"
Anthracene
ND
0.0208
0.0417
"
"
"
"
Benz(a)anthracene
ND
0.0208
0.0417
"
"
"
"
Benzo(a)pyrene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
Chrysene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
Dibenzofuran
ND
0.0208
0.0417
"
"
"
"
Fluoranthene
ND
0.0208
0.0417
"
"
"
"
Fluorene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
1-Methylnaphthalene
ND
0.0417
0.0833
"
"
"
"
2-Methylnaphthalene
ND
0.0417
0.0833
"
"
"
"
Naphthalene
ND
0.0417
0.0833
"
"
"
"
Phenanthrene
ND
0.0208
0.0417
"
"
"
"
Pyrene
ND
0.0208
0.0417
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020602
Recovery: 61 %
Limits: 44-120 %
"
"
"
95 %
Limits: 50-133 %
"
"
"
Page 7 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Result
Analyte
MDL
SW-03 (A6B0661-03)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0200
0.0400
ug/L
02/19/16 19:06
EPA 8270D (SIM)
Acenaphthylene
ND
0.0200
0.0400
"
"
"
"
Anthracene
ND
0.0200
0.0400
"
"
"
"
Benz(a)anthracene
ND
0.0200
0.0400
"
"
"
"
Benzo(a)pyrene
ND
0.0200
0.0400
"
"
"
"
ND
0.0200
0.0400
"
"
"
"
ND
0.0200
0.0400
"
"
"
"
ND
0.0200
0.0400
"
"
"
"
Chrysene
ND
0.0200
0.0400
"
"
"
"
ND
0.0200
0.0400
"
"
"
"
Dibenzofuran
ND
0.0200
0.0400
"
"
"
"
Fluoranthene
ND
0.0200
0.0400
"
"
"
"
Fluorene
ND
0.0200
0.0400
"
"
"
"
ND
0.0200
0.0400
"
"
"
"
1-Methylnaphthalene
ND
0.0400
0.0800
"
"
"
"
2-Methylnaphthalene
ND
0.0400
0.0800
"
"
"
"
Naphthalene
ND
0.0400
0.0800
"
"
"
"
Phenanthrene
ND
0.0200
0.0400
"
"
"
"
Pyrene
ND
0.0200
0.0400
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020602
Recovery: 52 %
Limits: 44-120 %
"
"
"
93 %
Limits: 50-133 %
"
"
"
Page 8 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Result
Analyte
MDL
SW-04 (A6B0661-04)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0194
0.0388
ug/L
02/19/16 19:32
EPA 8270D (SIM)
Acenaphthylene
ND
0.0194
0.0388
"
"
"
"
Anthracene
ND
0.0194
0.0388
"
"
"
"
Benz(a)anthracene
ND
0.0194
0.0388
"
"
"
"
Benzo(a)pyrene
ND
0.0194
0.0388
"
"
"
"
ND
0.0194
0.0388
"
"
"
"
ND
0.0194
0.0388
"
"
"
"
ND
0.0194
0.0388
"
"
"
"
Chrysene
ND
0.0194
0.0388
"
"
"
"
ND
0.0194
0.0388
"
"
"
"
Dibenzofuran
ND
0.0194
0.0388
"
"
"
"
Fluoranthene
ND
0.0194
0.0388
"
"
"
"
Fluorene
ND
0.0194
0.0388
"
"
"
"
ND
0.0194
0.0388
"
"
"
"
1-Methylnaphthalene
ND
0.0388
0.0777
"
"
"
"
2-Methylnaphthalene
ND
0.0388
0.0777
"
"
"
"
Naphthalene
ND
0.0388
0.0777
"
"
"
"
Phenanthrene
ND
0.0194
0.0388
"
"
"
"
Pyrene
ND
0.0194
0.0388
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020602
Recovery: 81 %
Limits: 44-120 %
"
"
"
99 %
Limits: 50-133 %
"
"
"
Page 9 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020602 - EPA 3510C (Acid Extraction)
NWTPH-Dx
Diesel
ND
90.9
182
ug/L
2.5
---
---
---
---
---
---
Oil
ND
182
364
"
"
---
---
---
---
---
---
---
---
Recovery: 88 %
Limits: 50-150 %
Dilution: 2.5x
LCS (6020602-BS2)
NWTPH-Dx
Diesel
991
100
200
Recovery: 90 %
ug/L
2.5
Limits: 50-150 %
1250
---
79
58-115%
Dilution: 2.5x
LCS Dup (6020602-BSD2)
Q-19
NWTPH-Dx
Diesel
1060
100
200
Recovery: 93 %
DRAFT REPORT
ug/L
2.5
Limits: 50-150 %
1250
---
84
58-115%
20%
Dilution: 2.5x
Page 10 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020583 - EPA 5030B
EPA 8260B
Benzene
ND
0.100
0.200
ug/L
---
---
---
---
---
---
Toluene
ND
0.500
1.00
"
"
---
---
---
---
---
---
Ethylbenzene
ND
0.250
0.500
"
"
---
---
---
---
---
---
Xylenes, total
ND
0.750
1.50
"
"
---
---
---
---
---
---
Naphthalene
ND
1.00
2.00
"
"
---
---
---
---
---
---

(MTBE)
Isopropylbenzene
ND
0.500
1.00
"
"
---
---
---
---
---
---
ND
0.500
1.00
"
"
---
---
---
---
---
---
n-Propylbenzene
ND
0.250
0.500
"
"
---
---
---
---
---
---
ND
0.500
1.00
"
"
---
---
---
---
---
---
ND
0.500
1.00
"
"
---
---
---
---
---
---
ND
0.250
0.500
"
"
---
---
---
---
---
---
ND
0.250
0.500
"
"
---
---
---
---
---
---
---
---
Recovery: 97 %
Limits: 80-120 %
Dilution: 1x
98 %
80-120 %
"
Toluene-d8 (Surr)
97 %
80-120 %
"
97 %
80-120 %
"
LCS (6020583-BS1)
EPA 8260B
Benzene
19.6
0.100
0.200
ug/L
20.0
---
98
70-130%
Toluene
20.3
0.500
1.00
"
"
"
---
102
"
---
---
Ethylbenzene
20.7
0.250
0.500
"
"
"
---
103
"
---
---
Xylenes, total
62.4
0.750
1.50
"
"
60.0
---
104
"
---
---
Naphthalene
18.5
1.00
2.00
"
"
20.0
---
93
"
---
---

(MTBE)
Isopropylbenzene
18.8
0.500
1.00
"
"
"
---
94
"
---
---
21.8
0.500
1.00
"
"
"
---
109
"
---
---
n-Propylbenzene
20.0
0.250
0.500
"
"
"
---
100
"
---
---
20.5
0.500
1.00
"
"
"
---
103
"
---
---
20.4
0.500
1.00
"
"
"
---
102
"
---
---
20.4
0.250
0.500
"
"
"
---
102
"
---
---
DRAFT REPORT
Page 11 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
Limits RPD
RPD
Limit
Notes
LCS (6020583-BS1)
%REC
Water
Batch 6020583 - EPA 5030B

Source
Result
18.4
0.250
0.500
ug/L
"
"
---
Recovery: 94 %
Limits: 80-120 %
Dilution: 1x
96 %
80-120 %
"
Toluene-d8 (Surr)
96 %
80-120 %
"
97 %
80-120 %
"
DRAFT REPORT
92
"
---
---
Page 12 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
EPA 8270D (SIM)
Acenaphthene
ND
0.0182
0.0364
ug/L
---
---
---
---
---
---
Acenaphthylene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Anthracene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Benz(a)anthracene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Benzo(a)pyrene
ND
0.0182
0.0364
"
"
---
---
---
---
---
-----
ND
0.0182
0.0364
"
"
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Chrysene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Dibenzofuran
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Fluoranthene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Fluorene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
1-Methylnaphthalene
ND
0.0364
0.0727
"
"
---
---
---
---
---
---
2-Methylnaphthalene
ND
0.0364
0.0727
"
"
---
---
---
---
---
---
Naphthalene
ND
0.0364
0.0727
"
"
---
---
---
---
---
---
Phenanthrene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Pyrene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
---
Recovery: 74 %
Limits: 44-120 %
Dilution: 1x
97 %
50-133 %
"
LCS (6020602-BS1)
EPA 8270D (SIM)
Acenaphthene
6.61
0.0200
0.0400
ug/L
8.00
---
83
47-122%
---
Acenaphthylene
6.67
0.0200
0.0400
"
"
"
---
83
41-130%
---
---
Anthracene
7.42
0.0200
0.0400
"
"
"
---
93
57-123%
---
---
Benz(a)anthracene
7.09
0.0200
0.0400
"
"
"
---
89
58-125%
---
---
Benzo(a)pyrene
7.37
0.0200
0.0400
"
"
"
---
92
54-128%
---
---
7.15
0.0200
0.0400
"
"
"
---
89
53-131%
---
---
7.57
0.0200
0.0400
"
"
"
---
95
57-129%
---
---
DRAFT REPORT
Page 13 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
LCS (6020602-BS1)
Source
Result
6.33
0.0200
0.0400
"
"
"
---
79
50-134%
---
---
Chrysene
7.06
0.0200
0.0400
"
"
"
---
88
59-123%
---
---
7.13
0.0200
0.0400
"
"
"
---
89
51-134%
---
---
Dibenzofuran
6.82
0.0200
0.0400
"
"
"
---
85
53-120%
---
---
Fluoranthene
7.26
0.0200
0.0400
"
"
"
---
91
57-128%
---
---
Fluorene
7.07
0.0200
0.0400
"
"
"
---
88
52-124%
---
---
6.17
0.0200
0.0400
"
"
"
---
77
52-133%
---
---
1-Methylnaphthalene
5.76
0.0400
0.0800
"
"
"
---
72
41-120%
---
---
2-Methylnaphthalene
5.98
0.0400
0.0800
"
"
"
---
75
40-121%
---
---
Naphthalene
5.76
0.0400
0.0800
"
"
"
---
72
"
---
---
Phenanthrene
6.99
0.0200
0.0400
"
"
"
---
87
59-120%
---
---
Pyrene
7.40
0.0200
0.0400
"
"
"
---
93
57-126%
---
---
Recovery: 79 %
Limits: 44-120 %
Dilution: 1x
94 %
50-133 %
"
Q-19
EPA 8270D (SIM)
Acenaphthene
6.83
0.0200
0.0400
ug/L
8.00
---
85
47-122%
30%
Acenaphthylene
6.79
0.0200
0.0400
"
"
"
---
85
41-130%
30%
Anthracene
7.61
0.0200
0.0400
"
"
"
---
95
57-123%
30%
Benz(a)anthracene
7.28
0.0200
0.0400
"
"
"
---
91
58-125%
30%
Benzo(a)pyrene
7.59
0.0200
0.0400
"
"
"
---
95
54-128%
30%
7.57
0.0200
0.0400
"
"
"
---
95
53-131%
30%
7.43
0.0200
0.0400
"
"
"
---
93
57-129%
30%
6.45
0.0200
0.0400
"
"
"
---
81
50-134%
30%
Chrysene
7.30
0.0200
0.0400
"
"
"
---
91
59-123%
30%
7.31
0.0200
0.0400
"
"
"
---
91
51-134%
30%
Dibenzofuran
7.06
0.0200
0.0400
"
"
"
---
88
53-120%
30%
Fluoranthene
7.45
0.0200
0.0400
"
"
"
---
93
57-128%
30%
Fluorene
7.21
0.0200
0.0400
"
"
"
---
90
52-124%
30%
8.20
0.0200
0.0400
"
"
"
---
103
52-133%
28
30%
1-Methylnaphthalene
6.08
0.0400
0.0800
"
"
"
---
76
41-120%
30%
DRAFT REPORT
Page 14 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
Q-19
2-Methylnaphthalene
6.25
0.0400
0.0800
"
"
"
---
78
Naphthalene
5.97
0.0400
0.0800
"
"
"
---
75
Phenanthrene
7.12
0.0200
0.0400
"
"
"
---
89
Pyrene
7.53
0.0200
0.0400
"
"
"
---
94
57-126%
Recovery: 81 %
Limits: 44-120 %
Dilution: 1x
94 %
50-133 %
"
DRAFT REPORT
Notes
Water
RPD
Limit
40-121%
30%
"
30%
59-120%
30%
30%
Page 15 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
1000mL/5mL
1000mL/5mL
1000mL/5mL
1000mL/5mL
0.42
0.42
0.40
0.39
Prep: EPA 3510C (Acid Extraction)

Lab Number
Matrix
Method
Sampled
Prepared
02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
Batch: 6020602
A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04
Water
Water
Water
Water
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
960mL/2mL
960mL/2mL
1000mL/2mL
1030mL/2mL

Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Prep: EPA 5030B

Lab Number
Matrix
Method
Sampled
Prepared
02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30
02/19/16 12:34
02/19/16 12:34
02/19/16 12:34
02/19/16 12:34
Batch: 6020583
A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04
Water
Water
Water
Water
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
1.00
1.00
1.00
1.00

Lab Number
Matrix
Method
Sampled
Prepared
02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
1.04
1.04
1.00
0.97
Batch: 6020602
A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04
Water
Water
Water
Water
EPA 8270D (SIM)

EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
DRAFT REPORT
960mL/2mL
960mL/2mL
1000mL/2mL
1030mL/2mL
Page 16 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/21/16 15:02

Qualifiers:
Q-19
Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

DET
Analyte DETECTED
ND
NR
Not Reported
dry
RPD
MDL
WMSC
Batch
QC
Blank
Policy
---
Spikes, etc.
***
DRAFT REPORT
Page 17 of 18

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/21/16 15:02
Page 18 of 18
Apex Labs

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Monday, February 22, 2016

Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

2/22/2016 at 8:30:00AM.
DRAFT REPORT
Page 1 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

