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SR.11.

10343

QUEST CO2 CAPTURE PROJECTAMINE UNIT

Basic Design Package

SR.11.10343

QUEST CO2 Capture Project - Amine Unit


Basic Design Package
by
Roger Rangi - SIEP-PTU/TDUA
Akanksha Joura - GSUSI-PTU/TDUA
Keywords: Amine, MDEA, ADIP-X, Carbon Dioxide, CO2 Capture

SR.11.10343

Document History:
Date

Issue

February 2011

February 2011

Reason for
change
Issued For
Comments
Final Issue

Author Name / Ref.Ind.


R. Rangi, SIEP-PTU/TDUA
A. Joura, GSUSI-PTU/TDUA
R. Rangi, SIEP-PTU/TDUA
A. Joura, GSUSI-PTU/TDUA

Approved Name / Ref.Ind.


Signature
P. Nasir, SIEP-PTU/TDUA
P. Nasir, SIEP-PTU/TDUA

SR.11.10343

Summary
Shell Canada Energy operates two existing Hydrogen Manufacturing Units (HMU1 & HMU2) and is in
the process of designing and constructing a 3rd HMU (Expansion 1 HMU) at the AOSP Scotford
Upgrader. The PSA feed gas stream in each HMU is relatively rich in CO2. As part of the Green House
Gas reduction initiatives, Shell has undertaken FED2 study for a CO2 capture facility to recover up to
80% CO2 from the PSA feed gas. The recovered CO2 will be compressed, dehydrated and transported
to sequestration sites by others. The CO2 capture facility is an ADIP-X based absorption and
regeneration system.
This Basic Design Package (BDP) provides design information on amine absorption and regeneration for
the CO2 capture portion of the QUEST CO2 Capture Project. In the absorption section, the three
untreated gas streams from Hydrogen Manufacturing Units are contacted with lean amine streams in
their respective amine absorbers (C-1, C-2 and C-3) where 80% of CO2 in the feed gas streams is
removed from the gas. The treated gas streams leave the top of the absorbers while the rich amine
streams containing the absorbed CO2 leave the bottom. Treated gas streams from the three amine
absorbers are further treated in their respective water wash sections to reduce amine carry over to
less than 1 ppmw amine and to cool the gas streams to 35C. The rich amine from the absorption
section is then sent to the regeneration section where CO2 is stripped from the rich solution. The
regeneration section consists of a reboiled amine stripper, an overhead condenser and a reflux drum.
The combined rich amine from the three absorbers is first preheated with lean amine in a heat
exchanger and then de-pressurized before it is fed to the low pressure amine stripper. The rich amine
is stripped counter-currently in the stripper column with steam generated in the reboiler. The
overhead vapor stream from the regenerator stripping section containing CO2 is routed through the
water wash section in the top of the column to an overhead condenser to recover water. The
condensed water is collected in an overhead reflux drum and pumped back to the top of the column.
The acid gas stream from the reflux vessel is then routed to CO2 compression facility.

Key Amine Unit Parameters


ITEM

UNIT

C-1

C-2

C-3

Feed Gas Flow

kg-mol/h

7106.4

7106.4

10342.8

Feed Gas CO2 Content

kg-mol/h

1173.3

1173.3

1766.6

Treated Gas CO2


Specification

kg-mol/h

234.7

234.7

353.3

Treated Gas Temperature

35

35

35

Lean Amine Temperature

30

30

30

Std. Lean Amine Flow Rate

m3/h

429.0

429.0

631.9

Lean Amine CO2 Loading

mole CO2 / mole Amine

0.03

0.03

0.03

SR.11.10343

Table of Contents
1

INTRODUCTION

BASIS OF DESIGN

2.1
2.2
2.3
2.4
2.5
2.6
2.7
2.7.1
2.7.2
3

PROCESS DESIGN
3.1
3.1.1
3.1.2
3.1.3
3.1.4
3.2
3.3
3.4
3.5
3.6
3.7
3.8
3.9
3.9.1
3.9.2
3.9.3
3.9.4
3.9.5
3.9.6
3.9.7
3.9.8
3.9.9
3.9.10
3.10
3.10.1
3.10.2
3.10.2.1
3.10.2.2

3.11
4

AMINE CONTACTOR FEED GAS RATES AND OPERATING CONDITIONS


AMINE CONTACTOR FEED GAS COMPOSITION
TOWER DESIGN FACTORS
TURNDOWN
SPECIFICATIONS
TYPE OF TREATING SOLVENT
UTILITY AND SITE CONDITIONS
Site Conditions
Utility Information
PROCESS DESCRIPTION
Absorption Section
Water Wash Section
Amine Regeneration Section
Cooling and Filtering Section
PROCESS FLOW DIAGRAM
BASIS FOR THE SELECTION OF PROCESS CONDITIONS
HEAT & MATERIAL BALANCE
CHEMISTRY OF THE ADIP-X PROCESS
ADIP-X LABORATORY METHODS
FORMATION OF SOLIDS
DEMAND FOR RECLAIMING
ESTIMATED UTILITY REQUIREMENTS
Electricity
Low Pressure Steam
Low Pressure Condensate
Low Pressure Boiler Feed Water
Cooling Water
Nitrogen / Inert Gas
Make-up Water
Instrument Air
Utility Air
Utility Water
CATALYST AND CHEMICAL SUMMARY
Catalyst
Chemicals
Amine
Antifoam

WASTE STREAMS

EQUIPMENT DESIGN CONSIDERATIONS


4.1
4.2
4.2.1
4.2.2
4.2.3
4.2.4

SIZED EQUIPMENT LISTS


TOWERS
Amine Absorber #1, C-1
Amine Absorber #2, C-2
Amine Absorber #3, C-3
Amine Stripper, C-4

8
9
9
9
9
10
10
10
12
13
13
13
14
16
17
17
18
18
18
18
18
19
19
20
20
20
20
20
21
21
21
21
22
22
22
22
22
23

23
24
24
24
24
25
26
27

SR.11.10343

4.3
4.3.1
4.3.2
4.3.3
4.3.4
4.3.5
4.3.6
4.3.7
4.4
4.4.1
4.4.2
4.4.3
4.5
4.5.1
4.5.2
4.5.3
4.5.4
4.5.5
4.5.6
4.5.7
4.5.8
4.6
4.6.1
4.6.2
4.6.3
4.6.4
4.6.5
4.6.6
4.6.7
4.6.8
4.7
4.7.1
4.8
4.8.1
4.8.2
4.8.3
4.8.4
4.8.5
4.9
5

VESSELS
Absorber #1 Water Wash Vessel, V-1
Absorber #2 Water Wash Vessel, V-2
Absorber #3 Water Wash Vessel, V-3
Reflux Drum, V-4
Closed Amine Drain Collection Drum, V-5
Lean Amine Carbon Filter, D-1
Lean Amine Surge / Storage Drum
FILTERS
Lean Amine Filter, F-1
Lean Amine Post Filter, F-2
Closed Amine Drain Collection Filter, F-3
EXCHANGERS
Absorber #1 Circulating Water Cooler, E-1
Absorber #2 Circulating Water Cooler, E-2
Absorber #3 Circulating Water Cooler, E-3
Lean / Rich Amine Exchanger, E-4
Stripper OVHD Condenser, E-5
Stripper Reboiler, E-6 A/B
Lean Amine Cooler, E-7 A/B
Lean Amine Trim Cooler, E-8 A/B
ROTATING EQUIPMENT
Lean Amine Booster Pumps, P-1 A/B
Stripper Reflux Pumps, P-2 A/B
Lean Amine Charge Pumps, P- 3 A/B
Absorber #1 Circulating Water Wash Pumps, P- 4 A/B
Absorber #2 Circulating Water Wash Pumps, P- 5 A/B
Absorber #3 Circulating Water Wash Pumps, P- 6 A/B
Amine Make-up Tank Pump, P-7
Closed Drain Amine Pump, P-8
TANKS
Amine Make-up Tank, T-1
PIPING
Two phase flow
Hot Lean Solvent Piping
Piping Upstream of Schoepentoeter
Rich Amine Piping Downstream of Control Valves
Sample Points
WINTERIZATION

PROCESS CONTROL PHILOSOPHY


5.1
5.2
5.2.1
5.2.2
5.3
5.3.1
5.3.2
5.3.3
5.3.4
5.3.5
5.4
5.4.1

GENERAL COMMENTS
AMINE ABSORPTION
Amine Absorbers
Water Wash Vessels
AMINE STRIPPER
Amine Stripper Feed Control
Reboiler Steam Control
Stripper Bottoms Level Control
Stripper Pressure Control
Regeneration Reflux Section Level Control
AMINE COOLING
Lean Amine

29
29
30
31
32
33
33
33
33
33
34
34
34
34
34
35
35
35
35
36
36
37
37
37
38
38
38
38
38
39
39
39
39
39
40
40
40
40
41
42
42
42
42
42
43
43
43
43
43
43
44
44

SR.11.10343

LEAN AMINE FILTRATION


AMINE WATER BALANCE

44
44

SAFEGUARDING PHILOSOPHY

45

5.5
5.6
6

6.1
6.1.1
6.2
6.3
6.3.1
6.3.2
7

EMERGENCY DEPRESSURIZING
Relief valves
INSTRUMENTED PROTECTED FUNCTIONS
ADDITIONAL SAFETY REQUIREMENTS
Good operating practices amine solutions
Spillage/disposal amine solutions

MATERIAL SELECTION

45
45
46
48
48
48
49

APPENDIX A:

SUMMARY OF PROCESS OPTIMIZATION STUDIES

51

APPENDIX B:

PROCESS FLOW DIAGRAM AND HEAT & MATERIAL BALANCES

60

APPENDIX C:

SIZED EQUIPMENT LIST

67

APPENDIX D:

PROCESS EQUIPMENT DATA SHEETS

70

APPENDIX D1- COLUMNS

71

APPENDIX D2- EXCHANGERS

72

APPENDIX D3- VESSELS

73

APPENDIX D4- ROTATING EQUIPMENT

74

APPENDIX D5- FILTERS

75

APPENDIX D6- TANKS

76

APPENDIX E:

MATERIAL SELECTION GUIDE

77

APPENDIX F:

MATERIAL SAFETY DATA SHEETS

79

BIBLIOGRAPHIC INFORMATION

102

REPORT DISTRIBUTION

103

SR.11.10343

Introduction

Shell Canada Energy operates two existing Hydrogen Manufacturing Units (HMU1 & HMU2) and is in
the process of designing and constructing a 3rd HMU (Expansion 1 HMU) at the AOSP Scotford
Upgrader. The PSA feed gas stream in each HMU is relatively rich in CO2. As part of the Green House
Gas reduction initiatives, Shell has undertaken FED2 study for a CO2 capture facility to recover up to
80% CO2 from the PSA feed gas. The recovered CO2 will be compressed, dehydrated and transported
to sequestration sites by others. The CO2 capture facility is an ADIP-X based absorption and
regeneration system.
This Basic Design Package (BDP) provides design information on amine absorption and regeneration for
the CO2 capture portion of the QUEST CO2 Capture Project. The amine absorption section is designed
to treat three separate gas streams from the three Hydrogen Manufacturing Units. C-1 and C-2
absorbers are each designed to treat 168031 m3/h of CO2 rich hydrogen gas from HMU1 and HMU2,
respectively and C-3 absorber is designed to treat 244556 m3/h of CO2 rich hydrogen gas from HMU3.
Feed composition, process conditions and flows for C-1 and C-2 absorbers are same and therefore the
two absorber columns (C-1 and C-2) have identical design. Each of the feed gas streams to C-1 and C-2
absorbers have 1173.3 kg-mol/h of CO2 that is equal to 16.51 mol% of the stream. The C-1 and C-2
amine absorbers will each remove 80% of the CO2 in the feed to achieve 234.7 kg-mol/h of CO2 in
their treated gas streams. The feed gas to C-3 absorber has 1766.6 kg-mol/h of CO2 equal to 17.08
mol% of the stream. The C-3 amine absorber will remove 80% of the CO2 in the feed to achieve 353.3
kg-mol/h of CO2 in the treated gas stream. The feed gases to the three absorbers are treated with
lean amine in their respective amine absorbers for CO2 removal. Treated gas streams from the three
amine absorbers are further treated in their respective water wash sections to reduce amine carry
over to less than 1 ppmw amine and to cool the gas streams to 35C.
The combined rich amine from the three absorbers is treated in the regeneration section where CO2 is
stripped from the rich solution. The regeneration section consists of a reboiled amine stripper, an
overhead condenser and a reflux drum. The combined rich amine from the three absorbers is first
preheated with lean amine in a lean/rich heat exchanger and then de-pressurized before it is fed to the
low pressure amine stripper. The CO2 in the rich amine is stripped in the amine stripper column by the
steam generated in the reboiler. The overhead vapor from the regenerator stripping section containing
CO2 is routed through the water wash section in the top of the column to an overhead condenser to
condense and recover water. The condensed water is collected in an overhead reflux drum and
pumped back to the top of the column. The acid gas stream from the reflux vessel is then routed to
CO2 compression facility. Low pressure steam (300 kPa(g)) is used in the reboiler to achieve a lean
amine CO2 loading of 0.03 mol/mol of amine. The lean amine is cooled, filtered and is returned to the
top of the absorbers.
This design is based on ADIP-X solvent composition of 40 wt% MDEA, 5 wt% DEDA and 55 wt% water.
The combined lean amine circulation through the CO2 Capture Amine Unit is 1489.9 (std.) m3/h.

SR.11.10343

Basis of design

The following sections summarize the Basis of Design (BOD) for the Amine Absorption and Amine
Regeneration Unit for QUEST CO2 Capture Project that was agreed with Shell Canada Energy. The
initial Design Basis information was provided by Shell Canada in an email dated March 31, 2008 and
included in Scope of Work Acceptance document dated May 05, 2008.
The composition, conditions and flow rates of the feed streams to all three absorbers were revised in
October 2008. The revised feed basis was provided in an email dated October 14, 2008. The revised
design is based on the October 2008 feed data.
The original premise and the process design was based on minimizing steam consumption in the CO2
capture unit. During Process Simplification Workshop in May 2010 it was recognized that additional
low pressure steam would be available for the CO2 capture unit. It was determined that the cost of
CO2 capture unit will be significantly reduced by changing the original design by utilizing this additional
steam for amine regeneration. Shell Canada revised the design premise to allow the use of additional
steam for CO2 capture unit. The process design of the CO2 capture unit was therefore updated in
October, 2010 based on the revised design premise. The design was based on cooling the amine to a
temperature of 35C using reused cooling water.
It was recognized by Shell Canada in November, 2010 that fresh cooling water could be made available
for the CO2 capture unit, therefore the lean amine can be cooled to a lower temperature (30C)
compared to the original design case. It was determined that cooler lean will require lower solvent
circulation to meet the treated gas specifications as well as lower steam consumption for amine
regeneration compared to the original design case. Shell Canada therefore revised the design premise
again to allow for the use of fresh cooling water for CO2 capture unit. Due to the revised design
premise, all the air coolers from the original design were replaced with cooling water exchangers.
The current process design premise of the CO2 capture unit is based on the revised cooling water and
low pressure steam availability.

2.1

Amine Contactor Feed Gas Rates and Operating Conditions

The operating conditions and gas flow rates were specified by Shell Canada. The following table
summarizes these conditions.
Feed Gas Definition
Temperature
Pressure
Flow

C
bar(a)
kg-mol/h

Base HMU1
(To C-1)
35
30.57
7106.4

Base HMU2
(To C-2)
35
30.57
7106.4

Expansion HMU
(To C-3)
35
30.97
10342.8

SR.11.10343

2.2

Amine Contactor Feed Gas Composition

The following table provides the composition of the feed gas streams to the amine absorbers.
Feed Gas Composition
H2O
CO2
CO
N2
H2
C1
Total

2.3

Base HMU1
(To C-1)
0.18
16.51
2.41
0.30
74.79
5.81
100

mol%
mol%
mol%
mol%
mol%
mol%
mol%

Base HMU2
(To C-2)
0.18
16.51
2.41
0.30
74.79
5.81
100

Expansion HMU
(To C-3)
0.18
17.08
2.92
0.27
72.38
7.17
100

Tower Design Factors

The Amine Absorbers and Amine Stripper have been designed with the following flood and foam
factors:
Amine absorbers
Foam Factor:
Maximum allowable percent of flood:

0.71
85%

Amine Stripper
Foam Factor:
Maximum allowable percent of flood:

0.71
85%

2.4

Turndown

The amine absorbers and Amine Stripper have been designed with the following turndown capabilities:
Vessel

Section

Internals

C1
C2
C3
C4
C4

Overall
Overall
Overall
Lower
Upper

Hi Fi Trays
Hi Fi Trays
Hi Fi Trays
Hi Fi Trays
CS Trays

2.5

Turndown Weeping
(Vapor Flow)
29%
29%
29%
26%
27%

Turndown - Slot Velocity


(Liquid Flow)
36%
36%
37%
48%
-----

Specifications

Specifications for the amine absorbers:


CO2 removal:

Up to 80% removal of total CO2 in the feed stream

Treated gas temperature:

The treated gas temperature shall not exceed 35 C

Gas entrainment:

Limit gas entrainment in rich amine to 1.0 vol % of amine circulation

SR.11.10343

Amine carryover:

10

Less than 1 ppmw of total amine in treated gas

Specifications for CO2 product stream leaving the Reflux Drum:


CO2 concentration:

The CO2 product gas shall contain at least 95 mol% CO2 (on dry basis)

Gas temperature:

CO2 wet gas temperature will be 36 C

Gas pressure:

Wet CO2 gas leaving the reflux drum will be at 144 kPa (a)

Hydrocarbon concentration:

Less than 5 mol%

Water Content:

No water specification as CO2 gas dehydration and compression are


excluded from this BDP scope.

2.6

Type of Treating Solvent

The Amine Unit will use the Shell ADIP-X solvent. The ADIP-X solvent composition that will be used is
40 wt% MDEA, 5 wt% DEDA, and 55 wt% water.

2.7

Utility and Site Conditions

2.7.1 Site Conditions


Listed below are Meteorological and Site Data provided by Shell Canada.

SR.11.10343

11

METEOROLOGICAL AND SITE DATA


The meteorological and site data will be the same as defined in the Base Plant Upgrader Project and
Upgrader Expansion 1 Specification.
Normal Atmospheric Pressure

kPa

93.5

1. For the purposes of mechanical design where design for full vacuum is required: full vacuum is
based on standard barometric pressure at sea level, 101.325 kPa(abs). That is, design for full
vacuum is design for 101.325 kPa external pressure. Design for vacuum is design for 50.663
kPa external pressure.
2. For the purposes of process design: use barometric pressure of 93.5 kPa(abs). For example:
suction pressure for air compressors, fans and blowers with atmospheric air suction; flare tip
barometric pressure, etc.
Ambient Temperature
Max
Min
Mean Daily
C
Normal
Hottest month
Coldest month

Maximum

Minimum

+33.9
+2.8 +15.6
+22.3
+10.8
+10.0
-43
-13.4
-9.0
-17.9
Design
-43
+19
+28
+25
With water cooled trim cooler
+28
Without water cooled trim cooler
+40
+40 / -43
-43
-43
-60
Max Min
75% @ 28C
<1 %

Minimum
Summer wet bulb
Summer dry bulb (July)
Air cooled exchanger:
(dry bulb temperature)
Design for motors
Design for pipe expansion
Design for freeze protection
Design for material selection
Instrument air dew point max.
Relative Humidity
Summer
Winter
Precipitation
Average annual
mm
430
15 minute max
mm
20
24 hour max
mm
88
Snow load and wind velocity, direction and pressure data to be in accordance with the Alberta
Building Code.
Earthquake
Design factor R, as per table 4.1.9B of National Bldg Code
Elevation
m
623.5
Frost Protection
Design depth - foundations
m
3

SR.11.10343

12

2.7.2 Utility Information


The utility information was provided by Shell Canada in an email dated March 31, 2008 and included in
Scope of Work Acceptance document dated May 05, 2008.
The project team at Shell Canada has evaluated climate data for this region from the past 30 years to
consider using a lower air temperature for air cooled exchanger design. The project team has decided
to lower the maximum air temperature for air cooled exchanger design from 28C to 21C for CO2
capture amine unit. With air temperature of 21C and 15C approach for air cooler design, the
minimum temperature of the process outlet stream from air cooled exchangers will be 36C. (Refer to
minutes of meeting for the Joint Process Meeting dated February 18, 2009 and document on Design
Premise for Cooling for Quest Carbon Capture Project from Flour Canada Ltd. Dated June 28, 2010.)

SR.11.10343

13

Process Design

The Amine Unit for AOSP CO2 capture project is designed to remove 80% CO2 from three HMU syngas
streams. The amine absorption section is designed to treat three separate gas streams from the three
Hydrogen Manufacturing Units in three separate amine absorbers (C-1, C-2 and C-3). The feed gases to
the three absorbers are first treated with lean amine in their respective amine absorbers for CO2
removal. This design is based on ADIP-X solvent composition of 40 wt% MDEA, 5 wt% DEDA and
55 wt% water. The combined standard lean amine circulation through the unit is 1489.9 m3/h.

3.1

Process Description

The ADIP-X process used in this Amine Unit is a regenerative amine based process where CO2 is
removed from the gas stream at relatively high pressure and low temperature with a mixture of water
and amine(s). The ADIP-X process is an accelerated MDEA process using piperazine (DEDA) to enhance
the CO2 absorption over that achievable with non-accelerated MDEA. The absorbed acid gases are
removed from the amine solution in the Amine Stripper of the amine regeneration section at low
pressure and high temperature.
Details of the specific sections of the amine unit are provided in the following sections.

3.1.1 Absorption Section


Amine absorbers C-1 and C-2 are each designed to treat 168031 m3/h of CO2 rich hydrogen gas from
HMU1 and HMU2, respectively and C-3 absorber is designed to treat 244556 m3/h of CO2 rich
hydrogen gas from HMU3. Feed composition, process conditions and flows for C-1 and C-2 absorbers
are same and therefore the two absorber columns (C-1 and C-2) have identical design. The feed gas to
C-1 and C-2 absorbers each have 1173.3 kg-mol/h of CO2 equal to 16.51 mol% of the stream. The C-1
and C-2 amine absorbers will each remove 80% of the CO2 in the feed to achieve 234.7 kg-mol/h of
CO2 in their treated gas streams. The feed gas to C-3 absorber has 1766.6 kg-mol/h of CO2 equal to
17.08 mol% of the stream. The C-3 amine absorber will remove 80% of the CO2 in the feed to achieve
353.3 kg-mol/h of CO2 in the treated gas stream.
Each absorber will be provided with a feed gas bypass arrangement to accommodate shutdown or any
upset situations in the CO2 capture unit. This arrangement allows a portion or 100% of the gas to
bypass the absorber and will be mixed with the treated gas to either bring the combined gas CO2
content to a desired level or sent directly to downstream PSA unit. The bypass arrangement is a better
control scheme than manipulating amine circulation or lean amine loading.
Two separate syngas gas streams from HMU1 and HMU2 at 35 C and 3057 kPa (a) with 16.51 mol%
CO2 are fed to the bottom of Amine Absorber #1 (C-1) and Amine Absorber #2 (C-2), respectively.
Feed gas enters the column through a half-pipe distributor. Lean amine solution enters these
contactors at the top of the tower and absorbs CO2 from the gas to achieve an overall 80% CO2
removal from these columns. Lean amine at a standard liquid rate of 429 m3/h and a temperature of

SR.11.10343

14

30 C with CO2 loading of 0.03 mol / mol of amine is introduced through a branched pipe distributor at
the top of the columns. The absorbers contain 25 Shell Hi Fi trays.
Syngas gas streams from the expansion HMU (HMU3) at 35 C and 3097 kPa (a) with 17.08 mol% CO2
is fed to the bottom of Amine Absorber #3 (C-3). Feed gas enters the column through a half-pipe
distributor. Lean amine solution enters the contactor at the top of the tower and absorbs CO2 from
the gas to achieve an overall 80% CO2 removal from the column. Lean amine at a standard liquid rate
of 631.9 m3/h and a temperature of 30 C with CO2 loading of 0.03 mol / mol of amine is introduced
through a branched pipe distributor at the top of the column. The absorber contains 25 Shell Hi Fi
trays.
Rich amine leaves the bottom of all three absorber columns under level control. Rich amine streams
from the three amine absorbers are combined in a single line. The combined rich amine from the three
absorbers is first preheated with lean amine in a heat exchanger and then de-pressurized before it is
fed to the low pressure amine stripper in the regeneration section. To minimize gas entrainment in
the rich amine and to reduce hydrogen loss, a collector tray with downpipes is added below the
bottom tray (tray1) of amine absorbers along with 600 mm bed of #2 Raschig Rings in the bottom
heads of these columns. This arrangement will limit gas entrainment in rich amine to 1.0 vol % of
amine circulation.
To minimize amine entrainment with the treated gas stream leaving the amine absorbers, demisters
are installed at the gas outlet of these columns.
The operating pressure of the amine absorbers depends on the feed gas pressure. No variations in the
feed gas supply pressure are expected from the HMU to the three amine absorbers.
Trays were used for this application because the absorption of CO2 into amine is controlled by the
reaction kinetics and trays provide much larger holdup for the amine than packing. Shell Hi Fi trays
were selected for the CO2 amine absorbers to provide the necessary holdup while minimizing column
diameter. The truncated downcomer design of the Hi Fi trays make them ideal for an application like
this. Structured packing would have a much smaller liquid holdup per foot of column height than the
trays. To achieve the same 80% CO2 removal with packing, the column heights of the amine absorbers
would have to be increased relative to amine absorbers with trays. Therefore, packing was not
considered for this service.

