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Evaluation of Thixotropy of SCC

and Inflence on Concrete Perfomance


Kamal Henri Khayat

54th Congresso Brasilleiro do Concreto


Maceio Oct. 9, 2012

IBRACON, October 9, 2012

HPC: Concrete with improved


mechanical properties & service life
Stress (MPa)

400
RPC + fibers
(pressed and
confined)

300

200
100
0

HPC
NSC
0
0.005

RPC + fibers

0.01

0.015

Strain (mm/mm)

IBRACON, October 9, 2012

0.02

230-MPa RPC
foot bridge,
Sherbrooke

Confederation Bridge, N.B. PEI


100-year design life

HPC: Concrete with improved


workability

IBRACON, October 9, 2012

Industrial Research Chair on High-Performance


Flowable Concrete with Adapted Rheology (FCAR)
Owners:

Material Suppliers:

Engineering Firms:

Testing Labs:

Inspecsol

Prefab:

Yield stress

Rheological parameters of FCAR

Flowable Mass Conc.


HPC
SF-SCC
Underwater Conc.
SCC

FR-SCC

Plastic viscosity

IBRACON, October 9, 2012

6
IBRACON, October 9, 2012

IRC Research Program


Theme III - Rheological Properties and
Granular Flow Modeling

Theme II Test Methods to Evaluate Flow


Properties of FCAR

Theme I Influence of Mixture Constituents, Mix


Design, & Temperature on Rheology of FCAR

Theme IV Mix Design


and Engineering
Properties of FCAR
Theme V - Field Validation and
Guidelines
IBRACON, October 9, 2012

Recommendations
for Design & Testing
of FCAR

Flow behavior of SCC is complex and must be


optimized to secure adequate performance
low resistance to flow (low t0)

high stability (moderate visc.)

Conventional
concrete

high passing ability (low


IBRACON, October 9, 2012

t0

+ mod. visc.)

Reduce water content to


8
enhance
viscosity
Torque (N m )

7
6

W/CM = 0.37

5
4

W/CM = 0.47

3
2

F = 650 mm

1
0
0

0.2

0.4

0.6

Speed (Rev/s)
IBRACON, October 9, 2012

0.8

1.0

Incorporate VEA to enhance viscosity


Moderate VEA

Torque (N m)

7
6

Low VEA

4
3

F = 650 mm

W/CM = 0.47

1
0

IBRACON, October 9, 2012

0.2

0.4
0.6
Speed (Rev/s)

0.8

1.0

Thixotropy variation of viscosity with time at constant shear


rate (reversable)

IBRACON, October 9, 2012

Negative Aspects of Structural Build-up

Multi-layer casting
After 5 min of rest time,
the 2 layers can mix well
After 20 min of rest time, the
2 layers do not mix at all

IBRACON, October 9, 2012

Casting point

Negative aspect of structural build-up (thixotropy)

IBRACON, October 9, 2012

Positive Aspects of Structural Build-up


Reduction in
formwork pressure
after casting due
to structural buildup at rest

Improved static
stability
50%

IBRACON, October 9, 2012

Factors Affecting Form Pressure of CVC


-

Fluidity level
Casting rate
Coarse aggregate volume
Binder content and type
Presence of admixtures
Temperature of fresh concrete
Minimum dimension of formwork
Degree of vibration
Etc.

IBRACON, October 9, 2012

Rodin, 1952

P(maximum) / P(hydrostatic)

Effect of Consistency Level


1.0

HRWRA
0.9

w/cm = 0.40
S/A = 0.46
Ternary cem. = 450 kg/m3
PC
H = 2.8 m

0.8

D = 200 mm
0.7

SF =
750 mm

0.6

SF = 650 mm

Slump = 220 mm SF = 550 mm

0.5
0

50

R = 10 m/h

100

150

200

250

300

Time after casting (min)

350

R ~ 1 m/hr

Lift height = 3.5 m


W = 0.9 m (9 x 4 m)

Lift height = 2.8 - 3 m


W = 0.2 m
R ~ 2 m/hr

Lift height > 3 m


W = 0.15 m
R ~ 8-10 m/hr

IBRACON, October 9, 2012

ACI 347-04 [Hurd, 2002]