SAMPLE INFORMATION
Sample ID
Laboratory ID
Matrix
Date Sampled
Date Received
SW-01
A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04
Water
Water
Water
Water
02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00
02/22/16 08:30
02/22/16 08:30
02/22/16 08:30
02/22/16 08:30
SW-02
SW-03
SW-04
DRAFT REPORT
Page 2 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Result
Analyte
MDL
SW-01 (A6B0703-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Benzene
ND
0.100
0.200
ug/L
02/22/16 13:47
EPA 8260B
Toluene
ND
0.500
1.00
"
"
"
"
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"
Recovery: 98 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
100 %
Limits: 80-120 %
"
"
"
100 %
Limits: 80-120 %
"
"
"
SW-02 (A6B0703-02)
Matrix: Water
Batch: 6020629
Benzene
ND
0.100
0.200
ug/L
02/22/16 14:16
EPA 8260B
Toluene
ND
0.500
1.00
"
"
"
"
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"
Recovery: 97 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
99 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
02/22/16 14:44
EPA 8260B
SW-03 (A6B0703-03)
Benzene
Matrix: Water
ND
DRAFT REPORT
0.100
0.200
Notes
Batch: 6020629
Batch: 6020629
ug/L
Page 3 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Result
Analyte
MDL
SW-03 (A6B0703-03)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Toluene
ND
0.500
1.00
ug/L
"
EPA 8260B
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"

Toluene-d8 (Surr)
SW-04 (A6B0703-04)
Recovery: 99 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
100 %
Limits: 80-120 %
"
"
"
98 %
Limits: 80-120 %
"
"
"
Matrix: Water
Batch: 6020629
Benzene
ND
0.100
0.200
ug/L
02/22/16 15:13
EPA 8260B
Toluene
ND
0.500
1.00
"
"
"
"
Ethylbenzene
ND
0.250
0.500
"
"
"
"
Xylenes, total
ND
0.750
1.50
"
"
"
"
Naphthalene
ND
1.00
2.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
Isopropylbenzene
ND
0.500
1.00
"
"
"
"
n-Propylbenzene
ND
0.250
0.500
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.500
1.00
"
"
"
"
ND
0.250
0.500
"
"
"
"
ND
0.250
0.500
"
"
"
"

Toluene-d8 (Surr)
DRAFT REPORT
Notes
Batch: 6020629
Recovery: 99 %
Limits: 80-120 %
"
"
"
98 %
Limits: 80-120 %
"
"
"
100 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
Page 4 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Result
Analyte
MDL
SW-01 (A6B0703-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0196
0.0392
ug/L
02/22/16 16:34
EPA 8270D (SIM)
Acenaphthylene
ND
0.0196
0.0392
"
"
"
"
Anthracene
ND
0.0196
0.0392
"
"
"
"
Benz(a)anthracene
ND
0.0196
0.0392
"
"
"
"
Benzo(a)pyrene
ND
0.0196
0.0392
"
"
"
"
ND
0.0196
0.0392
"
"
"
"
ND
0.0196
0.0392
"
"
"
"
ND
0.0196
0.0392
"
"
"
"
Chrysene
ND
0.0196
0.0392
"
"
"
"
ND
0.0196
0.0392
"
"
"
"
Dibenzofuran
ND
0.0196
0.0392
"
"
"
"
Fluoranthene
ND
0.0196
0.0392
"
"
"
"
Fluorene
ND
0.0196
0.0392
"
"
"
"
ND
0.0196
0.0392
"
"
"
"
1-Methylnaphthalene
ND
0.0392
0.0784
"
"
"
"
2-Methylnaphthalene
ND
0.0392
0.0784
"
"
"
"
Naphthalene
ND
0.0392
0.0784
"
"
"
"
Phenanthrene
ND
0.0196
0.0392
"
"
"
"
Pyrene
ND
0.0196
0.0392
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020635
Recovery: 75 %
Limits: 44-120 %
"
"
"
106 %
Limits: 50-133 %
"
"
"
Page 5 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Result
Analyte
MDL
SW-02 (A6B0703-02)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0208
0.0417
ug/L
02/22/16 17:00
EPA 8270D (SIM)
Acenaphthylene
ND
0.0208
0.0417
"
"
"
"
Anthracene
ND
0.0208
0.0417
"
"
"
"
Benz(a)anthracene
ND
0.0208
0.0417
"
"
"
"
Benzo(a)pyrene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
Chrysene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
Dibenzofuran
ND
0.0208
0.0417
"
"
"
"
Fluoranthene
ND
0.0208
0.0417
"
"
"
"
Fluorene
ND
0.0208
0.0417
"
"
"
"
ND
0.0208
0.0417
"
"
"
"
1-Methylnaphthalene
ND
0.0417
0.0833
"
"
"
"
2-Methylnaphthalene
ND
0.0417
0.0833
"
"
"
"
Naphthalene
ND
0.0417
0.0833
"
"
"
"
Phenanthrene
ND
0.0208
0.0417
"
"
"
"
Pyrene
ND
0.0208
0.0417
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020635
Recovery: 70 %
Limits: 44-120 %
"
"
"
102 %
Limits: 50-133 %
"
"
"
Page 6 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Result
Analyte
MDL
SW-03 (A6B0703-03)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0206
0.0412
ug/L
02/22/16 17:26
EPA 8270D (SIM)
Acenaphthylene
ND
0.0206
0.0412
"
"
"
"
Anthracene
ND
0.0206
0.0412
"
"
"
"
Benz(a)anthracene
ND
0.0206
0.0412
"
"
"
"
Benzo(a)pyrene
ND
0.0206
0.0412
"
"
"
"
ND
0.0206
0.0412
"
"
"
"
ND
0.0206
0.0412
"
"
"
"
ND
0.0206
0.0412
"
"
"
"
Chrysene
ND
0.0206
0.0412
"
"
"
"
ND
0.0206
0.0412
"
"
"
"
Dibenzofuran
ND
0.0206
0.0412
"
"
"
"
Fluoranthene
ND
0.0206
0.0412
"
"
"
"
Fluorene
ND
0.0206
0.0412
"
"
"
"
ND
0.0206
0.0412
"
"
"
"
1-Methylnaphthalene
ND
0.0412
0.0825
"
"
"
"
2-Methylnaphthalene
ND
0.0412
0.0825
"
"
"
"
Naphthalene
ND
0.0412
0.0825
"
"
"
"
Phenanthrene
ND
0.0206
0.0412
"
"
"
"
Pyrene
ND
0.0206
0.0412
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020635
Recovery: 72 %
Limits: 44-120 %
"
"
"
106 %
Limits: 50-133 %
"
"
"
Page 7 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Result
Analyte
MDL
SW-04 (A6B0703-04)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
0.0198
0.0396
ug/L
02/22/16 17:52
EPA 8270D (SIM)
Acenaphthylene
ND
0.0198
0.0396
"
"
"
"
Anthracene
ND
0.0198
0.0396
"
"
"
"
Benz(a)anthracene
ND
0.0198
0.0396
"
"
"
"
Benzo(a)pyrene
ND
0.0198
0.0396
"
"
"
"
ND
0.0198
0.0396
"
"
"
"
ND
0.0198
0.0396
"
"
"
"
ND
0.0198
0.0396
"
"
"
"
Chrysene
ND
0.0198
0.0396
"
"
"
"
ND
0.0198
0.0396
"
"
"
"
Dibenzofuran
ND
0.0198
0.0396
"
"
"
"
Fluoranthene
ND
0.0198
0.0396
"
"
"
"
Fluorene
ND
0.0198
0.0396
"
"
"
"
ND
0.0198
0.0396
"
"
"
"
1-Methylnaphthalene
ND
0.0396
0.0792
"
"
"
"
2-Methylnaphthalene
ND
0.0396
0.0792
"
"
"
"
Naphthalene
ND
0.0396
0.0792
"
"
"
"
Phenanthrene
ND
0.0198
0.0396
"
"
"
"
Pyrene
ND
0.0198
0.0396
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020635
Recovery: 78 %
Limits: 44-120 %
"
"
"
106 %
Limits: 50-133 %
"
"
"
Page 8 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020629 - EPA 5030B
EPA 8260B
Benzene
ND
0.100
0.200
ug/L
---
---
---
---
---
---
Toluene
ND
0.500
1.00
"
"
---
---
---
---
---
---
Ethylbenzene
ND
0.250
0.500
"
"
---
---
---
---
---
---
Xylenes, total
ND
0.750
1.50
"
"
---
---
---
---
---
---
Naphthalene
ND
1.00
2.00
"
"
---
---
---
---
---
---

(MTBE)
Isopropylbenzene
ND
0.500
1.00
"
"
---
---
---
---
---
---
ND
0.500
1.00
"
"
---
---
---
---
---
---
n-Propylbenzene
ND
0.250
0.500
"
"
---
---
---
---
---
---
ND
0.500
1.00
"
"
---
---
---
---
---
---
ND
0.500
1.00
"
"
---
---
---
---
---
---
ND
0.250
0.500
"
"
---
---
---
---
---
---
ND
0.250
0.500
"
"
---
---
---
---
---
---
---
---
Recovery: 98 %
Limits: 80-120 %
Dilution: 1x
98 %
80-120 %
"
100 %
80-120 %
"
97 %
80-120 %
"
Toluene-d8 (Surr)
LCS (6020629-BS1)
EPA 8260B
Benzene
19.1
0.100
0.200
ug/L
20.0
---
95
70-130%
Toluene
20.1
0.500
1.00
"
"
"
---
100
"
---
---
Ethylbenzene
20.4
0.250
0.500
"
"
"
---
102
"
---
---
Xylenes, total
61.6
0.750
1.50
"
"
60.0
---
103
"
---
---
Naphthalene
17.8
1.00
2.00
"
"
20.0
---
89
"
---
---

(MTBE)
Isopropylbenzene
18.3
0.500
1.00
"
"
"
---
92
"
---
---
21.5
0.500
1.00
"
"
"
---
107
"
---
---
n-Propylbenzene
19.6
0.250
0.500
"
"
"
---
98
"
---
---
20.4
0.500
1.00
"
"
"
---
102
"
---
---
20.3
0.500
1.00
"
"
"
---
102
"
---
---
20.3
0.250
0.500
"
"
"
---
102
"
---
---
DRAFT REPORT
Page 9 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
Limits RPD
RPD
Limit
Notes
LCS (6020629-BS1)
%REC
Water
Batch 6020629 - EPA 5030B

Source
Result
18.0
0.250
0.500
ug/L
"
"
---
Recovery: 95 %
Limits: 80-120 %
Dilution: 1x
96 %
80-120 %
"
Toluene-d8 (Surr)
99 %
80-120 %
"
98 %
80-120 %
"
DRAFT REPORT
90
"
---
---
Page 10 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
EPA 8270D (SIM)
Acenaphthene
ND
0.0182
0.0364
ug/L
---
---
---
---
---
---
Acenaphthylene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Anthracene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Benz(a)anthracene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Benzo(a)pyrene
ND
0.0182
0.0364
"
"
---
---
---
---
---
-----
ND
0.0182
0.0364
"
"
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Chrysene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Dibenzofuran
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Fluoranthene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Fluorene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
1-Methylnaphthalene
ND
0.0364
0.0727
"
"
---
---
---
---
---
---
2-Methylnaphthalene
ND
0.0364
0.0727
"
"
---
---
---
---
---
---
Naphthalene
ND
0.0364
0.0727
"
"
---
---
---
---
---
---
Phenanthrene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
Pyrene
ND
0.0182
0.0364
"
"
---
---
---
---
---
---
---
Recovery: 92 %
Limits: 44-120 %
Dilution: 1x
114 %
50-133 %
"
LCS (6020635-BS1)
EPA 8270D (SIM)
Acenaphthene
7.34
0.0200
0.0400
ug/L
8.00
---
92
47-122%
---
Acenaphthylene
7.43
0.0200
0.0400
"
"
"
---
93
41-130%
---
---
Anthracene
7.74
0.0200
0.0400
"
"
"
---
97
57-123%
---
---
Benz(a)anthracene
7.61
0.0200
0.0400
"
"
"
---
95
58-125%
---
---
Benzo(a)pyrene
7.92
0.0200
0.0400
"
"
"
---
99
54-128%
---
---
8.27
0.0200
0.0400
"
"
"
---
103
53-131%
---
---
7.91
0.0200
0.0400
"
"
"
---
99
57-129%
---
---
DRAFT REPORT
Page 11 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
LCS (6020635-BS1)
Source
Result
6.86
0.0200
0.0400
"
"
"
---
86
50-134%
---
---
Chrysene
7.46
0.0200
0.0400
"
"
"
---
93
59-123%
---
---
7.31
0.0200
0.0400
"
"
"
---
91
51-134%
---
---
Dibenzofuran
7.57
0.0200
0.0400
"
"
"
---
95
53-120%
---
---
Fluoranthene
8.05
0.0200
0.0400
"
"
"
---
101
57-128%
---
---
Fluorene
7.68
0.0200
0.0400
"
"
"
---
96
52-124%
---
---
7.04
0.0200
0.0400
"
"
"
---
88
52-133%
---
---
1-Methylnaphthalene
6.80
0.0400
0.0800
"
"
"
---
85
41-120%
---
---
2-Methylnaphthalene
7.18
0.0400
0.0800
"
"
"
---
90
40-121%
---
---
Naphthalene
6.93
0.0400
0.0800
"
"
"
---
87
"
---
---
Phenanthrene
7.70
0.0200
0.0400
"
"
"
---
96
59-120%
---
---
Pyrene
8.13
0.0200
0.0400
"
"
"
---
102
57-126%
---
---
Recovery: 91 %
Limits: 44-120 %
Dilution: 1x
104 %
50-133 %
"
Q-19
EPA 8270D (SIM)
Acenaphthene
7.41
0.0200
0.0400
ug/L
8.00
---
93
47-122%
30%
Acenaphthylene
7.60
0.0200
0.0400
"
"
"
---
95
41-130%
30%
Anthracene
7.78
0.0200
0.0400
"
"
"
---
97
57-123%
0.5
30%
Benz(a)anthracene
7.63
0.0200
0.0400
"
"
"
---
95
58-125%
0.3
30%
Benzo(a)pyrene
8.00
0.0200
0.0400
"
"
"
---
100
54-128%
30%
8.28
0.0200
0.0400
"
"
"
---
103
53-131%
0.08
30%
7.87
0.0200
0.0400
"
"
"
---
98
57-129%
0.5
30%
7.12
0.0200
0.0400
"
"
"
---
89
50-134%
30%
Chrysene
7.66
0.0200
0.0400
"
"
"
---
96
59-123%
30%
7.62
0.0200
0.0400
"
"
"
---
95
51-134%
30%
Dibenzofuran
7.56
0.0200
0.0400
"
"
"
---
94
53-120%
0.2
30%
Fluoranthene
7.98
0.0200
0.0400
"
"
"
---
100
57-128%
0.8
30%
Fluorene
7.65
0.0200
0.0400
"
"
"
---
96
52-124%
0.4
30%
7.20
0.0200
0.0400
"
"
"
---
90
52-133%
30%
1-Methylnaphthalene
6.96
0.0400
0.0800
"
"
"
---
87
41-120%
30%
DRAFT REPORT
Page 12 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
Q-19
2-Methylnaphthalene
7.34
0.0400
0.0800
"
"
"
---
92
Naphthalene
7.22
0.0400
0.0800
"
"
"
---
90
Phenanthrene
7.76
0.0200
0.0400
"
"
"
---
97
Pyrene
8.10
0.0200
0.0400
"
"
"
---
101
57-126%
Recovery: 92 %
Limits: 44-120 %
Dilution: 1x
104 %
50-133 %
"
DRAFT REPORT
Notes
Water
RPD
Limit
40-121%
30%
"
30%
59-120%
0.8
30%
0.4
30%
Page 13 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Prep: EPA 5030B