3.1.2 Water Wash Section


Treated gas streams from the three amine absorbers are further treated in their respective water wash
sections to reduce amine carry over to less than 1 ppmw amine and to cool the gas streams to 35C.
The cooled gas temperature will be the same as feed gas temperature and therefore there is no
temperature increase across the amine unit due to CO2 capture.
Each water wash section will consist of a water wash vessel, circulating water cooler and circulating
water wash pumps. Water wash vessel will have two sections, the bottom section is a recirculating
section with 6 valve trays and the top section is a polishing section with 3 bubble cap trays. The top

SR.11.10343

15

portion of the vessel above the polishing section will also include de-entrainment devices. The
circulating water will be cooled to 33 C by circulating water coolers using cooling water. Circulating
water wash pumps will circulate water from the bottom section of the vessel, through the circulating
water cooler, back to the top of recirculating section of the vessel. Fresh make-up water will be added
to the top of the polishing section.
Gas enters the vessel through a half open pipe distributor where it is contacted with cooled
recirculating liquid. The bottom section will remove most of the amine entrained in the gas as liquid
and also the amine in the vapor phase. In addition to this, the bottom section will also cool the gas
stream to 35 C. Recirculating water wash rate is established by heat transfer requirements to meet
treated gas temperature specification. The circulation rate will be maintained at the design rate as
there is no flow control on the circulating water. However, a flow control valve can be added to the
recirculating loop to adjust the circulation rate based on the treated gas temperature requirements
and the amine removal specifications of the system. Treated gas from recirculating section will be
contacted with fresh make-up water in the polishing section to remove trace amounts of amine in the
gas stream to ensure less than 1 ppmw amine carry over. Make-up water is added on flow control to
the top polishing section. Amine concentration in the recirculating water is controlled by make-up and
purge. A portion of the recirculating stream is removed from water wash section under level control to
maintain a continuous purge. The fresh water make-up rate can be adjusted based on the amine
removal performance of the system.
To minimize water carryover with the treated gas stream to the PSA units, a packed section and a
demister are added to each water wash vessel above the top tray of the polishing section. The treated
gas from the polishing section first passes through a packed bed of 4 half layers of 250Y Mellapak
packing, equivalent to 0.42 m of packed height, and then through a 0.15 m thick demister pad. This
combined arrangement will remove 99.9% of the entrained liquid from the gas stream leaving the
polishing section.
The predicted treated gas temperature from the amine absorbers to the water wash system is 32C.
The circulating water coolers of the water wash system will be designed to cool the treated gas
streams to 35C before sending them to the PSA units. However, it is necessary to add design margin
to circulating water coolers and the water wash system to ensure that the treated gas temperature
specification of 35C is achieved under all normal operating conditions. This margin will accommodate
any variations in lean solvent temperature and the uncertainties in accurate prediction of the
temperature of treated gas streams from the amine absorbers using simulation tools for bulk CO2
removal. Therefore, the circulating water coolers and the water wash system will be designed to cool
treated gas streams from the amine absorbers from a temperature of 39C to a temperature of 35C.
Water wash vessels V-1 and V-2 are each designed for recirculation rate of 39.1 m3/h and V-3 is
designed for recirculation rate of 56.3 m3/h. Water wash vessels V-1 and V-2 are each designed for
fresh water makeup rate of 4.5 m3/h and purge rate of 4.6 m3/hr. Water wash vessels V-3 is designed
for fresh water makeup rate of 6.6 m3/h and purge rate of 6.6 m3/hr

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3.1.3 Amine Regeneration Section


The combined rich amine from the absorbers is treated in the regeneration section where CO2 is
stripped from the solution. The regeneration section consists of a reboiled amine stripper, an overhead
condenser and a reflux drum. Rich amine is removed from the absorber bottoms on level control and
collected in a common line.
The combined rich stream first passes through the Lean / Rich Amine Exchanger where it is heated by
hot lean amine coming from the bottom of the Amine stripper. The heated rich amine from the heat
exchanger at 106 C is de-pressurized from 2752 kPa (a) to 162 kPa( a) through a pressure control valve
located upstream of the stripper column before entering the stripper column. The rich amine is fed at
the top of the column through two 50% schoepentoeter inlet distributors. The stripper column
contains 20 Shell Hi-Fi stripping trays.
The vapor stream from the regenerator stripping section containing CO2, hydrogen and some
hydrocarbons is washed in the water wash section (rectifying section) of the amine stripper and is then
routed to Stripper Overhead Condenser (E-5) where the vapor is cooled. The rectifying section of the
stripper column consists of 4 calming section trays.
The cooled vapor stream and the condensed water from the overhead condenser are separated in an
overhead Reflux Drum (V-4). The CO2 gas is sent to the compression unit through a back-pressure
control valve. This back pressure valve maintains 144 kPa (a) pressure in the reflux drum. The
condensed water is returned on flow control to the top of the amine stripper as reflux by Stripper
Reflux Pumps (P-2A/B). The flow control is reset by level controller to maintain proper level in the
reflux drum. The reflux water enters the column through a branched pipe distributor.
The rich amine piping downstream of the lean / rich amine exchanger will experience two-phase flow
and therefore should be designed appropriately. This is especially important for the piping
downstream of the back pressure control valve as the amount of vapor is even larger.
In the bottom stripping section of the amine stripper, the CO2 in the amine is removed by stripping
steam. CO2 is removed from the amine solution by a combination of high temperature, low pressure,
and stripping steam (to reduce the acid gas partial pressure). The contact between the stripping steam
and solvent is performed within the regenerator using trays. Steam generated by re-boiling the
solvent provides:
i)
ii)
iii)

Heat for raising the temperature of the feed (rich amine)


Heat of de-sorption of CO2
Heat to generate stripping steam (to reduce CO2 partial pressure).

The heat for generating stripping steam in the stripper reboiler (E-6 A/B) is provided by low pressure
steam. There are two heat exchangers for this reboiler service. Amine collected in the draw-off tray
below the bottom tray (tray 1) feeds the reboiler. Two draw nozzles on the draw-off tray feed the (2)
two reboiler exchangers. The vapors from the reboiler are returned to the column through two
separate nozzles through half pipe distributors. The liquid from the reboiler that overflows the weir in
the exchangers is sent to the bottom of the stripper column.

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To prevent amine degradation, the temperature of the unheated surface on the amine side should be
below 140C.
To minimize water and amine entrainment with CO2 gas stream leaving the amine stripper and the
reflux drums, demisters will be installed at the gas outlets of the amine stripper column and reflux
drum.
The regenerated lean amine leaves the bottom of the stripper column on level control. Lean amine at
standard liquid rate of 1489.9 m3/h leaves the stripper column at 119 C with CO2 loading of 0.03 mol /
mol amine.
The stripped CO2 gas from the amine stripper leaves the reflux drum as recovered CO2 gas at 36 C
and 144 kPa pressure to compression section. CO2 compression and dehydration are not in the scope
of amine unit.

3.1.4

Cooling and Filtering Section

The hot lean amine from amine stripper sump is pumped out by lean amine booster pumps under level
control. Before returning to the amine absorbers, the lean amine is cooled in a series of heat
exchangers. The first stage cooling is accomplished in the lean / rich amine exchanger (E-4) by
preheating the rich amine feed to amine stripper where the lean amine is cooled to 78 C temperature.
The lean amine is then further cooled to 50 C in the lean amine coolers (E-7 A/B). Lean amine trim
coolers (E-8 A/B) finally cools the lean amine to 30C. Maintaining proper temperature of the lean
amine supplied to the amine absorbers is important for the absorber operation. If the amine is too
hot, the treat achieved in the contactor may be negatively affected.
The cooled lean amine is treated in the filtration section before it is returned to the amine absorbers.
The filtration section consists of one main particulate filter (Lean Amine Filter, F-1) followed by a
slipstream Lean Amine Carbon Filter (D-1) and its after particulate filter (Lean Amine Post Filter, F-2).
The main particulate filter is sized for 25% of the lean amine flow whereas the, carbon filter is sized for
approximately 5% of the lean amine flow.
The filtered lean amine is finally pumped back to the amine absorbers by lean amine charge pump (P-3
A/B). The flow of amine to the amine absorbers is under flow control.
Water content of the amine can be determined by Karl Fischer analysis and should be checked at
regular intervals. If the percent weight of amine in the solution is being monitored daily, the water
content check by Karl Fischer can be performed two or three times a week. Otherwise, the water
content should be checked at least once per day. It is recommended that water content be measured
by each shift.

3.2

Process Flow Diagram

Process flow diagram for this unit can be found in Appendix B.

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3.3

18

Basis for the Selection of Process Conditions

Several optimization studies were carried out to establish the process design conditions for CO2
capture unit. The basis and results of these studies are summarized in Appendix A.

3.4

Heat & Material Balance

Heat and material balance to be used in conjunction with the Process Flow Diagram to define the
operation of the Amine Unit can be found in Appendix B.

3.5

Chemistry of the ADIP-X Process

The chemistry with respect to CO2 in the liquid phase is discussed here.
During absorption the equilibrium between CO2 and the amine solvent is directed towards the liquid
phase, while during regeneration (i.e. low pressure, high temperature) the equilibrium is shifted
towards the gas phase. The equations below show the overall reactions involved and their respective
speed of reaction.
Reaction with MDEA (bi-carbonate):

CO 2 + MDEA + H 2 O slow

MDEAH + + HCO3

(R 1)

Reaction with accelerator:


The accelerator is piperazine or DEDA, a cyclic diamine. The presence of an accelerator in an aqueous
MDEA solvent highly improves the CO2 removal efficiency of the process. Due to its nature, the
reaction products at elevated loadings block the accelerator, consequently neutralizing its effect.
fast
CO2 + Acc veryfast
AccCOO H + + MDEA

AccCOO + MDEAH +

(R 2)

fast
AccCOO + H 2 O

Acc + HCO3

(R 3)

3.6

ADIP-X Laboratory Methods

The test method SMS number 2930 "Regenerable Free Base, Actual Total Base and Piperazine
Contents of ADIP-X Containing Treating Solutions" is used for measuring and hence controlling MDEA
and DEDA concentration in the solvent.

3.7

Formation of Solids

It is known that under certain circumstances the following precipitation reactions with DEDA can
occur:

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Formation of DEDA-bicarbamate precipitation. This only happens below a certain temperature


limit and above a certain amine loading. Under normal operating conditions this will not occur.

Formation of hexa-hydrate precipitation of DEDA in lean solvent at low temperatures. This is a


normal solubility problem of DEDA in water (affected by the amount of MDEA present). If lean
solvent film temperature is kept above 20 C this precipitation can be avoided under all
circumstances.

3.8

Demand for Reclaiming

During normal operation, the ADIP-X process does not form by-products like oxazolidone and
therefore does not require a reclaimer unit for this reason.
However, as with any MDEA process there is the potential for degradation of amine. Monitoring of the
solvent quality remains necessary, and reclaiming (e. g. bleed/feed of the solvent) cannot be excluded
for ADIP-X. Based on the quality of gas streams being processed in this unit, the amount of
degradation is expected to be very low.

3.9

Estimated Utility Requirements

The following Utilities are required for the Amine Unit

Electricity

Low pressure steam

Cooling Water

Nitrogen / Inert Gas

Make-up Water

Instrument Air

Utility Air

Utility Water

The estimated utility consumption associated with the amine unit is summarized below. The utilities
listed below account for the process demand but not for the requirements of items like utility stations.

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3.9.1

20

Electricity

The electrical load information provided below reflects the estimated process equipment electrical
requirements. These values include estimates of pump efficiency but do not reflect the selection of
actual motor sizes.

Item
P-1A/B
P-2A/B
P-3A/B
P-4A/B
P-5A/B
P-6 A/B
P-7
P-8

Service
Lean Amine Booster Pump
Stripper Reflux Pump
Lean Amine Charge Pump
Absorber #1 Circulating Water Wash Pump
Absorber #2 Circulating Water Wash Pump
Absorber #3 Circulating Water Wash Pump
Amine Make-Up Tank Pump
Closed Drain Amine Pump
Total

BHP
(Per Item)
KW
653
10
1732
5
5
7
2
4

Electric Demand
(Per Item)
KW
817
12
2165
6
6
8
3
4

MW

3.02

Note 1: Electric demand for pumps is based on motor efficiency of 80%


Note 2: Pumps P-7 and P-8 are not in continuous operation

3.9.2 Low Pressure Steam


Low pressure steam will be used to supply the heat required for the amine stripper reboiler (E-6 A/B).
The heat duty of the reboiler is 96.08 MW and it requires 162,025 kg/h of saturated steam at 300 kPa
(g) pressure.

3.9.3 Low Pressure Condensate


Amine stripper reboiler (E-6 A/B) generates 162,025 kg/h of low pressure condensate by condensing
steam in the two heat exchangers.

3.9.4 Low Pressure Boiler Feed Water


As saturated steam is required in the amine stripper reboiler, 13,458 kg/h of low pressure boiler feed
water (BFW) may be required to de-superheat steam if LP steam is supplied to the amine unit at 350
kPa (g) and 240 C.

3.9.5 Cooling Water


Cooling water is required for cooling the following streams:
Circulating water streams in the absorber overhead water wash vessels
Amine stripper overhead acid gas stream

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Lean amine stream downstream of the lean rich exchanger

Heat duties and the cooling water demand for these heat exchangers are provided below.

Item

Description

E-1
E-2
E-3
E-5
E-7 A/B
E-8 A/B

Absorber #1 Circulating Water Cooler


Absorber #2 Circulating Water Cooler
Absorber #3 Circulating Water Cooler
Stripper OVHD Condenser
Lean Amine Coolers
Lean Amine Trim Coolers

Duty
MW
0.237
0.237
0.342
25.34
41.50
29.52

Total Consumption

Water
kg/h
40,734
40,734
58,880
1,284,240
2,102,836
1,495,800

DT
C
5
5
5
17
17
17

5,023,224

3.9.6 Nitrogen / Inert Gas


Inert gas is used intermittently during normal operation as blanket gas for closed amine drain
collection drum (V-5) and amine make-up tank (T-1). Required amounts are to be determined during
detailed design.

3.9.7 Make-up Water


During normal operation, make-up water is required to maintain the amine system water balance. The
water make-up can either be on a continuous or intermittent (batch) basis. Only steam condensate or
similar quality water shall be used for make-up. Additional discussion on water balance can be found in
Section 5, Process Control Philosophy.
Approximately 2.4 m3/h (2409 kg/h) of make-up water is required on continuous basis. This make-up
rate is based on vaporization losses associated with treated gas leaving amine absorbers at 32C. The
actual water make-up rates may vary depending on entrainment losses and leaks from the system.
Fresh make-up water of 4.5 m3/h (4509 kg/h) is required for each water wash vessel V-1 and V-2.
Absorber #3 Water Wash Vessel, V-3 will require 6.6 m3/h (6527 kg/h) fresh make-up water.

3.9.8 Instrument Air


Requirements to be determined during detailed design.

3.9.9 Utility Air


Requirements to be determined during detailed design.

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3.9.10 Utility Water


Requirements to be determined during detailed design.

3.10 Catalyst and Chemical Summary

3.10.1 Catalyst
There is no catalyst required for the Amine Unit

3.10.2 Chemicals
There are two chemicals utilized in the Amine Unit. These are:

Amine (continuous use)

Anti-foam (intermittent use)

3.10.2.1 Amine
The amine used in this unit is ADIP-X amine solution, which will be a combination of MDEA, DEDA
(piperazine), and water. The target concentration for the ADIP-X operation will be 40 wt% MDEA, 5
wt% DEDA, and 55 wt% water.
The maximum allowable amine concentration is 50 wt% amine. This applies to either MDEA only
operation or ADIP-X Operation (MDEA + DEDA). Additionally, the maximum allowable DEDA
concentration is 8.5 wt%.
The lean amine produced in the Amine Regenerator will have the following loading:
Lean Amine CO2 Loading:

0.03 mole CO2 / mole amine

The circulating solution should also satisfy the following requirements:

Content of heat stable salts < 1 wt% of total solvent

pH of solvent > 10.5

Suspended solids < 30 ppmw with a preferred target of < 10 ppmw

Chlorine level in the solvent is limited to 1000 ppmw

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3.10.2.2 Antifoam
The presence of particulates as well as amine degradation products in the amine solution can lead to
foaming problems in the amine absorbers or amine stripper. As a result, provision should be made to
allow antifoam injection into either the top of the amine absorbers (lean amine feed) or the top of the
amine stripper (rich amine feed). All connections are required but only the one serving the tower
foaming at the time is to be used. Depending on equipment layout and distance between them, one or
more antifoam systems may be required.
Generally two major types of antifoam are used in amine units. These are polyglycol and silicone
based antifoams. The polyglycol type is recommended and is preferred over the silicone antifoams.
While the silicone type can be effective (especially in the regenerator), it will tend to build-up in
systems without carbon filtration and can lead to fouling of equipment. Since this amine unit has a
carbon filtration system, the carbon filter will remove the silicone and this loads up the carbon and
consequently increases the required frequency of change-out. In effect, with silicone antifoam
addition for units that have carbon filtration, the silicone is removed from the system by carbon bed as
it is added. Betz MaxAmine is recommended for this unit.
Conventional chemical injection pumps, shot pots, and injection blowcases, or injection pots, have
been successfully used for antifoam addition.

3.11 Waste Streams


During operation, there are four waste stream generated in the Amine Unit. These are:
Water purge from the amine overhead reflux section to the Waste Water System. Normally,
there will be no flow in this stream as water addition is expected to maintain the system water
balance.
Water purge from Absorber #1 water wash vessel (V-1) and Absorber #2 water wash vessel (V2). A portion of these streams is used as water make-up for amine unit and the remaining goes
to the existing waste water treatment facility.
Water purge from Absorber #3 water wash vessel (V-3). This stream is sent to the existing
waste water treatment facility.

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Equipment Design Considerations

This section describes additional considerations for the design of equipment and provides a summary
of the equipment design. Process conditions, upon which the design of new equipment is based, are
provided in the Process Flow Diagrams, Material Balances, and Process Equipment Data Sheets.
Refer to Appendix D for the Process Equipment Data Sheets.
The following sections provide guidance to the designer of Shell specific requirements for individual
equipment items or appropriate groups of equipment or piping. The Engineering Contractor shall
perform the detailed design of equipment. Additional considerations may be warranted, based on
equipment manufactures margin or engineering contractors experience or plant operators
preference.

4.1

Sized Equipment Lists

Refer to Appendix C for Sized Equipment List developed for this unit as a part of this BDP.

4.2

Towers

There are four towers in the amine unit, these are:


1. Amine Absorber #1 (C-1)
2. Amine Absorber #2 (C-2)
3. Amine Absorber #3 (C-3)
4. Amine Stripper (C-4)
Amine absorber #1 and amine absorber #2 are designed to process same gas feed streams with same
process conditions and therefore towers C-1 and C-2 have similar design.

4.2.1 Amine Absorber #1, C-1


This amine absorber is a trayed column with Shell Hi Fi Trays as contacting medium to absorb CO2
from sour gas using lean amine solution.
The Main Design Features of the amine absorber are:
Overall column
Column ID = 3.35 m
Column Height = 23.4 m TL/TL
25 Shell Hi Fi Trays (numbered from bottom up bottom tray is #1 and top tray is #25)

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Number of tray downcomers = 6


System (Foam) Factor = 0.71
Design Percent Flood = 85%
Downcomer Inlet Velocity = 0.05 m/s
Downcomer Slot Velocity = max. 0.5 m/s and min. 0.15 m/s
Tray Spacing = min. 600 mm
Weir Height = min. 150 mm
Demister at the top of the vessel: 150 mm thick
Branched pipe distributor above tray #25 for lean amine feed
Half-pipe distributor below tray #1 for sour gas feed distribution
Collector tray below tray #1 to collect rich amine and direct it to the bottom of the column
Bed of Raschig rings in the bottom head of the column
Control time (HLL to LLL) = 2 minutes, NLL at midpoint of control range
Low level intervention time between LLL and LLLL = 2 minutes
Stress relieved (PWHT) carbon steel column with stainless steel internals. 3 mm thick stainless steel
cladding is required for the entire column.

4.2.2 Amine Absorber #2, C-2


This amine absorber is a trayed column with Shell Hi Fi Trays as contacting medium to absorb CO2
from sour gas using lean amine solution.
The Main Design Features of the amine absorber are:
Overall column
Column ID = 3.35 m
Column Height = 23.4 m TL/TL

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25 Shell Hi Fi Trays (numbered from bottom up bottom tray is #1 and top tray is #25)
Number of tray downcomers = 6
System (Foam) Factor = 0.71
Design Percent Flood = 85%
Downcomer Inlet Velocity = 0.05 m/s
Downcomer Slot Velocity = max. 0.5 m/s and min. 0.15 m/s
Tray Spacing = min. 600 mm
Weir Height = min. 150 mm
Demister at the top of the vessel: 150 mm thick
Branched pipe distributor above tray #25 for lean amine feed
Half-pipe distributor below tray #1 for sour gas feed distribution
Collector tray below tray #1 to collect rich amine and direct it to the bottom of the column
Bed of Raschig rings in the bottom head of the column
Control time (HLL to LLL) = 2 minutes, NLL at midpoint of control range
Low level intervention time between LLL and LLLL = 2 minutes
Stress relieved (PWHT) carbon steel column with stainless steel internals. 3 mm thick stainless steel
cladding is required for the entire column.

4.2.3 Amine Absorber #3, C-3


This amine absorber is a trayed column with Shell Hi Fi Trays as contacting medium to absorb CO2
from sour gas using lean amine solution.
The Main Design Features of the amine absorber are:
Overall column
Column ID = 4.27 m
Column Height = 23.5 m TL/TL

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25 Shell Hi Fi Trays (numbered from bottom up bottom tray is #1 and top tray is #25)
Number of tray downcomers = 8
System (Foam) Factor = 0.71
Design Percent Flood = 85%
Downcomer Inlet Velocity = 0.05 m/s
Downcomer Slot Velocity = max. 0.5 m/s and min. 0.15 m/s
Tray Spacing = min. 600 mm
Weir Height = min. 150 mm
Demister at the top of the vessel: 150 mm thick
Branched pipe distributor above tray #25 for lean amine feed
Half-pipe distributor below tray #1 for sour gas feed distribution
Collector tray below tray #1 to collect rich amine and direct it to the bottom of the column
Bed of Raschig rings in the bottom head of the column
Control time (HLL to LLL) = 2 minutes, NLL at midpoint of control range
Low level intervention time between LLL and LLLL = 2 minutes
Stress relieved (PWHT) carbon steel column with stainless steel internals. 3 mm thick stainless steel
cladding is required for the entire column.

4.2.4 Amine Stripper, C-4


The amine stripper is a trayed column designed for regenerating combined rich amine streams from
the amine absorbers, C-1, C-2 and C-3.
The main design features of the amine stripper are:
Overall Column
Column ID = 6.3 m

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Column Height = 30.4 m TL/TL


System (Foam) Factor = 0.71
Design Percent Flood = 85%
Demister at the top of the vessel: 150 mm thick
Downcomer Inlet Velocity = 0.05 m/s
Downcomer Slot Velocity = max. 0.3 m/s and min. 0.15 m/s
Stress relieved (PWHT) carbon steel column with stainless steel internals. 3 mm thick stainless steel
cladding is required for the top of the column through tray #16 (5th tray below rich amine inlet).
Corrosion allowance of 6 mm for the bottom of the column to the reboiler vapor return nozzles.
Top Section:
4 Calming Section Trays (numbered from bottom up- bottom tray is #21 and top tray is #24)
Tray Spacing = min. 600 mm
Number of tray downcomers = 15
Weir Height = 100 mm
Branched pipe distributor above tray #24 for reflux water feed
Bottom Section:
20 Shell Hi Fi Trays (numbered from bottom up- bottom tray is #1 and top tray is #20)
Tray Spacing = min. 600 mm
Number of tray downcomers = 12
Weir Height = 75 mm
Two 50% type 4 schoepentoeter distributors above tray #20 for rich amine feed
Chimney distribution for distributing feed liquid on tray #20
Draw-off tray below tray #1 to collect liquid from the trays above and to feed the two reboilers

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Two half pipe distributors below draw-off tray for two reboiler returns
Control time (HLL to LLL) = 5 minutes, NLL at midpoint of control range
Low level intervention between LLL and LLLL = 2 minutes

4.3

Vessels

4.3.1 Absorber #1 Water Wash Vessel, V-1


The amine absorber #1 overhead water wash vessel is a vertical vessel with a water wash section at
the bottom and a polishing section at the top. It is designed to minimize carryover of liquids with the
treated gas.
The main design features are:
Vessel ID = 1.80 m
Vessel Height = 10.50 m TL/TL
Top Section:
3 Bubble Cap Trays (numbered from bottom up bottom tray is #7 and top tray is #9)
Tray Spacing = 600 mm
Inlet Elbow for make-up water feed
A packed section above bubble cap trays for de-entrainment, Packing Height = 0.42 m
Packing Type = Sulzer Mellapk 250Y or Equivalent
Demister at the top of the vessel: 150 mm thick
Bottom Section:
Half-pipe feed gas inlet distributor
6 Valve Trays (numbered from bottom up bottom tray is #1 and top tray is #6)
Tray Spacing = 450 mm
Number of tray downcomers = 1

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Branched pipe distributor above tray #6 for circulating water feed


Control time of 5 minutes based on purge rate
Slug handling capacity = 3.0 m3
Distance between HLL-LLL provides control and slug volumes
High Level Intervention time of 2 minutes based on purge rate
Low Level Intervention time of 2 minutes based on total circulation rate

4.3.2 Absorber #2 Water Wash Vessel, V-2


The amine absorber #2 overhead water wash vessel is a vertical vessel with a water wash section at
the bottom and a polishing section at the top. It is designed to minimize carryover of liquids with the
treated gas.
The main design features are:
Vessel ID = 1.80 m
Vessel Height = 10.50 m TL/TL
Top Section:
3 Bubble Cap Trays (numbered from bottom up bottom tray is #7 and top tray is #9)
Tray Spacing = 600 mm
Inlet Elbow for make-up water feed
A packed section above bubble cap trays for de-entrainment, Packing Height = 0.42 m
Packing Type = Sulzer Mellapk 250Y or Equivalent
Demister at the top of the vessel: 150 mm thick
Bottom Section:
Half-pipe feed gas inlet distributor
6 Valve Trays (numbered from bottom up bottom tray is #1 and top tray is #6)
Tray Spacing = 450 mm

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Number of tray downcomers = 1


Branched pipe distributor above tray #6 for circulating water feed
Control time of 5 minutes based on purge rate
Slug handling capacity = 3.0 m3
Distance between HLL-LLL provides control and slug volumes
High Level Intervention time of 2 minutes based on purge rate
Low Level Intervention time of 2 minutes based on total circulation rate

4.3.3 Absorber #3 Water Wash Vessel, V-3


The amine absorber #3 overhead water wash vessel is a vertical vessel with a water wash section at
the bottom and a polishing section at the top. It is designed to minimize carryover of liquids with the
treated gas.
The main design features are:
Vessel ID = 2.10 m
Vessel Height = 10.70 m TL/TL
Top Section:
3 Bubble Cap Trays (numbered from bottom up bottom tray is #7 and top tray is #9)
Tray Spacing = 600 mm
Elbow for make-up water feed
Packing Height = 0.42 m
Packing Type = Sulzer Mellapk 250Y or Equivalent
Demister at the top of the vessel: 150 mm thick
Bottom Section:
Half-pipe feed gas inlet distributor

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6 Valve Trays (numbered from bottom up bottom tray is #1 and top tray is #6)
Tray Spacing = 450 mm
Number of tray downcomers = 1
Branched pipe distributor above tray #6 for circulating water feed
Control time of 5 minutes based on purge rate
Slug handling capacity = 4.3 m3
Distance between HLL-LLL provides control and slug volumes
High Level Intervention time of 2 minutes based on purge rate
Low Level Intervention time of 2 minutes based on total circulation rate

4.3.4 Reflux Drum, V-4


The regenerator reflux drum is used to separate condensed water from the acid gas. It also prevents
slugs of solvent from entering the downstream compression unit,
The main design features are:

Vessel ID = 3.66 m

Vessel Height = 6.9 m T/T

Demister at the top of the vessel

Half pipe distributor for feed inlet

Open nozzle with deflector plate for make-up water inlet

Slug handling capacity of 17.4 m3 is considered between NLL and HLL.