Normal concrete with slump < 175 mm at time of casting
Immersion of vibrator < 1.2 m in fresh concrete. Underneath concrete is not re-vibrated
R 4.5 m/h
Lateral pressure

785 R
pmax (kPa) CwCc 7.2

17.8

Cw

: Unit weight coefficient Cc : Chemistry coefficient

Walls (R < 2.1 m/h, H > 4.2 m) or walls 2.1 < R < 4.5 m/h, H not specified

1156
244 R
pmax (kPa) CwCc 7.2

17.8
T

17.8

30 Cw (kPa) Pmax
Pmax
IBRACON, October 9, 2012

150Cw Cc (kPa)
cH

Casting depth (H)

Columns (R and H not specified) or walls with R < 2.1 m/h, H 4.2 m

Pmax

Pumping from bottom:


Pmax = c H + 25% pump surge pressure

Modified ACI 347-04 [Hurd, 2002]


Density (kg/m3)

Cw : Unit weight coefficient

< 2240
2240 -2400
> 2400

Cw = 0.5 [1 + w/2320] 0.80


Cw = 1.0
Cw = w/2320 kg/m3

Cement type or blend

Cc: Chemistry coefficient


Type I, II, III without retarders
Type I, II, III with retarders

Other types or blends containing < 70% slag or 40% FA without retarder
Other types or blends containing < 70% slag or 40% FA with retarder
Blends containing > 70% slag or 40% FA

Cc
1.0
1.2

1.4

Retarders (set retarder, retarder water reducer, retarding midrange WRA, or HRWRA) that delay setting
IBRACON, October 9, 2012

Various models to evaluate lateral


pressure
R T H
Form
width

Time Thixotropy Slump

1- ACI 347-04

2- U.K. (CIRIA Report 108)

3- Japan - Standard
Specifications for Concrete
Structures (2002)

4- Sweden (Design of Vertical


Concrete Formwork)

IBRACON, October 9, 2012

Set
time

R = Rate of casting
T = Temperature
H = Casting depth
x

Waiting
period

Various models to evaluate lateral


R T H
pressure
Form
width

Time Thixotropy Slump

1- ACI 347-04

2- U.K. (CIRIA Report 108)

3- Japan - Standard
Specifications for Concrete
Structures (2002)

4- Sweden (Design of Vertical


Concrete Formwork)

5- Khayat & Assaad [2005]

6- Roussel and Ovarlez [2005]

7- Lange et al., [2005]

8- Khayat & Omran [2009]

9- DIN 18 218 :2010-01 (2010)

10- Gardner et al., 2011


IBRACON, October 9, 2012

Set
time

Waiting
period

R = Rate of casting
T = Temperature
H = Casting depth
x

x
x
x

x
x

x
x

x
Sflow
loss

Outline
Thixotropy determination: structural breakdown
and structural build-up at rest
Thixotropy vs. form pressure exerted by SCC
Structural build-up vs. drop in interlayer bond

IBRACON, October 9, 2012

Thixotropy variation of viscosity (or shear stress) with time under


constant shear rate - structural build-up when left at rest (reversible)
160

Shear stress (Pa)

= fixed
120

= 0.03 s-1
sample at rest

80

40

Structural build-up
(flocculation, coagulation)
0
0

200

400

600

Time (s)
IBRACON, October 9, 2012

800

1000 1200

Modified MK-III
rheometer

Importance of Restructuring !!
Viscosity of concrete (Pa.s)

Formwork pressure = f (restructuring of the concrete)


900

2 minutes resting time


4 minutes resting time

600

Slump = 200 mm
450 kg/m of binder
w/cm = 0.42
VMA

N = 0.9 rps
300

0
0

10

15

Time (sec)
IBRACON, October 9, 2012

20

25

Shear stress (Pa)

0.7 rps
te

ti

Time (s)

happ, i
happ, e

Shear rate (1/s)

t i t e
happ

IBRACON, October 9, 2012

te

app @ N=0.7 rps (Pa.s)

Shear stress (Pa)

1. Structural breakdown: drop in app. viscosity (app)

Typical SCC
mixtures

1400
1200
1000
800
600
400
200
0
0

15

30

45

Rest time (min)

60

Rotational speed (rps)

Time intervals for assessing thixotropy


0.9 rps

T1 = 0 - 30 min

0.7 rps

0.5 rps
0.3 rps

Time (min)
Testing & rehomogizing = 2.5 min
Rest of 5 min
IBRACON, October 9, 2012