Lab Number
Matrix
Method
Sampled
Prepared
02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00
02/22/16 12:40
02/22/16 12:40
02/22/16 12:40
02/22/16 12:40
Batch: 6020629
A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04
Water
Water
Water
Water
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
1.00
1.00
1.00
1.00

Lab Number
Matrix
Method
Sampled
Prepared
02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00
02/22/16 11:20
02/22/16 11:20
02/22/16 11:20
02/22/16 11:20
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
0.98
1.04
1.03
0.99
Batch: 6020635
A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04
Water
Water
Water
Water
EPA 8270D (SIM)

EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
DRAFT REPORT
1020mL/2mL
960mL/2mL
970mL/2mL
1010mL/2mL
Page 14 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/22/16 18:29

Qualifiers:
Q-19
analysis.

DET
Analyte DETECTED
ND
NR
Not Reported
dry
RPD
MDL
WMSC
Batch
QC
Blank
Policy
---
Spikes, etc.
***
DRAFT REPORT
Page 15 of 16

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/22/16 18:29
Page 16 of 16
Apex Labs

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Friday, February 26, 2016

Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

2/26/2016 at 6:35:00AM.
DRAFT REPORT
Page 1 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

SAMPLE INFORMATION
Sample ID
Laboratory ID
Matrix
Date Sampled
Date Received
SW-05
A6B0868-01
Water
02/25/16 13:00
02/26/16 06:35
DRAFT REPORT
Page 2 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Result
Analyte
MDL
SW-05 (A6B0868-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Benzene
ND
---
0.200
ug/L
02/26/16 13:07
EPA 8260B
Toluene
ND
---
1.00
"
"
"
"
Ethylbenzene
ND
---
0.500
"
"
"
"
Xylenes, total
ND
---
1.50
"
"
"
"
Naphthalene
ND
---
2.00
"
"
"
"
ND
---
1.00
"
"
"
"
Isopropylbenzene
ND
---
1.00
"
"
"
"
n-Propylbenzene
ND
---
0.500
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
0.500
"
"
"
"
ND
---
0.500
"
"
"
"

Toluene-d8 (Surr)
DRAFT REPORT
Notes
Batch: 6020814
Recovery: 100 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
102 %
Limits: 80-120 %
"
"
"
98 %
Limits: 80-120 %
"
"
"
Page 3 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Result
Analyte
MDL
SW-05 (A6B0868-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
---
0.0440
ug/L
02/26/16 12:14
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0440
"
"
"
"
Anthracene
ND
---
0.0440
"
"
"
"
Benz(a)anthracene
ND
---
0.0440
"
"
"
"
Benzo(a)pyrene
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
Chrysene
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
Dibenzofuran
ND
---
0.0440
"
"
"
"
Fluoranthene
ND
---
0.0440
"
"
"
"
Fluorene
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
1-Methylnaphthalene
ND
---
0.0879
"
"
"
"
2-Methylnaphthalene
ND
---
0.0879
"
"
"
"
Naphthalene
ND
---
0.0879
"
"
"
"
Phenanthrene
ND
---
0.0440
"
"
"
"
Pyrene
ND
---
0.0440
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020786
Recovery: 75 %
Limits: 44-120 %
"
"
"
112 %
Limits: 50-133 %
"
"
"
Page 4 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020814 - EPA 5030B
EPA 8260B
Benzene
ND
---
0.200
ug/L
---
---
---
---
---
---
Toluene
ND
---
1.00
"
"
---
---
---
---
---
---
Ethylbenzene
ND
---
0.500
"
"
---
---
---
---
---
---
Xylenes, total
ND
---
1.50
"
"
---
---
---
---
---
---
Naphthalene
ND
---
2.00
"
"
---
---
---
---
---
---

(MTBE)
Isopropylbenzene
ND
---
1.00
"
"
---
---
---
---
---
---
ND
---
1.00
"
"
---
---
---
---
---
---
n-Propylbenzene
ND
---
0.500
"
"
---
---
---
---
---
---
ND
---
1.00
"
"
---
---
---
---
---
---
ND
---
1.00
"
"
---
---
---
---
---
---
ND
---
0.500
"
"
---
---
---
---
---
---
ND
---
0.500
"
"
---
---
---
---
---
---
---
---
Recovery: 99 %
Limits: 80-120 %
Dilution: 1x
99 %
80-120 %
"
Toluene-d8 (Surr)
101 %
80-120 %
"
100 %
80-120 %
"
LCS (6020814-BS1)
EPA 8260B
Benzene
18.8
---
0.200
ug/L
20.0
---
94
70-130%
Toluene
20.2
---
1.00
"
"
"
---
101
"
---
---
Ethylbenzene
20.1
---
0.500
"
"
"
---
101
"
---
---
Xylenes, total
61.4
---
1.50
"
"
60.0
---
102
"
---
---
Naphthalene
17.9
---
2.00
"
"
20.0
---
90
"
---
---

(MTBE)
Isopropylbenzene
18.2
---
1.00
"
"
"
---
91
"
---
---
20.8
---
1.00
"
"
"
---
104
"
---
---
n-Propylbenzene
19.8
---
0.500
"
"
"
---
99
"
---
---
20.4
---
1.00
"
"
"
---
102
"
---
---
20.4
---
1.00
"
"
"
---
102
"
---
---
20.5
---
0.500
"
"
"
---
102
"
---
---
DRAFT REPORT
Page 5 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
Limits RPD
RPD
Limit
Notes
LCS (6020814-BS1)
%REC
Water
Batch 6020814 - EPA 5030B

Source
Result
17.7
---
0.500
ug/L
"
"
---
Recovery: 96 %
Limits: 80-120 %
Dilution: 1x
95 %
80-120 %
"
Toluene-d8 (Surr)
100 %
80-120 %
"
101 %
80-120 %
"
DRAFT REPORT
88
"
---
---
Page 6 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
EPA 8270D (SIM)
Acenaphthene
ND
---
0.0364
ug/L
---
---
---
---
---
---
Acenaphthylene
ND
---
0.0364
"
"
---
---
---
---
---
---
Anthracene
ND
---
0.0364
"
"
---
---
---
---
---
---
Benz(a)anthracene
ND
---
0.0364
"
"
---
---
---
---
---
---
Benzo(a)pyrene
ND
---
0.0364
"
"
---
---
---
---
---
-----
ND
---
0.0364
"
"
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
Chrysene
ND
---
0.0364
"
"
---
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
Dibenzofuran
ND
---
0.0364
"
"
---
---
---
---
---
---
Fluoranthene
ND
---
0.0364
"
"
---
---
---
---
---
---
Fluorene
ND
---
0.0364
"
"
---
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
1-Methylnaphthalene
ND
---
0.0727
"
"
---
---
---
---
---
---
2-Methylnaphthalene
ND
---
0.0727
"
"
---
---
---
---
---
---
Naphthalene
ND
---
0.0727
"
"
---
---
---
---
---
---
Phenanthrene
ND
---
0.0364
"
"
---
---
---
---
---
---
Pyrene
ND
---
0.0364
"
"
---
---
---
---
---
---
---
Recovery: 84 %
Limits: 44-120 %
Dilution: 1x
108 %
50-133 %
"
LCS (6020786-BS1)
EPA 8270D (SIM)
Acenaphthene
6.55
---
0.0400
ug/L
8.00
---
82
47-122%
---
Acenaphthylene
6.52
---
0.0400
"
"
"
---
82
41-130%
---
---
Anthracene
7.27
---
0.0400
"
"
"
---
91
57-123%
---
---
Benz(a)anthracene
7.29
---
0.0400
"
"
"
---
91
58-125%
---
---
Benzo(a)pyrene
7.85
---
0.0400
"
"
"
---
98
54-128%
---
---
7.84
---
0.0400
"
"
"
---
98
53-131%
---
---
7.60
---
0.0400
"
"
"
---
95
57-129%
---
---
DRAFT REPORT
Page 7 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
LCS (6020786-BS1)
Source
Result
7.13
---
0.0400
"
"
"
---
89
50-134%
---
---
Chrysene
7.26
---
0.0400
"
"
"
---
91
59-123%
---
---
7.46
---
0.0400
"
"
"
---
93
51-134%
---
-----
Dibenzofuran
6.69
---
0.0400
"
"
"
---
84
53-120%
---
Fluoranthene
7.26
---
0.0400
"
"
"
---
91
57-128%
---
---
Fluorene
6.83
---
0.0400
"
"
"
---
85
52-124%
---
---
7.14
---
0.0400
"
"
"
---
89
52-133%
---
---
1-Methylnaphthalene
5.60
---
0.0800
"
"
"
---
70
41-120%
---
---
2-Methylnaphthalene
5.84
---
0.0800
"
"
"
---
73
40-121%
---
---
Naphthalene
5.78
---
0.0800
"
"
"
---
72
"
---
---
Phenanthrene
7.19
---
0.0400
"
"
"
---
90
59-120%
---
---
Pyrene
7.29
---
0.0400
"
"
"
---
91
57-126%
---
---
Recovery: 83 %
Limits: 44-120 %
Dilution: 1x
100 %
50-133 %
"
Q-19
EPA 8270D (SIM)
Acenaphthene
6.86
---
0.0400
ug/L
8.00
---
86
47-122%
30%
Acenaphthylene
6.91
---
0.0400
"
"
"
---
86
41-130%
30%
Anthracene
7.76
---
0.0400
"
"
"
---
97
57-123%
30%
Benz(a)anthracene
7.26
---
0.0400
"
"
"
---
91
58-125%
0.5
30%
Benzo(a)pyrene
7.87
---
0.0400
"
"
"
---
98
54-128%
0.2
30%
7.58
---
0.0400
"
"
"
---
95
53-131%
30%
7.81
---
0.0400
"
"
"
---
98
57-129%
30%
7.11
---
0.0400
"
"
"
---
89
50-134%
0.4
30%
Chrysene
7.26
---
0.0400
"
"
"
---
91
59-123%
0.05
30%
7.42
---
0.0400
"
"
"
---
93
51-134%
0.5
30%
Dibenzofuran
6.91
---
0.0400
"
"
"
---
86
53-120%
30%
Fluoranthene
7.28
---
0.0400
"
"
"
---
91
57-128%
0.3
30%
Fluorene
7.03
---
0.0400
"
"
"
---
88
52-124%
30%
7.07
---
0.0400
"
"
"
---
88
52-133%
30%
1-Methylnaphthalene
6.30
---
0.0800
"
"
"
---
79
41-120%
12
30%
DRAFT REPORT
Page 8 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
2-Methylnaphthalene
6.60
Naphthalene
Phenanthrene
Pyrene
Q-19
---
0.0800
"
"
"
---
82
6.56
---
0.0800
"
"
"
---
82
7.24
---
0.0400
"
"
"
---
91
7.39
---
"
"
"
---
92
57-126%
0.0400
Recovery: 91 %
Limits: 44-120 %
Dilution: 1x
100 %
50-133 %
"
DRAFT REPORT
Notes
Water
Source
Result
40-121%
12
30%
"
13
30%
59-120%
0.7
30%
30%
Page 9 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Prep: EPA 5030B

Lab Number
Matrix
Method
Sampled
Prepared
02/25/16 13:00
02/26/16 12:03
Batch: 6020814
A6B0868-01
Water
EPA 8260B
5mL/5mL
5mL/5mL
1.00

Lab Number
Matrix
Method
Sampled
Prepared
02/25/16 13:00
02/26/16 09:16
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
910mL/2mL
1000mL/2mL
1.10
Batch: 6020786
A6B0868-01
Water
EPA 8270D (SIM)
DRAFT REPORT
Page 10 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/26/16 16:36

Qualifiers:
Q-19
analysis.

