This is to signify that

AGQ PER SAC

AV. SANTA ROSA 511
LA PERLA
CALLAO
PERU
Testing Laboratory TL-502
(Revised April 18, 2014)
has met the requirements of the IAS Accreditation Criteria for Testing Laboratories (AC89), has demonstrated compliance with
ISO/IEC Standard 17025:2005, General requirements for the competence of testing and calibration laboratories, and has been
accredited, commencing December 23, 2013, for the test methods listed in the approved scope of accreditation.

Patrick V. McCullen
Vice President, Chief Technical Officer

Print Date: 6/10/2014

C. P. Ramani, P.E.
President

(see attached scope of accreditation for fields of calibration and accredited calibration methods)

Page 1 of 5

AGQ PER SAC TL-502

(Revised April 18, 2014)
AGQ PER SAC
Av. Santa Rosa 511
La Perla, Callao
Peru
FIELDS OF TESTING
Mining

Preparation of
Samples
Elemental Analysis

Karina Soncco
Quality Manager
+51 1 7102700
MATERIAL

DETERMINANTS

Metallic Ores
Metallic Ores
and High
Grade Material
Metallic Ores

Multi-Element Analysis (Ag, Al, As, Ba, Bi, Ca, Cd,

Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, P, Pb, S,
Sb, Sn, Sr, Ti, Tl, V, Zn)
Multi-Element Analysis (Ag, Al, As, Ba, Bi, Ca, Cd,
Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, P, Pb, S,
Sb, Sn, Sr, Ti, Tl, V, Zn)
Gold and Silver
Cu, Pb, Fe, Zn y Ag

Copper

Metal present in water soluble

Interchangeable ions
Metal associated with carbonates
Metal associated with manganese oxides and
amorphous iron (Fe, Mn Oxam)
Metal bound to crystalline iron oxides (Fe Oxicryst)
Metals in sulfides
Remaining metal not extracted at earlier stages as
silicate resistant phases
Specific Gravity
pH Abrasion
pH Oxidation
Neutralization Potential
Maximum Potential Acidity
Net Neutralizing Potential
Fizz Rating
Total S

December 23, 2013

Commencement Date

Print Date: 6/10/2014

METHOD REFERENCE
PE-4017, Crushing and Sifted
PE-4006, ICP-OES and Aqua
Regia Digestion
PE-4006, ICP-OES and 4 Acid
Digestion
PE-4008, AA analysis
PE-4007, Fire Assay
PE-4026, Determination of
Metals by Atomic Absorption
Spectrophotometry
PE-4030, Soluble Copper in
Sulfuric Acid by Atomic
Absorption
PE-4406, Sequential Extraction
Method for Separation of Metals
on Mining Waste

PE-4029, Specific Gravity in

Minerals
PE-990, Determination of pH of
Abrasion
PE-991, pH Determination of
Oxidation
PE-4402, Neutralization
Potential (NP)
PE-4407, Maximum Potential
Acidity (MPA)
PE-4407, Net Neutralizing
potential (NNP)
PE-4409, Fizz Rating in
Minerals
PE-4408, Elemental Analyzers

C. P. Ramani, P.E.
President
Page 2 of 5

AGQ PER SAC TL-502

(Revised April 18, 2014)
FIELDS OF TESTING
Mining
(continued)

Food

MATERIAL

Gravimetric
and Volumetric
Analysis

Metallic Ores

Calculation
Pesticides
Residues

Metallic Ores
Fruits,
Vegetables,
Nuts, Cereal &
Dried Fruit,
Oils/Fatty
Matrices