1. Structural breakdown: structural breakdown area (Ab1)


800

600

600

N = 0.3 rps

Shear stress (Pa)

800

N = 0.7 rps

N = 0.5 rps N = 0.9 rps

400

200

400

Ab1 (J/m.s)
200

0
0

10

15

20

0.2

25

Ab1 =

0.9

- e(N)
dN
i
(N)

0.3

IBRACON, October 9, 2012

0.6

0.8

Rotational speed (rps)

Time (sec)
Lapasin et al. [1983]

0.4

J/m3 .s

Height of concrete (m)

Lateral pressure envelope of SCC


3.0

Slump flow = 650 mm

2.5

R = 10 m/hr

2.0

H = 2.8 m

at casting

D = 200 mm

1.5
1.0

rgh

~ 50% after 4 hr

0.5
0.0
0

10

20

30

40

50

Lateral pressure (kPa)


IBRACON, October 9, 2012

60

70

P(maximum) / P(hydrostatic) (%)

Thixotropy vs. Lateral Pressure


100

70 SCC
mixtures

80

60

40

Ab1 vs. Pressure at 0 min;


R = 0.89
Ab2 vs. Pressure at 100 min;
R = 0.85
Ab3 vs. Pressure at 200 min;
R = 0.84

20

0
50

200

350

500

Breakdown area (J/m.s)


IBRACON, October 9, 2012

650

800

R ~ 6-10 m/hr

IBRACON, October 9, 2012

Typical Formwork Pressure Diagram


Slump flow = 720 mm
S/A = 0.50
Ternary cement = 475 kg/m
w/cm = 0.40

Head of concrete (m)

6
5
4

R = 6.5 m/h

3
Hydrostatic pressure
2
3h

1h

P(max)
right after casting

0
0

20

40

60

80

100

Pressure developed on formwork (kPa)


IBRACON, October 9, 2012

120

P(maximum) / P(hydrostatic)

Pressure Variations with Thixotropy


0.6

BIN-0.50-Nap (Ab1 = 260 J/m.s)

PNS
R = 6 m/h

S/A

R = 6.5 m/h

0.4
R = 7.5 m/h

TER-0.50-Nap
(310 J/m.s)

TER-0.44-Nap
(405 J/m.s)

0.2

0.0
0

200

400

600

800

Time after casting (min)


IBRACON, October 9, 2012

1000

1200

2. Structural build-up at rest: Re-structuring


Structural build-up: increase in shear stress (or viscosity)
when the material is left at rest
160

Shear stress (Pa)

= fixed
120

= 0.03 s-1
sample at rest

80

40

Structural build-up
(flocculation, coagulation)

0
0
IBRACON, October 9, 2012

200

400

600

Time (s)

800

1000

1200

Static shear stress at rest (0rest)


T max

0.15
0.10

N = 0.03 rps

0.05
0.00

10

Time (sec)

15

Rheometer-0 rest (Pa)

Torque (N.m)

0.20

20

2500

Typical SCC mixtures


w/p
0.37-0.47

2000

Slump flow 600-720 mm


Ri (Pa)

1500
1000

R(t) (Pa/min)

500

RixR(t), (Pa2/min)

0
0
IBRACON, October 9, 2012

15
30
45
Rest time (min)

60

Portable vane (PV) test


10000
8000

PV 0rest (Pa)

0rest = Tmax /G

Typical SCC mixtures


w/p
0.37-0.47
Slump flow 600-720 mm

6000
4000
2000
0
0

15

30

45

Rest time (min)

IBRACON, October 9, 2012

60

75

Inclined plane (IP) test


Motion takes place in the form of
planer fluid layers gliding over each
others in the direction of the slope
60 mm
Step 1

120 mm

Step 2

t s r gh sin a
r = density of sample

Step 3

g = gravitation constant
h = mean central height of slumped sample
a = critical angle of plane at flow start
IBRACON, October 9, 2012

Inclined plane (IP) test


1000

Typical SCC mixtures


w/p
0.37-0.47
Slump flow 600-720 mm

IP t0rest (Pa)

800
600
400
200

IPt 0 rest r gh sin a


r = density of sample

g = gravitation constant
h = mean central height of slumped sample
a = critical angle of plane at flow start
IBRACON, October 9, 2012