DET
Analyte DETECTED
ND
NR
Not Reported
dry
RPD
MDL
WMSC
Batch
QC
Blank
Policy
---
Spikes, etc.
***
DRAFT REPORT
Page 11 of 12

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/26/16 16:36
Page 12 of 12
Apex Labs

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Monday, February 29, 2016

Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

2/29/2016 at 6:36:00AM.
DRAFT REPORT
Page 1 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

SAMPLE INFORMATION
Sample ID
Laboratory ID
Matrix
Date Sampled
Date Received
SW-01
A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05
Water
Water
Water
Water
Water
02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
SW-02
SW-03
SW-04
SW-05
DRAFT REPORT
Page 2 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-01 (A6B0905-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Benzene
ND
---
0.200
ug/L
02/29/16 12:13
EPA 8260B
Toluene
ND
---
1.00
"
"
"
"
Ethylbenzene
ND
---
0.500
"
"
"
"
Xylenes, total
ND
---
1.50
"
"
"
"
Naphthalene
ND
---
2.00
"
"
"
"
ND
---
1.00
"
"
"
"
Isopropylbenzene
ND
---
1.00
"
"
"
"
n-Propylbenzene
ND
---
0.500
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
0.500
"
"
"
"
ND
---
0.500
"
"
"
"
Recovery: 102 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
101 %
Limits: 80-120 %
"
"
"
100 %
Limits: 80-120 %
"
"
"
SW-02 (A6B0905-02)
Matrix: Water
Batch: 6020841
Benzene
ND
---
0.200
ug/L
02/29/16 13:10
EPA 8260B
Toluene
ND
---
1.00
"
"
"
"
Ethylbenzene
ND
---
0.500
"
"
"
"
Xylenes, total
ND
---
1.50
"
"
"
"
Naphthalene
ND
---
2.00
"
"
"
"
ND
---
1.00
"
"
"
"
Isopropylbenzene
ND
---
1.00
"
"
"
"
n-Propylbenzene
ND
---
0.500
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
0.500
"
"
"
"
ND
---
0.500
"
"
"
"

Toluene-d8 (Surr)
SW-03 (A6B0905-03)
Benzene
Recovery: 102 %
Limits: 80-120 %
"
"
"
98 %
Limits: 80-120 %
"
"
"
102 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
02/29/16 13:39
EPA 8260B
Matrix: Water
ND
DRAFT REPORT
---
0.200
Notes
Batch: 6020841
Batch: 6020841
ug/L
Page 3 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-03 (A6B0905-03)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Toluene
ND
---
1.00
ug/L
"
EPA 8260B
Ethylbenzene
ND
---
0.500
"
"
"
"
Xylenes, total
ND
---
1.50
"
"
"
"
Naphthalene
ND
---
2.00
"
"
"
"
ND
---
1.00
"
"
"
"
Isopropylbenzene
ND
---
1.00
"
"
"
"
n-Propylbenzene
ND
---
0.500
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
0.500
"
"
"
"
ND
---
0.500
"
"
"
"
Recovery: 104 %
Limits: 80-120 %
"
"
"
100 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
102 %
Limits: 80-120 %
"
"
"
98 %
Limits: 80-120 %
"
"
"
SW-04 (A6B0905-04)
Matrix: Water
Batch: 6020841
Benzene
ND
---
0.200
ug/L
02/29/16 14:08
EPA 8260B
Toluene
ND
---
1.00
"
"
"
"
Ethylbenzene
ND
---
0.500
"
"
"
"
Xylenes, total
ND
---
1.50
"
"
"
"
Naphthalene
ND
---
2.00
"
"
"
"
ND
---
1.00
"
"
"
"
Isopropylbenzene
ND
---
1.00
"
"
"
"
n-Propylbenzene
ND
---
0.500
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
0.500
"
"
"
"
ND
---
0.500
"
"
"
"

Toluene-d8 (Surr)
SW-05 (A6B0905-05)
Recovery: 105 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
101 %
Limits: 80-120 %
"
"
"
97 %
Limits: 80-120 %
"
"
"
Matrix: Water
Batch: 6020841
Benzene
ND
---
0.200
ug/L
02/29/16 14:36
EPA 8260B
Toluene
ND
---
1.00
"
"
"
"
DRAFT REPORT
Notes
Batch: 6020841
Page 4 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-05 (A6B0905-05)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Ethylbenzene
ND
---
0.500
ug/L
"
EPA 8260B
Xylenes, total
ND
---
1.50
"
"
"
"
Naphthalene
ND
---
2.00
"
"
"
"
ND
---
1.00
"
"
"
"
Isopropylbenzene
ND
---
1.00
"
"
"
"
n-Propylbenzene
ND
---
0.500
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
1.00
"
"
"
"
ND
---
0.500
"
"
"
"
ND
---
0.500
"
"
"
"
Recovery: 105 %
Limits: 80-120 %
"
"
"
101 %
Limits: 80-120 %
"
"
"
Toluene-d8 (Surr)
101 %
Limits: 80-120 %
"
"
"
99 %
Limits: 80-120 %
"
"
"
DRAFT REPORT
Notes
Batch: 6020841
Page 5 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-01 (A6B0905-01)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
---
0.0392
ug/L
02/29/16 12:57
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0392
"
"
"
"
Anthracene
ND
---
0.0392
"
"
"
"
Benz(a)anthracene
ND
---
0.0392
"
"
"
"
Benzo(a)pyrene
ND
---
0.0392
"
"
"
"
ND
---
0.0392
"
"
"
"
ND
---
0.0392
"
"
"
"
ND
---
0.0392
"
"
"
"
Chrysene
ND
---
0.0392
"
"
"
"
ND
---
0.0392
"
"
"
"
Dibenzofuran
ND
---
0.0392
"
"
"
"
Fluoranthene
ND
---
0.0392
"
"
"
"
Fluorene
ND
---
0.0392
"
"
"
"
ND
---
0.0392
"
"
"
"
1-Methylnaphthalene
ND
---
0.0784
"
"
"
"
2-Methylnaphthalene
ND
---
0.0784
"
"
"
"
Naphthalene
ND
---
0.0784
"
"
"
"
Phenanthrene
ND
---
0.0392
"
"
"
"
Pyrene
ND
---
0.0392
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020838
Recovery: 83 %
Limits: 44-120 %
"
"
"
114 %
Limits: 50-133 %
"
"
"
Page 6 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-02 (A6B0905-02)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
---
0.0404
ug/L
02/29/16 13:24
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0404
"
"
"
"
Anthracene
ND
---
0.0404
"
"
"
"
Benz(a)anthracene
ND
---
0.0404
"
"
"
"
Benzo(a)pyrene
ND
---
0.0404
"
"
"
"
ND
---
0.0404
"
"
"
"
ND
---
0.0404
"
"
"
"
ND
---
0.0404
"
"
"
"
Chrysene
ND
---
0.0404
"
"
"
"
ND
---
0.0404
"
"
"
"
Dibenzofuran
ND
---
0.0404
"
"
"
"
Fluoranthene
ND
---
0.0404
"
"
"
"
Fluorene
ND
---
0.0404
"
"
"
"
ND
---
0.0404
"
"
"
"
1-Methylnaphthalene
ND
---
0.0808
"
"
"
"
2-Methylnaphthalene
ND
---
0.0808
"
"
"
"
Naphthalene
ND
---
0.0808
"
"
"
"
Phenanthrene
ND
---
0.0404
"
"
"
"
Pyrene
ND
---
0.0404
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020838
Recovery: 82 %
Limits: 44-120 %
"
"
"
115 %
Limits: 50-133 %
"
"
"
Page 7 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-03 (A6B0905-03)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
---
0.0421
ug/L
02/29/16 13:52
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0421
"
"
"
"
Anthracene
ND
---
0.0421
"
"
"
"
Benz(a)anthracene
ND
---
0.0421
"
"
"
"
Benzo(a)pyrene
ND
---
0.0421
"
"
"
"
ND
---
0.0421
"
"
"
"
ND
---
0.0421
"
"
"
"
ND
---
0.0421
"
"
"
"
Chrysene
ND
---
0.0421
"
"
"
"
ND
---
0.0421
"
"
"
"
Dibenzofuran
ND
---
0.0421
"
"
"
"
Fluoranthene
ND
---
0.0421
"
"
"
"
Fluorene
ND
---
0.0421
"
"
"
"
ND
---
0.0421
"
"
"
"
1-Methylnaphthalene
ND
---
0.0842
"
"
"
"
2-Methylnaphthalene
ND
---
0.0842
"
"
"
"
Naphthalene
ND
---
0.0842
"
"
"
"
Phenanthrene
ND
---
0.0421
"
"
"
"
Pyrene
ND
---
0.0421
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020838
Recovery: 67 %
Limits: 44-120 %
"
"
"
109 %
Limits: 50-133 %
"
"
"
Page 8 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-04 (A6B0905-04)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
---
0.0408
ug/L
02/29/16 14:19
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0408
"
"
"
"
Anthracene
ND
---
0.0408
"
"
"
"
Benz(a)anthracene
ND
---
0.0408
"
"
"
"
Benzo(a)pyrene
ND
---
0.0408
"
"
"
"
ND
---
0.0408
"
"
"
"
ND
---
0.0408
"
"
"
"
ND
---
0.0408
"
"
"
"
Chrysene
ND
---
0.0408
"
"
"
"
ND
---
0.0408
"
"
"
"
Dibenzofuran
ND
---
0.0408
"
"
"
"
Fluoranthene
ND
---
0.0408
"
"
"
"
Fluorene
ND
---
0.0408
"
"
"
"
ND
---
0.0408
"
"
"
"
1-Methylnaphthalene
ND
---
0.0816
"
"
"
"
2-Methylnaphthalene
ND
---
0.0816
"
"
"
"
Naphthalene
ND
---
0.0816
"
"
"
"
Phenanthrene
ND
---
0.0408
"
"
"
"
Pyrene
ND
---
0.0408
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020838
Recovery: 86 %
Limits: 44-120 %
"
"
"
110 %
Limits: 50-133 %
"
"
"
Page 9 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Result
Analyte
MDL
SW-05 (A6B0905-05)
Reporting
Limit
Dilution
Units
Matrix: Water
Date Analyzed
Method
Acenaphthene
ND
---
0.0440
ug/L
02/29/16 14:46
EPA 8270D (SIM)
Acenaphthylene
ND
---
0.0440
"
"
"
"
Anthracene
ND
---
0.0440
"
"
"
"
Benz(a)anthracene
ND
---
0.0440
"
"
"
"
Benzo(a)pyrene
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
Chrysene
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
Dibenzofuran
ND
---
0.0440
"
"
"
"
Fluoranthene
ND
---
0.0440
"
"
"
"
Fluorene
ND
---
0.0440
"
"
"
"
ND
---
0.0440
"
"
"
"
1-Methylnaphthalene
ND
---
0.0879
"
"
"
"
2-Methylnaphthalene
ND
---
0.0879
"
"
"
"
Naphthalene
ND
---
0.0879
"
"
"
"
Phenanthrene
ND
---
0.0440
"
"
"
"
Pyrene
ND
---
0.0440
"
"
"
"

DRAFT REPORT
Notes
Batch: 6020838
Recovery: 78 %
Limits: 44-120 %
"
"
"
115 %
Limits: 50-133 %
"
"
"
Page 10 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Analyte
Result
MDL
Reporting
Limit
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020841 - EPA 5030B
EPA 8260B
Benzene
ND
---
0.200
ug/L
---
---
---
---
---
---
Toluene
ND
---
1.00
"
"
---
---
---
---
---
---
Ethylbenzene
ND
---
0.500
"
"
---
---
---
---
---
---
Xylenes, total
ND
---
1.50
"
"
---
---
---
---
---
---
Naphthalene
ND
---
2.00
"
"
---
---
---
---
---
---

(MTBE)
Isopropylbenzene
ND
---
1.00
"
"
---
---
---
---
---
---
ND
---
1.00
"
"
---
---
---
---
---
---
n-Propylbenzene
ND
---
0.500
"
"
---
---
---
---
---
---
ND
---
1.00
"
"
---
---
---
---
---
---
ND
---
1.00
"
"
---
---
---
---
---
---
ND
---
0.500
"
"
---
---
---
---
---
---
ND
---
0.500
"
"
---
---
---
---
---
---
---
---
Recovery: 100 %
Limits: 80-120 %
Dilution: 1x
99 %
80-120 %
"
101 %
80-120 %
"
99 %
80-120 %
"
Toluene-d8 (Surr)
LCS (6020841-BS1)
EPA 8260B
Benzene
18.9
---
0.200
ug/L
20.0
---
94
70-130%
Toluene
20.0
---
1.00
"
"
"
---
100
"
---
---
Ethylbenzene
20.2
---
0.500
"
"
"
---
101
"
---
---
Xylenes, total
61.0
---
1.50
"
"
60.0
---
102
"
---
---
Naphthalene
17.1
---
2.00
"
"
20.0
---
86
"
---
---

(MTBE)
Isopropylbenzene
18.7
---
1.00
"
"
"
---
93
"
---
---
20.5
---
1.00
"
"
"
---
103
"
---
---
n-Propylbenzene
19.6
---
0.500
"
"
"
---
98
"
---
---
20.2
---
1.00
"
"
"
---
101
"
---
---
19.9
---
1.00
"
"
"
---
100
"
---
---
20.7
---
0.500
"
"
"
---
103
"
---
---
DRAFT REPORT
Page 11 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020841 - EPA 5030B
LCS (6020841-BS1)
Source
Result
19.0
---
0.500
ug/L
"
"
---
Recovery: 98 %
Limits: 80-120 %
Dilution: 1x
95 %
80-120 %
"
Toluene-d8 (Surr)
99 %
80-120 %
"
99 %
80-120 %
"
95
"
---
---
QC Source Sample: SW-01 (A6B0905-01)
EPA 8260B
Benzene
ND
---
0.200
ug/L
---
ND
---
---
---
30%
Toluene
ND
Ethylbenzene
ND
---
1.00
"
"
---
ND
---
---
---
30%
---
0.500
"
"
---
ND
---
---
---
30%
Xylenes, total
Naphthalene
ND
---
1.50
"
"
---
ND
---
---
---
30%
ND
---
2.00
"
"
---
ND
---
---
---
30%