Control time (HLL to LLL) = 4 minutes


Low level intervention between LLL and LLLL = 2 minutes
High level intervention between HLL and HHLL = 2 minutes

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4.3.5 Closed Amine Drain Collection Drum, V-5


The closed amine drain collection drum is a below grade horizontal vessel that is used to collect amine
from miscellaneous amine drains. This vessel will be sized during the detailed design phase of the
project after Shell Canada has defined their drain strategy.

4.3.6 Lean Amine Carbon Filter, D-1


The lean amine carbon filter is used for hydrocarbon (and potentially anti-foam) removal. It is sized for
approximately 5% of lean amine flow, which is equivalent to 75 m3/h of lean amine. The amine sent to
this filter is first passed through the lean amine pre-filter for particulate removal.
A bypass should be provided for change out of the carbon. Differential pressure indication is to be
provided
The main design features are:

Vessel ID = 3.2 m

Vessel Height = 6.0 m T/T

Bed Height = 4.8 m

4.3.7 Lean Amine Surge / Storage Drum


A lean amine surge / storage drum was not included or designed for this BDP package as Shell Canada
is yet to establish their requirements for surge or storage capacity of lean amine. This vessel will be
sized during the detailed design phase of the project after Shell Canada has defined their strategy.
Alternatively, the bottom of columns C-4 can be used for surge by increasing the heights of the bottom
sections and consequently providing more residence time.

4.4

Filters

4.4.1 Lean Amine Filter, F-1


The lean amine pre-filter is a cartridge type filter for particulate removal installed downstream of the
lean amine trim cooler. The filter is sized to process 25% of the lean amine flow, which is equivalent to
355 m3/h of lean amine.
The particulate filter is to be specified with a 10 micron absolute rated filter media. A bypass should
be provided for change out of the particulate filter media. Differential pressure indication is also to be
provided.

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4.4.2 Lean Amine Post Filter, F-2


To prevent carbon fines from the carbon filter from entering the circulating amine it is necessary to
follow the carbon filter with a post filter. The lean Amine Post-Filter is a cartridge type filter for
particulate removal installed immediately downstream of the Lean Amine Carbon Filter. This filter is
sized for approximately 5% of lean amine flow, which is equivalent to 75 m3/h of lean amine.
The particulate filter is to be specified with a 10 micron absolute rated filter media. A bypass should
be provided for change out of the particulate filter media. Differential pressure indication is also to be
provided.

4.4.3 Closed Amine Drain Collection Filter, F-3


Amine collected in the closed amine drain collection tank that is to be returned to the circulating
system needs to be filtered first to remove any potential particulates. The closed amine drain
collection filter is a cartridge type filter for general particulate removal. The filter is sized to process 11
m3/h of amine.
It is recommended that the particulate filter be specified with a 10 micron absolute rated filter media.
A bypass is not required for this filter since it is only used intermittently when emptying the drain tank.
Differential pressure indication is to be provided.

4.5

Exchangers

Fouling factors recommended by Shell for shell and tube heat exchangers are shown on the data
sheets. Heat transfer coefficients should be calculated using the fluid properties provided, boiling
profiles where applicable, and the equipment mechanical details. All fluids have a linear heat release
curve (temperature-duty) unless otherwise noted on the data sheets

4.5.1 Absorber #1 Circulating Water Cooler, E-1


The absorber #1 circulating water cooler is provided to cool the circulating wash water from 38C to
33 C. The maximum allowable pressure drop through this exchanger is 70 kPa.
A shell and tube type of exchanger has been selected for this service. This exchanger will be designed
to use cooling water to remove heat from the process stream. Cooling water to be supplied at 25 C
temperature.

4.5.2 Absorber #2 Circulating Water Cooler, E-2


The absorber #2 circulating water cooler is provided to cool the circulating wash water from 38C to
33 C. The maximum allowable pressure drop through this exchanger is 70 kPa.
A shell and tube type of exchanger has been selected for this service. This exchanger will be designed
to use cooling water to remove heat from the process stream. Cooling water to be supplied at 25 C
temperature.

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4.5.3 Absorber #3 Circulating Water Cooler, E-3


The absorber #3 circulating water cooler is provided to cool the circulating wash water from 38C to
33 C. The maximum allowable pressure drop through this exchanger is 70 kPa.
A shell and tube type of exchanger has been selected for this service. This exchanger will be designed
to use cooling water to remove heat from the process stream. Cooling water to be supplied at 25 C
temperature.

4.5.4 Lean / Rich Amine Exchanger, E-4


The lean / rich amine exchanger preheats the rich amine feed to the amine stripper by cross
exchanging with the hot lean amine from the bottom of the amine stripper. The operation of this
exchanger impacts the operation of the amine stripper and the quality of the lean amine. If less heat is
supplied to the rich amine (as the exchanger becomes fouled) additional duty is required from the
stripper reboiler(s) to compensate for the heat input. Also, if less heat is supplied to the rich amine the
lean amine leaves the exchanger at a higher temperature increasing the load on the lean amine
coolers.
A plate and frame type exchanger has been selected for this service. The main design parameters for
this exchanger are:
Approach temperature = 13.7 oC (rich amine inlet to the exchanger vs. the lean amine outlet)

Maximum allowable pressure drop (shell side) = 200 kPa

Maximum allowable pressure drop (tube side) = 300 kPa

Strainers shall be provided at the inlet to the exchanger to minimize fouling. The particle size to be
removed is > 500 m absolute. The strainers should be located directly upstream of the exchanger
inlets.

4.5.5 Stripper OVHD Condenser, E-5


The stripper OVHD condenser is provided to cool the CO2 gas from the top of the amine stripper to
36C. The maximum allowable pressure drop through this exchanger is 3.4 kPa.
A shell and tube type of exchanger has been selected for this service. This exchanger will be designed
to use cooling water to remove heat from the process stream. Cooling water to be supplied at 25 C
temperature.

4.5.6 Stripper Reboiler, E-6 A/B


The amine stripper reboiler(s) provide heat input for the amine stripper. Two 50% heat exchangers are
required to provide the required heat input to the amine stripper. The heating medium used for the
reboiler is low-pressure steam. The exchangers are designed to use saturated steam at 300 kPa (g)
pressure. The vapor (steam) generated from boiling the solution in the reboiler(s) provides the
required stripping in the amine stripper.

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To provide the maximum flexibility, a kettle type shell and tube exchanger is selected for this service.
The low-pressure steam will be on the tube side and lean amine is on the shell side. Good solvent
circulation around the bundle is essential.
To provide good circulation of the solvent around the tubes and to reduce localized fouling or
corrosion, the tube bundle should be placed on a slide a minimum of 300 mm (6 inches) above the
bottom of the reboiler shell. The reboiler weir should submerge the tube bundle by a minimum of 300
mm (6 inches). An alternative approach to provide the required space above and below the tubes is to
not fill in the entire tube field.
A square pitch tube pattern is recommended to promote rapid escape of vapors and reduce potential
scrubbing action associated with the two-phase flow.
To ensure good solvent circulation through the reboiler, care must be taken (during detailed design)
when specifying the dimensions of the sumps and chimneys on the draw off tray relative to the
elevation and baffle height in the kettle reboiler. If the relative elevations of the draw off tray and
reboiler are incorrectly set, flow may be difficult to maintain through the reboiler. In general, the
elevation of the draw off tray should be above the reboiler weir elevation. The liquid head between
the draw off tray and baffle in the reboiler should be at least double the reboiler circuit pressure drop,
including the vapor return line and entrance losses. To limit degradation of the solvent, the skin (tube
wall) temperature at the process side is restricted to 150C.

4.5.7 Lean Amine Cooler, E-7 A/B


The lean amine cooler is provided to further cool the lean amine exiting the lean / rich amine
exchanger to 50 C. The maximum allowable pressure drop through this exchanger is 70 kPa. Two 50%
heat exchangers are required for this service.
A shell and tube type of exchanger has been selected for this service. This exchanger will be designed
to use cooling water to remove heat from the process stream. Cooling water to be supplied at 25 C
temperature.

4.5.8 Lean Amine Trim Cooler, E-8 A/B


The lean amine trim cooler is provided to cool the lean amine from the Lean Amine Air Cooler from
50C to 30C. The maximum allowable pressure drop through this exchanger is 140 kPa. Two 50% heat
exchangers are required for this service.
A plate and frame type exchanger has been selected for this service. This exchanger will be designed to
use fresh cooling water to remove heat from the process stream. Cooling water to be supplied at 25C
temperature.
The exchange shall be equipped with lean amine bypass piping to allow for temperature control of the
lean amine. The lean amine temperature must be maintained such that the temperature of the lean

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amine leaving the cooler does not go below 30C to achieve optimum performance in the amine
absorbers.
Strainers shall be provided at the inlet to the exchanger to minimize fouling. The particle size to be
removed is > 500 m absolute. The strainers should be located directly upstream of the exchanger
inlets.

4.6

Rotating Equipment

Strainers should be provided on the suction of pumps for startup. Pumps should be equipped with
fresh water (steam condensate quality) or fresh lean amine seal flush. Seal materials must be resistant
to degradation by the solvent.
The required head specified on the data sheets is approximate and must be verified during detailed
design. More precise values may be established once information such as vessel heights, piping and
distributor details, equipment designs and control requirements are known. NPSH requirements must
be established between the pump manufacture and design details and checked against the process
properties.

4.6.1 Lean Amine Booster Pumps, P-1 A/B


The lean amine booster pumps are centrifugal type. A spare pump is required as this pump is in
continuous operation.
The rated capacity of each pump is 1662 m3/h and 1139 kPa differential head. The turndown of the
pumps must accommodate the required Amine Stripper turndown.
For calculating the NPSH available, the lean solvent from the bottom of the amine stripper is at its
bubble point so the solution vapor pressure is the same as the regenerator bottom pressure.
Therefore, the NPSHA for this pump is due only to the elevation difference between the pump
centerline and the low-low liquid level in the amine stripper sump. The pump should be located as
close to the amine stripper as possible and the inlet piping should be designed to minimize pressure
drop.

4.6.2 Stripper Reflux Pumps, P-2 A/B


The stripper reflux pumps are centrifugal type. A spare pump is required as this pump is in continuous
operation
The rated capacity of each pump is 42 m3/h and 514 kPa differential head. The turndown of the pumps
must accommodate the required Amine Stripper rectifying section turndown.
For calculating the NPSH available, the reflux water from the reflux drum is assumed to be at its bubble
point so the solution vapor pressure is assumed to be the same as the pressure in the reflux drum.
Therefore, the NPSHA for this pump is due only to the elevation difference between the pump

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centerline and the low-low liquid level in the reflux drum. The pump should be located as close to the
reflux drum as possible and the inlet piping should be designed to minimize pressure drop.

4.6.3 Lean Amine Charge Pumps, P- 3 A/B


The lean amine charge pumps are centrifugal type. A spare pump is required as this pump is in
continuous operation.
The rated capacity of each pump is 1560 m3/h and 3211 kPa differential head. The turndown of the
pumps must accommodate the required combined amine absorbers turndown requirements. These
pumps have ample NPSH available.

4.6.4 Absorber #1 Circulating Water Wash Pumps, P- 4 A/B


The circulating water wash pumps are centrifugal type. A spare pump is required as this pump is in
continuous operation.
The rated capacity of each pump is 44 m3/h and 248 kPa differential head. The turndown of the pumps
must accommodate the required water wash section turndown requirements.

4.6.5 Absorber #2 Circulating Water Wash Pumps, P- 5 A/B


The circulating water wash pumps are centrifugal type. A spare pump is required as this pump is in
continuous operation.
The rated capacity of each pump is 44 m3/h and 248 kPa differential head. The turndown of the pumps
must accommodate the required water wash section turndown requirements.

4.6.6 Absorber #3 Circulating Water Wash Pumps, P- 6 A/B


The circulating water wash pumps are centrifugal type. A spare pump is required as this pump is in
continuous operation.
The rated capacity of each pump is 63 m3/h and 253 kPa differential head. The turndown of the pumps
must accommodate the required water wash section turndown requirements.

4.6.7 Amine Make-up Tank Pump, P-7


The amine make-up tank pump is centrifugal type. A spare pump is not required as this pump is only
used on an intermittent basis.
The required capacity is 10 m3/h. The pump specification is based on pumping a 45 wt% ADIP-X
solution. If the pump is also going to be used to pump high purity (90+ %) MDEA, it should be checked
for this case during detailed design.

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Note: This pump may not be required if Shell Canada decides to use the Lean Amine Surge / Storage
Tank as the make-up tank.

4.6.8 Closed Drain Amine Pump, P-8


The closed drain amine pump is a submerged centrifugal type. A spare pump is not required as this
pump is only used on an intermittent basis.
The required capacity is currently specified as 11 m3/h and 474 kPa differential head. The actual
required capacity is to be confirmed during detailed design.

4.7

Tanks

4.7.1 Amine Make-up Tank, T-1


The amine make-up tank provides storage for fresh amine for use as make-up to the amine unit. The
tank nominal capacity is 10 m3. A nitrogen blanket/purge connection is provided in the tank.
Note: This tank may not be required if Shell Canada decides to use the lean amine surge / storage Tank
as the make-up tank. However, a separate make-up tank is recommended.

4.8

Piping

Liquid piping velocities for pump suction and reboiler inlet lines for carbon steel and stainless piping
should be limited to 1 m/s (3.3 ft/s). This criteria is a typical design guideline to minimize pressure drop
and to mitigate flashing. Velocity in liquid amine lines should be limited to 2 m/s for carbon steel piping
and 3 m/s for stainless steel piping.
Gas lines should slope so that lines will drain into equipment, preferably in the direction of flow; piping
should not be the low point. They should be designed without pockets to avoid the formation of liquid
slugs.
Steam lines must be trapped and should have liquid T knockouts at equipment connections to trap
condensate slugs.

4.8.1 Two phase flow


The presence of liquid and gas two-phase flow in process piping can lead to hydrodynamic instability,
slugging, and equipment damage.
Two-phase flow is encountered in:

Piping downstream of level control valve on the rich amine from amine absorbers.

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Piping from the outlet of the Lean / Rich Amine Exchanger on the rich amine service to the
control valve and piping from the control valve to the inlet of amine stripper.

This piping must be checked for flow stability and slug flow should be avoided. Stainless steel piping is
suggested for two phase amine services as the velocities are high.

4.8.2 Hot Lean Solvent Piping


Special attention is required for the hot lean solvent piping segment from the amine stripper to Lean
Amine Booster Pumps. This piping must not be pocketed. The piping and equipment layout should be
arranged so that the entire system is sloped from the stripper and is self-draining and self-venting.

4.8.3 Piping Upstream of Schoepentoeter


The piping upstream of Schoepentoeter inlet device should be free of bends in the horizontal plane for
at least 10 pipe diameters. This prevents unbalanced forces as a result of liquid accumulation on one
side of the pipe. Bends in the vertical plane upstream of Schoepentoeter are not a problem.

4.8.4 Rich Amine Piping Downstream of Control Valves


A pipe elbow immediately downstream of a control valve in rich amine services should be avoided.
Gas breakout from the rich solution may cause erosion if the fluid impinges on an elbow. Although the
use of stainless steel pipe can mitigate this concern, elbows should be placed 8 to 10 pipe diameters
downstream of a control valve.

4.8.5 Sample Points


Sample points should be located at the top (preferably on horizontal runs) or side of lines. The sample
piping configuration should include straight through piping and full open valve type (not globe,
butterfly or rotating disk) with access space. Access space is for maintenance and also for sample
probe. Nitrogen purge should be available. A flow inducer (eductor or vacuum pump) may be
required to draw sample in low pressure areas.
Suggested sample points:
Lean Amine Service provide two sample points
o Upstream of Lean Amine Charge Pumps
o Upstream of Lean / Rich Amine Exchanger

Rich Amine Service Provide with sample coolers


o Upstream of level control valves from individual absorbers

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o Upstream of Lean / Rich Amine Exchanger on the main line

Absorber feed gas lines

Absorber off-gases provide two sample points for each absorber


o Sample ahead of bypass / block valves
o Sample downstream of bypass / block valves

4.9

Stripped CO2 gas from Reflux Drum

Reflux return line

Water wash recirculating water lines.

Winterization

The plant geographic location must be considered during the detailed design.
requirements appropriate to the local conditions should be incorporated.

Winterization

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5.1

42

Process Control Philosophy


General comments

The measuring ranges of the flow controllers and all control valves have to be designed with sufficient
spare capacity for compensation of usual variations of the process conditions. Special considerations
are described in the text below.

5.2

Amine Absorption

5.2.1 Amine Absorbers


The basic process control requirements for the amine absorbers are flow controls of the lean amine to
the tower and tower bottom level control. Rich amine removed from the bottom of the three amine
absorbers based on their individual level controls is collected in common rich amine line.
A pressure differential indicator (with alarm) is required across the trays within the absorber tower.
The important function of this is to detect increases or fluctuations in differential pressure that are
warnings of tower foaming. Depending on experience, a differential pressure level alarm or a
differential pressure rate of change alarm can be applied.
Differential temperature measurements between the feed gas and lean amine should be applied. This
will help in monitoring amine temperatures. This measurement may be linked to lean solvent
temperature alarms. It is recommended that the lean amine temperature be equal to the feed gas
temperature for the optimum performance of the absorption systems. The lean amine temperature
should not be allowed to go below 30C for feed gas temperature of 35C
It is recommended to operate the contactor with a fixed solvent rate and manually adjust the solvent
rate when significant changes in gas flow are expected for extended periods of time.
Feed gas bypass flow control arrangement is required for each absorber to accommodate the
shutdown or any upset situations in the CO2 capture unit. This arrangement allows 100% of the gas to
bypass the absorber and will be sent directly to downstream PSA unit. This bypass arrangement can
also be modified to control the CO2 removal to 80% or less if required.

5.2.2 Water Wash Vessels


The basic process control requirements for the water wash vessels are flow control of fresh water
make-up to the polishing section of the vessels and vessel bottom level control. Purge water removed
from the bottom of the three water wash vessels is based on their individual level controls. Purge
water from vessels V-1 and V-2 downstream of the level control valves is collected in a common purge
line and purge from V-3 will be removed in a separate line.

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A level transmitter with low and low-low level alarms should be provided to allow the operator to
monitor the level and to protect the downstream pumps used to recirculate wash water through the
water wash vessels.

5.3

Amine Stripper

The amine stripper receives combined rich amine stream from the three amine absorbers and strips
CO2 from the solution thereby generating lean amine. The stripping steam used in the tower is
generated in the amine stripper reboiler(s) by boiling the bottom lean solution with low pressure
steam.

5.3.1 Amine Stripper Feed Control


The combined rich amine from the three amine absorbers is fed to amine stripper though a
backpressure control valve. The rich amine stream pressure is reduced from 2752 kPa (a) to 162 kPa
(a) as the rich amine passes through the pressure control valve located upstream of the column.

5.3.2 Reboiler Steam Control


The flow of low pressure steam to the reboiler is on flow control. The flow controller receives
adjustments to its set point based on the flow of rich amine to the amine stripper. Essentially, the flow
of steam is set to maintain a desired ratio to the flow of rich amine. The system is designed for steam
rate of 114 kg of low pressure steam per cubic meter of amine flow. This ratio can be adjusted based
on amine stripper overhead temperature and the quality of lean amine. The adjustment to steam ratio
will be based on actual column performance after gathering operating data with respect to the steam
rate, lean amine loading and amine stripper overhead temperature.

5.3.3 Stripper Bottoms Level Control


Lean amine from the bottom of the Amine Stripper is removed using lean amine booster pump. The
level in the bottom of the stripper column will be maintained by controlling the flow of lean amine to
the three absorbers. The Calculator Block will adjust the flow of lean amine to the absorbers based
on the signal from the level controller on the stripper bottom. Low liquid level in the column will cause
the lean amine flow control valves to the absorbers to close, and high level in the column will cause
the flow control valves to open. Low-Low level alarm would be used to shut the pumps down for
protection. Fluctuations in the liquid level are not expected to occur in the stripper as it is a closed loop
system.

5.3.4 Stripper Pressure Control


The pressure in the amine stripper is maintained by a pressure control valve in the acid gas line from
the reflux drum.

5.3.5 Regeneration Reflux Section Level Control


The gas exiting the top of the amine stripper is cooled by the stripper OVHD condenser. The water that
is condensed from the gas due to cooling is removed in a reflux drum.

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44

The basic control requirements for the reflux drum are flow control on the make-up water to the drum
and drum bottom level control. The reflux water is returned on flow control to the top of the amine
stripper. The flow control is reset by level controller to maintain proper level in the reflux drum. The
flow controller on the reflux drum should be provided with a low flow alarm and a high level alarm.
Liquid level alarms would allow the operator to monitor the level in the drum. A high level alarm will
cause the flow control valves to open in order to prevent liquid building up in the drum and low-low
level alarm would be used to shut the pumps down for protection.
Maintenance of the amine system water balance is also handled in the reflux drum of the amine unit. If
there is excess water in the system or if the overhead section needs to be purged, it can be done by
bleeding off the water to the waste water system from the reflux stream. This bleed can be continuous
or intermittent depending on the operating experience from running the unit. A flow control loop is to
be provided on the bleed line on the discharge of the stripper reflux pumps for this purpose.
Steam condensate quality water is recommended for water make-up to the unit. Also, water removed
from purge streams of the water wash section can be used to supplement make-up water to the amine
unit. Water make-up can be added to the unit through a connection provided on the reflux drum. This
allows for maintenance of the amine-water balance. The make-up water is to be added under flow
control.

5.4

Amine Cooling

Maintaining the temperatures of the lean streams is important to maintaining proper operation of the
amine absorbers.

5.4.1 Lean Amine


Lean amine from the lean / rich amine exchanger is cooled to 50 C in lean amine cooler and then to
30C in lean amine trim cooler using cooling water before it is returned to the amine absorber. The
lean amine trim cooler shall also be equipped with lean amine bypass control to allow for temperature
control of the lean amine.

5.5

Lean Amine Filtration

The main particulate filter (lean amine filter) sized for 25% of lean amine flow is provided with a bypass
around it. The lean amine carbon filter and lean amine post filter are each sized for approximately 5%
of the lean amine flow. The flow rate to these two filters is controlled by a flow control loop.
Differential pressure gauges with alarms are provided across each of the filters to indicate when they
need to be changed.

5.6

Amine Water Balance

During steady state operation, water leaves the amine system with the treated gas from the amine
absorbers, with the acid gas from the reflux drum and with the reflux water purge (if in use). Steam
condensate quality water is recommended for water make-up to the unit. Also, water removed from
purge streams of the water wash section can be used to supplement make-up water to the amine unit.
Water make-up can be added to the unit through a connection provided on the reflux drum. This is
discussed in section 5.3.5 above.

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Safeguarding Philosophy

Operation of an Amine Unit involves the management of toxic materials and risks to plant personnel
and equipment. These hazards are managed safely day-to-day in Amine Unit operations but require
the use of good design, construction, and operating practices.
A safeguarding system is required to protect the people working in the plant and to protect the plant
from internal damage. To protect the people, the unit has to be designed such that it maintains its
mechanical integrity and that a release of gas is prevented. This section summarizes the main
safeguarding requirements for this unit and has to be subjected to safety reviews (HAZOP, etc) in later
stages of the project. Any additional safeguarding required by national and local codes and regulations
shall be considered during detailed engineering.
Experience shows that start up and shut down operations greatly increase the risk of equipment
damage. The safeguarding system should be designed to avoid unnecessary trips.

6.1

Emergency Depressurizing

In general, relief valves shall not depressurize a vessel or a system; it can only limit the pressure rise to
the relief valve set point during an upset or emergency conditions.

6.1.1 Relief valves


Typically, the criteria for setting equipment design pressure is that a piece of equipment should be
designed based on the maximum operating pressure plus a safety margin with a minimum design
pressure of 350 kPa (g). For process side of heat exchangers and filters the equipment as a minimum
should be designed for maximum shut-off head of the pumps upstream. The utilities side of the
exchangers should be designed for the design pressure indicated by utility data provided by the
project. Where required by process hazard analysis, the piece of equipment should be equipped with
well functioning relief valves relieving to the flare. In general, each section of the unit that can be
blocked in should be protected with a relief valve.
The following table provides a summary of the major locations for relief devices (not necessarily all) in
the Amine Unit. In addition the relief scenarios to be considered are given. This list is intended to
provide guidance to the detailed engineering contractor who will be responsible for the plant relief
philosophy and design.

Location
C-1
(Note 3)

Amine Unit Relief valves


Service
Cases to be considered as a minimum
Amine Absorber #1 (C-1)
- Feed gas pressure control failure in the
Absorber #1 Water Wash Vessel (V-1)
upstream unit
Circulating Water Cooler (E-1)
- Blocked discharge with Lean Amine Charge
Pumps (P-3A/B) running.
- Make-up water flow control valve failure.

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Location
C-2
(Note 3)

C-3
(Note 3)

C-4
(Note 4)

46

Service
Amine Absorber #1 (C-2)
Absorber #2 Water Wash Vessel (V-2)
Circulating Water Cooler (E-2)

Amine Absorber #1 (C-3)


Absorber #3 Water Wash Vessel (V-3
Circulating Water Cooler (E-3))

Amine Stripper (C-4)


Reflux Drum (V-4)

T-1

Amine Make-Up Tank

V-5

Closed Amine Drain Collection Drum

Cases to be considered as a minimum


Feed gas pressure control failure in the
upstream unit
Blocked discharge with Lean Amine Charge
Pumps (P-3A/B) running.
Make-up water flow control valve failure.
Feed gas pressure control failure in the
upstream unit
Blocked discharge with Lean Amine Charge
Pumps (P-3A/B) running.
Make-up water flow control valve failure.
Reboiler steam control valve failure causing
valve to open completely
Blocked discharge with steam supply on
Make-up water flow control valve failure
Atmospheric Tank should be designed with a
proper breath and vent valve.
Vapor breakthrough from different sources
Failure of pressure control valve in nitrogen
supply line

Notes:
1. The possibility of a pool fire in the unit has to be determined during Detailed Engineering. In that case relief
valves are required for every pressure vessel that could be subjected to external fire.
2. Relief valve location (vessel or piping) to be determined during Detailed Engineering.
3. A common relief valve can protect absorber Water Wash Vessel and the Amine Absorber of each train if they
are designed such that they cannot be isolated from each other.
4. A common relief valve can protect Amine Stripper (C-4) and Reflux Drum (V-4) if they are designed such that
they cannot be isolated from each other.