December 23, 2013

Commencement Date

Print Date: 6/10/2014

High Grade
Material

DETERMINANTS

METHOD REFERENCE

Total Sulphate
Elemental S
Copper
Zinc
Lead
Iron
Total Sulphide
Acefato, Acetoclor, Acrinatrina, Alacloro, Aldrin,
Amitraz Atrazina, Azinfos Etil, Azinfos Metil,
Benalaxil, Benfluralin, Bifenazato, Bifenilo,
Bifentrin, Bitertanol, Bromofos Methyl,
Bromopropilato, Bupirimato, Buprofezin, Captan,
Carbaril I, Carbaril II, Carbaril, Carbofenotion,
Carbosulfan, Chinometionato, Ciflutrin,
Cipermetrina, Ciproconazol, Ciprodinil,
Clorbenzilat, Clordane, Clorfenapir,
Clorfenvinfos, Cloropropilato, Clorpirifos,
Clorprofam, Clortal-Dimetil, Clortalonil,
Clortoluron,
DDD-pp + DDT-pp, DDE-pp, DDT-op,
Deltametrina, Diafenturion, Diclobenil,
Diclofention, Diclofluanida, Dicloran, Diclorvos,
Dicofol, Dicrotofos, Dieldrin, Difenilamina,
Difenoconazol, Diflufenican, Dimetoato,
Diniconazol, Dinobuton, Disulfoton sulfone,
Disulfoton sulfoxide, Disulfoton, Ditalimfos,
Diuron, Endosulfan I, Endosulfan sulfato, Endrin,
Etalfluralin, Etiofencarb, Etion, Etofumesato,
Etoprofos, Etoxiquina, Etridiazol, Etrimfos,
Fenamifos, Fenarimol, Fenazaquin, Fenitrotion,
Fenoxicarb, Fenpropatrin, Fensulfuton, Fention,
Fentoato, Fenvalerato+ Esfenvalerato,
Fluazifop-Butil, Flucitrinato, Fludioxonil,
Fluquinconazol, Flusilazol, Flutriafol,
Fluvalinato tau, Folpet, Fonofos, Fosmet,
Heptenofos, Hexaclorobenceno,
Hexaclorobutadieno, Hexaconazol, Imazalil,
Iprodiona, Iprovalicarb, Isazofos, Isofenfos Metil,
Isofenfos, Kresoxim Metil, Lambda-Cihalotrin,
Lindano, Malation, Mecarbam, Mepronil,
Metacrifos, Metalaxil, Metamidofos, Metazachlor,
Metidation, Metil, Metiocarb, Metoxiclor,
Metribuzina, Mevinfos, Miclobutanil, Mirex,
Molinato, Napropamida, Nuarimol, Ofurace, OPP,
Oxadiazon, Oxadixil, Oxifluorfen, Paclobutrazol,
Paration Etil, Paration Metil, Penconazol,
Pendimetalina, Pentacloroanilina,
Pentacloroanisol, Pentaclorobenceno, Permetrina,

PE-4005, Gravimetric Methods

PE-4004, Gravimetric Methods
PE-4009, Volumetric Methods
PE-4010, Volumetric Methods
PE-4011 Volumetric Methods
PE-4012, Volumetric Methods
PE-4016, Calculation Methods
PE-614, Determination of
Pesticide residue using Miniluke
and Quecher by GC - MS/MS

C. P. Ramani, P.E.
President
Page 3 of 5

AGQ PER SAC TL-502

(Revised April 18, 2014)
FIELDS OF TESTING
Food
(continued)

Pesticides
Residues

December 23, 2013

Commencement Date

Print Date: 6/10/2014

MATERIAL
Fruits,
Vegetables,
Nuts, Cereal &
Dried Fruit,
Oils/Fatty
Matrices

DETERMINANTS

METHOD REFERENCE

Pirazofos, Piridaben, Piridafention, Pirifenox,

Pirimetanil, Pirimicarb, Pirimifos Etil, Pirimifos
Metil, Piriproxifen, Procimidona, Procloraz,
Profam, Profenofos, Profluralin, Prometrina,
Propargita, Propiconazol, Propizamida, Protiofos,
Quinalfos, Quinometionato, Quintozene,
Simazina, Sulfotep, Tebuconazol, Tebufenpirad,
Tecnazen, Teflutrin, Terbacil, Terbufos,
Terbutilazina, Terbutrina, Tetraclorvinfos,
Tetraconazol, Tetradifon, Tetrametrina,
Tiabendazol LC-MS, Tiometon, Tolclofos metil,
Tolilfluanida, Transflutrin, Triadimefon,
Triadimenol, Triazofos, Triciclazole, Triclorfon,
Trifluralin, Uniconazol-P, Vinclozolina, Zoxamida
Abamectina, Acetamiprid, Aclonifen, Aldicarb,
Aldicarb Sulfona, Aldicarb Sulfoxido, Azoxistrobin,
Bendiocarb, Benomilo-Carbendazima, Bentazone,
Bentiovalicarb, Boscalid, Bromacilo, Bromoxinil,
Bromuconazol, Butoxicarboxim, Cadusafos,
Captafol, Carbofuran, Chloridazon, Ciazofamida,
Cicloxidin, Cimoxanilo, Ciromazina, Cletodim,
Clofentezina, Clopyralid, Clorantraniliprole,
Clothianidin, Demeton-S-Metil, Demeton-S-Metil
Sulfoxido, Desmedifan, Diclormid, Diclorprop,
Dietofencarb, Dimetoato, Dimetomorf, Dinocap,
Dodemorph, Dodine, Emamectin Benzoato,
Espinosad A+D, Espirodiclofen, Etiprol,
Etofenprox, Etoxazol, Famoxadona, Fenamidona,
Fenbuconazol, Fenhexamida, Fenmedifan,
Fenpropimorf, Fipronil, Flazasulfuron, Flonicamid,
Fluacinan, Flubendiamida, Flufenoxuron,
Fluometuron, Fluopicolid, Fluotrimizole,
Fluratiocarb, Flutalonil, Forato, Forato Sulfona,
Forato Sulfoxido, Forclorfenuron, Formetanato,
Fostiazato, Hexaflumuron, Hexitiazox,
Hymexazol, I Imazamox, Imazamox, Imidacloprid,
Indoxacarb, Ioxinil, Isocarbofos, Isoproturon,
Isoxaben, Lenacilo, Linuron, Lufenuron,
Mepanipirin, Meptil Dinocap, Meptyl Dinocap,
Metaflumizona, Metamitrona, Metiltiofanato,
Metolaclor, Metolcarb, Metomilo, Metoxuron,
Monocrotofos, Monolinuron, Nicosulfuron,
Nitenpiram, Ometoato, Oxadiargil, Oxamilo,
Pencicuron, Picoxistrobin, Pimetrozina, Piridato,
Propaquizafop, Propoxur, Proquinazid,
Prosulfocarb, Quinclorac, Quinmerac, Quinoxifen,