(MTBE)
Isopropylbenzene
ND
---
1.00
"
"
---
ND
---
---
---
30%
ND
---
1.00
"
"
---
ND
---
---
---
30%
n-Propylbenzene
ND
---
0.500
"
"
---
ND
---
---
---
30%
ND
---
1.00
"
"
---
ND
---
---
---
30%
ND
---
1.00
"
"
---
ND
---
---
---
30%
ND
---
0.500
"
"
---
ND
---
---
---
30%
ND
---
0.500
"
"
---
ND
---
---
---
30%
Recovery: 102 %
Limits: 80-120 %
Dilution: 1x
99 %
80-120 %
"
102 %
80-120 %
"
98 %
80-120 %
"
Toluene-d8 (Surr)

EPA 8260B
Benzene
20.8
---
0.200
ug/L
20.0
ND
104
70-130%
---
---
Toluene
21.5
---
1.00
"
"
"
ND
108
"
---
---
Ethylbenzene
21.8
---
0.500
"
"
"
ND
109
"
---
---
DRAFT REPORT
Page 12 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Analyte
Result
MDL
Reporting
Limit
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
Batch 6020841 - EPA 5030B

Xylenes, total
65.0
---
1.50
ug/L
"
60.0
ND
108
"
---
---
Naphthalene
16.8
---
2.00
"
"
20.0
ND
84
"
---
---

(MTBE)
Isopropylbenzene
19.3
---
1.00
"
"
"
ND
96
"
---
---
22.2
---
1.00
"
"
"
ND
111
"
---
---
n-Propylbenzene
20.8
---
0.500
"
"
"
ND
104
"
---
---
20.8
---
1.00
"
"
"
ND
104
"
---
---
21.0
---
1.00
"
"
"
ND
105
"
---
---
21.6
---
0.500
"
"
"
ND
108
"
---
---
20.5
---
0.500
"
"
"
ND
102
"
---
---
Recovery: 100 %
Limits: 80-120 %
Dilution: 1x
97 %
80-120 %
"
Toluene-d8 (Surr)
99 %
80-120 %
"
97 %
80-120 %
"
DRAFT REPORT
Page 13 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
Source
Result
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
EPA 8270D (SIM)
Acenaphthene
ND
---
0.0364
ug/L
---
---
---
---
---
---
Acenaphthylene
ND
---
0.0364
"
"
---
---
---
---
---
---
Anthracene
ND
---
0.0364
"
"
---
---
---
---
---
---
Benz(a)anthracene
ND
---
0.0364
"
"
---
---
---
---
---
---
Benzo(a)pyrene
ND
---
0.0364
"
"
---
---
---
---
---
-----
ND
---
0.0364
"
"
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
Chrysene
ND
---
0.0364
"
"
---
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
Dibenzofuran
ND
---
0.0364
"
"
---
---
---
---
---
---
Fluoranthene
ND
---
0.0364
"
"
---
---
---
---
---
---
Fluorene
ND
---
0.0364
"
"
---
---
---
---
---
---
ND
---
0.0364
"
"
---
---
---
---
---
---
1-Methylnaphthalene
ND
---
0.0727
"
"
---
---
---
---
---
---
2-Methylnaphthalene
ND
---
0.0727
"
"
---
---
---
---
---
---
Naphthalene
ND
---
0.0727
"
"
---
---
---
---
---
---
Phenanthrene
ND
---
0.0364
"
"
---
---
---
---
---
---
Pyrene
ND
---
0.0364
"
"
---
---
---
---
---
---
---
Recovery: 97 %
Limits: 44-120 %
Dilution: 1x
126 %
50-133 %
"
LCS (6020838-BS1)
EPA 8270D (SIM)
Acenaphthene
6.88
---
0.0400
ug/L
8.00
---
86
47-122%
---
Acenaphthylene
6.99
---
0.0400
"
"
"
---
87
41-130%
---
---
Anthracene
7.45
---
0.0400
"
"
"
---
93
57-123%
---
---
Benz(a)anthracene
7.32
---
0.0400
"
"
"
---
92
58-125%
---
---
Benzo(a)pyrene
7.90
---
0.0400
"
"
"
---
99
54-128%
---
---
7.86
---
0.0400
"
"
"
---
98
53-131%
---
---
8.18
---
0.0400
"
"
"
---
102
57-129%
---
---
DRAFT REPORT
Page 14 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
Notes
Water
LCS (6020838-BS1)
Source
Result
6.28
---
0.0400
"
"
"
---
78
50-134%
---
---
Chrysene
7.23
---
0.0400
"
"
"
---
90
59-123%
---
---
7.25
---
0.0400
"
"
"
---
91
51-134%
---
-----
Dibenzofuran
7.12
---
0.0400
"
"
"
---
89
53-120%
---
Fluoranthene
7.07
---
0.0400
"
"
"
---
88
57-128%
---
---
Fluorene
7.17
---
0.0400
"
"
"
---
90
52-124%
---
---
6.66
---
0.0400
"
"
"
---
83
52-133%
---
---
1-Methylnaphthalene
6.48
---
0.0800
"
"
"
---
81
41-120%
---
---
2-Methylnaphthalene
6.84
---
0.0800
"
"
"
---
85
40-121%
---
---
Naphthalene
6.62
---
0.0800
"
"
"
---
83
"
---
---
Phenanthrene
7.43
---
0.0400
"
"
"
---
93
59-120%
---
---
Pyrene
7.02
---
0.0400
"
"
"
---
88
57-126%
---
---
Recovery: 91 %
Limits: 44-120 %
Dilution: 1x
112 %
50-133 %
"
Q-19
EPA 8270D (SIM)
Acenaphthene
6.36
---
0.0400
ug/L
8.00
---
80
47-122%
30%
Acenaphthylene
6.48
---
0.0400
"
"
"
---
81
41-130%
30%
Anthracene
7.06
---
0.0400
"
"
"
---
88
57-123%
30%
Benz(a)anthracene
7.19
---
0.0400
"
"
"
---
90
58-125%
30%
Benzo(a)pyrene
7.78
---
0.0400
"
"
"
---
97
54-128%
30%
8.07
---
0.0400
"
"
"
---
101
53-131%
30%
7.91
---
0.0400
"
"
"
---
99
57-129%
30%
6.03
---
0.0400
"
"
"
---
75
50-134%
30%
Chrysene
7.16
---
0.0400
"
"
"
---
89
59-123%
30%
7.05
---
0.0400
"
"
"
---
88
51-134%
30%
Dibenzofuran
6.67
---
0.0400
"
"
"
---
83
53-120%
30%
Fluoranthene
6.63
---
0.0400
"
"
"
---
83
57-128%
30%
Fluorene
6.79
---
0.0400
"
"
"
---
85
52-124%
30%
6.49
---
0.0400
"
"
"
---
81
52-133%
30%
1-Methylnaphthalene
5.81
---
0.0800
"
"
"
---
73
41-120%
11
30%
DRAFT REPORT
Page 15 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Analyte
Result
Reporting
Limit
MDL
Units
Dil.
Spike
Amount
%REC
%REC
Limits RPD
RPD
Limit
2-Methylnaphthalene
6.05
Naphthalene
Phenanthrene
Pyrene
---
0.0800
"
"
"
---
76
5.95
---
0.0800
"
"
"
---
7.07
---
0.0400
"
"
"
---
6.59
---
"
"
"
---
0.0400
Recovery: 83 %
Limits: 44-120 %
Dilution: 1x
113 %
50-133 %
"
DRAFT REPORT
Notes
Water
Source
Result
Q-19
40-121%
12
30%
74
"
11
30%
88
59-120%
30%
82
57-126%
30%
Page 16 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
Prep: EPA 5030B

Lab Number
Matrix
Method
Sampled
Prepared
02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
Batch: 6020841
A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05
Water
Water
Water
Water
Water
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
1.00
1.00
1.00
1.00
1.00

Lab Number
Matrix
Method
Sampled
Prepared
02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
Sample
Default
RL Prep
Initial/Final
Initial/Final
Factor
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
0.98
1.01
1.05
1.02
1.10
Batch: 6020838
A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05
Water
Water
Water
Water
Water
EPA 8270D (SIM)

EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
DRAFT REPORT
1020mL/2mL
990mL/2mL
950mL/2mL
980mL/2mL
910mL/2mL
Page 17 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
Reported:
02/29/16 17:54

Qualifiers:
Q-19
analysis.

DET
Analyte DETECTED
ND
NR
Not Reported
dry
RPD
MDL
WMSC
Batch
QC
Blank
Policy
---
Spikes, etc.
***
DRAFT REPORT
Page 18 of 19

Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax
Apex Labs
NRC-CB&I
6211 N Ensign St
Portland, OR 97217
DRAFT REPORT
Reported:
02/29/16 17:54
Page 19 of 19
AppendixB
BiostimulationProductInformation
Overview'of'OSE'II!
OSE$II:$
! Invented$in$1989.$$
! Manufactured$in$the$USA.$
! Used$in$more$than$40$countries$across$the$world.$$
! Remediated$more$than$28,000$spills$and$contaminated$sites.$
$
$
Features$of$OSE$II$include:$
! 100%$biodegradable$and$nonItoxic.$
! Effective$in$remediating$all$types$of$hydrocarbons$$fresh$and$weathered.$
! Easily$applied$and$no$need$for$special$protective$clothing.$
! Effective$in$a$large$range$of$temperatures.$
! Enhances$natures$process$for$bioIremediating$hydrocarbons.$
How$OSE$II$works:$
Process'and'benets!
When$combined$with$fresh$or$salt$water,$OSE$II$breaks$down$the$molecular$
structure$of$hydrocarbons$through$the$effects$of$bioIsurfactants,$followed$
by$enzymes$developing$protein$binding$sites$and$acting$as$a$catalyst,$while$
enhancing$indigenous$bacteria$to$rapidly$colonize.$$$
$
The$enhanced$bacteria$use$the$detoxiSied$hydrocarbons$as$a$food$source$via$
the$enzymatic$catalyst,$digesting$the$hydrocarbon$based$material$to$carbon$
dioxide$and$water.$
BeneSits$of$using$OSE$II:$$
!
Remediating$hydrocarbon$contaminated$soil,$water$and$waste.$$
The$toxins$and$contaminants$are$removed$from$the$environment,$
not$transferred.$
Cleaning$up$oil$spills$/$contaminated$areas$without$having$to$
separate$and$dispose$of$hydrocarbon$contaminated$waste.$$$
OSE$II$is$effective$in$cleaning$large$contaminated$sites$enabling$
land$to$be$returned$to$preIspill$conditions$and$re#vegetated$and$
restored$for$beneSicial$use.$$$
Kadhema$ScientiSic$Consultancy$&$Services$will$manage$the$
revegetation$for$the$project.$
Its$ability$to$be$used$in$sensitive$environments$as$it$is$nonI
hazardous$and$can$be$applied$in$a$variety$of$ways$preventing$
physical$damage$as$a$result$of$access$to$difSicult$to$reach$
locations.$
Comparing'OSE'II'with'tradi;onal'methods!
Excavation$
Contaminated$materials$are$
dug$up$and$loaded$into$trucks$
for$transport$I$expensive$
process$and$risks$associated$
with$transporting$hazardous$
waste.$
Dust$is$generated$from$the$
excavation$and$truck$
movements.$
Waste$requires$disposal$at$
facility$licensed$to$receive$
hazardous$waste.$$Expensive$
to$dispose$of$hazardous$waste$
I$limited$facilities$available.$
Equipment$used$for$
extraction$must$be$thoroughly$
cleaned$and$decontaminated$
prior$to$leaving$the$site.$
Digging$up$and$hauling$off$
soil$/$sand$may$have$impacts$
on$local$ecology.$
Incineration$
Requires$extremely$high$
temperatures$(therefore$
energy)$to$break$down$
contaminants$into$nontoxic$
substances,$such$as$water,$
carbon$dioxide,$and$nitrogen$
oxides.$
Unlikely$that$100%$of$the$
hazardous$waste$is$destroyed$
during$the$incineration$
process.$
Leftover$ash$and$material$
removed$from$the$incinerator$
is$hazardous$and$requires$
disposal$at$a$facility$licenced$
to$receive$hazardous$waste.$
Air$emissions$and$odour$
possible$if$process$is$not$
efSicient.$
Thermal$desorption$
Extreme$safety$precautions$
required$due$to$elevated$
heating$at$the$site.$
Responders$need$to$wear$
special$protective$gear.$
Size$of$particles$can$restrict$
clean$up,$or$produce$a$
secondary$required$process.$
Bioremediation$OSE$II$
No$speciSic$precautions$need$
to$be$taken.$
No$speciSic$protective$clothing$
required$when$handling$OSE$
II.$
Particle$size$does$not$affect$
remediation.$
No$vapours$emitted.$
Harmful$vapours$given$off$
that$need$to$be$captured$for$
secondary$processing.$
Soil$needs$reprocessing$to$
complete$removal$of$
contaminants.$
Area$to$be$heated$up,$or$
mobile$unit$has$limitations$of$
size$or$amount$of$soil$to$be$
addressed$at$one$time.$
Potentially$higher$risks$and$
insurance$costs.$
In$relation$to$soil.$$Sterilizes$
soil,$making$it$virtually$
useless.$
OSE$II$is$a$oneItime$
application$and$treats$
contamination$at$the$source.$$
No$disposal$of$waste$is$
required.$
OSE$II$can$be$applied$to$an$
indeSinite$area.$
Emulates$natures$process$
allowing$soil$to$be$returned$to$
pre$contamination$conditions,$
converting$soil$into$a$valuable$
top$soil$for$resale.$
Tes;ng'&'approval'across'the'world'!
Extensive$efSicacy$and$toxicity$testing$have$contributed$to$OSE$II$being$recognized$as$an$effective$oil$spill$and$
bioremediation$product$and$is$approved$for$the$following:$
!
Regional$Organization$for$the$Protection$of$the$Marine$Environment$(ROPME)$Marine$Emergency$Mutual$
Aid$Centre$(MEMAC)$Oil$Spill$Combating$Product$(approval$Ref:$337/12IRHD).$$This$includes:$
o State$of$Kuwait$
o State$of$Oman$
o State$of$Qatar$
$
$
$
$
$
$
o Kingdom$of$Saudi$
o United$Arab$Emirates$
o Kingdom$of$Bahrain$
o Islamic$Republic$of$Iran$
o Republic$of$Iraq$
US$Environmental$Protection$Agencys$National$Contingency$Plan$for$Oil$Spills$(US$EPA$NCP$#$B53).$
UK$Marine$Management$Organization$(ODA$241/2015).$
Australian$Maritime$Safety$Authoritys$National$Plan$to$Combat$the$Pollution$of$the$Sea$by$Oil$and$Other$
Noxious$and$Hazardous$Substances$(#OBA$Bioremediation$Oil$Spill$Control$Agent).$
New$Zealand$Environment$Protection$Authority,$Status$of$Substance$(SOS$#1001797).$
Greece$(ID$no:$17554);$Philippines$(accreditation$#PCGI14I06I112);$Nigeria$(NOSDRA$cert:$189);$Mexico;$
Israel;$Trinidad$and$Tobago;$and$South$Korea$(cert$no:$SI007).$$
$$
Business'case'for'OSE'II!
OSE$II$is$suited$to$large$contaminated$areas$due$to$the$ease$of$application$and$ability$to$treat$
contaminated$soil$at$the$source.$
$$
The$following$expenses$are$eliminated$when$OSE$II$is$used:$
! Clean$up$and$/$or$disposal$of$equipment$and$material$contaminated$with$hydrocarbons.$
! Treatment$of$contaminated$soil,$contaminated$water,$oily$sludge$or$mud$prior$to$disposal.$
! Extraction,$transport$and$disposal$of$contaminated$soil$(including$mud,$sludge)$and$water.$
$$
The$following$risks$are$eliminated$when$OSE$II$is$used:$
! Accidental$release$and$spill$during$transit$to$waste$facility.$
! Contaminants$not$completely$removed$from$the$environment$resulting$in$long$term$impact.$
! Having$to$relocate$the$contaminated$soil$for$treatment$at$another$facility.$
$$
Conclusion!
Clean$up$using$OSE$II$will$return$contaminated$land$to$pre$spill$conditions,$suitable$for$reI
vegetating$and$restoring.$$
OIL SPILL EATER II | NCP Product Schedule | Emergency Management | US EPA
Page 1 of 4
Emergency Management
You are here: EPA Home Emergency Management
Schedule OIL SPILL EATER II
NCP Subpart J
NCP Product
OIL SPILL EATER II
TECHNICAL PRODUCT BULLETIN #B-53