6.2

Instrumented Protected Functions

It should be noted that this section does not cover safeguards by instruments installed for equipment.
The following trip functions are to be considered:
Location
C-1

Service
Amine Absorber #1

Trip
Low level

Identification
LLLL

C-2

Amine Absorber #2

Low level

LLLL

C-3

Amine Absorber #3

Low level

LLLL

C-4
C-4

Amine Stripper
Amine Stripper

High pressure
Low level

PZA (HH)
LLLL

Action
Close TSO on the rich amine
outlet line
Close TSO on the rich amine
outlet line
Close TSO on the rich amine
outlet line
Cut off steam to the reboiler
Close TSO on the lean amine
outlet line and stop the
pumps

SR.11.10343

Location
V-1

47

V-4

Service
Amine Absorber #1
Water Wash Vessel
Amine Absorber #2
Water Wash Vessel
Amine Absorber #3
Water Wash Vessel
Amine Absorber #1
Water Wash Vessel
Amine Absorber #2
Water Wash Vessel
Amine Absorber #3
Water Wash Vessel
Reflux Drum

V-4

Reflux Drum

V-2
V-3
V-1
V-2
V-3

Trip
Low level

Identification
LLLL

Action
Close TSO on the purge line

Low level

LLLL

Close TSO on the purge line

Low level

LLLL

Close TSO on the purge line

High level

HHLL

High level

HHLL

High level

HHLL

Low level

LLLL

High level

HHLL

Close gas feed to the


absorber C-1
Close gas feed to the
absorber C-2
Close gas feed to the
absorber C-3
Close TSO on the reflux water
outlet line and stop the
pumps
Cut off steam to the reboiler

Protection against back flow through the lean solvent system is required, to prevent gas back flow
from the amine absorbers to the Amine Stripper. Backflow prevention by IPF should be applied at the
absorber solvent supply and the solvent circulation pumps. Where IPF is not acceptable for final
containment, amine stripper relief valve must be sized accordingly.
The following instruments with alarms are recommended:
Location
F-1, F-2, F-3, D-2
C-1, C-2, C-3

Service
All Filters
Amine Absorbers

V-1, V-2, V-3


V-4

Absorber Water Wash


Vessels
Reflux Drum

C-4

Amine Stripper

V-5
T-1

Closed Amine Drain


Collection Drum
Amine Make-Up Tank

E-1, E-2, E-3

Circulating Water Coolers

Type
Pressure differential
Pressure differential
Pressure
Level
Feed gas flow
Level

Identification
PDIA (H)
PDIA (H)
PIA (H)
LICA (H/L)
FIA (H/L)
LICA (H/L)

Level
Reflux water flow rate
Make-up water flow rate
Pressure Differential
Pressure
Amine flow rate
Steam flow ratio
Level
Overhead temperature
Level
Pressure
Level
Pressure
Outlet temperature

LICA (H/L)
FICA (L/H)
FIA (L/H)
PDIA (H)
PIA (H)
FIA (L/H)
FRCA (H/L)
LICA (H/L)
TICA (H/L)
LIA (H/L)
PIA (H)
LIA (H/L)
PIA (H)
TIA (H/L)

SR.11.10343

Location
E-5
E-8 A/B
Analyzers

6.3

48

Service
Stripper OVHD Condenser
Lean Amine Trim Cooler
All on line analyzers

Type
Outlet temperature
Outlet temperature
Quality parameter (CO2, etc)

Identification
TICA (H/L)
TICA (H/L)
QRCA (H/L)

Additional Safety Requirements

Safety Material Data Sheets for MDEA, DEDA and CO2 are attached in Appendix F. The below advice
applies equally to MDEA and DEDA.

6.3.1 Good operating practices amine solutions


The amine solution is alkaline. Normally the concentration of amine in water will range from 2 to 4
molar. The standard procedures for handling alkaline solutions must be followed. Safety showers and
eye wash solutions must be kept ready for immediate use.
Operators and maintenance workers shall use eye shields or safety goggles, (rubber) gloves and, if
necessary, (rubber) boots whenever contact with the chemical solution may occur (e.g. during
sampling, opening lines, working on pumps, solution make-up operations etc.).

6.3.2 Spillage/disposal amine solutions


Do not touch spilled material. Stop leak if possible without personal risk.
Small spills: Absorb with sand or other non-combustible material.
appropriate container for disposal.

Collect spilled material in

Small dry spills: Move containers away from spill to a safe area.
Large spills: Dike for later disposal. Keep unnecessary people away, isolate hazard area and deny
entry. Dispose recovered material according to local environmental requirements

SR.11.10343

49

Material selection

See Appendix E for Amine Unit Material Selection Guide (MSG) for detailed discussions.
The following discussions should be considered in addition to discussions in the attached MSG.
The attached selection guide written by Shell Materials Selection Group in its current version indicates
0.6 mol CO2 / mol amine as the limit for material selection. However, this group recently approved
CO2 loading higher than 0.6 mol CO2 / mol amine. The new guideline issued by the materials group
states CO2 loading can be higher than MSG specified limit - up to 0.8 mol / mol amine with SS
metallurgy, provided other specifications in MSG such as solvent quality and operation conditions are
met. This new guideline will be included in the next update. In the interim, this guideline is being
followed globally on CO2 projects by Shell Global Solutions. Since the rich amine loading from all three
amine absorbers is approximately 0.6 mol CO2 / mol amine at design conditions, material selection for
rich amine service will be based on rich higher amine loading (higher than 0.6 mol CO2 / mol amine
loading).
Additional considerations for material selection is discussed below:
Amine Absorbers:
Based on the new guidelines and consultation with experts in Shell Global Solutions, as a minimum SS
clad is recommended for the entire absorber columns. Similarly, all the piping in rich amine service
from the absorbers to the amine stripper will have to be stainless steel.
Amine Stripper:
Stainless steel cladding is recommended for amine stripper in CO2 service for the top portion of the
amine stripper column extending from the top head through 5th tray below rich amine feed inlet. This
is to avoid corrosion in the absence of the protective FeS layer and condensing vapor environment in
the top section. Per MSG guidelines, carbon steel is adequate for the bottom section of the amine
stripper for a properly operated and maintained unit. However, using SS cladding for the entire column
will provide improved corrosion protection and will extend the life of the equipment.
Water wash system:
Stainless steel cladding is recommended for the water wash vessels. Carbon steel vessels with SS
cladding are adequate for this service instead of SS material because amine carryover from the
absorber will partially neutralize the acidic environment due to presence of CO2 in circulating water.
The piping associated with water wash section also needs to be stainless steel material.
For the circulating water wash exchangers, tubes need to be stainless steel and the shell needs to be
carbon steel with SS cladding.
Stainless piping is recommended for the following services:
Overhead line from amine stripper to the OVHD condenser
Line from the OVHD condenser to the reflux drum

SR.11.10343

50

Reflux line from reflux drum to the amine stripper


Lean amine lines from amine stripper to the reboiler
Vapor and liquid returns lines from reboiler to the amine stripper
Recirculating water wash lines of the water wash vessels
Lean amine line from the bottom of amine stripper to the lean rich exchanger

SR.11.10343

Appendix A:

51

Summary of Process Optimization Studies

Several optimization studies were performed to establish process design conditions for CO2 capture
amine unit. The results are summarized in the following section. Following is a list of some of these
studies.

Amine Circulation vs. Steam Rate


Amine Circulation vs. Amine Strength:
Effect of Stripper Operating Pressure
Process Configuration for rectifying section
Lean Solvent Temperature
Rich Amine Feed Temperature

Process simulations for these evaluations were performed using PROMAX software. PROMAX is widely
used in the industry for amine simulations. This simulation tool was used to perform several
optimization cases because of its flexibility, speed of convergence, ease of use and ability to handle
variations in process conditions. However, the heat and material balance data and the final design of
the unit was based on Shells official in-house simulation tool PROGASP.
Since the optimization studies were performed using PROMAX simulation tool and the heat and
material balance data was generated using PROGASP simulation tool there will be differences in the
process data. However the data is representative of the performance and requirement of the
processing unit for the options considered for these evaluations.
Amine Circulation vs. Steam Rate:
The process was evaluated for a wide range of steam flows from 130 tons/h to 170 ton/h
corresponding to steam rates from 0.56 lb of steam per gallon amine solvent to 1.0 lb of steam per
gallon amine solvent. The evaluations were performed for amine strengths of 45 wt% and 40 wt%.
The purpose of this evaluation was to establish an optimum steam rate in lb of steam/gal of lean
solvent for the capture unit based on amine circulation rate and life cycle cost of the unit. These
evaluations were done with hot side approach of 20F (11C) for the lean-rich cross exchanger. The
results are presented in the figure below.
The results are summarized below:

The optimum steam flows are in the 150 to 160 ton/hr range
Optimum steam rates (lb of steam/gallon amine) are 0.83 to 0.91 for 40 wt% amine
Optimum steam rates (lb of steam/gallon amine) are 0.90 for 45 wt% amine

For 40 wt% amine, the lean amine loadings corresponding to steam rate of 0.83 lb of steam/gallon
amine was 0.045 mol CO2/mol amine. This lean loading is relatively high and is not recommended.
However, the lean amine loadings corresponding to steam rate of 0.91 lb of steam/gallon amine was in
the acceptable range of 0.03 mol CO2/mol amine.

SR.11.10343

52

For 45 wt% amine the lean amine loadings corresponding to steam rate of 0.90 lb of steam/gallon
amine was in the acceptable range of 0.03 mol CO2/mol amine

Evaluations on the effect of steam flow on circulation rates for 40 wt% and 45 wt% amine
An optimum steam rate of 0.9 lb/gal was selected based on the lower solvent circulation and minimum
life cycle cost for the unit corresponding to amine solution strength of 45 wt%.
PROGASP simulation tool required approximately 10% higher solvent circulation rate for the amine
absorbers compared to PROMAX predictions to achieve same amount of CO2 removal. The steam
consumption was adjusted accordingly for the design case to reflect the optimum steam rate of 0.9
lb/gal of solvent. Steam flow rate of 167.5 tons/h was selected for 45 wt% amine solvent based on the
acceptable lean amine loadings of 0.03 mol/mol, lower solvent circulation requirement and lower life
cycle cost of the unit.

SR.11.10343

53

Amine Circulation vs. Amine Strength:


The amine unit was evaluated using 40 wt% amine (35 wt% MDEA & 5 wt% DEDA) and 45 wt% amine
(40 wt% MDEA & 5 wt% DEDA). The evaluations were performed for steam flow rates of 150 ton/hr
and 155 ton/hr. The purpose of these evaluations was to access the impact of higher amine strength
on amine circulation rate and life cycle cost of the unit. The results are presented in the next page.
The results are summarized below:

There is a significant reduction in solvent circulation at 45 wt% amine strength (40 wt% MDEA
+ 5 wt% DEDA) compared to 40 wt% amine strength (35 wt% MDEA + 5 wt% DEDA)

The Capex for amine unit with higher amine strength is approximately 25 million dollars lower
than with lower amine strength.

There was a corrosion concern earlier regarding the use of higher amine strength (45 wt%) along with
higher rich amine loading (0.59 mol CO2/mole amine). After discussions with Shell Global Solutions
materials experts, it was agreed that the amine unit can be designed for higher solvent strength but,
this design would require cladding portion of inside section of amine absorber columns with stainless
steel and using stainless steel material for rich amine piping.
Higher amine strength of 45 wt% along with steam flow of 155 ton/hr (corresponding to steam rate of
0.91 lb steam /gal of solvent) is considered the optimum. The required solvent circulation for this
optimum case is 6200 gpm. The lean loading corresponding to 0.91 lb/gal of steam is 0.03 moles of
CO2/moles of amine and the rich amine loading is approximately 0.59 moles of CO2/ moles of amine.

SR.11.10343

54

Impact of amine strength on amine circulation rate and life cycle cost of the unit

SR.11.10343

55

Effect of Stripper Operating Pressure:


The CO2 capture process was evaluated for the following stripper overhead pressures to access the
impact on amine regeneration and the life cycle cost of the unit. The amine stripper was evaluated for
the following reflux drum overhead pressures.

3.9 psig (120 kPa (a))


7.3 psig (144 kPa (a))
14.0 psig (190 kPa (a))

The results of this evaluation are presented in the table and graph shown on the next page.
Some of the results are summarized below:

For a given steam rate, the lean amine loading improves as the stripper overhead pressure is
increased from 3.9 psig to 14.0 psig. However, the reduction in lean amine loading is not
significant enough to reduce amine circulation rate for this application involving bulk CO2
removal.

The heat duties and required heat transfer areas of the reboiler and lean-rich cross exchangers
increase with increasing overhead operating pressure.

The condenser and lean solvent cooler duties did not change much with pressure (not shown in
the attached table).

There is no significant benefit to amine unit process, involved in bulk CO2 removal, by
operating the amine stripper at higher pressure. However, the effect of stripper overhead
operating pressure on CO2 compression needs to evaluated.

The cost of amine unit will be higher for units operating at a higher stripper overhead
pressure. The cost increase is due to the increase in reboiler size due lower LMTD and increase
in the duty of lean-rich cross exchanger

Evaluation performed by other on the cost of CO2 compression unit with the CO2 overhead gas at
higher pressure did not show any significant savings. Therefore the intermediate pressure of 7.3 psig
(144 kPa (a)) was selected as stripper overhead pressure for the process design.

SR.11.10343

56

Impact of stripper overhead pressure life cycle cost of the unit

SR.11.10343

57

Overhead reflux arrangement for amine entrainment in acid gas:


The rectifying section of the amine stripper was evaluated for the following two configurations:
Standard overhead reflux arrangement
Pump around reflux arrangement
The purpose of this evaluation was to estimate amine carryover in the acid gas going to the
compression unit. The schematic of both configurations is shown below:

Standard Overhead Reflux Case

Pump Around Reflux Case

The standard overhead reflux scheme consists of an overhead acid gas condenser, reflux drum and a
reflux pump. The overhead vapor stream from the regenerator stripping section containing CO2 gas
components is routed through the rectification/water wash section (consisting of 3-4 trays) in the
column top to an overhead condenser where it is cooled to the desired temperature to recover water.
The condensed water is collected in an overhead reflux drum and pumped back to the top of the
column through reflux pumps.
The pump around reflux scheme consists of a quench water cooler, quench recirculating pumps and a
collecting chimney tray for drawing water from the rectification section. The overhead vapor stream
for the regenerator stripping section containing CO2 is contacted with cooled pump around liquid in
the top rectifying section consisting of 4 trays. This cools the acid gas and also helps in removing
solvent components from the acid gas. Liquid collected at the bottom of this section on a collector tray
is removed through a draw nozzle to quench water pumps. The recirculating water is pumped through

SR.11.10343

58

a quench water cooler where the quench water is cooled to a desired temperature before returning
back to the top of the column.
The above configurations were evaluated for the following parameters:
Amine entrainment in the acid gas going to the compression section
Equipment count and associated CAPEX
Operability
The results are summarized below:

Amine entrainment for standard overhead reflux scheme was estimated to be less than 10
ppmw and less than 50 ppmw for pump around reflux case. The concentration of amine was
found to be more for pump around scheme because of higher circulating liquid flow with
higher dissolved amine in it compared to small reflux flow for standard reflux scheme which
results in higher amine entrainment in the acid gas.

The preliminary cost evaluation study showed that the overall CAPEX requirement for pump
around case was higher compared to the standard reflux option. This was primarily due to high
pumping cost, taller regenerator column due to additional draw-off tray and bigger quench
water exchanger.

Standard overhead reflux is simple and more reliable operation in comparison to pump around
reflux case.

Based on the above evaluations, the standard overhead reflux arrangement was selected as the reflux
configuration for the rectifying section for the regenerator because of lower amine carryover in the
acid gas, lower cost and operational simplicity and reliability.

SR.11.10343

59

Lean amine solvent temperature:


The amine unit was evaluated for a wide range of lean solvent temperatures ranging from 20C to
35C. These evaluations were performed to predict the effect of lean amine temperature on the CO2
removal efficiency and to establish optimum temperature for lean amine feeding the amine absorbers.
The table below shows the effect of lean solvent temperature on column CO2 removal efficiency. The
optimum temperature for CO2 removal is 30C. However a lean solvent temperature of 35C was
selected for the process design to allow for the use of re-used cooling water in the lean amine trim
cooler to reduce the load on the existing cooling water system. The lean amine trim cooler will be
designed for using 32 C re-used cooling water and a cold side temperature approach of 3C for a
plate and frame type heat exchanger.
Lean Solvent
Temperature
35C
30C
25C
20C

% CO2 removal, C-1

% CO2 removal, C-2

% CO2 removal, C-3

80
82.3
80
73.7

80
82.3
80
73.7

80
83
82
76.4

Rich Amine Feed Temperature:


The process was evaluated for different cold side temperature approaches on the lean/rich heat
exchanger. The purpose of the study was to estimate an optimum approach for the lean/rich
exchanger with respect to the heat transfer area and size of the exchanger and also an optimum
approach with respect to the energy load for reboiler, condenser and lean/rich heat exchanger. The
following cold side temperature approaches were studied
cold side approach of 12F (6.7C)
cold side approach of 21F (11.7C)
The above evaluations were done using PROMAX. The rich amine temperatures from PROGASP were
lower and therefore cold side approach is increased. The cold side approach of 14 C in PROGASP
corresponds to 11.7 C in PROMAX.
A cold side approach of 14C was chosen based on an optimum energy load for reboiler, condenser
and lean/rich heat exchanger for the regeneration section. As the cold side approach decreases, the
rich amine feed temperature increases. Increasing the rich amine feed temperature to the regenerator
helps in reducing the reboiler energy load to a certain point and beyond that the higher rich amine
temperature adds additional energy load to the condenser.

SR.11.10343

Appendix B:

60

Process Flow Diagram and Heat & Material Balances

Process Flow Diagram

CO2 Capture Unit


PFD 1-27-2011.pdf

Heat & Material Balance

Material
Balance-01-27-2011.p

SR.11.10343

61
C-1
Amine Absorber #1

C-2
Amine Absorber #2
E-4
Lean / Rich
Amine Exchanger

E-3
Absorber #3
Circulating Water Cooler

Make-up
Water

C-3
Amine Absorber #3
E-5
Stripper OVHD
Condenser

E-7 A/B
Lean Amine
Cooler

E-6 A/B
Stripper
Reboiler

23
A

P-1 A/B
Lean Amine
Booster Pumps

PDI

CW

F-2

LC

V-1

F-1

E-5

FC

V-2

PC

15

5
A

FC

Drain
20

E-4

4
B

18

14

11
Condensate

P-3 A/B

LC

P-1 A/B

Notes:
1. Portion of Streams 24A and 24B will be used as water
make-up to the amine unit (Stream 19) and the
remaining goes to waste water treatment facility.

5
B

2. Purge stream to flash drum (by others).

FC

20
C

E-6
E-7A/B
E-7A/B

13

1
B

2
C

LC

Steam

12

FC

FC

FI

C-2

V-3

P-2 A/B

21

C-4

25

10

24

2
B

FC

E-3

LC

20
B

21
C

V-4

TC

LC

LC

19
CW

E-7A/B

22
C

Water
Make-up
9

16

17

4
A

1
A

3
C

CW

CW

FC

P-5 A/B

Note 2

P-6 A/B
Absorber #3
Circulating Water Wash Pumps

PC

22
B

E-2

E-2
Absorber #2
Circulating Water Cooler

PDI

C-1

21
B

Purge

P-5 A/B
Absorber #2
Circulating Water Wash Pumps

25

LC

24
C

E-1
Absorber #1
Circulating Water Cooler

FC

23
C

D-1
Lean Amine
Carbon Filter

2
A

20
A

CW

F-2
Lean Amine
Post Filter

P-4 A/B
Absorber #1
Circulating Water Wash Pumps

E-8A/B

FC

24
B

P-3 A/B
Lean Amine
Charge Pumps

3
B

Purge
Note 1

PDI

22
A

P-4 A/B

23
B

P-2 A/B
Stripper Reflux
Pumps

F-1
Lean Amine
Filter

D-1

21
A

E-1

V-4
Reflux Drum

CW

FC

24
A

V-3
Absorber #3
Water Wash Vessel

FT

Make-up
Water

V-2
Absorber #2
Water Wash Vessel

E-8 A/B
Lean Amine
Trim Cooler

3
A

Purge
Note 1

Make-up
Water

V-1
Absorber #1
Water Wash Vessel

C-4
Amine Stripper

4
C

25

P-6 A/B

C-3

PROCESS FLOW DIAGRAM


Shell CANADA
QUEST CO2 Capture Unit

1
C

LC
LOCATION:

Scotford
5
C

PLANT:
Amine Unit

SHELL GLOBAL SOLUTIONS (US), INC.

CLIENT:
Shell Canada

Rev: 0
January 27, 2011

SR.11.10343

62

Client: Shell Canada


Project: Quest CO2 Capture Unit

Date: January 27, 2011


By / Rev'd : AJ / RR

Heat and Material Balance

Stream Number
Stream Description

1A

1B

1C

2A

2B

2C

Feed Gas to
Absorber #1

Feed Gas to
Absorber #2

Feed Gas to
Absorber #3

Treated Gas from


Absorber #1

Treated Gas from


Absorber #2

Treated Gas from


Absorber #3

2A (Design,Note 1) 2B (Design,Note 1) 2C (Design,Note 1)


Treated Gas to
Absorber #1 Water
Wash Vessel

Treated Gas to
Absorber #2 Water
Wash Vessel

Treated Gas to
Absorber #3 Water
Wash Vessel

Cooled treated gas


from Absorber #1
Water Wash Section

3A

35
3057

35
3057

35
3097

32
3014

32
3014

32
3054

39
3014

39
3014

39
3054

35
2987

7106.4
74599
10.50
-6881.2
1.00

7106.4
74599
10.50
-6881.2
1.00

10342.8
114312
11.05
-6882.7
1.00

6133.3
32157
5.24
-4163.2
1.00

6133.3
32157
5.24
-4163.2
1.00

8877.4
50387
5.68
-4270.6
1.00

6138.5
32259
5.26
-4150.0
1.00

6138.5
32259
5.26
-4150.0
1.00

8884.8
50531
5.69
-4257.7
1.00

6136.3
32206
5.25
-4156.4
1.00

7106.4
74599
168030.8
5985.1
10.50
1.005
-6881.2
3.00
12.46
0.096
0.014

7106.4
74599
168030.8
5985.1
10.50
1.005
-6881.2
3.00
12.46
0.096
0.014

10342.8
114312
244555.5
8589.9
11.05
1.004
-6882.7
2.87
13.31
0.093
0.015

6133.3
32157
145021.7
5222.2
5.24
1.013
-4163.2
5.71
6.16
0.107
0.010

6133.3
32157
145021.7
5222.2
5.24
1.013
-4163.2
5.71
6.16
0.107
0.010

8877.4
50387
209906.5
7460.5
5.68
1.013
-4270.6
5.30
6.75
0.105
0.010

6138.5
32259
145145.7
5358.7
5.26
1.013
-4150.0
5.71
6.01
0.108
0.010

6138.5
32259
145145.7
5358.7
5.26
1.013
-4150.0
5.71
6.01
0.108
0.010

8884.8
50531
210080.7
7652.6
5.69
1.013
-4257.7
5.31
6.60
0.106
0.010

6136.3
32206
145092.1
5336.5
5.25
1.014
-4156.4
5.73
6.03
0.131
0.012

12.8
1173.3
171.3
21.3
5314.9
412.9
0.0
0.0

12.8
1173.3
171.3
21.3
5314.9
412.9
0.0
0.0

18.6
1766.6
302.0
27.9
7486.1
741.6
0.0
0.0

9.2
211.1
171.1
21.3
5308.5
412.1
0.0
0.0

9.2
211.1
171.1
21.3
5308.5
412.1
0.0
0.0

13.3
317.4
301.6
27.9
7477.0
740.2
0.0
0.0

14.4
211.1
171.1
21.3
5308.5
412.1
0.037
0.061

14.4
211.1
171.1
21.3
5308.5
412.1
0.037
0.061

20.5
317.4
301.6
27.9
7477.0
740.2
0.054
0.088

12.5
210.9
171.1
21.3
5308.4
412.1
0.0
0.0

0.037
0.061
4.67
325

0.037
0.061
4.67
325

0.054
0.088
6.88
300

0.90
<1

Total Stream
Temperature
Pressure

C
kPa

Molar Rate
Mass Rate
Molecular Weight
Enthalpy
Mole Fraction Vapor

kg-mol/h
kg/h
kJ/kg

Vapor
Molar Rate
Mass Rate
Std. Vol. Rate
Actual Vol. Rate
Molecular Weight
Compressibility (from K)
Enthalpy
CP
Density
Th. Conductivity
Viscosity

kg-mol/h
kg/h
m3/h
3
m /h
kJ/kg
o
kJ/kg. C
3
kg/m
kW/m.oC x 10-3
mPa.s

Liquid
Molar Rate
Mass Rate
Actual Vol. Rate
Molecular Weight
Enthalpy
CP
Density
Surface Tension
Th. Conductivity
Viscosity
Density @ STD conditions

kg-mol/h
kg/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
mN/m
kW/m.oC x 10-3
mPa.s
kg/m3

Total Stream Composition kg-mol/h


H2O
CO2
CO
N2
H2
C1
DEDA
MDEA
Entrainment
DEDA
MDEA
Water (as free liquid)
Total Amine

kg-mol/h
kg-mol/h
kg/h
ppmw
Note 1 : Water wash section is designed for a higher treated gas temperature of 39C from the amine absorbers.