PE-614, Determination of
Pesticide residue using Miniluke
and Quecher by GC - MS/MS

PE-618, Determination of
Pesticide Residue using
MiniLuke and Quecher by LC MS/MS

C. P. Ramani, P.E.
President
Page 4 of 5

AGQ PER SAC TL-502

(Revised April 18, 2014)
FIELDS OF TESTING
Food
(continued)

MATERIAL

DETERMINANTS

Pesticides
Residues

Fruits,
Vegetables, Nuts,
Cereal & Dried
Fruit, Oils/Fatty
Matrices

Organic
Chemistry

Fish &
Hydrobiological

Quizalofap Ethil, Rinsulfuron, Rotenona,

Spinetoram, Spinosin A+D, Spirotetramat,
Spiroxamina, Sulcotriona, Tebufenocida,
Teflubenzuron, Thiadizuron, Thiociclam,
Tiabendazol, Tiacloprid, Tiametoxan, Tiodicarb,
Tridemorf, Trifloxistrobin, Triflumizol, Triflumuron,
Triforina
Hystamine

Chemistry

Fruits and
Vegetables

Dithiocarbamates (as CS2)

Fruits and
Vegetables/Fish &
Hydrobiological

Multi Element Analysis (Hg, As, Cr, Cd, Sn, Pb,

Cu, Ni, V, Fe, Zn, Mn)

Fruit and
Vegetables High
Water and Low
Fat

Quaternary Ammonium

PE-655, Determining Quaternary

Ammonium Compounds by
Chromatography

Water & Waste

Water

Colony Count by inoculation in a nutrient agar

culture medium at 22C and 36C
Escherichia coli
Coliform bacteria
Fecal coliform in water (filtration)
Fecal coliform Fermentation technique
Escherichia coli using Fluorogenic Substrate
Detection of pathogenic Bacteria - Salmonella
Detection of pathogenic Bacteria - Vibrio
Colony Count techniques at 30C. Horizontal
method for the enumerations of microorganisms
Detection of Salmonella spp. Horizontal method
for the detection of Salmonella spp. 37C
Coagulase positive staphylococci. Technique
using Baird-Parker agar medium. 37C
Detection and enumeration of Listeria
monocytogenes. Part 1: Detection method
Enumeration of of beta-glucuronidase-positive
Escherichia coli. Colony-count technique at 44C
using 5-bromo-4-chloro-3-indolyl -D-glucoronide.
Emumeration of yeast and mold Dilution plating
technique. Spread-plate method

ISO 6222

Microbiology

Food

December 23, 2013

Commencement Date

Print Date: 6/10/2014

METHOD REFERENCE
PE-618, Determination of
Pesticide Residue using
MiniLuke and Quecher LCMS/MS

PE-516, Determination of
Residues of Hystamine by LCMS/MS Chromatography
PEC-032, Determination of
Dithiocarbomates through
Spectrophotometric Ultraviolet
Visible Spectrophotometry
PC-230, Determination of Base
Metal by ICP/OES

ISO 9308-1
ISO 9308-1
PE 403
SM 9221 B & E
SM 9221 B & F
SM9260B
SM 9260 H
ISO 4833:2003, 5.2.2.1
ISO 6579
ISO 6888-1, 9.2.1
ISO 11290-1
ISO 16549-2

FDA BAM Ch 18, B.1

C. P. Ramani, P.E.
President
Page 5 of 5