10

20

30

Rest time (min)

40

50

Yield stress at rest: PV and IP tests vs. rheometer


Data at 15 min rest time
1200

2500

y = 1.00 x
R = 0.82

1500

IP 0rest (Pa)

PV0 rest (Pa)

2000

1000

y = 0.95 x
R = 0.82

900
600
300

500

0
0

1000

2000

Rheometer 0rest (Pa)


Good relationships between static yield
stress from PV and IP vs. rheometer
IBRACON, October 9, 2012

3000

300

600

900 1200 1500

Rheometer 0rest (Pa)

Thixotropy as input to evaluate formwork


pressure for SCC
Pmax = gH [a1H + a2R + a3T + a4Dmin + a5TI

@fixed Temp.

Pmax = gH [a1H + a2R + a3T + a4Dmin + a5TI

@various Temp.

: unit weight of SCC


RMC Research & Education Foundation
H: casting depth in the form Strategic Development Council of ACI
R: casting rate
SDC Members (2007 2009)
T: concrete temperature
Dmin: formwork width
TI: thixotropy index:TI@fixed temperature (22C) or TI@various temperature (ti).
IBRACON, October 9, 2012

Pressure device to determine


lateral pressure
63 mm

Pressure
19 mm
sensor

577 mm

500 mm

700 mm

19 mm
63 mm

Pressure
sensor

Fresh
concrete

190 mm

IBRACON, October 9, 2012

Digital
manometer to
control overhead
air pressure
(up to 13 m high)

Honeywell pressure
sensor
(1400-kPa capacity)

Pressure variations
320
320
SCC4
=
=560
560mm
mm
RR==10
10m/hr
m/hr
VMA = 2.8 L/m3

(kPa) (kPa)
Pressure
Lateral pressure

280
280
240
240

Hydrostatic
Eq. pressure
hydrostatic pressure
H = 13 m @ 72 min
Reach to hydrostatic

200
200

Sudden
increase in
pressure
reflects "blowup" of
overhead
pressure at
sensor location

H = 0.35 m

160
160
120
120

H = 0.5 m

80
80
decrease in pressure
reflects material
restructuring

40
40
00
00

20
20

40
40

60
60

80
80

Time
Time(min)
(min)
IBRACON, October 9, 2012

100
100

120
120

140
140

Use of pressure device to validate mix design


Lateral pressure (kPa)
0

50

100 150 200 250

50

100 150 200 250 300

Slump
flow

Casting depth (m)

Paste
volume
R = 10 m/hr

4
6

Hydrostatic
pressure

340 l/m3

10
12

560 mm

14

IBRACON, October 9, 2012

400 l/m3

660 mm
370 l/m3

Empirical models for K0 = f (H, R, T, Dmin, PVthixo index)


800 data points to
derive models

NCSS, 2007 software

H = 1 - 13 m
R = 2 - 30 m/h
T = 10 - 32 C
c = unit weight (e.g. 23.5 kN/m3)
d = min. formwork dimension
(0.2 1.0 m)
Dmin = Equivalent to d
For 0.2 < d < 0.5 m, Dmin = d
For 0.5 < d < 1.0 m, Dmin = 0.5 m

cH
112.5 - 3.8 H + 0.6 R - 0.6 T + 10 Dmin - 0.021 PVt 0rest@15 min f MSA fWT

100
cH
Pmax =
109.5 - 3.9 H + 0.7 R - 0.6 T + 3 Dmin - 0.29 PVt 0rest (t) f MSA fWT
100
H
Pmax = c 106 - 4 H + 0.6 R - 0.63 T + 10 Dmin - 0.00015 PVt 0rest@15min PVt 0rest (t) f MSA fWT
100
Pmax =

IBRACON, October 9, 2012

Empirical models for K0 = f (H, R, T, Dmin, IPthixo index)


Static yield stress after 15 min of rest [Ri] (Pa)

100

K0 (%)

80

K0@H=1m
K0@H=2m
K0@H=4m
K0@H=6m
K0@H=8m
K0@H=10m
K0@H=12m

60
40

R = 2 m/hr
T = 22 oC
Dmin = 200 mm
MSA = 14 mm
Waiting Time = 0

20
0
0

400

800

1200

1600

2000

IP0 rest@15min (Pa)