Page 1 of 5

SR.11.10343

63

Client: Shell Canada


Project: Quest CO2 Capture Unit

Date: January 27, 2011


By / Rev'd : AJ / RR

Heat and Material Balance

Stream Number
Stream Description

3B

3C

4A

4B

4C

5A

5B

5C

Cooled treated gas


from Absorber #2
Water Wash Section

Cooled treated gas


from Absorber #3
Water Wash Section

Lean amine to
Absorbers

Lean amine to
Absorber #1

Lean amine to
Absorber #2

Lean amine to
Absorber #3

Rich amine from


Absorber #1

Rich amine from


Absorber #2

Rich amine from


Absorber #3

Rich amine from


Absorbers

35
2987

35
3027

30
3711

30
3711

30
3711

30
3711

64
3057

64
3057

64
3097

64
2752

6136.3
32206
5.25
-4156.4
1.00

8881.8
50458
5.68
-4264.3
1.00

50766.1
1475491
29.06
-8720.5
0.00

14618.5
424879
29.06
-8720.5
0.00

14618.5
424879
29.06
-8720.5
0.00

21529.1
625733
29.06
-8720.5
0.00

15591.6
467321
29.97
-8741.0
0.00

15591.6
467321
29.97
-8741.0
0.00

22994.5
689658
29.99
-8741.5
0.00

54177.7
1624300
29.98
-8741.2
0.00

6136.3
32206
145092.1
5336.5
5.25
1.014
-4156.4
5.73
6.03
0.131
0.012

8881.8
50458
210009.7
7619.2
5.68
1.014
-4264.3
5.32
6.62
0.127
0.012

4.3
35
100.6
3.9
8.27
1.010
-6109.3
3.76
8.94
0.107
0.013

4.3
35
100.6
3.9
8.27
1.010
-6109.3
3.76
8.94
0.107
0.013

6.4
58
151.7
5.9
9.08
1.009
-6247.7
3.45
9.93
0.104
0.014

16.8
154
397.4
17.3
9.18
1.008
-6379.9
3.41
8.95
0.104
0.014

Total Stream
Temperature
Pressure

C
kPa

Molar Rate
Mass Rate
Molecular Weight
Enthalpy
Mole Fraction Vapor

kg-mol/h
kg/h
kJ/kg

Vapor
Molar Rate
Mass Rate
Std. Vol. Rate
Actual Vol. Rate
Molecular Weight
Compressibility (from K)
Enthalpy
CP
Density
Th. Conductivity
Viscosity

kg-mol/h
kg/h
m3/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
kW/m.oC x 10-3
mPa.s

Liquid
Molar Rate
Mass Rate
Actual Vol. Rate
Molecular Weight
Enthalpy
CP
Density
Surface Tension
Th. Conductivity
Viscosity
Density @ STD conditions

kg-mol/h
kg/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
mN/m
kW/m.oC x 10-3
mPa.s
kg/m3

50766.1
1475491
1418.3
29.06
-8720.5
3.57
1040.3
47.68
0.378
5.457
990.3

14618.5
424879
408.4
29.06
-8720.5
3.57
1040.3
47.68
0.378
5.457
990.3

14618.5
424879
408.4
29.06
-8720.5
3.57
1040.3
47.68
0.378
5.457
990.3

21529.1
625733
601.5
29.06
-8720.5
3.57
1040.3
47.68
0.378
5.457
990.3

15587.3
467286
424.0
29.98
-8741.2
2.97
1102.1
43.47
0.364
4.108
971.6

15587.3
467286
424.0
29.98
-8741.2
2.97
1102.1
43.47
0.364
4.108
971.6

22988.1
689599
625.1
30.00
-8741.7
2.96
1103.2
43.38
0.364
4.105
971.2

54160.8
1624146
1473.1
29.99
-8741.4
2.97
1102.5
43.43
0.364
4.099
971.4

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

12904.4
49.9
0.0
0.0
0.0
0.0
245.4
1418.8

12904.4
49.9
0.0
0.0
0.0
0.0
245.4
1418.8

19004.7
73.5
0.0
0.0
0.0
0.0
361.3
2089.5

12908.0
1012.1
0.2
0.0
6.4
0.8
245.4
1418.8

12908.0
1012.1
0.2
0.0
6.4
0.8
245.4
1418.8

19010.0
1522.7
0.4
0.0
9.1
1.4
361.3
2089.5

44825.9
3547.0
0.8
0.1
21.8
2.9
852.1
4927.1

Total Stream Composition kg-mol/h


H2O
CO2
CO
N2
H2
C1
DEDA
MDEA

12.5
210.9
171.1
21.3
5308.4
412.1
0.0
0.0

18.1
317.1
301.6
27.9
7476.9
740.2
0.0
0.0

0.90
<1

1.30
<1

Entrainment
DEDA
MDEA
Water (as free liquid)
Total Amine

kg-mol/h
kg-mol/h
kg/h
ppmw

Page 2 of 5

SR.11.10343

64

Client: Shell Canada


Project: Quest CO2 Capture Unit

Date: January 27, 2011


By / Rev'd : AJ / RR

Heat and Material Balance

Stream Number
Stream Description

10

11

12

13

14

15

Rich amine from


Cross Exch.

Rich amine feed to


Stripper

Stripped CO2 gas from


Stripper to OVHD
Condenser

Acid gas from


Reflux Drum

Condensed liquid from


Reflux drum

Stripper Reboiler
Feed

Vapor from Stripper


Reboiler

Liquid from Stripper


Reboiler

Pumped Lean amine


from Stripper to
Cross Exch.

Lean amine from


Cross Exch.

106
2452

83
162

85
147

36
144

36
144

116
175

119
175

119
175

119
1309

78
1109

54177.7
1624300
29.98
-8599.4
0.01

54177.7
1624300
29.98
-8599.4
0.05

5421.4
185017
34.13
809.0
1.00

3544.9
151218
42.66
352.8
1.00

2009.8
36208
18.02
149.9
0.00

58924.0
1625978
27.56
-9035.9
0.00

8158.0
150487
18.45
-13084.7
1.00

50766.1
1475491
29.06
-8386.2
0.00

50766.1
1475491
29.06
-8393.3
0.00

50766.1
1475491
29.06
-8549.4
0.00

379.4
15262
8972.0
464.7
40.22
0.952
-8932.0
1.07
32.84
0.035
0.020

2792.9
101695
66038.9
50601.7
36.41
0.995
-9500.8
1.05
2.01
0.027
0.015

5421.4
185017
128189.1
108975.8
34.13
0.998
809.0
1.12
1.70
0.022
0.016

3544.9
151218
83815.1
62978.3
42.66
0.994
352.8
0.88
2.40
0.018
0.015

53798.2
1609038
1513.0
29.91
-8596.3
3.30
1063.5
38.57
0.379
1.863
971.4

51384.7
1522605
1458.0
29.63
-8539.2
3.37
1044.3
41.37
0.387
1.978
971.4

50766.1
1475491
1510.6
29.06
-8386.2
3.87
976.7
37.33
0.413
0.749
990.3

50766.1
1475491
1505.9
29.06
-8393.3
3.84
979.8
37.32
0.412
0.771
990.3

50766.1
1475491
1459.1
29.06
-8549.4
3.69
1011.2
42.14
0.403
1.584
990.3

44825.9
3547.0
0.8
0.1
21.8
2.9
852.1
4927.1

44825.9
3547.0
0.8
0.1
21.8
2.9
852.1
4927.1

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

Total Stream
Temperature
Pressure

C
kPa

Molar Rate
Mass Rate
Molecular Weight
Enthalpy
Mole Fraction Vapor

kg-mol/h
kg/h
kJ/kg

Vapor
Molar Rate
Mass Rate
Std. Vol. Rate
Actual Vol. Rate
Molecular Weight
Compressibility (from K)
Enthalpy
CP
Density
Th. Conductivity
Viscosity

kg-mol/h
kg/h
m3/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
kW/m.oC x 10-3
mPa.s

8158.0
150487
192895.1
151328.8
18.45
0.994
-13084.7
1.88
0.99
0.033
0.010

Liquid
Molar Rate
Mass Rate
Actual Vol. Rate
Molecular Weight
Enthalpy
CP
Density
Surface Tension
Th. Conductivity
Viscosity
Density @ STD conditions

kg-mol/h
kg/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
mN/m
kW/m.oC x 10-3
mPa.s
kg/m3

2009.8
36208
36.4
18.02
149.9
4.18
993.6
70.20
0.624
0.707
999.0

58924.0
1625978
1659.5
27.56
-9035.9
3.89
979.8
38.37
0.437
0.698
991.0

2009.8
0.0
0.0
0.0
0.0
0.0
0.0
0.0

52836.1
308.7
0.0
0.0
0.0
0.0
852.1
4927.1

Total Stream Composition kg-mol/h


H2O
CO2
CO
N2
H2
C1
DEDA
MDEA

2022.2
3373.6
0.8
0.1
21.8
2.9
0.0
0.0

145.5
3373.7
0.8
0.1
21.9
2.9
0.0
0.0

Entrainment
DEDA
MDEA
Water (as free liquid)
Total Amine

kg-mol/h
kg-mol/h
kg/h
ppmw

7.24
<1

Page 3 of 5

8022.6
135.4
0.0
0.0
0.0
0.0
0.0
0.0

SR.11.10343

65

Client: Shell Canada


Project: Quest CO2 Capture Unit

Date: January 27, 2011


By / Rev'd : AJ / RR

Heat and Material Balance

Stream Number
Stream Description

16

17

18

Lean amine from


Cooler, E-7A/B

Lean amine from


Trim Cooler, E-8 A/B

Filtered Lean amine


to pumps

19 (Note 2)
Make-up Water
to Column

20A

20B

20C

Liquid from Water


Wash
section #1

Liquid from Water


Wash
section #2

Liquid from Water


Wash section #3

50
998

30
816

30
506

50766.1
1475491
29.06
-8650.6
0.00

50766.1
1475491
29.06
-8722.7
0.00

50766.1
1475491
1433.7
29.06
-8650.6
3.62
1029.1
45.36
0.391
3.019
990.3

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

21A

21B

21C

33
3000

38
3014

38
3014

38
3054

38
3244

38
3244

38
3289

50766.1
1475491
29.06
-8722.7
0.00

133.4
2409
18.06
-15790.3
0.00

2404.4
43436
18.06
-15771.1
0.00

2404.4
43436
18.06
-15771.1
0.00

3467.3
62641
18.06
-15770.6
0.00

2404.4
43436
18.06
-15770.6
0.00

2404.4
43436
18.06
-15770.6
0.00

3467.3
62641
18.06
-15770.1
0.00

50766.1
1475491
1418.3
29.06
-8722.7
3.57
1040.3
47.68
0.378
5.458
990.3

50766.1
1475491
1418.4
29.06
-8722.7
3.57
1040.3
47.68
0.378
5.445
990.3

133.4
2409
2.4
18.06
-15790.3
4.17
994.3
71.09
0.613
0.773
998.7

2404.4
43436
43.7
18.06
-15771.1
4.17
992.7
70.18
0.619
0.705
998.1

2404.4
43436
43.7
18.06
-15771.1
4.17
992.7
70.18
0.619
0.705
998.1

3467.3
62641
63.1
18.06
-15770.6
4.17
992.7
70.18
0.620
0.705
998.0

2404.4
43436
43.7
18.06
-15770.6
4.17
992.7
70.17
0.619
0.704
998.1

2404.4
43436
43.7
18.06
-15770.6
4.17
992.7
70.17
0.619
0.704
998.1

3467.3
62641
63.1
18.06
-15770.1
4.17
992.7
70.17
0.619
0.704
998.0

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

44813.5
173.4
0.0
0.0
0.0
0.0
852.1
4927.1

133.2
0.1
0.0
0.0
0.0
0.0
0.02
0.03

2400.6
1.9
0.0
0.0
0.8
0.1
0.356
0.581

2400.6
1.9
0.0
0.0
0.8
0.1
0.356
0.581

3461.7
2.9
0.0
0.0
1.2
0.2
0.509
0.839

2400.6
1.9
0.0
0.0
0.8
0.1
0.356
0.581

2400.6
1.9
0.0
0.0
0.8
0.1
0.356
0.581

3461.7
2.9
0.0
0.0
1.2
0.2
0.509
0.839

Pumped liquid from


Pumped liquid from
Pumped liquid from
Water Wash Vessel #1 Water Wash Vessel #2 Water Wash Vessel #3
to cooler
to cooler
to cooler

Total Stream
Temperature
Pressure

C
kPa

Molar Rate
Mass Rate
Molecular Weight
Enthalpy
Mole Fraction Vapor

kg-mol/h
kg/h
kJ/kg

Vapor
Molar Rate
Mass Rate
Std. Vol. Rate
Actual Vol. Rate
Molecular Weight
Compressibility (from K)
Enthalpy
CP
Density
Th. Conductivity
Viscosity

kg-mol/h
kg/h
m3/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
kW/m.oC x 10-3
mPa.s

Liquid
Molar Rate
Mass Rate
Actual Vol. Rate
Molecular Weight
Enthalpy
CP
Density
Surface Tension
Th. Conductivity
Viscosity
Density @ STD conditions

kg-mol/h
kg/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
mN/m
kW/m.oC x 10-3
mPa.s
kg/m3

Total Stream Composition kg-mol/h


H2O
CO2
CO
N2
H2
C1
DEDA
MDEA
Entrainment
DEDA
MDEA
Water (as free liquid)
Total Amine

kg-mol/h
kg-mol/h
kg/h
ppmw
Note 2 : Make-up water is based only on vaporization losses associated with treated gas leaving amine absorbers at 32C. It needs to include entrainment losses from the system based on operational experience.

Page 4 of 5

SR.11.10343

66

Client: Shell Canada


Project: Quest CO2 Capture Unit

Date: January 27, 2011


By / Rev'd : AJ / RR

Heat and Material Balance

Stream Number
Stream Description

22A

22B

22C

23C
Make-up Water to
Water Wash
Vessel #3

24C

Cooled circulating
liquid to Water Wash
Vessel #3

23B
Make-up Water to
Water Wash
Vessel #2

24B

Cooled circulating
liquid to Water Wash
Vessel #2

23A
Make-up Water to
Water Wash
Vessel #1

24A

Cooled circulating
liquid to Water Wash
Vessel #1

Purge from Water


Wash
Section #1

Purge from Water


Wash
Section #2

Purge from Water


Wash
Section #3

33
3141

33
3141

33
3186

35
3014

35
3014

35
3054

33
3141

33
3141

33
3186

2151.8
38873
18.06
-15790.3
0.00

2151.8
38873
18.06
-15790.3
0.00

3102.0
56041
18.06
-15789.8
0.00

250.3
4509
18.02
-15820.2
0.00

250.3
4509
18.02
-15820.2
0.00

362.3
6527
18.02
-15820.2
0.00

252.6
4563
18.06
-15790.3
0.00

252.6
4563
18.06
-15790.3
0.00

365.3
6599
18.06
-15789.8
0.00

2151.8
38873
39.1
18.06
-15790.3
4.17
994.3
71.09
0.613
0.773
998.1

2151.8
38873
39.1
18.06
-15790.3
4.17
994.3
71.09
0.613
0.773
998.1

3102.0
56041
56.3
18.06
-15789.8
4.17
994.3
71.09
0.613
0.773
998.0

250.3
4509
4.5
18.02
-15820.2
4.17
993.7
70.83
0.620
0.744
999.0

250.3
4509
4.5
18.02
-15820.2
4.17
993.7
70.83
0.620
0.744
999.0

362.3
6527
6.6
18.02
-15820.2
4.17
993.7
70.83
0.620
0.744
999.0

252.6
4563
4.6
18.06
-15790.3
4.17
994.3
71.09
0.613
0.773
998.1

252.6
4563
4.6
18.06
-15790.3
4.17
994.3
71.09
0.613
0.773
998.1

365.3
6599
6.6
18.06
-15789.8
4.17
994.3
71.09
0.613
0.773
998.0

2148.4
1.7
0.0
0.0
0.7
0.1
0.319
0.520

2148.4
1.7
0.0
0.0
0.7
0.1
0.319
0.520

3097.0
2.6
0.0
0.0
1.0
0.2
0.455
0.751

250.3
0.0
0.0
0.0
0.0
0.0
0.0
0.0

250.3
0.0
0.0
0.0
0.0
0.0
0.0
0.0

362.3
0.0
0.0
0.0
0.0
0.0
0.0
0.0

252.2
0.2
0.0
0.0
0.1
0.0
0.037
0.061

252.2
0.2
0.0
0.0
0.1
0.0
0.037
0.061

364.7
0.3
0.0
0.0
0.1
0.0
0.054
0.088

Total Stream
Temperature
Pressure

C
kPa

Molar Rate
Mass Rate
Molecular Weight
Enthalpy
Mole Fraction Vapor

kg-mol/h
kg/h
kJ/kg

Vapor
Molar Rate
Mass Rate
Std. Vol. Rate
Actual Vol. Rate
Molecular Weight
Compressibility (from K)
Enthalpy
CP
Density
Th. Conductivity
Viscosity

kg-mol/h
kg/h
m3/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
kW/m.oC x 10-3
mPa.s

Liquid
Molar Rate
Mass Rate
Actual Vol. Rate
Molecular Weight
Enthalpy
CP
Density
Surface Tension
Th. Conductivity
Viscosity
Density @ STD conditions

kg-mol/h
kg/h
m3/h
kJ/kg
kJ/kg.oC
kg/m3
mN/m
kW/m.oC x 10-3
mPa.s
kg/m3

Total Stream Composition kg-mol/h


H2O
CO2
CO
N2
H2
C1
DEDA
MDEA
Entrainment
DEDA
MDEA
Water (as free liquid)
Total Amine

kg-mol/h
kg-mol/h
kg/h
ppmw

Page 5 of 5

SR.11.10343

Appendix C:

Equipment List
01-27-11-rev0.pdf

67

Sized Equipment List

SR.11.10343

68
SHELL GLOBAL SOLUTIONS (US), INC.

Client
Project
Description

Shell Canada
Quest CO2 Capture Unit
Equipment List

Equipment No.

Description

January 27, 2011 / Rev. 0


By / Rev'd : AJ / RR
Type

Total
Qty.

Minimum Design Conditions


kPa (g) / Deg C

Size

Volume / Duty

Material

Comments

TOWERS
C-1

Amine Absorber #1

Trayed

3.35 m ID x 23.4 m T/T

3500 / 95 & HV / 150

C-2

Amine Absorber #2

Trayed

3.35 m ID x 23.4 m T/T

3500 / 95 & HV / 150

C-3

Amine Absorber #3

Trayed

4.27 m ID x 23.5 m T/T

3500 / 95 & HV / 150

C-4

Amine Stripper

Trayed

6.3 m ID x 30.4 m T/T

Shell: CS / SS Clad
Internals: SS
Shell: CS / SS Clad
Internals: SS
Shell: CS / SS Clad
Internals: SS

Twenty five (25) Shell Hi Fi valve trays .


The entire column is SS cladded.
Twenty five (25) Shell Hi Fi valve trays .
The entire column is SS cladded.
Twenty five (25) Shell Hi Fi valve trays .
The entire column is SS cladded.

Twenty (20) Shell Hi Fi valve trays in the bottom (stripping) section.


Shell: CS (PWHT) / SS Clad Four (4) Calming Section trays in the top (rectifying) section. The top 9.8
Internals: SS
m of the column (from top to 5th tray below rich amine feed inlet) is
claded.

350 / 200 & FV / 150

EXCHANGERS
E-1

Absorber #1 Circulating Water Cooler

Shell and Tube


(Cooling Water)

To be provided by others

P
id 3500 / 95 & HV / 150
Proc. side:
CW side: 800 / 60
(See Comments)

0.237 MW

Sh
ll CS / SS Cl
d
Shell:
Clad
Channel: CS
Tubes: SS

D
i pressure sett by
b Amine
A i Absorber
Ab b #1 design
d i pressure off 3500
Design
kPa(g). Shell side can be either CS or SS. However, if CS material is
used then 3mm SS cladding required. Tubes and tube sheet to be SS.

E-2

Absorber #2 Circulating Water Cooler

Shell and Tube


(Cooling Water)

To be provided by others

Proc. side: 3500 / 95 & HV / 150


CW side: 800 / 60
(See Comments)

0.237 MW

Shell: CS / SS Clad
Channel: CS
Tubes: SS

Design pressure set by Amine Absorber #2 design pressure of 3500


kPa(g). Shell side can be either CS or SS. However, if CS material is
used then 3mm SS cladding required. Tubes and tube sheet to be SS.

E-3

Absorber #3 Circulating Water Cooler

Shell and Tube


(Cooling Water)

To be provided by others

Proc. side: 3500 / 95 & HV / 150


CW side: 800 / 60
(See Comments)

0.342 MW

Shell: CS / SS Clad
Channel: CS
Tubes: SS

Design pressure set by Amine Absorber #3 design pressure of 3500


kPa(g). Shell side can be either CS or SS. However, if CS material is
used then 3mm SS cladding required. Tubes and tube sheet to be SS.

E-4

Lean / Rich Amine Exchanger

Plate and Frame


Lean / Rich Solvent

To be provided by others

Hot side: 1530 / 150 & HV / 150


Cold side: 3500 / 150 & HV / 150
(See Comments)

64.0 MW

SS Plates and
EPDM Gaskets

E-5

Stripper OVHD condenser

Shell and Tube


(Cooling Water)

To be provided by others

Proc. side: 350 / 200 & FV / 150


CW side: 800 / 60
(See Comments)

25.35 MW

Shell: SS
Channel: CS
Tubes: SS

96 08 MW
96.08

Shell: CS / SS Clad
Channel: CS
Tubes: SS

E 6 A/B
E-6

Stripper Reboiler

E-7 A/B

Lean Amine Cooler

E-8 A/B

Lean Amine Trim Cooler

Design pressure for hot side to be set by lean amine pump shut-off head.
Design pressure for cold side set by absober column design pressure at
3500 kPa(g)
Design pressure set by Amine Stripper Column design pressure of 350
kPa(g).
Saturated low pressure steam on the tube side
Shell side can be either CS or SS. However, if CS material is used then
3mm SS cladding required. Tubes and tube sheet to be SS. Duty given is
for both exchangers combined.

Shell / Tube
Kettle Type (Steam)

To be provided by others

Tube side: 500/ 250 & FV / 150


Shell side: 350 / 200 & FV / 150

Shell and Tube


(Cooling Water)

To be provided by others

Proc. side: 1530 / 150 & HV / 150


CW side: 800 / 60
(See Comments)

41.5 MW

Shell: SS
Channel: CS
Tubes: SS

Design pressure to be set by pump shut-off head - estimated at 1530


kPa(g). Duty given is for both exchangers combined.

Plate and Frame


Lean Amine/ Cooling Water

To be provided by others

Proc. side: 1530 / 150 & HV / 150


CW side: 800 / 60
(See Comments)

29.52 MW

Titaniunm Plates and


EPDM Gaskets

Design pressure to be set by pump shut-off head - estimated at 1530


kPa(g). Duty given is for both exchangers combined.

(See Comments) / 150

817 KW per pump


(Estimate)

Impeller: SS
Casing: SS

Pump head requirements are preliminary and to be confirmed during


detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 1530
kPa (g).
Added 10% to flow rate as design margin.

Impeller: SS
Casing: SS

Pump head requirements are preliminary and to be confirmed during


detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 710 kPa
(g).
Added 15% to flow rate as design margin
margin.
Pump head requirements are preliminary and to be confirmed during
detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 4420
kPa (g).
Added 10% to flow rate as design margin.

PUMPS
P-1 A/B

P-2 A/B

P-3 A/B

P-4 A/B

Lean Amine Booster Pumps

Stripper Reflux Pumps

Lean Amine Charge Pumps

Absorber #1 Circulating Water Wash Pumps

Centrifugal

Centrifugal

1 oper.
1 spare

2 x 100% Pumps
3
Each 1662 m /h @ 1139 kPa Head

1 oper.
1 spare

2 x 100% Pumps
3
Each 42 m /h @ 514 kPa Head

Centrifugal

1 oper.
1 spare

2 x 100% Pumps
3
Each 1560 m /h @ 3211 kPa Head

Centrifugal

1 oper.
1 spare

2 x 100% Pumps
3
Each 44 m /h @ 248 kPa Head

Page 1/2

(See Comments) / 150

12 KW per pump
(Estimate)

(See Comments) / 150

2165 KW per pump


(Estimate)

Impeller: SS
Casing: SS

(See Comments) / 150

6 KW per pump
(Estimate)

Impeller: SS
Casing: SS

Pump head requirements are preliminary and to be confirmed during


detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 3250
kPa (g).

SR.11.10343

69
SHELL GLOBAL SOLUTIONS (US), INC.

Client
Project
Description

Shell Canada
Quest CO2 Capture Unit
Equipment List

Equipment No.

P-5 A/B

P-6 A/B

P-7

P-8

Description

Absorber #2 Circulating Water Wash Pumps

Absorber #3 Circulating Water Wash Pumps

Amine Make-Up Tank Pump

Closed Drain Amine Pump

January 27, 2011 / Rev. 0


By / Rev'd : AJ / RR
Type

Total
Qty.

Minimum Design Conditions


kPa (g) / Deg C

Size

Centrifugal

1 oper.
1 spare

2 x 100% Pumps
3
Each 44 m /h @ 248 kPa Head

Centrifugal

1 oper.
1 spare

2 x 100% Pumps
3
Each 63 m /h @ 253 kPa Head

1 oper.

1 x 100% Pumps
3
Each 10 m /h @ 338 kPa Head

1 oper.

1 x 100% Pumps
3
Each 11 m /h @ 474 kPa Head

Centrifugal

Centrifugal

Volume / Duty

Material

Comments
Pump head requirements are preliminary and to be confirmed during
detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 3250
kPa (g).

(See Comments) / 150

6 KW per pump
(Estimate)

Impeller: SS
Casing: SS

(See Comments) / 150

8 KW per pump
(Estimate)

Impeller: SS
Casing: SS

(See Comments) / 150

3 KW per pump
(Estimate)

Impeller: SS
Casing: SS

Pump head requirements are preliminary and to be confirmed during


detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 430 kPa
(g).
Pump routed to Amine Stripper bottom sump

(See Comments) / 150

4 KW per pump
(Estimate)

Impeller: SS
Casing: SS

Pump head requirements are preliminary and to be confirmed during


detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 600 kPa
(g).
Pump routed to Amine Stripper bottom sump

Pump head requirements are preliminary and to be confirmed during


detailed design. Electric demand estimate based on 80% motor efficiency.
Design pressure to be set by pump shut-off head - estimated at 3300
kPa (g).

FILTERS
F-1

Lean Amine Filter

Cartridge

3
355 m /h

1530 / 150 & HV / 150


(See comments)

CS (PWHT)

Sized for 25% of Lean Amine Flow. Filtration required is 99% at 10 micron
absolute. Design pressure to be set by pump shut-off head - estimated at
1530 kPa(g).

F-2

Lean Amine Post Filter

Cartridge

3
75 m /h

1530 / 150 & HV / 150


(See comments)

CS (PWHT)

Sized for approximately 5% of Lean Amine Flow. Filtration required is 99%


at 10 micron absolute. Design pressure to be set by pump shut-off head estimated at 1530 kPa(g).

F-3

Closed Amine Drain Collection Filter

Cartridge

3
11 m /h

600 / 150 & HV / 150


(See comments)

CS (PWHT)

Filtration required is 99% at 10 micron absolute.


Design pressure to be set by pump shut-off head - estimated at 600
kPa(g).

T-1

Amine Make-Up Tank

Atmospheric Tank

2.15 m ID x 3.7 m T/T

TANKS
ATM / 150

10 m3 (nominal)

CS

Required working volume is 10 m3.

VESSELS
V-1

Absorber #1 Water Wash Vessel

Vertical

1.8 m ID x 10.5 m T/T

3500 / 95 & HV / 150

Shell: CS / SS Clad
Internals: SS

Three (3) bubble cap trays and 0.42 m Mellapak 250Y packing in the top
section & Six (6) Valve trays in bottom section. The entire vessel is SS
cladded.

V-2

Absorber #2 Water Wash Vessel

Vertical

1.8 m ID x 10.5 m T/T

3500 / 95 & HV / 150

Shell: CS / SS Clad
Internals: SS

Three (3) bubble cap trays and 0.42 m Mellapak 250Y packing in the top
section & Six (6) Valve trays in bottom section. The entire vessel is SS
cladded.

V-3

Absorber #3 Water Wash Vessel

Vertical

2.1 m ID x 10.7 m T/T

3500 / 95 & HV / 150

Shell: CS / SS Clad
Internals: SS

Three (3) bubble cap trays and 0.42 m Mellapak 250Y packing in the top
section & Six (6) Valve trays in bottom section. The entire vessel is SS
cladded.

V-4

Reflux Drum

Vertical

3.66 m ID x 6.9 m T/T

350 / 150 & FV / 150

Shell: SS
Internals: SS

V-5

Closed Amine Drain Collection Drum

Horizontal

Hold m ID x Hold m T/T

350 / 150 & HV / 150

CS (PWHT)
Internals: SS

Sizing to be determined by engineering contractor during detailed


engineering phase of the project after Shell Canada has defined their
drain strategy.