USEPA, OFFICE OF EMERGENCY MANAGEMENT
REGULATION AND POLICY DEVELOPMENT DIVISION
ORIGINAL LISTING DATE: AUGUST 26, 1996
REMOVAL DATE: AUGUST 16, 2005
RELISTING DATE: SEPTEMBER 18, 2009
"OIL SPILL EATER II (OSE II)"
I. NAME, BRAND, OR TRADEMARK
OIL SPILL EATER II (OSE II)
Type of Product: Bioremediation Agent (Biological Enzyme Additive [previously listed as a
Nutrient Additive])
II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
OSEI Corporation (Formerly Sky Blue Chems)
P.O. Box 515429
Dallas, TX 75251-5429
Phone: (972) 669-3390
E-mail: oseicorp@msn.com
Web Site: www.osei.us
(Mr. Steven Pedigo, Chairman, CEO, Inventor)
III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
OSEI Corporation (Formerly Sky Blue Chems)
P.O. Box 515429
Dallas, TX 75251-5429
Phone: (972) 669-3390
E-mail: oseicorp@msn.com
Web Site: www.osei.us
(Mr. Steven Pedigo, Chairman, CEO, Inventor)
IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION
1. Flammability: Water-based, non-flammable
2. Ventilation: Needs no ventilation; aqueous-based product; does not emit hazardous
vapors
3. Skin and eye contact; protective clothing; treatment in case of contact: OSE II is not a
primary dermal irritant. Avoid eye contact, and wear goggles if possible for the spray to
come in direct contact with eyes. Facilities for quick and copious eye flushing should be
provided and prompt medical attention should be sought if exposure and irritation persists.
Protective rubber gloves are suggested during handling. Before mixing the product has a
smell of fermentation. The product does not give off any harmful vapors.
4.a. Maximum storage temperature: 120F
http://www.epa.gov/emergencies/content/ncp/products/oseater.htm
4/3/2011
Page 2 of 4
4.b. Minimum storage temperature: None; OSE II can freeze and thaw without adverse
effects
4.c. Optimum storage temperature range: 72F
4.d. Temperatures of phase separations and chemical changes: 120F
V. SHELF LIFE
OSE II has a recommended shelf life of 5 years. After 5 years at optimum storage
temperature, there is an approximate 10% decrease per year in product capability.
VI. RECOMMENDED APPLICATION PROCEDURE
1. Application Method:
A. Use surface spray apparatus, such as small hand held tanks, back pack, large mixing
tanks with mechanical pumping devices, vessels with booms for spraying wide paths, or
spray devices on airplanes or helicopters.
B. OSE II can be applied by eductor systems from vessels, fire trucks, etc. Set the eductor
system to 2% and apply 1 gallon of mixed OSE II to each spilled gallon of hydrocarbon.
2. Concentration/Application Rate:
General - OSE II generally takes 3 to 30 minutes to penetrate the molecular walls of
hydrocarbons. However, once you spray OSE II on the hydrocarbons, OSE II attaches itself
and will eventually engulf the hydrocarbons regardless of where the hydrocarbons may
spread on the surface of salt or fresh water. Additionally, once you spray OSE II, the
hydrocarbons cannot attach itself to the shoreline, rocks, or any equipment in its path. OSE
II breaks down the adhesion properties of hydrocarbons and causes hydrocarbons to float,
thereby, eliminating secondary contamination of the water column or any other areas, and
holding the contaminated area to the waters surface, the original contaminated area.
If OSE II is to be used on ocean spills or on intertidal zones OSE II should be mixed
with ocean water.
If OSE II is to be used on lakes, rivers, streams, ponds, or on land mix the product
with water from a lake, stream, or pond.
If you are performing a clean up, make sure the water used to mix with OSE II, and
the water used to keep the area saturated, is the type of water normally associated
with that area.
If you use fresh water in an area normally contacted with salt water or vice versa,
the different types of bacteria and competition could occur, not to mention the
problems with salinity for fresh water organisms.
[Note: Do not mix tap water with OSE II if possible: Chlorine in tap water slows bacterial
enhancement]
Spills on Water:
Dilute each gallon of OSE II with 50 gallons of fresh, brackish, or salt water - depending on
the water associated with the area that has been impacted by the spill. Apply OSE II at a
ratio of 1 gallon mixed OSE II to each gallon of hydrocarbon spilled. Apply using hand held
sprayers, tank sprayers, booms from vessels, helicopters, or airplanes; by spraying the
perimeter first then working toward the middle of the spilled area. Next spray the entire
surface of the spill. If the spill is very heavy (more than 2 inches thick) it is recommended
that OSE II be applied every day until you have met a 1:1 ratio of OSE II and water
mixture to spilled oil/hydrocarbons.
Use 1 gallon OSE II for every 50 gallons of hydrocarbons.
Use 1 drum of OSE II for every 2,750 gallons of hydrocarbons.
If you know gallons of hydrocarbons spilled, multiply gallons of hydrocarbons by
0.02 to get amount of OSE II needed [gallons of hydrocarbons x 0.02 = gallons of
OSE II].
If you know barrels of crude oil spilled, multiply barrels of crude oil by 0.015 to get
drums of OSE II needed [barrels of crude oil x 0.015 = drums of OSE II].
If you do not know gallons of hydrocarbons or barrels of crude oil, multiply size of
spill by 0.0023 to get drums of OSE II needed or by 0.12 to get gallons of OSE II
4/3/2011
Page 3 of 4
needed [(yards long x yards wide x inches thick) x 0.0.0023 = drums of OSE II or
(yards long x yards wide x inches thick) x 0.015 = gallons of OSE II].
Intertidal Zone:
Mix each 55 gallon drum of OSE II with 2,750 gallons of fresh, brackish, or salt water. The
water used is determined by the type of water associated with the site. OSE II should be
applied as the tide recedes (if there is a tide) and once the tide comes in the application
should cease until the tide recedes again. Additional applications should only be warranted
if spill has been allowed time to percolate into the depths of the soil.
If there is no tide, but waves have pushed the spill into the intertidal zone, then there will
be direct access to the spill at all times. If possible use string or stakes to grid off the beach
or intertidal zone area, and then you can calculate how much premixed OSE II to apply to a
given area. If unable to grid off an area then calculate how much OSE II to apply and then
determine how much premixed OSE II will flow through a nozzle (gallons per minute) then
let application technician know how many gallons to apply in a given area and this can be
determined by applying product for a certain time period to get the correct amount of OSE
II applied to gain the 1:1 ratio.
Note: If the intertidal zone is associated with the sea then mix OSE II with salt water. If the
spill area is in an area of brackish water then mix OSE II with brackish water. If the
intertidal zone is associated with fresh water such as lakes, rivers, streams, ponds, creeks,
aquifers, or drinking water wells then use fresh water to mix OSE II.
3. Conditions for Use:
OSE II can remediate hydrocarbon-based material including chlorinated
hydrocarbons, PCB's, dioxins, and some pesticides.
As the age of spilled hydrocarbons increases, the time necessary for bioremediation
increases. In general, fresh crude, gasoline of BTEX takes from 72 hours to 30 days
to completely bioremediate.
Variations of sea water salinity should have no effect, but as long as microbial life
can exist, then OSE II will be effective.
OSE II bioremediation slows somewhat at temperatures below 40F. OSE II
however, will continue to work at any liquid water temperature that will sustain
microbial life.
VII. TOXICITY AND EFFECTIVENESS

a. Effectiveness:
Summary Data Table:
PRODUCT
TOTAL MEAN
DAYS
3
ALKANES
REPS/PROD
(ppm)
RED%
28
DAYS
TOTAL MEAN
AROMATICS
(ppm)
RED%
28
DAYS
CONTROL
NUTRIENT
OSE II
43,170
40,569
41,730
11,435
11,785
12,155
CONTROL
NUTRIENT
OSE II
39,250
34,815
26,316
9.1
14.2
36.9
10,355
9,898
8,072
9.4
16.0
33.6
28
CONTROL
NUTRIENT
OSE II
35,797
26,507
4,273
17.1
34.7
89.8
9,534
8,938
1,268
16.6
24.2
89.6
Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
4/3/2011
Control: 16.5%
Nutrient: 52.0%
Product: 85.4%
Page 4 of 4
Last updated on Thursday, January 27, 2011
VIII. MICROBIOLOGICAL ANALYSIS

1. Listing of each component of the total formulation, other than enzymes, by chemical
name and percentage by weight: CONFIDENTIAL
2. Enzyme Names: CONFIDENTIAL
3. I.U.B.: CONFIDENTIAL
4. Source of Enzymes: Fermentation process
5. Units: No less than 1% and no more than 50% by weight
6. Specific Gravity: 1.05
7. Optimum Conditions:
a.
b.
c.
d.
e.
f.
pH: 7.0
Temperature: 72F
Salinity Ranges: Fresh water to salt water
Maximum and Minimum pH: 3.5 - 8.0
Maximum and Minimum Temperature: 28F - 128F
Maximum and Minimum Salinity Levels - Salinity level above that will support
microbial activity will adversely effect OSE II's performance
g. Enzyme Shelf Life: Up to 5 years when properly stored
h. Enzyme Optimal Storage Conditions: 72F is optimal, enzyme range is freezing to
120F, never leave OSE II in direct sunlight for more than a couple of hours
IX. PHYSICAL PROPERTIES

NA
X. ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED HYDROCARBONS
NA
4/3/2011
23
US Safety Data Sheet

Issued: June 1, 2015
1. IDENTIFICATION OF THE SUBSTANCE PREPARATION AND
COMPANY
Product Name:
Oil Spill Eater II, OSE II
Product Code, GHS code:

(Export Code)
3821000000
Product Type:
Hydrocarbon Bioremediation Product
Supplier:
Oil Spill Eater International Corporation
Address:
P.O. Box 515429

Dallas, Texas 75251
USA
Contact Numbers:
Telephone:
(972) 669-3390
Fax:
(469)241-0896
E-mail:
oseicorp@msn.com
Emergency Telephone Number:
(972) 669-3390
Emergency Covers:
24 hours a day 7 days a week
2. HAZARDOUS IDENTIFICATION
Human Health Hazards:
None. Potentially toxic if more than 1liter

ingested.
Safety Hazards:
Will not burn. Is, in fact, a fire retardant.
Environmental Hazards:
None. Protects environment;100%biodegradable;

no known allergens.
Page 2 of 9 US Safety Data Sheet
3. COMPOSITION INFORMATION ON INGREDIENTS

Preparation Description:
A hydrocarbon bioremediation product containing

all natural nonhazardous ingredients.
Contains:
Ingredient
CAS Number
80-90%
7732-18-5
1) Water
2) Nitrogen (Urea)
0.01-0.09% 57 -13-6
3) Molasses
1-2%
None
4) Bio Surfactant
0.06-0.08% 68131-40-8
5) Sugar
1.5%-2%
50-99-7
6) Protease
0.01-0.03% 9000/90/2
7) Amylase
0.01-0.03% 9014-01-1
8) Malt
1-2%
8029-43-4
4. FIRST AID MEASURES

Symptoms and Effects:
Prolonged exposure would have minimal effect,

if any at all.
First Aid - Inhalation:
Inhalation of vapors from this product pose

no acute or chronic hazard.
First Aid - Skin:
Prolonged exposure to skin may cause some

drying of the skin. Wash off with water.
First Aid - Eye:
Flush eyes with copious quantities of water. If

irritation persists, seek medical attention.
First Aid - Ingestion:
If less than 59 ml / 2 ounces is ingested, no toxic

symptoms should occur, to most humans
Wash out mouth and seek medical attention if
more than59ml or 2 ounces is ingested.
Advice to Physicians:
Treat symptomatically. Wash skin or eyes

thoroughly. Treat as you would for any large
ingestion of mild soap or tooth paste.
5. FIRE FIGHTING MEASURES

Specific Hazards:
OSE ll is a fire retardant. However, if applied to

a burning fire, there can be a slight flash before
fire goes out.
Extinguishing Media:
None required. Product is a fire retardant.