K0 = [112 - 3.83 H + 0.6R - 0.6T + 0.01Dmin - 0.023 IP0rest@15min] x fMSA x fWT
IBRACON, October 9, 2012

Effect of casting rate on lateral pressure characteristics


Pressure can be reduced by:

100

H=3m

lowering casting speed, or


increasing thixotropy
K0 (%)

80
60

SCC40
SCC51
SCC52
SCC53
SCC54
SCC46
SCC55
SCC56

40

20
0
0

10

(High
thixotropy)

20

Casting rate (m/hr)


IBRACON, October 9, 2012

30

Charts for relative lateral pressure K0


PV0rest@15min = 1200 Pa

PV0rest@15min = 200 Pa
1

10

15

20

25

30

22

22

22

23

23

24

25

26

41

42

42

44

45

47

48

49

59

60

61

63

65

67

69

71

76

76

78

81

83

86

89

90

91

93

96

100

103

103

104

106

110

114

114

115

118

123

123

124

128

131

132

10

136

11

< 50 kPa
50- 80 kPa
80 - 110 kPa
110 - 140 kPa
140 - 170 kPa
>170 kPa

R (m/hr)
1

10

15

20

25

30

17

17

17

18

19

19

20

21

32

32

33

34

35

37

38

40

45

45

46

49

51

53

55

57

92

56

57

58

61

64

67

70

72

107

110

66

67

69

72

76

79

82

86

119

123

127

74

75

77

81

85

90

94

98

127

132

137

142

80

81

84

89

94

98

103

108

133

139

144

150

155

84

86

89

94

100 105 111

117

136

142

148

154

161

167

87

88

92

98

105 111 117

123

138

142

149

156

163

170

177

10

88

89

94

100 107 114 121

128

140

142

147

154

162

169

177

185

11

87

89

93

101 108 116 124

131

12

143

144

151

158

166

174

183

191

12

85

86

93

100 108 116 124

133

13

143

145

154

159

168

177

186

195

13

80

82

91

96

132

IBRACON, October 9, 2012

H (m)

H (m)

R (m/hr)

105 114 123

Integrated research laboratory on materials valorization and


innovative and durable structures - 2007-2009

IBRACON, October 9, 2012

Formwork

16 mm bars
@ 30 x 40 cm
Sheathing
& form ties

Snap
form ties

Tie clamps
Wall
studs &
Wales

2 walls/day
Wall
#6
IBRACON, October 9, 2012

Wall
#7

Wall
#8

Investigated parameters
Level 1000, H = 3.7 m
(effect of casting rate)
Wall #1 Wall #2
VCC
SCC1
Slump/
slump flow (mm)

Wall
#3
SCC1

Wall
#4
SCC1

Level 2000, H = 4.4 m


(effect of thixo.)
Wall
#5
VCC
120
30

120
30

650 25

HRWRA type

---

PCP

---

Vp (L/m3)

---

Low, 330

---

R (m/hr)
W/CM

7.5
0.40

10
0.35

15

7.5
0.40

Wall
#6
SCC1

Wall #8
SCC3

650 25
PCP
Low
330
0.37

Air content < 3.5%, concrete temp. = 22 25 oC


IBRACON, October 9, 2012

Wall
#7
SCC2

PNS
High
370
10
0.35

Low
330
0.42+VMA

Full characterization
10 persons to carry out > 17 tests

h2 = 150 - H2
h1 = 600 - H1

Strength
H1

Shrinkage
H2

IBRACON, October 9, 2012

Lateral pressure [wall # 6, SCC1, R = 10 m/h]


Pmax (kPa)

70

Pmax (kPa)
0

60

20
10

Formwork height (m)

@ 2.33 m
@ 1.82 m

30

200

400

1.2 m PVC
column

600

800

Time (min)

IBRACON, October 9, 2012

80

100

1,0
1,5

1000

1200

Hydrostatic
pressure

2,0
2,5
3,0
3,5

60

0,5

@ 3.34 m

40

40

0,0

@ 3.85 m from top

50

20

4,0
4,5

@2 hr
@4 hr

@6 hr
formwork base

Pmax

8 full-scale R/C columns


Casting rate (m/h)