D-1

Lean Amine Carbon Filter

Activated Carbon

3.2 m ID x 6.0 m T/T

1530 / 150 & HV / 150


(See comments)

CS (PWHT)
Internals: SS

Sized for approximately 5% of Lean Amine Flow. Design pressure to be


set by pump shut-off head - estimated at 1530 kPa(g).

Page 2/2

SR.11.10343

70

Appendix D:

Process Equipment Data Sheets

Towers

C-1-rev0-1-27-2011.
pdf

C-2-rev0-1-27-2011.
pdf

C-3-rev0-1-27-2011. C-4-rev0-1-27-2011.
pdf
pdf

Exchangers

E-1-rev0-1-27-2011.
pdf

E-2-rev0-1-27-2011.
pdf

E-3-rev0-1-27-2011. E-4-rev1-2-7-2011.
pdf
pdf

E-6-rev0-1-27-2011.
pdf

E-7-rev0-1-27-2011. E-8-rev0-1-27-2011.
pdf
pdf

E-5-rev0-1-27-2011.
pdf

Vessels

V-1-rev0-01-27-2011 V-2-rev0-01-27-2011 V-3-rev0-01-27-2011 V-4-rev0-01-27-2011


.pdf
.pdf
.pdf
.pdf

Rotating Equipment

P-1-rev0-1-27-2011.
pdf

P-2-rev0-1-27-2011. P-3-rev0-1-27-2011.
pdf
pdf

P-6-rev0-1-27-2011.
pdf

P-7-rev0-1-27-2011. P-8-rev0-1-27-2011.
pdf
pdf

P-4-rev0-1-27-2011.
pdf

Filters

F-1-rev0-1-27-2011.
pdf

Tanks

T-1-rev0-1-27-2011.
pdf

F-2-rev0-1-27-2011
.pdf

F-3-rev0-1-27-2011. D-1-rev0-1-27-2011.
pdf
pdf

P-5-rev0-1-27-2011.
pdf

SR.11.10343

71

APPENDIX D1- COLUMNS

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #1

ITEM No:

C-1

SERVICE:

PROJECT No:

REVISION

27 Jan 2011

DATE

DOCUMENT CAT. - CLASS 1

BKK / AJ

ORIG. BY

DOCUMENT No.

REVIEWED

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1 of 14

OPERATING / MECHANICAL DATA


Description

Units

AMINE CONTACTOR

Contents
69

76

Working Temperature, max. / normal / min.

3057

Working Pressure - max. / normal / min.

kPa

- normal / min. vac. conditions


Design pressure, internal / external

kPa
95

Design temperature, upper / lower


(Note 4)

3500

HV @ 150 C

VAPOR

LIQUID

kPa (g)

Test pressure, hydrostatic / pneumatic

Feed Gas

Lean Amine

Treated Gas

Rich Amine

kPa

Quantity

74599

kg / hr

Molecular Weight

10.50

kg / kg mol

Density

12.46

kg/m3
424879

Quantity

kg / hr

Molecular Weight

29.06

kg / kg mol

Density

1040.3

kg/m3

32157

Quantity

kg / hr

Molecular Weight

5.24

Density

6.16

Quantity

35.2

467286

Molecular Weight

8.27

29.98

kg / kg mol

Density

8.94

1102.1

kg/m3

kg / kg mol
kg / m3
kg / hr

kg / kg mol
kg / kg mol
Vessel Orientation

Vertical

Overall Tangent - Tangent Length

23.4 m

Vessel Diameter

3.35 m

kg/m3
m

Description
Tray Numbers -

1 - 25

(Note 3)

3.35

Total Packed Height -

Note 1

Number of Packed Beds -

Note 1

Size and Type of Packing -

Note 1

Inside Diameter of Shell -

25

Number Trays Required Type of Trays -

Shell Hi Fi

Tray Spacing -

600

m
mm

Number of Tray Downcomers

m
Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm
Semielliptical

Type of heads
Minimum skirt height
Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:

Relief valve(s)

Earthquake factor

1) 600 mm layer of #2 Raschig Rings in bottom head of column. Vortex breaker to be covered with screen to prevent ring migration
2) Drawings to be reviewed by Shell Global Solutions (US) Inc
3) Trays are numbered from bottom to top (bottom tray is tray 1)
4) HV stands for half vacuum

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #1

ITEM No:

C-1

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
2 of 14

NOZZLE DATA

Mark

Number

NPS / Flange Class

Internal(s)

N1

Vapor Feed

Service

NPS 18" / 300

Half Open Pipe Internal

N2

Lean Amine Inlet

NPS 16" / 300

Branched Pipe Distributor

N3

Vapor Outlet

NPS 12" / 300

N4

Rich Amine Outlet

NPS 16" / 300

N5

Drain

NPS 3" / 300

Final Sizing by EPC Contractor

N6

Steam Out

NPS 3" / 300

Final Sizing by EPC Contractor

N7

Vent

NPS 6" / 300

Final Sizing by EPC Contractor

N8

Relief

TBD / 300

Final Sizing by EPC Contractor

Remarks

Vortex Breaker with Screen

INSTRUMENT CONNECTIONS
L1 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

L2 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

L3 A/B

Level Transmitter

NPS 2
2" / 300

Final Sizing by EPC Contractor

P1

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

MANHOLES
M1

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

M2

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

M3

Manhole

NPS 36" / 300

Include Blind (Manway Cover)

Material Note:

Internals to be fabricated from 316 SS

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #1

ITEM No:

C-1

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

Part

Material

Part

Carbon Steel

Shell

SS (Note 1)

Cladding/lining of shell

Carbon Steel

Heads

SS (Note 1)

Cladding/lining of heads

Material

Trays

316 SS

Distributors

316 SS

Downcomers

316 SS

Baffles

316 SS

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

3 of 14

Nuts, internal
Note 2

Nozzles (line pipe/plate)

Gaskets, external

Liner of nozzles and manholes

Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
316 SS

Internal parts

FABRICATION AND INSPECTION REQUIREMENTS


Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS internal cladding required on entire column
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer
is responsible for ensuring that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to
the manufacturer are for information and tendering purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to
all the applicable codes and national statutory regulations, and he shall obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1) Trays are numbered from bottom to top (i.e. bottom tray = tray 1)
2) Dimensions are in meters

DOCUMENT No.
4 of 14

TRAY SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

DOCUMENT No.

TRAY SECTION
Case
Tray number included (Note 1)
Loading on Actual Tray No.
Number of Trays Required
TRAY LOAD INFORMATION

DESIGN
1 - 25
1
25

Vapor Flow Rate to Tray, kg/hr

74599

Vapor Density, kg/m3

12.46

Vapor Viscosity, Pa s

1.4E-05

Liquid Flow Rate from Tray, kg/hr

467321

Liquid Density, kg/m3

1102.1

Surface Tension, N/m

0.043

Viscosity, Pa s

4.11E-03

Derating Factor
Purpose for Derating (Foaming, System, Safety)
TRAYS
Tower Inside Diameter, m
Tray Spacing, m
Type of Tray
Number of Downcomers per Tray
BUBBLING AREA
Required Net Free Area
Type of perforation
Perforation Type
Number of Valves Per Tray
Diameter of holes, m
Nominal Leg Length, m
Valve Thickness, m
Deck Thickness, m
Calculated Dry Tray Pressure Drop, Pa
Place valves below Downcomer Slots?
DOWNCOMERS
Downcomer Top Area
Downcomer Width @ Top, m
Downcomer Width @ Bottom, m
Downcomer Depth below Tray, m
Number of HiFi Downcomer slots per tray
Downcomer Slot Width, m
WEIRS
Weir Height, m
Picket Fence Weirs?
Picket Fence % Open
MATERIALS OF CONSTRUCTION
Tray Decks
Valves
Distributors

0.71
Foaming
3.35
0.600
Shell HiFi
6
0.053
Valves
Sulzer RV-1
393
0.0389
0.009525
0.002
0.002
490.8
Yes
0.281
0.360
0.190
0.350
100
0.015
0.15
No

316 SS
316 SS
316 SS

NOTES:
1) Perforations shall be evenly distributed on tray
2) Hi Fi slots to be distributed along bottom of downcomer - tray sketch indicates the number of slots per downcomer
3) Alternate trays are mirror images
4) Complete panel area to be equipped with valves including beneath downcomers and downcomer slots
5) All parts to fit within a nominal 24" manway
6) Valves to be Sulzer RV-1 or equivalent
7) Trays numbered from bottom to top (bottom tray = tray 1)
8) Note: estimated pressure drop per tray = 1704 Pa

5 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

HALF PIPE DISTRIBUTOR

Note: 1) End of distributor to be attached to clip on the vessel shell


2) Opening to face downwards
3) Approx 1.3 m spacing from nozzle centerline to collector tray deck above

DOCUMENT No.
6 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

COLLECTOR TRAY

Number of downpipes
Downpipe nominal size
Number of troughs
Width of trough, A

2
NPS 16
1
0.500 m

Depth of trough, B

0.250 m

Depth of gutters, C

0.575 m

Bottom of gutters to tray above, D

0.900 m

Gutter width (W)

0.450 m

Length of downpipes

6.000 m

1) Design and construction to be in accordance with DEP 31.20.20.31-Gen


2) Vortex Breakers shall be in compliance with Standard Drawing S 10.010 type B
3) Gutters shall have a slope of 1:200 towards the respective troughs
4) No drain holes required
5) Down pipes shall be supported to the vessel wall

7 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada Ltd

PROJECT No:

LOCATION:

Scotford, Alberta

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
0

REV

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

TRAYS 1 - 25

3.35

NOTES:

1) Odd trays shown. Even trays are mirror image.


2) Numbers on sketch denote the slot count in each downcomer. Downcomer bottom slots are 15 mm wide.
3) See also sheet 5.

8 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

LEAN AMINE DISTRIBUTOR

1) ENDS OF MAIN HEADER AND BRANCH HEADERS TO BE SECURED TO ATTACHMENTS ON COLUMN SHELL
2) TWO 10 mm DRAIN HOLES IN BOTTOM OF MAIN HEADER

DOCUMENT No.
9 of 14

MESH PAD SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 1

ITEM No:

C-1

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

INTERNAL
Case
Vapor Flow Rate to Mesh Pad, kg/hr
Vapor Density, kg/m3
Design Liquid Load, kg/hr
Liquid Density, kg/m3
Liquid Viscosity, Pa s
Surface Tension, N/m
MAT
Tower Inside Diameter, m
Required Mesh Pad Diameter, m
Required Mesh Pad Thickness, m
SPECIFICATIONS
Minimum Surface Area, 1/m
Minimum free volume of mat
Wire thickness, mm
Hold down grid required?
Mesh Material

DOCUMENT No.
10 of 14

Mesh Pad
DESIGN
32157
6.16
425
1040.3
0.00546
0.048
3.35
1.5
0.150
350
97%
0.23 - 0.28
YES
316SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be placed between two grids with a minimum free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 1

ITEM No:

SERVICE:
REVISION
DATE

C-1

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.028

DOCUMENT No.

11 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 1

ITEM No:

SERVICE:

DATE

C-1

REVISION

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

SEQUENCE No.

DWG S 20.029

DOCUMENT No.
12 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 1

ITEM No:

SERVICE:

DATE

C-1

REVISION

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.030

DOCUMENT No.
13 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 1

ITEM No:

SERVICE:
REVISION
DATE

C-1

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
14 of 14

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #2

ITEM No:

C-2

SERVICE:

PROJECT No:

REVISION

27 Jan 2011

DATE

DOCUMENT CAT. - CLASS 1

BKK / AJ

ORIG. BY

DOCUMENT No.

REVIEWED

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1 of 14

OPERATING / MECHANICAL DATA


Description

Units

AMINE CONTACTOR

Contents
69

76

Working Temperature, max. / normal / min.

3057

Working Pressure - max. / normal / min.

kPa

- normal / min. vac. conditions


Design pressure, internal / external

kPa
95

Design temperature, upper / lower


(Note 4)

3500

HV @ 150 C

VAPOR

LIQUID

kPa (g)

Test pressure, hydrostatic / pneumatic

Feed Gas

Lean Amine

Treated Gas

Rich Amine

kPa

Quantity

74599

kg / hr

Molecular Weight

10.50

kg / kg mol

Density

12.46

kg/m3
424879

Quantity

kg / hr

Molecular Weight

29.06

kg / kg mol

Density

1040.3

kg/m3

32157

Quantity

kg / hr

Molecular Weight

5.24

Density

6.16

Quantity

35.2

467286

Molecular Weight

8.27

29.98

kg / kg mol

Density

8.94

1102.1

kg/m3

kg / kg mol
kg / m3
kg / hr

kg / kg mol
kg / kg mol
Vessel Orientation

Vertical

Overall Tangent - Tangent Length

23.4 m

Vessel Diameter

3.35 m

kg/m3
m

Description
Tray Numbers -

1 - 25

(Note 3)

3.35

Total Packed Height -

Note 1

Number of Packed Beds -

Note 1

Size and Type of Packing -

Note 1

Inside Diameter of Shell -

25

Number Trays Required Type of Trays -

Shell Hi Fi

Tray Spacing -

600

m
mm

Number of Tray Downcomers

m
Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm
Semielliptical

Type of heads
Minimum skirt height
Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:

Relief valve(s)

Earthquake factor

1) 600 mm layer of #2 Raschig Rings in bottom head of column. Vortex breaker to be covered with screen to prevent ring migration
2) Drawings to be reviewed by Shell Global Solutions (US) Inc
3) Trays are numbered from bottom to top (bottom tray is tray 1)
4) HV stands for half vacuum

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #2

ITEM No:

C-2

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
2 of 14

NOZZLE DATA

Mark

Number

NPS / Flange Class

Internal(s)

N1

Vapor Feed

Service

NPS 18" / 300

Half Open Pipe Internal

N2

Lean Amine Inlet

NPS 16" / 300

Branched Pipe Distributor

N3

Vapor Outlet

NPS 12" / 300

N4

Rich Amine Outlet

NPS 16" / 300

N5

Drain

NPS 3" / 300

Final Sizing by EPC Contractor

N6

Steam Out

NPS 3" / 300

Final Sizing by EPC Contractor

N7

Vent

NPS 6" / 300

Final Sizing by EPC Contractor

N8

Relief

TBD / 300

Final Sizing by EPC Contractor

Remarks

Vortex Breaker with Screen

INSTRUMENT CONNECTIONS
L1 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

L2 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

L3 A/B

Level Transmitter

NPS 2
2" / 300

Final Sizing by EPC Contractor

P1

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

MANHOLES
M1

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

M2

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

M3

Manhole

NPS 36" / 300

Include Blind (Manway Cover)

Material Note:

Internals to be fabricated from 316 SS

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #2

ITEM No:

C-2

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

Part

Material

Part

Carbon Steel

Shell

SS (Note 1)

Cladding/lining of shell

Carbon Steel

Heads

SS (Note 1)

Cladding/lining of heads

Material

Trays

316 SS

Distributors

316 SS

Downcomers

316 SS

Baffles

316 SS

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

3 of 14

Nuts, internal
Note 2

Nozzles (line pipe/plate)

Gaskets, external

Liner of nozzles and manholes

Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
316 SS

Internal parts

FABRICATION AND INSPECTION REQUIREMENTS


Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS internal cladding required on entire column
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer
is responsible for ensuring that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to
the manufacturer are for information and tendering purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to
all the applicable codes and national statutory regulations, and he shall obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1) Trays are numbered from bottom to top (i.e. bottom tray = tray 1)
2) Dimensions are in meters

DOCUMENT No.
4 of 14

TRAY SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

DOCUMENT No.

TRAY SECTION
Case
Tray number included (Note 1)
Loading on Actual Tray No.
Number of Trays Required
TRAY LOAD INFORMATION

DESIGN
1 - 25
1
25

Vapor Flow Rate to Tray, kg/hr

74599

Vapor Density, kg/m3

12.46

Vapor Viscosity, Pa s

1.4E-05

Liquid Flow Rate from Tray, kg/hr

467321

Liquid Density, kg/m3

1102.1

Surface Tension, N/m

0.043

Viscosity, Pa s

4.11E-03

Derating Factor
Purpose for Derating (Foaming, System, Safety)
TRAYS
Tower Inside Diameter, m
Tray Spacing, m
Type of Tray
Number of Downcomers per Tray
BUBBLING AREA
Required Net Free Area
Type of perforation
Perforation Type
Number of Valves Per Tray
Diameter of holes, m
Nominal Leg Length, m
Valve Thickness, m
Deck Thickness, m
Calculated Dry Tray Pressure Drop, Pa
Place valves below Downcomer Slots?
DOWNCOMERS
Downcomer Top Area
Downcomer Width @ Top, m
Downcomer Width @ Bottom, m
Downcomer Depth below Tray, m
Number of HiFi Downcomer slots per tray
Downcomer Slot Width, m
WEIRS
Weir Height, m
Picket Fence Weirs?
Picket Fence % Open
MATERIALS OF CONSTRUCTION
Tray Decks
Valves
Distributors

0.71
Foaming
3.35
0.600
Shell HiFi
6
0.053
Valves
Sulzer RV-1
393
0.0389
0.009525
0.002
0.002
490.8
Yes
0.281
0.360
0.190
0.350
100
0.015
0.15
No

316 SS
316 SS
316 SS

NOTES:
1) Perforations shall be evenly distributed on tray
2) Hi Fi slots to be distributed along bottom of downcomer - tray sketch indicates the number of slots per downcomer
3) Alternate trays are mirror images
4) Complete panel area to be equipped with valves including beneath downcomers and downcomer slots
5) All parts to fit within a nominal 24" manway
6) Valves to be Sulzer RV-1 or equivalent
7) Trays numbered from bottom to top (bottom tray = tray 1)
8) Note: estimated pressure drop per tray = 1704 Pa

5 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

HALF PIPE DISTRIBUTOR

Note: 1) End of distributor to be attached to clip on the vessel shell


2) Opening to face downwards
3) Approx 1.3 m spacing from nozzle centerline to collector tray deck above

DOCUMENT No.
6 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

COLLECTOR TRAY

Number of downpipes
Downpipe nominal size
Number of troughs
Width of trough, A

2
NPS 16
1
0.500 m

Depth of trough, B

0.250 m

Depth of gutters, C

0.575 m

Bottom of gutters to tray above, D

0.900 m

Gutter width (W)

0.450 m

Length of downpipes

6.000 m

1) Design and construction to be in accordance with DEP 31.20.20.31-Gen


2) Vortex Breakers shall be in compliance with Standard Drawing S 10.010 type B
3) Gutters shall have a slope of 1:200 towards the respective troughs
4) No drain holes required
5) Down pipes shall be supported to the vessel wall

7 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada Ltd

PROJECT No:

LOCATION:

Scotford, Alberta

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
0

REV

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

TRAYS 1 - 25

3.35

NOTES:

1) Odd trays shown. Even trays are mirror image.


2) Numbers on sketch denote the slot count in each downcomer. Downcomer bottom slots are 15 mm wide.
3) See also sheet 5.

8 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

LEAN AMINE DISTRIBUTOR

1) ENDS OF MAIN HEADER AND BRANCH HEADERS TO BE SECURED TO ATTACHMENTS ON COLUMN SHELL
2) TWO 10 mm DRAIN HOLES IN BOTTOM OF MAIN HEADER

DOCUMENT No.
9 of 14

MESH PAD SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 2

ITEM No:

C-2

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

INTERNAL
Case
Vapor Flow Rate to Mesh Pad, kg/hr
Vapor Density, kg/m3
Design Liquid Load, kg/hr
Liquid Density, kg/m3
Liquid Viscosity, Pa s
Surface Tension, N/m
MAT
Tower Inside Diameter, m
Required Mesh Pad Diameter, m
Required Mesh Pad Thickness, m
SPECIFICATIONS
Minimum Surface Area, 1/m
Minimum free volume of mat
Wire thickness, mm
Hold down grid required?
Mesh Material

DOCUMENT No.
10 of 14

Mesh Pad
DESIGN
32157
6.16
425
1040.3
0.00546
0.048
3.35
1.5
0.150
350
97%
0.23 - 0.28
YES
316SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be placed between two grids with a minimum free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 2

ITEM No:

SERVICE:
REVISION
DATE

C-2

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.028

DOCUMENT No.

11 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 2

ITEM No:

SERVICE:

DATE

C-2

REVISION

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

SEQUENCE No.

DWG S 20.029

DOCUMENT No.
12 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 2

ITEM No:

SERVICE:

DATE

C-2

REVISION

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.030

DOCUMENT No.
13 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Absorber # 2

ITEM No:

SERVICE:
REVISION
DATE

C-2

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
14 of 14

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber #3

ITEM No:

C-3

SERVICE:

PROJECT No:

REVISION

27 Jan 2011

DATE

DOCUMENT CAT. - CLASS 1

BKK / AJ

ORIG. BY

DOCUMENT No.

REVIEWED

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1 of 14

OPERATING / MECHANICAL DATA


Description

Units

AMINE CONTACTOR

Contents
70

77

Working Temperature, max. / normal / min.


Working Pressure - max. / normal / min.

3097

kPa

- normal / min. vac. conditions

kPa
95

Design temperature, upper / lower


Design pressure, internal / external

(Note 4)

3500

HV @ 150 C

VAPOR

LIQUID

kPa (g)

Test pressure, hydrostatic / pneumatic

Feed Gas

Lean Amine

Treated Gas

Rich Amine

kPa

Quantity, kg/hr

114312

Molecular Weight

11.05

Density, kg/m3

13.31

kg / hr
kg / kg mol
kg / m3

Quantity, kg/hr

kg / hr

625733

Molecular Weight

29.06

kg / kg mol

Density, kg/m3

1040.3

kg / m3

Quantity, kg/hr

kg / hr

50387

Molecular Weight

5.68

Density, kg/m3

6.75

kg / kg mol

Quantity, kg/hr

58

689599

Molecular Weight

9.08

30.00

kg / kg mol

Density, kg/m3

9.9

1103.2

kg / m3

kg / m3
kg / hr

kg / hr
kg / kg mol
Vessel Orientation

Vertical

Overall Tangent - Tangent Length

23.5 m

Vessel Diameter

4.27 m

kg / m3
m

Description
Tray Numbers -

1 - 25

(Note 3)

Inside Diameter of Shell -

4.270

Total Packed Height -

Note 1

Number of Packed Beds -

Note 1

Size and Type of Packing -

Note 1

25

Number Trays Required Type of Trays -

Shell Hi Fi

Tray Spacing -

600

mm

Number of Tray Downcomers

m
Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm
Semielliptical

Type of heads
Minimum skirt height
Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:

Relief valve(s)

Earthquake factor

1) 600 mm layer of #2 Raschig Rings in bottom head of column. Vortex breaker to be covered with screen to prevent ring migration
2) Drawings to be reviewed by Shell Global Solutions (US) Inc
3) Trays are numbered from bottom to top (bottom tray is tray 1)
4) HV stands for half vacuum

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
2 of 14

NOZZLE DATA

Mark

Number

NPS / Flange Class

Internal(s)

N1

Vapor Feed

Service

NPS 24" / 300

Half Open Pipe Internal

N2

Lean Amine Inlet

NPS 18" / 300

Branched Pipe Distributor

N3

Vapor Outlet

NPS 16" / 300

N4

Rich Amine Outlet

NPS 20" / 300

N5

Drain

NPS 3" / 300

Final Sizing by EPC Contractor

N6

Steam Out

NPS 3" / 300

Final Sizing by EPC Contractor

N7

Vent

NPS 6" / 300

Final Sizing by EPC Contractor

N8

Relief

TBD / 300

Final Sizing by EPC Contractor

Remarks

Vortex Breaker with screen

INSTRUMENT CONNECTIONS
L1 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

L2 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

L3 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P1

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

MANHOLES
M1

Manhole

NPS 24" / 300

M2

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

M3

Manhole

NPS 36" / 300

Include Blind (Manway Cover)

Material Note:

Include Blind (Manway Cover)

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

Part

Material

Part

Carbon Steel

Shell

SS (Note 1)

Cladding/lining of shell

Carbon Steel

Heads

SS (Note 1)

Cladding/lining of heads

Material

Trays

316 SS

Distributors

316 SS

Downcomers

316 SS

Baffles

316 SS

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

3 of 14

Nuts, internal
Note 2

Nozzles (line pipe/plate)

Gaskets, external

Liner of nozzles and manholes

Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
316 SS

Internal parts

FABRICATION AND INSPECTION REQUIREMENTS


Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS cladding required for the entire column
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer
is responsible for ensuring that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to
the manufacturer are for information and tendering purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to
all the applicable codes and national statutory regulations, and he shall obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

Note:

1) 25 trays required. Trays are numbered from the bottom to the top
2) Column dimensions are in meters

DOCUMENT No.
4 of 14

TRAY SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

TRAY SECTION
Case
Tray number included (Note 1)
Loading on Actual Tray No.
Number of Trays Required
TRAY LOAD INFORMATION
Vapor Flow Rate to Tray, kg/hr
Vapor Density, kg/m 3
Vapor Viscosity, Pa s
Liquid Flow Rate from Tray, kg/hr
Liquid Density, kg/m3
Surface Tension, N/m
Liquid Viscosity, Pa s
Derating Factor
Purpose for Derating (Foaming, System, Safety)
TRAYS
Tower Inside Diameter, m
Tray Spacing, m
Type of Tray
Number of Downcomers per Tray
BUBBLING AREA
Required Net Free Area
Type of perforation
Perforation Type
Number of Valves Per Tray
Diameter of holes, m
Nominal Leg Length, m
Valve Thickness, m
Deck Thickness, m
Dry Tray Pressure Drop, Pa
Place valves below Downcomer Slots?
DOWNCOMERS
Downcomer Top Area
Downcomer Width @ Top, m
Downcomer Width @ Bottom, m
Downcomer Depth below Tray, m
Number of HiFi Downcomer slots per tray
Downcomer Slot Width, m
WEIRS
Weir Height, m
Picket Fence Weirs?
Picket Fence % Open
MATERIALS OF CONSTRUCTION
Tray Decks
Valves
Distributors

DOCUMENT No.