Method - ASTM-D56.
Unsuitable Extinguishing Media:
None required. Product is a fire retardant.

Protective Equipment:
Proper protective equipment including breathing

apparatus must be worn when approaching any
fire.
6. ACCIDENTAL RELEASE MEASURES

Personal Precautions:
Avoid contact with eyes. Wash from skin or

eyes as needed.
Personal Protection:
Wear goggles if applying in windy conditions.

Wear protective rubber gloves if applying
directly in a prolonged situation.
Environmental Precautions:
Wash down with water. Will help clean soil,

drains, or water.
Clean-up methods - small spillage:
Wash down with water. Non-toxic to the

environment.
Clean-up methods - large spillage:
Same as for small spills.
7. HANDLING AND STORAGE

Handling:
When handling product in drums, safety

Footwear should be worn. However No
special handling procedures required.
Storage:
Keep in cool, dry area. A void direct sunlight

and excessive heat.
Storage Temperatures:
Do not store where temperature exceeds

120 F.
Recommended Materials:
Polyethylene drums or PVC are acceptable.
Unsuitable Materials:
None known.
Other Information:
Product can freeze / thaw without any negative

effect on product.

8. EXPOSURE CONTROL/PERSONAL PROTECTION
Occupational Exposure Standards:
None established (none toxic).
Hygiene Measures:
Wash hands before eating or drinking.
Respiratory Protection:
Not normally required.
Hand Protection:
Any plastic or rubber glove if needed; not

normally required.
Eye Protection:
Wear safety glasses or goggles if applying

in windy conditions.
Body Protection:
Not normally required.
9. PHYSICAL AND CHEMICAL PROPERTIES

Physical State:
Liquid with the same density of H20.
Color:
Amber to brown .
Odor:
Some smell of ferment.
Vapor Pressure:
Same as H20.1.0215
Density:
Same as H20. 1.0215
Vapor Density:
Same as H20. 1.0215
Dropping Point:
Same as H20.
Flash Point:
Same as H20 in excess of 7000 F.
Flammability Limit - Lower:
Nonflammable.
Flammability Limit - Upper:
Nonflammable.
Auto-ignition Temperature:
Non-igniting
Solubility in Water:
100%
N-octanol/water Partition Coefficient:
100% soluble - non partitioning
Elements Content:
None.

10. STABILITY REACTIVITY
Stability:
Stable.
Conditions to Avoid:
Temperatures in excess of 120 F and

direct sunlight during storage or transporting.
Materials to Avoid:
Strong oxidizing agents.
Hazardous Decomposition Products:
None decomposes to CO2 and H20.
11. TOXICOLOGICAL INFORMATION

Basis for Assessment:
Toxicity tests have been performed

Determining OSE II is (virtually nontoxic).
Acute Toxicity - Oral:
Can become toxic if more than 60 ml ot 2

ounces is ingested.
Acute Toxicity - Dermal:
None.
Eye Irritation:
Slight irritant alleviated by copious eye

washing.
Skin Irritation:
Skin can dry slightly if prolonged direct

exposure occurs.
Respiratory Irritation:
Virtually none.
Skin Sensitization:
Not expected to be a skin sensitizer.
(Sub )chronic Toxicity:
None expected.
Carcinogenicity:
Not a carcinogen.
Mutagenicity:
Not a mutagenic.
Human Effects:
None expected.
Other Information:
Not applicable.
12. ECOLOGICAL INFORMATION

Basis for Assessment:
Ecotoxicological data has been determined

specifically for this product. Information
given is for specific sensitive (aquatic)
species in fresh and salt water.

Mobility:
Liquid that floats on water and solubilizes

rapidly. If it comes in contact with soil
will percolate at the same rate as H20 and
will biodegrade rapidly.
PersistencelDegradability:
Product completely biodegrades in water

or soil environments and will not persist.
100% biodegradable as testing has
confirmed
Bioaccumulation:
None
Ecotoxicity:
US EAP
100% soluble.
LC50 Brine shrimp: >1,900
mg/l up to 10,000 mg/l.
LC50 Fundulus Heterocletus
96 hour: 5,258 mg/l.
Environment Canada
LC50 Rainbow Trout:10,000
mg/l.
OSEI with the city of Plano Tx LC50 Fathead Minnows
(Pimephale promelas): 9,300
mg/l.
Australia NATA test results:
IC10(milky oyster,
Saccostrea echinata): 11.0
(10.0-11.9)mg/l/48h
EC50(milky oyster,
Saccostrea echinata): 16.5
(16.0-17.1)mg/l/48h
NOEC(milky oyster,
Saccostrea echinata):
10.0mg/l
LOEC(milky oyster,
Saccostrea echinata):
20.0mg/l
EC10(mussel, Mytilus
galloprovincialis):
>20.0mg/l/72h
EC50(mussel, Mytilus
galloprovincialis):
>20.0mg/l/72h
NOEC(mussel, Mytilus
galloprovincialis):
20.0mg/l
LOEC(mussel, Mytilus
galloprovincialis):
>20.0mg/l

13. DISPOSAL CONSIDERATIONS
Waste Disposal:
No special disposal.
Product Disposal:
Container Disposal:
Local Legislation:
Not applicable.
14. TRANSPORT INFORMATION
Not dangerous for conveyance under UN, IMO, ADRiRID.

Marine Transport (IMO/IMDG): Not classified as Dangerous
Goods by the criteria of the International Maritime
Dangerous Goods Code (IMDG Code) for transport by sea.
Air Transport (ICAO/IATA): Not classified as Dangerous
Goods by the criteria of the International Air Transport
Association (IATA) Dangerous Goods Regulations for
transport by air.
IMDG Marine No
15. REGULATORY INFORMATION
EC Classification:
Not Known.
EC Symbols:
Not Known.
EC Risk Phrases:
Not Known.
EINECS (EC):
Not Known.
TSCA (USA):
Other Information:
US DOT class 55 non hazardous
Dangerous Constituents:
None.

16. OTHER INFORMATION
Only bioremediation product successfully used to permanently remove oil on U.S. navigable
waters under U.S. EPA Government observation.
Government approvals or approved listings:
!!
!
!
!
!
!
US!EPA!NCP!#!B53,!!
New!Zealand!EPA!SOS # 1001797,
Australia #OBA
Oil Spill Control agent Greek registration ID
no:17554
Gulf States MEMAC approval Ref:337/12RHD,
Philippine accreditation #PCG-14-06-112
Nigeria NOSDRA cert: 189,
Mexico Coatzacoalcos.Ver.,a 30 de Julio de
2014,
Israel approval,
UK approval #ODA 241/2015 ,
Trinidad and Tobago approval#
MEEA:12.1.5 Vol. XXXXII, South Korea cert
no: S-007 !
Uses and Restrictions:
Bioremediation product that converts

hydrocarbons, chlorinated
hydrocarbons,
and most organic based material or
waste to CO2 and H20.
Technical Contact Point:
Steven Pedigo
Technical Contact Number:
(972) 669-3390
Fax Number:
(469) 241-0896
E-Mail:
oseicorp@msn.com
SDS History:
Not Applicable
Revisions Highlighted
None.

!
last!revision!of!SDS!
Literature!References!
SDS Created: June 2015
Preparation of Safety Data Sheets for Hazardous Chemicals
Code of Practice. Standard for the Uniform Scheduling of
Medicines and Poisons. Australian Code for the Transport of
Dangerous Goods by Road & Rail. Model Work Health and
Safety Regulations, Schedule 10: Prohibited carcinogens,
restricted carcinogens and restricted hazardous chemicals.
Workplace exposure standards for airborne contaminants,
Safe work Australia. American Conference of Industrial
Hygienists (ACGIH). Globally Harmonised System of
classification and labelling of chemicals. ...End Of
MSDS...
!
!
Written and Compiled

by the
Science & Technology Advisory Board

Marynette Herndon, Environ Eng, REM (Registered Environmental Manager),
CHMM (Certied Hazardous Materials Manager)
President, Herndon & Associates, Inc.
Chairperson, LAEO Science & Technology Advisory Board
Paul W. Sammarco, PhD
Professor and Senior Scientist
Louisiana Universities Marine Consortium (LUMCON)
Alex Nicholson, Mech Eng, MBA, PE
Former NASA Aerospace Engineer
Environmental Specialist
Jeanne Pascal, Esq
EPA Northwest District Debarment Counsel, retired (19842010)
Former in-house EPA attorney for oil spill relief
Barbara Wiseman
International President
Lawrence Anthony Earth Organization
Diane Wagenbrenner
Advisory Board Member
Lawrence Anthony Earth Organization
Identication of Nontoxic Methods

for Contingency Plans
The establishment and enactment of new
contingency plans associated with remediation
of oil spills (including those response plans
submitted by oil companies requesting permits)
is urgently needed, using methodologies other
than intensive application of chemical dispersants. The commencement and acceleration
of new deep-water drilling in the Gulf of
Mexico and the Beaufort Sea in Alaska, for
instance, particularly in the absence of
updated contingency plans in the event of
a spill, is quite concerning. In other words,
hundreds of permits have been issued since
September 2010 with no signicant change in
spill contingency planningother than more
advanced deep-water dispersant injection
systems that have been added to plans, which
would produce a repeat of the Deepwater
Horizon toxic response.
The information presented here is for distribution to Regional/Area Committees and all
stakeholders responsible for maintaining upto-date contingency plans for safeguarding our
aquatic, marine, and terrestrial environments.
The article included regarding bioremediation
category denitions and their modes of action,
along with further information below, should overwrite previous guidance on bioremediation
because it clarifies use of the Bioremediation
Agent EA Type as a FIRST-RESPONSE agent.
Bioremediation Agent Enzyme Additive

Type can clearly serve as a rst-response
alternative to the use of chemical
dispersants, which no longer have a
place in modern-day oil spill cleanup in
US navigable waters.
NCP-Listed Bioremediation Agent

(EA Type) as a Solution and
Alternative to Chemical Dispersants
We encourage independent investigation of
EA Type as a promising potential solution to
oil spill response in deep-water drilling and
difcult access environments, particularly as a
rst-response method for open-water oil spills,
in lieu of chemical dispersants of any kind.
It is the position of the Science & Technology
Advisory Board of the Lawrence Anthony
Earth Organization that Bioremediation Agent
Enzyme Additive Type can clearly serve as a
rst-response alternative to the use of chemical dispersants, which no longer have a place
in modern-day oil spill cleanup in US
navigable waters.
The EPA is now being pressed to nd safer
response agents to replace these outdated
modes, which, when combined with oil
pollutants, are more toxic than the oil itself
and therefore contrary to the intent of the US
Clean Water Act (CWA).29 To reiterate, the
CWA stipulates that, for a response method
to be utilized, it must REMOVE oil from the
environment. Dispersants do not fulll this
requirement; in fact, studies have shown that
use of dispersants prolongs the time that oil
plus chemical dispersants remain in the
environment, resulting in adverse impacts to
ora and fauna for up to ve years or longer.30,31
The good news is that there are developed
protocols for identifying and assessing
the degree of usefulness of spill-response
products, and they are not complicated.
20
How Oil Spill Cleanup Products