Mixture

Relative
thixotropy

5+
20 WP

SCC-L
SCC-M
SCC-H

Low
Medium
High

--Col.#5

-Col.#7
Col.#3

-Col.#8
--

IBRACON, October 9, 2012

10

13

-Col.#1
-Col.#4
--

15

22

--

Col.#2

Col.#6

--

ACI 347-04 vs. field measurements


Casting rate limited to 4.5 m/h (ACI 347-04)
Limited data
Walls and columns cast of 5 m/h are considered
Predicted Pmax (kPa)

100
y = 1.16x
R = 0.62

80
60

Pmax

40

785R

= CW CC 7.19 +

17.78 T

Wall element #2
3 columns (# 3, 5, 7)

20
0
0

20
40
60
80
100
Measured Pmax in field (kPa)

IBRACON, October 9, 2012

Cc : Chemistry coefficient = 1.2

Khayat & Omran [2009] vs. field measurements

Measured Pmax in field (kPa)

100
8 column elements
C
C
6 wall elements cast

80

y = 1.01 x
R = 0.97

60

with SCC

40
20
0
0

20

40

60

Predicted Pmax (kPa)


IBRACON, October 9, 2012

80

100

Round-Robin Tests for prediction of


form pressure (May 2012)

Member
T. Proske, Germany
M. Beitzel, Germany
N. Roussel, France

K. Khayat, USA
A. Omran, Canada
D. Lange, USA
J. Gardner, Canada
Y. Vanhove, France
IBRACON, October 9, 2012

Special property to be measured


Setting time
Structural build up / BT2
Structural build up / Plate test
Structural build up / Inclined plane,
Portable Vane
Pressure column
Pressure decay
Slump loss
:.
Friction stress
/ Tribometer

Outline
Thixotropy determination: structural breakdown
and structural build-up at rest
Thixotropy vs. form pressure exerted by SCC
Structural build-up vs. drop in interlayer bond

IBRACON, October 9, 2012

Structural build-up can lead to aesthetic problems in terms of


casting folds in multi-layer placements

Top layer
New layer

Bottom layer

Lift line
(U de Sherbrooke, 1997)

IBRACON, October 9, 2012

Interlayer bond strength (slanted shear strength)


2

Casting

200 mm

Small notch

30

100 mm

IBRACON, October 9, 2012

Variation of residual bond strength with thixotropy and


delay time between successive lifts
Delay time = 0 min

Residual bond strength, %

100

15 min

80

30 min
60
45 min

40
60 min
20
P

0
0

10000 20000 30000 40000 50000 60000 70000 80000 90000 100000
Thixotropy index from PV, Pa.Pa/min

IBRACON, October 9, 2012

Statistical model
RB SSh % 0.1608 DT Ln A thix2PV 1.0922 DT 100
DT = Delay time between 2 layers

90%

100

strength, (%)
d
n
o
B
l
a
u
id
s
e
R

RBS = Residual bond strength

90

80%

80
70

70%

60

60%

50
40

30
0
00
10 0000 00
2 00
t
3 0000 0
s(1
4 000 0
5) R
5 000 0
SB
6
00
U , (P
a.P 70 0000 0
a/m 8 000
in 9

IBRACON, October 9, 2012

R2 = 0.99

0
10

20
30
40
50
60

De

la

im
yt

i
, (m

n)

Residual bond strength


Flexural stress

Direct shear stress

Casting point

Casting point

100 mm

2
1

200 mm

2
25 mm

200 mm

100 mm

P
1

150 mm

25 mm

100 mm

50 50

50 mm

P/2
IBRACON, October 9, 2012

P/2

Critical delay time to reach 90% residual bond strength


Variation in residual bond with thixotropy and test methods
80
70

tc, min

60
50
40
30

20
10
0
0

10

20

30

40

50

60

70

Athix, Pa.Pa/min 1000


IBRACON, October 9, 2012

80

90

100

Conclusions
Thixotropy of SCC can be assessed by structural breakdown
and structural build-up at rest
Breakdown area (Ab) or drop in apparent viscosity to assess
thixotropy are determined using concrete rheometer
Structural build-up at rest can be determined as:
Variation of drop in apparent viscosity with time using
concrete rheometer
Variation of static yield stress at rest using concrete
rheometer
Variation of static yield stress at rest using empirical tests
(inclined plane and portable vane tests)