DESIGN
1 - 25
1
25
114312
13.31
1.5E-05
689658
1103.2
0.043
4.1E-03
0.71
Foaming
4.27
0.600
Shell HiFi
8
0.048
Valves
Sulzer RV-1
578
0.0389
0.009525
0.002
0.002
499
Yes
0.2548
0.305
0.1625
0.350
178
0.015
0.15
No

316 SS
316 SS
316 SS

NOTES:
1) Perforations shall be evenly distributed
2) Hi Fi slots to be evenly distributed - tray sketch indicates the number of slots in each group
3) Alternate trays are mirror image
4) Complete panel area to be equipped with valves including beneath downcomers and downcomer slots
5) All parts to fit within a nominal 24" manway
6) Valves to be Sulzer RV-1 or equivalent
7) Trays numbered from bottom to top (bottom tray = tray 1)
8) Estimated tray pressure drop per tray = 1712 Pa

5 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

PROJECT No:

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

HALF PIPE DISTRIBUTOR

1) End of distributor to be attached to clip on vessel shell


2) Opening to face downwards
3) Approx 1.2 m spacing from nozzle centerline to collector tray deck above

DOCUMENT No.
6 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

PROJECT No:

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

COLLECTOR TRAY

Inner diameter of column


Number of downpipes
Downpipe nominal size

4.27

2
NPS 18

Number of troughs

Width of trough, A

0.750

Depth of trough, B

0.3

Depth of gutters, C

0.675

Bottom of gutter to tray above, D

1.000

Gutter width, W

0.600

Downpipe Length

6.000

1) Design and construction to be in accordance with DEP 31.20.20.31-Gen


2) Vortex Breakers shall be in compliance with Standard Drawing S 10.010 type B
3) Gutters shall have a slope of 1:200 towards the respective troughs
4) No drain holes required
5) Down pipes shall be supported to the vessel wall

7 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada Ltd

PROJECT No:

LOCATION:

Scotford, Alberta

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
0

REV

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

NOTES:

28

30

23

23

30

28

TRAYS 1 - 25

1) Odd tray shown. Even trays are mirror image.


2) Numbers on sketch denote the slot count in each slot group. Downcomer bottom slots are 15 mm wide.
3) See also sheet 5.

8 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1) END OF MAIN HEADER AND BRANCH HEADERS TO BE CLIPPED TO VESSEL WALL


2) TWO 10 mm DRAIN HOLES NEEDED ON BOTTOM OF MAIN HEADER

DOCUMENT No.
9 of 14

MESH PAD SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

INTERNAL
Case
Vapor Flow Rate to Mesh Pad, kg/hr
Vapor Density, kg/m3
Design Liquid Load, kg/hr
Liquid Density, kg/m3
Liquid Viscosity, Pa s
Surface Tension, N/m
MAT
Tower Inside Diameter, m
Required Mesh Pad Diameter, m
Required Mesh Pad Thickness, m
SPECIFICATIONS
Minimum Surface Area, 1/m
Minimum free volume of mat
Wire thickness, mm
Hold down grid required?
Mesh Material

DOCUMENT No.
10 of 14

Mesh Pad
DESIGN
50387
6.75
626
1040.3
0.0055
0.0477
4.27
2.00
0.15
350
97%
0.23 - 0.28
YES
316 SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be places between two grids with free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.028

DOCUMENT No.
11 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.029

DOCUMENT No.
12 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.030

DOCUMENT No.
13 of 14

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Absorber # 3

ITEM No:

C-3

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK / AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
14 of 14

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE
ORIG. BY

BKK

REVIEWED

WDV

DOCUMENT CAT. - CLASS 1


DOCUMENT No.
1 of 21

SHEET

RR

APP. BY

DOCUMENT SEQUENCE No.


OPERATING / MECHANICAL DATA

Description

Units

AMINE REGENERATOR

Contents
Working Temperature, max. / normal / min.

119

Working Pressure - max. / normal / min.

175

kPa

- normal / min. vac. conditions

kPa

Design temperature, upper / lower

200

Design pressure, internal / external

350

FV @ 150 C

Vapor

Liquid

kPa (g)

Test pressure, hydrostatic / pneumatic

Amine Feed

Overhead

Reflux

Lean Amine

kPa

Quantity

101695

1522605

Molecular Weight

36.4

29.6

Density

2.01

1044.3

Quantity

185017

Molecular Weight

34.1

Density

1.70

kg / hr
kg / kg mol
kg/m3
kg / hr
kg / kg mol
kg/m3

Quantity

kg / hr

36208

Molecular Weight

18.0

kg / kg mol

Density

993.6

kg/m3

Quantity

1475491

Molecular Weight

29.1

Density

976.7

Vessel Orientation

Vertical

Overall Tangent - Tangent Length

30.4 m
6.3 m

Vessel Diameter

Tray section

lower

upper

Tray Numbers

1 - 20

21 - 24

Tray Diameter

6.3 m

6.3 m

Total Packed Height

NA

NA

Number of Packed Beds

NA

NA

Size and Type of Packing

NA

NA

Number Trays Required

20

Shell Hi Fi

Calming Section

Tray Spacing

600

600

Number of Tray Downcomers

12

15

Tray Type

m
mm

m
Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm

Semielliptical

Type of heads
Minimum skirt height

Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:

1) Drawings to be reviewed by Shell Global Solutions (US) Inc


2) Trays numbered from the bottom, i.e. bottom tray = 1

Relief valve(s)

Earthquake factor

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

SHEET

APP. BY

RR

2 of 21

DOCUMENT SEQUENCE No.


NOZZLE DATA

Service

NPS / Flange Class

Internal(s)

NPS 36" / 150

Type 4 Schoepentoeter

Mark

Number

N1A/B

Rich Amine Feed

N2

Vapor Outlet

NPS 42" / 150

N3

Lean Amine Outlet

NPS 30" / 150

N4

Drain

NPS 3" / 150

N5A/B

Reboiler Vapor Return

NPS 36" / 150

N6

Steam Out

NPS 3" / 150

Final Sizing by EPC Contractor

N7

Vent

NPS 6" / 150

Final Sizing by EPC Contractor

N8

Relief

TBD / 150

N9A/B

Reboiler Feed Liquid

NPS 30" / 150

Remarks

Vortex Breaker
Final Sizing by EPC Contractor
Half Pipe Internal

Final Sizing by EPC Contractor

Final Sizing by EPC Contractor

N10A/B

Reboiler Liquid Return

NPS 24" / 150

N11

Reflux

NPS 3" / 150

Vortex Breaker

Final Sizing by EPC Contractor


Final Sizing by EPC Contractor

Branched Pipe Distributor

INSTRUMENT CONNECTIONS
L1 A/B

Level Transmitter

NPS 2" / 150

Final Sizing by EPC Contractor

L2 A/B

Level Transmitter

NPS 2" / 150

Final Sizing by EPC Contractor

L3 A/B

Level Transmitter

NPS 2
2" / 150

Final Sizing by EPC Contractor

P1

Pressure Transmitter

NPS 2" / 150

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 150

Final Sizing by EPC Contractor

P3

Pressure Transmitter

NPS 2" / 150

Final Sizing by EPC Contractor

T1

Thermowell

NPS 2" / 150

Final Sizing by EPC Contractor

T2

Thermowell

NPS 2" / 150

Final Sizing by EPC Contractor

T3

Thermowell

NPS 2" / 150

Final Sizing by EPC Contractor

MANHOLES
M1

Manhole

NPS 24" / 150

Include Blind (Manway Cover)

M2

Manhole

NPS 24" / 150

Include Blind (Manway Cover)

M3

Manhole

NPS 24" / 150

Include Blind (Manway Cover)

M4

Manhole

NPS 24" / 150

Include Blind (Manway Cover)

Note:

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

SHEET

APP. BY

RR
Part

Material

Part

Carbon Steel (PWHT)

Shell

Note 1

Cladding/lining of shell

Carbon Steel (PWHT)

Heads

3 of 21

DOCUMENT SEQUENCE No.

Note 1

Cladding/lining of heads

316 SS

Distributors

316 SS

Downcomers

316 SS

Baffles

316 SS

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

Material

Trays

Nuts, internal
Note 2

Nozzles (line pipe/plate)

Gaskets, external

Liner of nozzles and manholes

Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
316 SS

Internal parts

FABRICATION AND INSPECTION REQUIREMENTS


Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS cladding required for the top of the column through tray 16 (ie top through 5 trays below feed inlet nozzle N1)
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details
Note 4: Corrosion allowance of 6 mm is required for the bottom of the column up to the reoiler vapor return nozzles N5A/B

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer
is responsible for ensuring that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to
the manufacturer are for information and tendering purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to
all the applicable codes and national statutory regulations, and he shall obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

ORIG. BY

BKK

REVIEW

WDV

APP. BY

RR

1) All dimensions are in meters

DOCUMENT CAT.-CLASS 1
DOCUMENT No.
SHEET
DOCUMENT SEQUENCE No.

4 of 21

TRAY SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

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TRAY SECTION
Case
Tray number included (Note 1)
Loading on Actual Tray No.
Number of Trays Required
TRAY LOAD INFORMATION
Vapor Flow Rate to Tray, kg/hr
Vapor Density, kg/m3
Vapor Viscosity, Pa s
Liquid Flow Rate from Tray, kg/hr
Liquid Density, kg/m3
Surface Tension, N/m
Viscosity, Pa s
Derating Factor
Purpose for Derating (Foaming, System, Safety)
TRAYS
Tower Inside Diameter, m
Tray Spacing, m
Type of Tray
Number of Downcomers per Tray
BUBBLING AREA
Required Net Free Area
Type of perforation
Perforation Type
Number of Valves Per Tray
Diameter of holes, m
Nominal Leg Length, m
Valve Thickness, m
Deck Thickness, m
Dry Tray Pressure Drop, Pa
(Note 7)
Place valves below Downcomers?
DOWNCOMERS
Downcomer Top Area Fraction of Column Area
Downcomer Width @ Top, m
Downcomer Width @ Bottom, m
Downcomer Length @ Top, m
Downcomer Length @ Bottom, m
Downcomer Depth below Tray, m
Number of HiFi Downcomer slots per tray
Downcomer Slot Width, m
Spacing between slots in a group
Downcomer Seal Pans Required?
WEIRS

DOC.SEQUENCE No.
Lower
DESIGN
1 - 20
1
20

Upper
DESIGN
21 - 24
21
24

150487
0.99
9.7E-06
1625978
979.8
0.038
0.00070
0.71
Foaming

193096
1.74
1.4E-05
39185
968.8
0.062
0.00033
0.71
Foaming

6.30
0.600
Shell HiFi
12

6.30
0.600
Calming Section
15

0.120
Valves
RV-1 or equiv
3147
0.0389
0.0127
0.002
0.002
296
Yes

0.110
Valves
RV-1 or equiv
2885
0.0389
0.0127
0.002
0.002
330
Yes

0.310
0.350
0.185
------------0.400
480
0.015
0.015
No

0.058
0.200
0.200
0.600
0.600
0.400
------------------Yes

0.075
No
-------

0.10
Yes
15%
0.20

316 SS
316 SS
316 SS
NPS 24

316 SS
316 SS
316 SS
NPS 24

Weir Height, m
Picket Fence Weirs?
Picket Fence % Open
Picket Fence Height, m
MATERIALS OF CONSTRUCTION
Tray Decks
Valves
Distributors
Manhole Size
NOTES:
1) Perforations shall be evenly distributed

2) Hi Fi slots to be arranged in groups - tray sketch indicates the number of slots in each group
3) Alternate trays are mirror image
4) Complete panel area to be equipped with valves including beneath downcomers and downcomer slots
5) Trays numbered from the bottom up (bottom tray = Tray 1)
6) Valves are Sulzer RV-1 or equivalent
7) The estimated total tray pressure drop for trays 1-20 is 828 Pa per tray ; for trays 21-24, 854 Pa per tray

5 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

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APP. BY

RR

DOCUMENT SEQUENCE No.

6 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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DOCUMENT SEQUENCE No.

COLLECTOR TRAY

Number of draw off nozzles


Draw-off Nozzles
Internal nozzle nominal size
Number of troughs
Width of trough, A

2
N9A/B
NPS 30
1
0.900 m

Depth of trough, B

0.370 m

Height of gutters, C

0.650 m

Bottom of gutters to tray floor above, D

1.000 m

Gutter width (W)

0.900 m

Notes: 1) Design and construction to be in accordance with DEP 31.20.20.31-Gen


2) Vortex Breakers shall be in compliance with Standard Drawing S 10.010 type B
3) Gutters shall have a slope of 1:200 towards the respective troughs
4) No drain holes required
5) Materials of construction to be 316 SS
6) Gutter connections to be gasketed

7 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada Ltd

PROJECT No:

LOCATION:

Scotford, Alberta

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

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APP. BY

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SKETCH OF TRAYS 1-20

NOTES:

1) Odd trays shown. Even trays are mirror image.


2) Numbers on sketch denote the slot count in each slot group. Downcomer bottom slots are 15 mm wide.

DOCUMENT SEQUENCE No.

8 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada Ltd

PROJECT No:

LOCATION:

Scotford, Alberta

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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APP. BY

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SKETCH OF TRAYS 21 - 24

NOTES:

1) Odd trays shown. Even trays are mirror image.

DOCUMENT SEQUENCE No.

9 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada Ltd

PROJECT No:

LOCATION:

Scotford, Alberta

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

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DOCUMENT No.

REVIEW

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CALMING SECTION TRAY DETAILS

NOTES:

1) Dimensions are in meters

DOCUMENT SEQUENCE No.

10 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

Amine Stripper

ITEM No:

SERVICE:
REVISION
DATE

C-4

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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11 of 21

SEQUENCE No.

CHIMNEY DISTRIBUTION TRAY

RISER

RISER

RISER

RISER

RISER

RISER

RISER

BLANK AREA
RISER

RECTANGULAR RISERS
EQUIPPED WITH HATS.
RISERS 0.3M WIDE

0.3 M HIGH OVERFLOW


WEIRS

1.6 m

RISER

RISER

6.3 m

DOWNCOMERS HAVE PICKET


FENCE WEIRS 30% OPEN AREA.
50% BOTTOM SLOT AREA

10 DOWNCOMERS DISCHARGING ONTO


BUBBLING AREA BELOW. BOTTOM OF
DOWNCOMERS EQUIPPED WITH 15 MM WIDE
SLOTS. DOWNCOMERS 0.35 M WIDE

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

ORIG. BY

BKK

REVIEW

WDV

APP. BY

RR

DOCUMENT CAT.-CLASS 1
DOCUMENT No.
SHEET
DOCUMENT SEQUENCE No.

12 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION

27 Jan 2011

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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Inner diameter of column

6.3

Feed nozzle number

N11

Nozzle nominal size

NPS3

Same diameter for all branches

Notes:

Non perforated length of branches

0.09

HOLES

Hole diameter

0.008

Number of holes

1)

Design and construction shall be in accordance

2)

Holes above bubbling area. No holes above calming sections

3)

Holes at positions indicated

4)

Centerline of feed nozzle N11 to be 600 mm above Tray 24

5)

Calming sections of tray 24 are displayed.

6)

Pipe end(s) to be closed and supported to clips on column wall

7)

Main header should be provided with a 10 mm drain hole.

with the requirements of DEP 31.20.20.31-Gen.

YES

Number of branches per side

Type of perforations

13 of 21

DOCUMENT SEQUENCE No.

40
MATERIALS

Pipe material
Corrosion allowance

Branch No

316SS
---

mm

Number of holes

Angle, deg

Pitch, mm

Left

Right

Left

Right

Left

Right

-62

62

236

295

-62

395

MESH PAD SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOC. CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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INTERNAL
Case
Vapor Flow Rate to Mesh Pad, kg/hr
Vapor Density, kg/m3
Design Liquid Load, kg/hr
Liquid Density, kg/m3
Liquid Viscosity, Pa s
Surface Tension, N/m
MAT
Tower Inside Diameter, m
Required Mesh Pad Diameter, m
Required Mesh Pad Thickness, m
SPECIFICATIONS
Minimum Surface Area, 1/m
Minimum free volume of mat
Wire thickness, mm
Hold down grid required?
Mesh Material

14 of 21

DOC.SEQUENCE No.
Mesh Pad
DESIGN
185017
1.70
36.2
993.5
0.0007
0.0702
6.30
4.50
0.15
350
97%
0.23 - 0.28
YES
316 SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be places between two grids with free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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DOCUMENT SEQUENCE No.

Nozzle

N1A / B

Schoepentoeter Type

Type IV

Nozzle size

NPS 36

Feed nozzle ID

889 mm

Required schoepentoeter length

3023 mm

Length straight part of the vanes (Lv)

100 mm

Vane radius (Rv)

100 mm

Plate thickness

3 mm

Number of vanes per side (nv)

29 -

Top angle

8.7

Vane angle

10

Actual vane opening (Wvo)

29.5 mm

Nozzle protrusion

100 mm

Ladder width

260 mm

Multiple vane ladders

Yes

Catcher Cap?

Not Allowed

NOTES:
1) All parts must pass through a nominal NPS24 manhole
2) Refer to schoepentoeter drawings S 20.017/19 for details

15 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION
DATE

27 Jan 2011

ORIG. BY

BKK

REVIEW

WDV

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DWG S 20.028

DOCUMENT CAT.-CLASS 1
DOCUMENT No.
SHEET
DOCUMENT SEQUENCE No.

16 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

ORIG. BY

BKK

REVIEW

WDV

APP. BY

RR

DWG S 20.029

DOCUMENT CAT.-CLASS 1
DOCUMENT No.
SHEET
DOCUMENT SEQUENCE No.

17 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION
DATE

27 Jan 2011

ORIG. BY

BKK

REVIEW

WDV

APP. BY

RR

DWG S 20.030

DOCUMENT CAT.-CLASS 1
DOCUMENT No.
SHEET
DOCUMENT SEQUENCE No.

18 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

19 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
REVISION
DATE

0
27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

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DWG S 20.017

DOCUMENT SEQUENCE No.

20 of 21

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Amine Stripper

ITEM No:

C-4

SERVICE:
0

REVISION
DATE

27 Jan 2011

DOCUMENT CAT.-CLASS 1

ORIG. BY

BKK

DOCUMENT No.

REVIEW

WDV

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DWG S 20.019

DOCUMENT SEQUENCE No.

21 of 21

SR.11.10343

72

APPENDIX D2- EXCHANGERS

SHELL GLOBAL SOLUTIONS (US)


SHELL & TUBE HEAT EXCHANGER DATA SHEET
Shell Canada Limited
1 Customer
HMU CO2 Capture Project
2 Project
3 Plant Location Scotford
4
5 Service of Unit Absorber #1 Circulating Water Cooler
6 Frame Size (LxWxH)
7 Surface Area / Unit
8

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

m
2
m

1
2
3
4

1 of 1
1
E-1
Parallel

Series
m2

PERFORMANCE OF ONE UNIT

Shell Side
Tube Side
9 Fluid Allocation
Cooling Water
10 Fluid Name
Circulating Wash Water
43,436
40,734
11 Fluid Quality, Total
kg/h
12 Vapor (In/Out)
kg/h
kg/h
13 Liquid
43,436
43,436
40,734
40,734
14 Steam
kg/h
kg/h
15 Water
kg/h
16 Non-Condensable
C
37.7
25.0
30.0
33.0
17 Temperature (In/Out)
Liquid / Vapor
kg / m3
992.7
994.3
995.0
996.5
18 Density,
/
/
/
/
Liquid / Vapor
0.70
cP
0.91
0.82
0.77
19 Viscosity,
/
/
/
/
18.06
18.02
18.02
18.06
20 Molecular Weight, Liquid / Vapor
/
/
/
/
21 Molecular Weight, Non-Condensable
/
/
/
/
kJ / kgC
4.18
4.17
4.18
4.17
22 Specific Heat, Liquid / Vapor
/
/
/
/
0.613
W/m-C
0.606
0.613
0.619
23 Thermal Cond., Liquid / Vapor
/
/
/
/
kJ / kg @C
24 Latent Heat
kPa (g)
3,150
420
25 Inlet Pressure
m/s
26 Velocity
kPa
70
70
27 Pressure Drop, Allowable / Calc
28 Overall Fouling Allowance
% Excess Area
2
m -C/W
0.00036
0.00025
29 Fouling Resistance (min)
kPa
30 Wall Shear Stress
31 Heat Exchanged
237
kW
MTD (Corrected)
C
W/m2C
32 Transfer Rate, Service
Dirty
Clean
Sketch (Pass Arrangement / Nozzle Orientation)
33
CONSTRUCTION OF ONE UNIT
Tube Side
34
Shell Side
3500
800 (Note1) /
35 Design / Test Pressure
(Note 2,5) kPa (g)
/
HV
36 Design/ MDMT Temperature
(Note 2) C
95
/
150
60
/
37 No Passes/ No. Channels per pass
38 Corrosion Allowance
in
Connection
3 / 150#
3 / 300#
39
In
(Note 4) in
3 / 300#
3 / 150#
40
Size &
Out
(Note 4) in
2 / 300#
2 / 150#
41
Rating
Vent & Drain (Note 4) in
42 Tube No.
OD
mm
Thk.
mm
m
Pitch
Layout
Stainless Steel (Note 3)
43 Tube Type
Material
Shell Cover
Carbon Steel (Note 3)
44 Shell
ID
inch
Channel Cover
Carbon Steel
45 Channel or Bonnet
Tubesheet-Float
Stainless Steel (Note 3)
46 Tubesheet-Stationary
Impingement Plate
47 Floating Head Cover
%Cut (Area)
Spacing(c/c)
48 Baffles-Cross
Inlet
in
Seal Type
49 Baffles-Long
U-Bend
Type
50 Supports-Tube
Tube-Tubesheet Joint
51 Bypass Seal Arrangement
Type
52 Expansion Joint
Bundle Entrance
Bundle Exit
53 Rho-V2-Inlet Nozzle
Floating Head
Tube Side
54 Gaskets-Shell Side
55
56
57
58
59
60
61
62
63

Code Requirements

TEMA Class

Weight/Shell
Filled with Water
Bundle
NOTES:
1. Cooling water design conditions per utilities design data.
2. Design temperature and pressure conditions to be confirmed in detailed engineering.
3. Shell side can be either CS or SS. However if CS material is used then 3mm SS cladding is required. Tubes and tubesheet to be
SS. Refer to the Materials Section of the BDP for additional detail.
4. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.
5. HV stands for half vacuum.

64
REVISION NO:
65
INITIAL / DATE
66 PROCESS ENGINEER

0
AJ

1/27/11

lb

5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66

SHELL GLOBAL SOLUTIONS (US)


SHELL & TUBE HEAT EXCHANGER DATA SHEET
Shell Canada Limited
1 Customer
HMU CO2 Capture Project
2 Project
3 Plant Location Scotford
4
5 Service of Unit Absorber #2 Circulating Water Cooler
6 Frame Size (LxWxH)
7 Surface Area / Unit
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63

Fluid Allocation
Fluid Name
Fluid Quality, Total
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
kg/h
Temperature (In/Out)
C
Density,
Liquid / Vapor
kg / m3
Viscosity,
Liquid / Vapor
cP
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
Specific Heat, Liquid / Vapor
kJ / kgC
Thermal Cond., Liquid / Vapor
W/m-C
Latent Heat
kJ / kg @C
Inlet Pressure
kPa (g)
Velocity
m/s
Pressure Drop, Allowable / Calc
kPa
Overall Fouling Allowance
% Excess Area
2
Fouling Resistance (min)
m -C/W
kPa
Wall Shear Stress
Heat Exchanged
237
Transfer Rate, Service

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

m
2
m

1 of 1
1
E-2
Parallel

Series
m2

PERFORMANCE OF ONE UNIT


Shell Side
Circulating Wash Water
43,436
43,436

40,734

40,734

992.7
0.70
18.06

37.7
/
/
/

994.3
0.77
18.06

33.0
/
/
/

996.5
0.91
18.02

25.0
/
/
/

995.0
0.82
18.02

30.0
/
/
/

4.17
0.619

/
/
/

4.17
0.613

/
/
/

4.18
0.606

/
/
/

4.18
0.613

/
/
/

70

70
0.00036

0.00025

kW
MTD (Corrected)
Dirty
CONSTRUCTION OF ONE UNIT
Shell Side
Tube Side
3500
HV
/
800 (Note1) /
95
150
60
/
/

Code Requirements

21
22
23
24
25

420

3,150

C
Clean

W/m2C

Sketch (Pass Arrangement / Nozzle Orientation)

3 / 150#
3 / 150#
2 / 150#
m
Pitch
Layout
Stainless Steel (Note 3)
Material
Shell Cover
Channel Cover
Tubesheet-Float
Impingement Plate
Spacing(c/c)
Inlet

in

Type

Bundle Exit
Tube Side

0
AJ

1/27/11

26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54

TEMA Class

Weight/Shell
Filled with Water
Bundle
NOTES:
1. Cooling water design conditions per utilities design data.
2. Design temperature and pressure conditions to be confirmed in detailed engineering.
3. Shell side can be either CS or SS. However if CS material is used then 3mm SS cladding is required. Tubes and tubesheet to be
SS. Refer to the Materials Section of the BDP for additional detail.
4. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.
5. HV stands for half vacuum.

5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20

Tube Side
Cooling Water
40,734

43,436

Design / Test Pressure


(Note 2,5) kPa (g)
Design/ MDMT Temperature
(Note 2) C
No Passes/ No. Channels per pass
Corrosion Allowance
in
Connection
3 / 300#
In
(Note 4) in
3 / 300#
Size &
Out
(Note 4) in
2 / 300#
Rating
Vent & Drain (Note 4) in
Tube No.
OD
mm
Thk.
mm
Tube Type
Shell
Carbon Steel (Note 3)
ID
inch
Channel or Bonnet
Carbon Steel
Tubesheet-Stationary
Stainless Steel (Note 3)
Floating Head Cover
Baffles-Cross
%Cut (Area)
Baffles-Long
Seal Type
Supports-Tube
U-Bend
Bypass Seal Arrangement
Tube-Tubesheet Joint
Expansion Joint
Type
2
Bundle Entrance
Rho-V -Inlet Nozzle
Gaskets-Shell Side
Floating Head

64
REVISION NO:
65
INITIAL / DATE
66 PROCESS ENGINEER

1
2
3
4

lb

55
56
57
58
59
60
61
62
63
64
65
66

SHELL GLOBAL SOLUTIONS (US)


SHELL & TUBE HEAT EXCHANGER DATA SHEET
Shell Canada Limited
1 Customer
HMU CO2 Capture Project
2 Project
3 Plant Location Scotford
4
5 Service of Unit Absorber #3 Circulating Water Cooler
6 Frame Size (LxWxH)
7 Surface Area / Unit
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63

Fluid Allocation
Fluid Name
Fluid Quality, Total
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
kg/h
Temperature (In/Out)
C
3
Density,
Liquid / Vapor
kg / m
Viscosity,
Liquid / Vapor
cP
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
Specific Heat, Liquid / Vapor
kJ / kgC
Thermal Cond., Liquid / Vapor
W/m-C
Latent Heat
kJ / kg @C
Inlet Pressure
kPa (g)
Velocity
m/s
Pressure Drop, Allowable / Calc
kPa
Overall Fouling Allowance
% Excess Area
2
Fouling Resistance (min)
m -C/W
kPa
Wall Shear Stress
Heat Exchanged
342
Transfer Rate, Service

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

m
2
m

1 of 1
1
E-3
Parallel

Series
m2

PERFORMANCE OF ONE UNIT


Shell Side
Circulating Wash Water
62,641
62,641

58,880

58,880

992.7
0.70
18.06

37.7
/
/
/

994.3
0.77
18.06

33.0
/
/
/

996.5
0.91
18.02

25.0
/
/
/

995.0
0.82
18.02

30.0
/
/
/

4.17
0.619

/
/
/

4.17
0.613

/
/
/

4.18
0.606

/
/
/

4.18
0.613

/
/
/

70

70
0.00036

0.00025

kW
MTD (Corrected)
Dirty
CONSTRUCTION OF ONE UNIT
Shell Side
Tube Sie
3500
HV
800 (Note1) /
/
95
150
60
/
/

Code Requirements

21
22
23
24
25

420

3,196

C
Clean

W/m2C

Sketch (Pass Arrangement / Nozzle Orientation)

4 / 150#
4 / 150#
2 / 150#
m
Pitch
Layout
Stainless Steel (Note 3)
Material
Shell Cover
Channel Cover
Tubesheet-Float
Impingement Plate
Spacing(c/c)
Inlet

in

Type

Bundle Exit
Tube Side

0
AJ

1/27/11

26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54

TEMA Class

Weight/Shell
Filled with Water
Bundle
NOTES:
1. Cooling water design conditions per utilities design data.
2. Design temperature and pressure conditions to be confirmed in detailed engineering.
3. Shell side can be either CS or SS. However if CS material is used then 3mm SS cladding is required. Tubes and tubesheet to be
SS. Refer to the Materials Section of the BDP for additional detail.
4. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.
5. HV stands for half vacuum.