Should Be Assessed and Prioritized
Its use and application must be economically

reasonable and within acceptable ranges of
expected remediation costs.
The LAEO has conducted nearly three years Eliminates or signicantly reduces the
of research to nd methods for remediating
necessity for secondary cleanup, such as
oil spills that are more effective and less toxic
cleaning up tar mats formed by sinking the
than those currently used. We have also been
oil using dispersants, disposal of hydroworking to gain the necessary authorizations
carbon-based material in landlls, or other
for utilizing these more effective techniques to
methods of disposal.
clean up the waters of the Gulf and its shorelines
Our extensive search revealed only one product
still impacted by the Macondo spill.
that fullled all of these requirementsone
Our rst step was to vet the applicable products under the Bioremediation subcategory EA
on the EPA NCP Product Schedule. We developed
on the NCP list: Oil Spill Eater II (OSE II).
a set of guidelines by which to review products
We continue to look for other products that
and determine their eligibility for use in US
fulll these criteria, but in the meantime, at
navigable waters. We were not looking for any least there is one bioremediation category
given product but merely those that fell under that could effectively lead response methods
our criteria for desired effectiveness, as follows:
into the twenty-rst century; and as of the
writing of this paper, the only product that
On the NCP list.
has been able to meet our guidelines has been
Swift and effective removal of the oil, not
OSE II.
just dispersal of it by solubilizing or disLAEO produced a documentary lm to
solving it into the water column.
educate the public on bioremediation and to
Nontoxic with no destructive trade-offs
encourage researchers and companies with
associated with its application.
products that meet the above criteria to step
Able to also detoxify chemical disperforward.32 Several products have since been
santse.g., the two types of Corexit that
submitted to us for our advocacy, and some,
have been broadly used domestically and
although promoted as nontoxic, were found
internationally.
to be at least as toxic as crude oil.
Using neither nonindigenous microbes nor
New and innovative solutions utilizing all
genetically modied organisms.
available technology are needed for the
Complete scientic documentation subsituation in the Gulf of Mexico, as well as
stantiating the products efcacy.
future hydrocarbon-based spills that will
A track record of success in the eld.
continue to occur in all the waters of the
world. If we stay on the same track, we run the
Pretested and screened as usable anyrisk of having sheries collapse, a chemically
whereopen water, sandy beaches,
stressed ecosystem worldwide, and progresmarshes, etc., as a rst-response method
sively worsening human health issues.33
(i.e., predetermined as applicable in all
environments to enable rapid response
Characteristics of an
without the need for assessment during an
Effective Solution
emergency).
Feasibility Assessment Criteria
The manufacturer has sufcient quantities in
stock and immediate production capabilities
The protection of human health should be
to handle a spill of signicance.
the foremost concern of any oil spill cleanup
21
decision-making process. Human health is

4. Understanding that nature uses surfactantsxiii
dependent upon the relative health of the
in the natural process of cleaning up an oil
surrounding environment; hence it is important
spill, an effective product would have no
to understand the criteria by which cleanup
toxic surfactants such as are contained
methods must be gauged as to their value and
in both Corexit 9527 and 9500. (For instance,
effectiveness. To reiterate, the primary reason
Bioremediation EA Type OSE II contains no
to clean up an oil spill or hazardous materials
toxic surfactants and is fully tested and valiis to rapidly reduce the impact of their toxicity
dated as nontoxic. Comparing toxicity levels
so that all living organisms can survive. And
using established EPA standards cited earlier,
again, if even the smallest organisms can
Corexit 9500 had a high toxicity level of
survive, then the ecosystem will be able to
0.065 to 0.354 ppm compared to OSE II,
sustain itself.
which had a reading of 10,000 ppm for one
of the most sensitive marine species tested
Thus, our recommended standards for the
[the higher the number, the lower the toxicity
ideal technology or agent for use in cleaning
level]. This means that Corexit is as much
up a hazardous spill would be these:
as 150,000 times more toxic than the bioremediation alternative. See Toxicity Values
1. Must swiftly and thoroughly detoxify the
chart below.)
oil or hazardous substances as a rst step
in order to protect the indigenous microbial
populations and all life forms.
5. Must have a scientically substantiated

and predictable end point that could be
standardly achieved from its proper
2. Must nullify the oils adhesive qualities so
application. This end point would be that
that it does not stick to marine life, wildlife,
within
a matter of days to, maximally, a few
marsh grass, rocky shorelines, sandy beaches,
weeks, close to 100 percent of the oil would
or seabed sediment.
have been converted into CO2 and water
two benign substanceswithout any adverse
3. Must keep the oil on the surface so that it
side
effects, or trade-offs related to its applican most rapidly be digested by indigenous
cation, thereby protecting the responders,
microbes, utilizing existing airborne oxygen
wildlife, and marine life.
and protecting the 60 percent of marine life
that resides in the subsurface area. (Note:
6. Its application must be economically
This also makes it accessible for physical
viablefor example, comparable in cost
removal methods working in tandem with
to current methods and, ideally,
nontoxic agents.)
signicantly less.
LC 50 = Lethal concentration values in parts per million measuring level in which there is mortality with 50 percent of
species being tested over a specific period of time. Higher # = less toxic, lower # = greater toxicity in ppm.
Sample Toxic ity Com par ison, Envi ronment Canada and US EPA Tests,
Bioremediation vs. Corexits 34
xiii. surfactant. A substance that lowers the surface tension of water, making it easier for organic compounds to be dissolved in the water.
There are toxic and nontoxic surfactants; i.e., chemical based with various degrees of toxicity, and plant/living-organism based = nontoxic.
22
Our research found that an EA Type bioremediation technology that meets the above
criteria exists today and is being used in over
30 countries. Its results contrast strongly with
those derived from dispersants predominantly
used in US navigable waters. Additionally,
it costs a fraction of the other methods and
would therefore represent an economic boon,
not only to the responsible parties, who could
avoid damage claims and heavy nes, but also
to those living in the environment, reducing
business disruptions with rapid cleanup,
bringing a quick return to their livelihoods.
In other words, in addition to preserving the
health and safety of the waters, there would
be little impact on tourism, coastal

businesses, and fisheries.
The value of a product could be rated and
characterized by how rapidly and thoroughly
it meets the above criteria while introducing
no additional toxicity to the scene already
created by the hazardous spill.
Due to the many common misconceptions
about bioremediation, and especially the
subcategory EA Type on the NCP list, LAEOs
Science & Technology Advisory Board has
provided the above summary of our vetting
process of spill-response methods for use by
all interested parties.
We encourage independent investigation of EA Type as a promising potential

solution to oil spill response in deep-water drilling and difcult access environments,
particularly as a rst-response method for open-water oil spills, in lieu of chemical
dispersants of any kind. To reiterate, the primary reason to clean up an oil spill or
hazardous materials is to rapidly reduce the impact of their toxicity so that all living
organisms can survive. And again, if even the smallest organisms can survive, then
the ecosystem will be able to sustain itself.
Because None Survive Alone
23
Material Safety Data Sheet
U.S. Department of Labor
May be used to comply with OSHAs Hazard

Communication Standard, 29 CFR 1910 1200. Standard
must be consulted for specific requirements.
Occupational Safety and Health Administration

(Non-Mandatory Form)
Form Approved
OMB No. 1218-0072
Note: Blank spaces are not permitted. If any item is not
applicable or no information is available, the space
must be marked to indicate that.
IDENTITY)
Micro-Blaze
Non-Formulated
Section I
Manufacturers name
Address
Verde Environmental, Inc.
Emergency Telephone Number
9223 Eastex Freeway

Houston, Texas 77093-7001
Telephone Number for Information

Date Prepared
800 / 626-6598
713 / 691-6468
01/01/13
Signature of Preparer
William L. Scogin, President
Section IIHazardous Ingredients/Identity Information

Hazardous Components (Specific Chemical Identity, Common Name(s))
PART A HAZARDOUS INGREDIENTS
CAS Number:
NONE
OSHA PEL
N/A
Other Limits
Recommended
ACGIH TLV
N/A
% (optional)
N/A
PART B OTHER INGREDIENTS

Water and viable Non-Pathogenic and Non-Toxic
Bacillus Spore Forming Bacteria Cultures
7732-18-5
Components not listed are either proprietary, or non-hazardous.

Section IIIPhysical/Chemical Characteristics
Boiling Point
100C
Specific Gravity (H20 = 1)
Vapor Pressure (mm Hg)
Equiv. water
Melting Point
N/A
Equiv. water
Evaporation Rate (Butyl Acetate = 1)
N/A
Vapor Density (AIR = 1)

Solubility in Water
Appearance and Odor
1.0
100%
Opaque liquid, slight odor
Section IVFire and Explosion Hazard Data

Flammable Limits
Flash Point (Method Used)
Extinguishing Media
N/A
Non-flammable
LEL
UEL
----
----
Non-flammable
Special Fire Fighting Procedures
Unusual Fire and Explosion Hazards
None
None - NON-FLAMMABLE
OSHA 174 Sept. 1985
Section VReactivity Data

Stability
Unstable
Conditions to Avoid
Stable
Incompatibility (Materials to Avoid)
XXXX
Strong acids or alkali compounds may inactivate biological cultures.
Hazardous Decomposition or Byproducts

May Occur
Hazardous
Polymerization
Conditions to Avoid
Will Not Occur
XXXX
Section VIHealth Hazard Data
Route(s) of Entry
Inhalation?
Health Hazards (Acute and Chronic)
Skin?
Ingestion?
May cause diarrhea if ingested in large amounts.
Organisms used are non-pathogenic. These organisms are susceptible to commonly used antibiotics.
Carcinogenicity
NTP?
N/A
IARC Monographs?
N/A
N/A
OSHA Regulated?
N/A
Signs and Symptoms of Exposure
Skin: slight redness on hands and forearms if individual has a history of dermal allergic
reaction. Inhalation: if inhaled, remove victim to fresh air. Give oxygen or artificial respiration as needed. Obtain
emergency medical attention.
Medical Conditions
Generally Aggravated by Exposure Dermal
Emergency and First Aid Procedures
allergic reaction on skin if susceptible person has continual exposure.
Ingestion: Drink water or milk to dilute. Induce vomiting only if advised by

physician or poison control center.
Section VIIPrecautions for Safe Handling and Use
Steps to Be Taken in Case Material Is Released or Spilled
May mop up spills; may flush down sanitary drain into waste water
treatment lines.
Waste Disposal Method
Disposal of this product or its residue must be done in accordance with all local, state and
federal requirements.
Precautions to Be Taken in Handling and Storing
Avoid eye contact.
Other Precautions
To maintain shelf life, avoid temperatures under 32 F or over 120 F for long periods of time.
Microbes are viable up to 180 F. KEEP FROM PROLONGED FREEZING.
Section VIIControl Measures
Respiratory Protection (Specify Type
Ventilation
) Avoid breathing mists; mask advised if spraying in enclosed, unventilated spaces.
Local Exhaust
Special
Mechanical (General)
Other
Protective Gloves
Use if prolonged exposure or dermal

sensitivity to surfactants.
Other Protective Clothing or Equipment
Work/Hygienic Practices
Eye Protection
Normal room ventilation.

Avoid splashing in eyes; may irritate.
None required; rubber or latex recommended.
Minimize exposure in accordance with good hygiene practices.
We believe the statements, technical information and recommendations herein

are reliable, but they are given without warranty or guarantee of any kind,
express or implied, and we assume no responsibility for any loss, damage, or
expense, direct or consequential, arising out of their use.
VERDE ENVIRONMENTAL, INC.

HOME OF
Non-Formulated
Verde Environmental, Inc.

9223 Eastex Freeway
Houston, TX 77093
Office: 713.691.6468
Toll Free: 800.626.6598
Fax: 713.691.2331
www.micro-blaze.com
Partnering with Nature for a Cleaner Tomorr ow
Non-Formulated
Product Details
Appearance:
Light brown
pH:
7.0 8.0
Shelf Life:
10 Years
Storage:
Avoid temperatures over 48C for long

periods of time. Avoid prolonged
freezing.
Micro-Blaze Non-Formulated is a safe

non-toxic microbial formulation used
for bioremediation where the use of
surfactants are not desired or permited. It
is used primarily in contaminated ground
water clean-up and also in and around
surface water, such as creeks, rivers, ponds,
and lakes. It breaks down, degrades, and
digests waste. The residue and run-off can
be safely sent to the facility waste water
treatment plant. The numerous strains of
microbes in Micro-Blaze Non-Formulated
provide a synergistic degradation of the
organic and hydrocarbon pollutants.
Uses:
Remediation
of
ground
water
contamination
Packaging:
Remediation of contamination in and
1-Gallon Pail
5-Gallon Pail
55-Gallon Drum
275-Gallon Tote
around creeks, rivers, ponds, and lakes
SURFACTANT FREE
* Always obtain regulatory approval prior to putting any
product into a waterway
To receive more information:
Other Micro-Blaze Microbial

Products:
0912
Emergency Liquid Spill Control FOG

Micro-Blaze Out AGRO APT Budkicker
CSR Turf Care

AT&amp;T Hall Ridge Work Plan 03-07-2016

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AT&amp;T Hall Ridge Work Plan 03-07-2016

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CB&I

500 Penn Center Blvd.

12232 S.W. Garden Place

Sunday, February 28, 2016

RE: AT&T Hall Ridge / 156319

DRAFT REPORT, DATA SUBJECT TO CHANGE

12232 S.W. Garden Place

Project Number: 156319

Project Manager: Ron Malec

ANALYTICAL REPORT FOR SAMPLES

DRAFT REPORT, DATA SUBJECT TO CHANGE

12232 S.W. Garden Place

Project Number: 156319

Project Manager: Ron Malec

ANALYTICAL SAMPLE RESULTS

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT, DATA SUBJECT TO CHANGE

12232 S.W. Garden Place

Project Number: 156319

Project Manager: Ron Malec

ANALYTICAL SAMPLE RESULTS

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT, DATA SUBJECT TO CHANGE

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

12232 S.W. Garden Place

Project Number: 156319

Project Manager: Ron Malec

ANALYTICAL SAMPLE RESULTS

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT, DATA SUBJECT TO CHANGE

Surrogate: o-Terphenyl (Surr)

12232 S.W. Garden Place

Project Number: 156319

Project Manager: Ron Malec

ANALYTICAL SAMPLE RESULTS

Methyl tert-butyl ether (MTBE)

Surrogate: Dibromofluoromethane (Surr)

Methyl tert-butyl ether (MTBE)

Surrogate: Dibromofluoromethane (Surr)

DRAFT REPORT, DATA SUBJECT TO CHANGE

12232 S.W. Garden Place

Project Number: 156319

Project Manager: Ron Malec

ANALYTICAL SAMPLE RESULTS

Methyl tert-butyl ether (MTBE)

Surrogate: Dibromofluoromethane (Surr)

Methyl tert-butyl ether (MTBE)

Surrogate: Dibromofluoromethane (Surr)

AT&T Hall Ridge Work Plan 03-07-2016

AT&T Hall Ridge Work Plan 03-07-2016