IBRACON, October 9, 2012

Conclusions
Increase of thioxotropy leads to reduction in form pressure
exerted by SCC
Residual interlayer bond of SCC increases with decrease
thixotropy (structural build-up at rest)
Long delayed time between casting two successive SCC
layers leads to reduction in interlayer bond
Residual inter-layer bond strength is more critical in shear
than in flexural or compression failure modes

IBRACON, October 9, 2012

Acknowledgment
NRMC Research & Education Foundation, ACI Foundation
NSERC IRC HP-Flowable Concrete with Adapted Rheology

J. Assaad, A. Omran, W. Magdi


S. Naji, P. Billberg, A. Yahia,
O. Bonneau, N. Petrov
R. Morin, M. DAmbrosia

IBRACON, October 9, 2012

Outline
Thixotropy determination: structural breakdown
and structural build-up at rest
Thixotropy vs. form pressure exerted by SCC
Structural build-up vs. drop in interlayer bond
Mixture parameters affecting thixotropy (form
pressure) of SCC

IBRACON, October 9, 2012

Effect of Consistency Level


Slump flow = 650 mm
w/cm = 0.40
S/A = 0.46
Ternary cement = 450 kg/m3
PC HRWRA

P(maximum) / P(hydrostatic)

1.0

HRWRA
0.9
0.8

SF =
750 mm

0.7

SF = 650 mm

0.6

Slump = 220 mm

SF = 550 mm

0.5
0

R = 10 m/h

50

100

150

200

250

Time after casting (min)

300

350

P(maximum) / P(hydrostatic)

Effect of Set-Modifiers (Cohesion)


Slump flow = 650 mm
w/cm = 0.42
Sand-to-total agg. = 0.44
Ternary binder = 450 kg/m3

1.0
0.9
0.8

Set-retarding
agent
Without setmodifying agent

0.7
0.6

Set-accelerating
agent

0.5
0

50

100

150

200

250

Time after casting (min)

300

350

P(maximum) / P(hydrostatic)

Effect of HRWRA Type


Slump flow = 650 mm
w/cm = 0.36
Sand-to-total aggregate ratio = 0.46
Ternary cement = 450 kg/m

1.0
0.9
0.8

Polycarboxylate
HRWRA

0.7

Naphthalene
HRWRA

0.6
0.5

Melamine
HRWRA

0.4

50

100

150

200

250

Time after casting (min)

300

350

Effect of powder polysaccharide-based VEA


content with variable SP dosages
P(maximum) / P(hydrostatic)

1.0

Slump flow = 650 mm


w/cm = 0.40
Sand-to-aggregate ratio = 0.46
Ternary cement = 450 kg/m

0.9
0.8

high VEA dosage

0.7
N-no VEA
(reference SCC )

0.6

Naphthalene
HRWRA

low VEA dosage

0.5
0

50

100

150
200
250
300
Time after casting (min)

350

400

Effect of Stabilizers
Incorporation of low thickener VEA in SCC with 0.40
w/cm can lead to lower lateral pressure than in SCC
with 0.36 w/cm and no VEA
Medium or high content of polysaccharide-based
VEA + PNS-based HRWRA resulted in higher
residual pressure and lower rate of pressure drop
after casting compared to SCC with low dosage of
VEA (attributed to increased HRWRA demand)
Similar results with cellulose VEA + polycarboxylatebased HRWRA

P(maximum) / P(hydrostatic)

Effect of Thickner Type (low concentration)


Slump flow = 650 mm
w/cm = 0.40
Sand-to-total aggregate ratio = 0.46
Ternary cement = 450 kg/m

1.0
0.9
0.8

C-Cell-L

0.7
0.6

N-Poly-L
M-PC-L

0.5

N-Pow-L

0.4
0

50

100

150

200

Time after casting (min)

250

300

Effect of Stabilizers
Mixtures incorporating TEA exhibited the lowest

initial pressure and the fastest rate of pressure drop


Unlike conventional VEA, increase in TEA lead to
further reduction in initial pressure and increased
rate of drop in pressure

Effect of Binder Type


Slump flow = 650 mm
w/cm = 0.40
S/A = 0.46

P(maximum) / P(hydrostatic)

