Figure 1. Troubleshooting may require a variety of test equipmentsome typical items are shown here
Having the right tools is important, too. They need not be expensive, but it helps if you have them in
your gear bag ready to use. Figure1
shows (left to right) a Pitot tube for
flow measurement, a measuring
tape, pipe-thread-to-barbed tubing
adapters and connectors, a digital
manometer, thermocouples and a
field readout, a hand-held infrared
temperature probe, a clamp-on ammeter and multimeter, a combination
pressure/vacuum gage, a roll of electrical tape, and of course a flashlight.
They will help you get the hard data
you need to back up your hunches.
One can also use bigger and more
expensive tools, like the combustion test system shown in Figure 2,
to provide fast feedback on what
is going on inside the process. For
those who want to learn about the
wide variety of tools used by many
trades, government training manuals
and other source materials are available online [1, 2].
Chemical Engineering
June 2016
spite being equipped with a state-ofthe-art venturi scrubber and packedtower acid-gas absorber. After three
failed stack tests, we were called in
to fix the problem. First step was to
get the stack test data. It was horrible. Emissions exceeded the normal
particulate-matter guaranteewith
no air pollution controlof 0.08
grains/dry std. ft3 (180 mg/dry std.
m3). We called the test company to
ask about the M5 filter paper used in
the test: what did it look like? They
said it had a heavy coating of white
dust. The heavy coating was no surprise, but white dust? From an incinerator? This was the first clue, since
the expected color would range from
brown to gray.
The white color suggested a spraydried sub-micron salt fume from the
caustic scrubber, which turns HCl
into NaCl. The venturi was designed
with a freshwater pre-quench to preclude sub-micron salt fume generation; the aim was to reduce the temperature to below 600F before the
gas entered the venturi throat. The
venturi itself had a high flow of recirculated salt water sprayed in downstream of the pre-quench. This salt
water, if vaporized, would produce
the salt particlesand this was
clearly happening in practice.
The venturi vendor had changed
the pre-quench nozzle several times,
hoping to address the issue, and finally changed the original solid-cone
spray to a radial-fan spray. This was
pointless, since the replacement
nozzle had less time for gas/water
contact and quenching than did the
original. It seemed that the real problem lay elsewhere.
The piping was straightforward:
fresh makeup water went to the prequench nozzle at a relatively steady
rate to handle the adiabatic quench
Chemical Engineering
www.chemengonline.com
June 2016
Finding leaks
Notches from
ball clamping the
poppet stem
Preventing bypassing
Upstream problems
June 2016
Victaulic
coupling
Perfection is
www.sturtevantinc.com
Circle 28 on p. 74 or go to adlinks.chemengonline.com/61496-28
www.chemengonline.com
June 2016
65
Original
cooler duct
Oxidizer
New duct
Chemistry 101
June 2016
Melted copper
Electrical issues
chesterton.com/chemical
24338 2016 A.W. Chesterton Company.
Circle 01 on p. 74 or go to adlinks.chemengonline.com/61496-01
www.chemengonline.com
June 2016
67
Uncooperative machinery
Summary
References
1. Tools and Their Uses an Armed Forces training manual
www.maritime.org/doc/pdf/tools.pdf.
2. Voltmeter and Amprobe Instructions www.wikihow.com/
Use-a-Multimeter.
3. McGowan, T., Disperse-Phase Pneumatic Conveying
of Glass Beads in a Four-Inch Diameter Plexiglas Loop,
M.S. Thesis, Department of Chemical Engineering, Manhattan College, New York, May, 1974.
Authors
Thomas F. McGowan is president
and founder of TMTS Associates
Inc. (399 Pavillion Street, Atlanta,
GA 30315; Phone: 404627
4722;Email:tmtsassociates1000@
mindspring.com; Website: www.
tmtsassociates.com), a firm that
specializes in thermal systems and
air-pollution control. Prior to starting the firm in 1998, he was employed by RMT/Four Nines, Envirite, the Georgia Tech
Research Institute, and Particulate Solid Research, Inc.
McGowan has 40 years of experience in troubleshooting
combustion, air pollution control, and solids handling, and
received the Chemical Engineering magazine 2010
Award for Personal Achievement. He holds an M.S. ChE
from Manhattan College in New York City, and a masters
degree in Industrial Management from Georgia Tech. He
is a registered professional engineer (PE).
Dennis J. Coughlin is an engineering and management consultant, primarily supporting TMTS
Associates, Inc. (contact details as
above). He serves companies in
manufacturing and the chemical
process industries, and focuses
predominantly on combustion,
thermal treatment, air-pollution
control, application of alternative
fuels, and power generation. He was previously employed by Westinghouse, GTRI, and Lucent Technologies. He held a number of positions at various facilities
with Lucent, including director of manufacturing, director of facilities and construction, and manager of global
procurement. He has over 40 years of engineering and
management experience, and holds a B.S. in industrial
engineering from Georgia Tech.
www.chemengonline.com
June 2016