1.0

0.9
Type I cement
0.8

8% SF

0.7

0.6

6% SF +

Binder content =
450 kg/m

22% FA

Type III cement

0.5
0

50

100

150

200

250

Time after casting (min)

300

350

P(maximum) / P(hydrostatic)

Effect of Binder Content

0.9

Slump flow = 650 mm


w/cm = 0.40
Sand-to-total agg. = 0.46

0.8

Ternary cement

1.0

400 kg/m

0.7
0.6

450 kg/m

0.5

500 kg/m
550 kg/m

0.4
0

50

100

150

200

250

Time after casting (min)

300

350

P(maximum) / P(hydrostatic)

Effect of w/cm
Slump flow = 650 mm
Sand-to-total aggregate ratio = 0.46
Polycarboxylate-based HRWRA
Ternary cement = 450 kg/m

1.0
0.9

w/cm = 0.36
0.8
0.7

w/cm = 0.40

Higher
HRWRA dosage

0.6

w/cm = 0.46
0.5
0

50

100

150

200

250

Time after casting (min)

300

350

Effect of S/A (Internal Friction)


Slump flow = 650 mm; w/cm = 0.40
Ternary cement = 450 kg/m

P(maximum) / P(hydrostatic)

1.0

0.9

R = 1.0
0.8

R = 0.75

0.7

R = 0.50

0.6

R : sand-to-total
agg. ratio

R = 0.40
R = 0.30

R = 0.36

0.5
0

100

200

Time after casting (min)

300

400

tc

K(t)

K0 at various H

Units

Statistical models to predict: K0@Hi, K(t), tc


Predicting model in CODED values
(, Vca, S/A ) = -1 to +1

R2

Relative
error 95%
conf. limit
(%)

K0@H=4 m = 82 - 3.175 Vca - 3.015 + 1.6875 S/A + 0.9 . Vca

0.94

2.4

K0@H=8 m = 67.2 - 4.7275 Vca + 4.0675 + 1.96 S/A + 1.1775 . Vca

0.94

2.3

K0@H=12 m = 53.5 - 6.2775 Vca + 5.1175 + 2.2325 S/A

0.91

%/min K(t)(0-60min) = 0.1683 + 0.0325 Vca - 0.0175 S/A - 0.0075 S/A. Vca

0.98

1.4

%/min K(t)(0-tc) = 0.16 - 0.00625 + 0.0044 S/A + 0.0006 Vca

0.88

4.6

0.98

5.5

min tc = 587.7 - 48.56 Vca + 38.06 + 24.19 S/A + 9.9375 .S/A

Contour diagrams
= 720 mm

Vca, by volume

K0@H=4m (%)

S/A, by volume

Conclusions
Thixotropy of SCC can be assessed by structural breakdown
and structural build-up at rest
Breakdown area (Ab) or drop in apparent viscosity to assess
thixotropy are determined using concrete rheometer
Structural build-up at rest can be determined as:
Variation of drop in apparent viscosity with time using
concrete rheometer
Variation of static yield stress at rest using concrete
rheometer
Variation of static yield stress at rest using empirical tests
(inclined plane and portable vane tests)

IBRACON, October 9, 2012

Conclusions
Increase of structural breakdown or structural build-up at
rest leads to reduction in form pressure exerted by SCC
Residual interlayer bond of SCC increases with decrease in
structural build-up at rest
Long delayed time between casting two successive SCC
layers leads to reduction in interlayer bond
Residual inter-layer bond strength is more critical in shear
than in flexural or compression failure modes
Key parameters affecting thixotropy are similar for form
pressure and interlayer bonds characteristics

IBRACON, October 9, 2012

Conclusions 1/2
Field studies validate importance of thixotropy
on form pressure characteristics

SCC of high thixotropy can exhibit:


lower initial lateral pressure
faster drop in pressure with time

Conclusions 2/2
Formwork pressure of SCC = f (shear strength properties)
1) Internal friction

Maximum initial pressure

(higher aggregate volume, lower binder content


and w/cm, use of SCM, lower consistency level, ...)
2) Cohesion

Rate of pressure drop with time

(higher binder content, use of SCM and setaccelerator, lower HRWRA, higher temperature,
lower consistency level, ...)

IBRACON, October 9, 2012

IBRACON, October 9, 2012

IBRACON, October 9, 2012

IBRACON, October 9, 2012

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