5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20

Tube Side
Cooling Water
58,880

62,641

Design / Test Pressure


(Note 2,5) kPa (g)
Design/ MDMT Temperature
(Note 2) C
No Passes/ No. Channels per pass
Corrosion Allowance
in
Connection
4 / 300#
In
(Note 4) in
4 / 300#
Size &
Out
(Note 4) in
2 / 300#
Rating
Vent & Drain (Note 4) in
Tube No.
OD
mm
Thk.
mm
Tube Type
Shell
Carbon Steel (Note 3)
ID
inch
Channel or Bonnet
Carbon Steel
Tubesheet-Stationary
Stainless Steel (Note 3)
Floating Head Cover
Baffles-Cross
%Cut (Area)
Baffles-Long
Seal Type
Supports-Tube
U-Bend
Bypass Seal Arrangement
Tube-Tubesheet Joint
Expansion Joint
Type
2
Bundle Entrance
Rho-V -Inlet Nozzle
Gaskets-Shell Side
Floating Head

64
REVISION NO:
65
INITIAL / DATE
66 PROCESS ENGINEER

1
2
3
4

lb

55
56
57
58
59
60
61
62
63
64
65
66

SHELL GLOBAL SOLUTIONS (US)


PLATE & FRAME HEAT EXCHANGER DATA SHEET
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54

Customer
Project
Plant Location

Service of Unit Lean / Rich Amine Exchanger


Frame Size (LxWxH)
Surface Area / Unit

m
m2

1 of 2
1
E-4
Parallel

Series
m2

PERFORMANCE OF ONE UNIT


Fluid Allocation
Fluid Name
Fluid Quality, Total
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
kg/h
Temperature (In/Out)
C
Density,
Liquid / Vapor
kg / m3
Viscosity,
Liquid / Vapor
cP
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
Specific Heat, Liquid / Vapor
kJ / kgC
Thermal Cond., Liquid / Vapor
W/m-C
Latent Heat
kJ / kg @C
Inlet Pressure
kPa (g)
Velocity
m/s
Pressure Drop, Allowable / Calc
kPa
Overall Fouling Allowance
% Excess Area
Fouling Resistance (min)
m2-C/W
kPa
Wall Shear Stress
Heat Exchanged
64,000
Transfer Rate, Service

Design / Test Pressure


(Note 4)
kPa (g)
Design/ MDMT Temperature
(Note 4) C
No Passes/ No. Channels per pass
Corrosion Allowance
in
Connection
In
(Note 3) in
Size &
Out
(Note 3) in
Rating
Vent & Drain (Note 3) in
Pass No.
No. of Channels per Fluid
No. of Plates
Plate Model
Chevron Angle
Surface Area Enhancement Factor
Plate Materials
Plate Thickness
Place Spacing
Area per Plate
Port Diameter
Vertical Distance between Port Centers
Horizontal Distance between Port Centers

55
56

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

Shell Canada Limited


HMU CO2 Capture Project
Scotford

Materials

Hot Side
Lean Amine
1,475,491
1,475,491

Cold Side
Rich Amine
1,624,300
15,262
1,609,038

154
1,624,146

1,475,491

979.8
0.77
29.06

119.2
/
/
/

1011.2
1.58
29.06

77.7
/
/
/

1102.5
4.10
29.99

64.0
/
/
/

9.0
0.01
9.18

1063.5
1.86
29.91

3.84
0.412

/
/
/

3.69
0.403

/
/
/

2.97
0.364

/
/
/

3.41
0.104

3.30
0.379

106.2
32.8
/
0.02
/
40.22
/
/
/
/

1.07
0.035

2659

1,216
200

300
0.000009 (Note 6)

0.000009 (Note 6)

kW
MTD (Corrected)
Dirty
Clean
CONSTRUCTION OF ONE UNIT
Cold Side
Hot Side
1530 (Note 1) / HV (Note 5)
3500
/ HV (Note 5)
150
150
150
150
/
/

24 / 150#
24 / 150#
2 / 150#

W/m2C

Sketch (Pass Arrangement / Nozzle Orientation)

18 / 300#
18 / 300#
2 / 300#

Note 2

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54

Note 2

Gaskets

Gasket Type

Connections

55

Frame

Bolts/Nuts

Nozzle Lining

56

57

(Note 2) Tie Bars


Surface Finish
Shroud
58 Maximum No. Plates per Frame
Spare Plates
59 Code
Stamp
Other
60 Weights per FrameDry
kg
Flooded
61 NOTES:
62 1. Lean Solvent side design pressure to be set by pump shut-off head - estimated at 1530 kPa(g). Nozzle class to be confirmed in detailed engineering.
63 2. See Materials Section in the BDP for details. General Materials: SS Plates; EPDM Gaskets
64 3. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.
65 4. Design temperature and pressure conditions to be confirmed in detailed engineering.
66 5. HV stands for half vacuum.
67 6. To be verified during detailed engineering. This fouling resistance is equivalent to 0.00036 m2-C/W for shell and tube exchangers.
0
1
68 REVISION NO:
69 PROCESS ENGINEER

INITIAL / DATE

AJ

1/27/11

AJ

2/7/11

57
58
kg

59
60
61
62
63
64
65
66
67
68
69

SHELL GLOBAL SOLUTIONS (US)


Generic Data Sheet
1 CLIENT:
2 PROJECT:
3 LOCATION:
4 ITEM NO.:
5 SERVICE:

JOB/REQ:

Shell Canada Limited


HMU CO2 Capture Project
Scotford

BY:
PAGE:

AJ
2 of 2

2
3
4

E-4
Lean / Rich Amine Exchanger

Cold Side - Rich Amine

Temp.

Enthalpy

Liquid Flow

Vapor Flow

Vaporization

kJ/kg

kg/h

kg/h

% wt

10

64.0

-8,741.2

1624146

154

0.01

10

11

68.7

-8,727.0

1624106

194

0.01

11

12

73.4

-8,712.9

1624031

269

0.02

12

13

78.1

-8,698.7

1623932

368

0.02

13

14

82.8

-8,684.5

1623782

518

0.03

14

15

87.3

-8,670.3

1623497

803

0.05

15

16

91.8

-8,656.1

1622987

1,313

0.08

16

17

96.0

-8,642.0

1621892

2,408

0.15

17

18

99.9

-8,627.8

1619500

4,800

0.30

18

19

103.3

-8,613.6

1615044

9,256

0.57

19

20

106.2

-8,599.4

1609038

15,262

0.94

20

21

21

22

22

Vapor Properties

23

Temp.

24

25

64.0

26

MW

Density

Sp. Heat

Viscosity

Th. Cond.

23

kg/m3

kJ/kg-C

cP

W/m-C

24

9.18

9.0

3.411

0.014

0.104

25

68.7

10.78

10.3

2.955

0.016

0.101

26

27

73.4

12.81

11.9

2.542

0.017

0.096

27

28

78.1

15.35

14.0

2.178

0.019

0.090

28

29

82.8

18.49

16.5

1.867

0.021

0.081

29

30

87.3

22.31

19.6

1.610

0.023

0.071

30

31

91.8

26.8

23.2

1.403

0.023

0.068

31

32

96.0

31.68

27.0

1.247

0.023

0.055

32

33

99.9

36.09

30.4

1.145

0.022

0.044

33

34

103.3

38.89

32.3

1.093

0.021

0.038

34

35

106.2

40.22

32.8

1.071

0.020

0.035

35

36

36

37

37

Liquid Properties

38

Temp.

39

40

64.0

41

MW

Density

Sp. Heat

Viscosity

Th. Cond.

Surface Tension

38

kg/m3

kJ/kg-C

cP

W/m-C

dyne/cm

39

29.99

1102.5

2.967

4.099

0.364

43.43

40

68.7

29.99

1099.2

2.983

3.731

0.366

42.88

41

42

73.4

29.99

1095.8

3.002

3.410

0.368

42.33

42

43

78.1

29.99

1092.4

3.026

3.130

0.369

41.79

43

44

82.8

29.99

1088.9

3.055

2.884

0.371

41.25

44

45

87.3

29.99

1085.3

3.089

2.667

0.372

40.73

45

46

91.8

29.98

1081.6

3.128

2.475

0.373

40.22

46

47

96.0

29.98

1077.8

3.171

2.303

0.375

39.73

47

48

99.9

29.97

1073.5

3.217

2.146

0.376

39.28

48

49

103.3

29.94

1068.7

3.261

2.000

0.377

38.90

49

50

106.2

29.91

1063.5

3.304

1.863

0.379

38.57

50

51

51

52

52

53

53

54 REVISION
55 Engineer

0
DATE

AJ

54

1
1/27/11

AJ

2/7/11

55

SHELL GLOBAL SOLUTIONS (US)


SHELL & TUBE HEAT EXCHANGER DATA SHEET
Shell Canada Limited
1 Customer
HMU CO2 Capture Project
2 Project
3 Plant Location Scotford
4
5 Service of Unit Stripper OVHD Condenser
6 Frame Size (LxWxH)
7 Surface Area / Unit
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

m
2
m

1 of 1
1
E-5
Parallel

Series
m2

PERFORMANCE OF ONE UNIT

Fluid Allocation
Fluid Name
Fluid Quality, Total
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
kg/h
Temperature (In/Out)
C
3
Density,
Liquid / Vapor
kg / m
Viscosity,
Liquid / Vapor
cP
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
Specific Heat, Liquid / Vapor
kJ / kgC
Thermal Cond., Liquid / Vapor
W/m-C
Latent Heat
kJ / kg @C
Inlet Pressure
kPa (g)
Velocity
m/s
Pressure Drop, Allowable / Calc
kPa
Overall Fouling Allowance
% Excess Area
2
Fouling Resistance (min)
m -C/W
kPa
Wall Shear Stress
Heat Exchanged
25,345
Transfer Rate, Service

Shell Side
Acid Gas
185,017
185,017

151,218
33,798

1,284,240

1,284,240

84.8
/
/
/

1.7
0.016
34.13

993.6
0.70
18.02

36.0
/
/
/

2.4
0.015
42.66

996.5
0.91
18.02

25.0
/
/
/

990.7
0.65
18.02

42.0
/
/
/

/
/
/

1.12
0.022

4.18
0.625

/
/
/

0.88
0.018

4.18
0.606

/
/
/

4.18
0.628

/
/
/

54
70
0.00034
kW
MTD (Corrected)
Dirty
CONSTRUCTION OF ONE UNIT
Shell Side
Tube Side
350
FV
/
800 (Note1) /
200
150
60
/
/

Code Requirements

21
22
23
24
25

420

3.45

0.00025
C
Clean

W/m2C

Sketch (Pass Arrangement / Nozzle Orientation)

in

0
AJ

1/27/11

26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54

TEMA Class

Weight/Shell
Filled with Water
Bundle
NOTES:
1. Cooling water design conditions per utilities design data.
2. Design temperature and pressure conditions to be confirmed in detailed engineering.
3. Refer to the Materials Section of the BDP for additional detail.
4. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.

5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20

Tube Side
Cooling Water
1,284,240

Design / Test Pressure


(Note 2)
kPa (g)
Design/ MDMT Temperature
(Note 2) C
No Passes/ No. Channels per pass
Corrosion Allowance
in
Connection
18 / 150#
42 / 150#
In
(Note 4) in
42 / 150#
18 / 150#
Size &
Out
(Note 4) in
2 / 150#
2 / 150#
Rating
Vent & Drain (Note 4) in
Tube No.
OD
mm
Thk.
mm
m
Pitch
Layout
Tube Type
Stainless Steel (Note 3)
Material
Shell
Shell Cover
Stainless Steel (Note 3)
ID
inch
Channel or Bonnet
Channel Cover
Carbon Steel (Note 3)
Tubesheet-Stationary
Tubesheet-Float
Stainless Steel (Note 3)
Floating Head Cover
Impingement Plate
Baffles-Cross
%Cut (Area)
Spacing(c/c)
Inlet
Baffles-Long
Seal Type
Supports-Tube
U-Bend
Type
Bypass Seal Arrangement
Tube-Tubesheet Joint
Expansion Joint
Type
2
Bundle Entrance
Bundle Exit
Rho-V -Inlet Nozzle
Gaskets-Shell Side
Floating Head
Tube Side

64
REVISION NO:
65
INITIAL / DATE
66 PROCESS ENGINEER

1
2
3
4

lb

55
56
57
58
59
60
61
62
63
64
65
66

SHELL GLOBAL SOLUTIONS (US)


Generic Data Sheet
1 CLIENT:

Shell Canada Limited

JOB/REQ:

2 PROJECT:

HMU CO2 Capture Project

BY:

AJ

3 LOCATION:

Scotford

PAGE:

2 of 2

4 ITEM NO.:

E-5

5 SERVICE:

Stripper OVHD Condenser

4
5

Condensing Curves

Temp.

Enthalpy

Liquid Flow

Vapor Flow

Condensation

kJ/kg

kg/h

kg/h

% wt

10

84.8

809.0

185,017

0.00

10

11

83.9

808.0

185,017

0.00

11

12

82.1

759.7

3,720

181,297

2.01

12

13

80.0

710.4

7,490

177,527

4.05

13

14

77.6

661.1

11,210

173,807

6.06

14

15

74.8

611.8

14,870

170,147

8.04

15

16

71.5

562.5

18,450

166,567

9.97

16

17

67.5

513.2

21,940

163,077

11.86

17

18

62.6

463.8

25,300

159,717

13.67

18

19

56.3

414.5

28,470

156,547

15.39

19

20

47.9

365.2

31,360

153,657

16.95

20

21

36.0

315.9

33,798

151,218

18.27

21

22

22

Vapor Properties

23

Temp.

24

MW

Density

Sp. Heat

Viscosity

Th. Cond.

23

kg/m3

kJ/kg-C

cP

W/m-C

24

25

25

26

84.8

34.13

1.70

1.12

0.016

0.022

26

27

83.9

34.13

1.70

1.12

0.016

0.022

27

28

82.1

34.77

1.74

1.10

0.016

0.022

28

29

80.0

35.47

1.78

1.08

0.016

0.022

29

30

77.6

36.22

1.83

1.06

0.016

0.021

30

31

74.8

37.02

1.88

1.03

0.016

0.021

31

32

71.5

37.88

1.93

1.01

0.016

0.021

32

33

67.5

38.80

2.00

0.99

0.016

0.020

33

34

62.6

39.76

2.07

0.96

0.016

0.020

34

35

56.3

40.75

2.16

0.94

0.016

0.019

35

36

47.9

41.75

2.27

0.91

0.016

0.019

36

37

36.0

42.66

2.40

0.88

0.015

0.018

37

38

38

Liquid Properties

39

Temp.

40

MW

Density

Sp. Heat

Viscosity

Th. Cond.

Surface Tension

39

kg/m3

kJ/kg-C

cP

W/m-C

dyne/cm

40

41

41

42

84.8

n/a

n/a

n/a

n/a

n/a

n/a

42

43

83.9

n/a

n/a

n/a

n/a

n/a

n/a

43

44

82.1

18.02

970.6

4.20

0.34

0.669

62.65

44

45

80.0

18.02

971.9

4.20

0.35

0.667

63.03

45

46

77.6

18.02

973.4

4.19

0.36

0.665

63.46

46

47

74.8

18.02

975.0

4.19

0.38

0.663

63.95

47

48

71.5

18.02

977.0

4.19

0.39

0.661

64.53

48

49

67.5

18.02

979.2

4.19

0.41

0.657

65.22

49

50

62.6

18.02

981.9

4.18

0.45

0.653

66.05

50

51

56.3

18.02

985.1

4.18

0.49

0.647

67.08

51

52

47.9

18.02

989.0

4.18

0.56

0.638

68.41

52

53

36.0

18.02

993.6

4.18

0.70

0.625

70.18

53

54

54

55 REVISION
56 Engineer

55

0
DATE

AJ

1/27/11

56

SHELL GLOBAL SOLUTIONS (US)


SHELL & TUBE HEAT EXCHANGER DATA SHEET
1 Customer
2 Project
3 Plant Location
4
5 Service of Unit
6 Size

Shell Canada Limited


HMU CO2 Capture Project
Scotford

7 Surface / Unit
8

(Effective)

9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Connected In

Stripper Reboiler

Fluid Allocation
Fluid Name
Fluid Quality, Total
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
kg/h
Temperature (In/Out)
C
3
Density,
Liquid / Vapor
kg / m
Viscosity,
Liquid / Vapor
cP
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
Specific Heat, Liquid / Vapor
kJ/ kgC
Thermal Cond., Liquid / Vapor
W/m-C
Latent Heat
kJ / kg
Inlet Pressure
kPa (g)
Velocity
m/s
Pressure Drop, Allowable / Calc
kPa
2
m -C/W
Fouling Resistance (min)
Heat Exchanged
96,080
Transfer Rate, Service

m
2
m

Type

Kettle

1
2
3
4

1 of 2
E-6 A/B
Parallel

Series
m2

Surface / Shell (Gross / Eff)

Shell / Unit
PERFORMANCE OF ONE UNIT
Shell Side
Lean Amine
1,625,978 (Note 4)
150,487
1,475,491
1,625,978

162,025
162,025
116.3
/
/
/

976.7
0.75
29.06

119.1
/
/
/

0.99
0.01
18.45

142.7
/
/
/

142.7
/
/
/

3.89
0.437

/
/
/

3.87
0.413

/
/
/

1.88
0.033

/
/
/

/
/
/

81

INITIAL / DATE

26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42

Nil
0.00036

0.00009

kW
MTD (Corrected)
Dirty
Clean
CONSTRUCTION OF ONE SHELL
Shell Side
Tube Side
350
/
500
/
FV
FV
200
150
250
150
/
/

2
W/m C

Sketch (Bundle / Nozzle Orientation)

Design / Test Pressure


(Note 2) kPa (g)
Orientation: Horizontal
Design Temperature
(Note 2)
C
No Passes per Shell
Corrosion Allowance
in
Connection
24 / 150#
24 / 150#
In
(Note 3,6)
in
8 / 150#
24 / 30 (Two) / 150#
Size &
Out (Liq/Vap) (Note 3,6) in
Rating
Vent & Drain (Note 3,6)
in
Tube No.
OD
mm
Thk.
mm
m
Pitch
Layout
Tube Type
Stainless Steel (Note 1)
Material
Shell
Shell Cover
Carbon Steel (Note 1)
ID
inch
Channel or Bonnet
Channel Cover
Carbon Steel
Tubesheet-Stationary
Tubesheet-Float
Stainless Steel (Note 1)
Floating Head Cover
Impingement Plate
Baffles-Cross
%Cut (Area)
Spacing(c/c)
Inlet
Baffles-Long
Seal Type
Supports-Tube
U-Bend
Type
Bypass Seal Arrangement
Tube-Tubesheet Joint
Expansion Joint
Type
2
Bundle Entrance
Bundle Exit
Rho-V -Inlet Nozzle
Gaskets-Shell Side
Floating Head
Tube Side
Code Requirements
TEMA Class
ASME Section VIII, Division 1
Filled with Water
Weight/Shell
Bundle
NOTES:
1. Shell side can be either CS or SS. However if CS material is used then 3mm SS cladding is required. Tubes and tubesheet to be
SS. Refer to the Materials Section of the BDP for additional detail.
2. Design temperature and pressure conditions to be confirmed in detailed engineering.
3. Nozzle details to be determined during detailed design in coordination with the exchanger vendor.
4. Duty and flow given are for both exchangers combined. Each exchanger will be deisgned for 50% of the total duty.
5. Add extra 10% heat transfer area to the exchanger for design margin.
6. Nozzle sizes and the number shown are for one exchanger. Two exchangers are required for this service.
REVISION NO:
0
1

64 PROCESS ENGINEER

21
22
23
24
25

300

(Note 4)

AJ

12/16/10

AJ

1/27/11

7
8
9
10
11
12
13
14
15
16
17
18
19
20

Tube Side
LP Steam
162,025

979.8
0.70
27.56

5
6

in

lb

43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64

SHELL GLOBAL SOLUTIONS (US)


Generic Data Sheet
1 CLIENT:

Shell Canada Limited

JOB/REQ:

2 PROJECT:

HMU CO2 Capture Project

BY:

AJ

3 LOCATION:

Scotford

PAGE:

2 of 2

4 ITEM NO.:

E-6 A/B

5 SERVICE:

Stripper Reboiler

4
5

Shell Side - Lean amine at a constant pressure of 81 kPa (g)

Temp.

Enthalpy

Liquid Flow

Vapor Flow

Vaporization

kJ/kg

kg/h

kg/h

% wt

10

116.3

-9,035.9

1,625,978

0.00

10

11

117.2

-9,014.4

1,612,478

13,500

0.83

11

12

117.7

-8,993.0

1,597,978

28,000

1.72

12

13

118.1

-8,971.5

1,583,078

42,900

2.64

13

14

118.3

-8,949.9

1,567,978

58,000

3.57

14

15

118.5

-8,928.5

1,552,678

73,300

4.51

15

16

118.7

-8,907.2

1,537,278

88,700

5.46

16

17

118.8

-8,885.7

1,521,878

104,100

6.40

17

18

118.9

-8,864.0

1,506,478

119,500

7.35

18

19

119.0

-8,842.6

1,490,978

135,000

8.30

19

20

119.1

-8,821.1

1,475,491

150,487

9.26

20

21

21

22

22

Vapor Properties

23

Temp.

24

MW

Density

Sp. Heat

Viscosity

Th. Cond.

23

kg/m3

kJ/kg-C

cP

W/m-C

24

25

25

26

116.3

n/a

n/a

n/a

n/a

n/a

26

27

117.2

19.64

1.06

1.78

0.010

0.033

27

28

117.7

19.25

1.04

1.81

0.010

0.033

28

29

118.1

19.01

1.03

1.83

0.010

0.033

29

30

118.3

18.85

1.02

1.85

0.010

0.033

30

31

118.5

18.74

1.01

1.86

0.010

0.033

31

32

118.7

18.65

1.01

1.87

0.010

0.033

32

33

118.8

18.58

1.00

1.87

0.010

0.033

33

34

118.9

18.53

1.00

1.88

0.010

0.033

34

35

119.0

18.48

1.00

1.88

0.010

0.033

35

36

119.1

18.45

0.99

1.88

0.010

0.033

36

37

37

38

38

Liquid Properties

39

Temp.

40

MW

Density

Sp. Heat

Viscosity

Th. Cond.

Surface Tension

39

kg/m3

kJ/kg-C

cP

W/m-C

dyne/cm

40

41

41

42

116.3

27.56

979.8

3.89

0.70

0.437

38.37

42

43

117.2

27.66

978.3

3.89

0.69

0.435

38.21

43

44

117.7

27.77

977.4

3.90

0.69

0.434

38.09

44

45

118.1

27.90

977.0

3.90

0.69

0.431

37.98

45

46

118.3

28.04

976.7

3.89

0.70

0.429

37.88

46

47

118.5

28.19

976.6

3.89

0.70

0.427

37.79

47

48

118.7

28.35

976.5

3.89

0.71

0.424

37.70

48

49

118.8

28.51

976.5

3.88

0.72

0.422

37.60

49

50

118.9

28.68

976.6

3.88

0.73

0.419

37.51

50

51

119.0

28.85

976.6

3.87

0.74

0.416

37.42

51

52

119.1

29.06

976.7

3.87

0.75

0.413

37.33

52

53
54
55

53

REVISION
Engineer

0
DATE

AJ

54

1
12/16/10

AJ

1/27/11

55

SHELL GLOBAL SOLUTIONS (US)


SHELL & TUBE HEAT EXCHANGER DATA SHEET
Shell Canada Limited
1 Customer
HMU CO2 Capture Project
2 Project
3 Plant Location Scotford
4
5 Service of Unit Lean Amine Cooler
6 Frame Size (LxWxH)
7 Surface Area / Unit
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64

Fluid Allocation
Fluid Name
Fluid Quality, Total
(Note 6)
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
kg/h
Temperature (In/Out)
C
Density,
Liquid / Vapor
kg / m3
Viscosity,
Liquid / Vapor
cP
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
Specific Heat, Liquid / Vapor
kJ / kgC
Thermal Cond., Liquid / Vapor
W/m-C
Latent Heat
kJ / kg @C
Inlet Pressure
kPa (g)
Velocity
m/s
Pressure Drop, Allowable / Calc
kPa
Overall Fouling Allowance
% Excess Area
Fouling Resistance (min)
m2-C/W
kPa
Wall Shear Stress
Heat Exchanged
41,500
Transfer Rate, Service

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

m
2
m

1
2
3
4

1 of 1
1
E-7 A/B
Parallel

Series
m2

PERFORMANCE OF ONE UNIT


Shell Side
Lean Amine
1,475,491
1,475,491

9
10
11
12
13
14
15
16
17
18
19
20

Tube Side
Cooling Water
2,102,836
2,102,836

1,475,491

2,102,836

1011.2
1.58
29.06

77.7
/
/
/

1029.1
3.02
29.06

50.0
/
/
/

996.5
0.91
18.02

25.0
/
/
/

990.7
0.65
18.02

42.0
/
/
/

3.69
0.403

/
/
/

3.62
0.391

/
/
/

4.18
0.606

/
/
/

4.18
0.628

/
/
/

21
22
23
24
25

420

974
70

70
0.00036

kW
MTD (Corrected)
Dirty
CONSTRUCTION OF ONE UNIT
Shell Side
Tube Sie
1,530 (Note 4) / HV (Note 5) 800 (Note1) /
150
150
60
/
/

0.00025
C

(Note 6)

Clean

Code Requirements

in

26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54

TEMA Class

Weight/Shell
Filled with Water
Bundle
NOTES:
1. Cooling water design conditions per utilities design data.
2. Design temperature and pressure conditions to be confirmed in detailed engineering.
3. For additional materials considerations, see the Materials Section of the BDP.
4. Design pressure to be set by pump shut-off head - estimated at 1530 kPa(g)
5. HV stands for half vacuum.
6. Duty and flow given are for both exchangers combined. Each exchanger will be deisgned for 50% of the total duty.
7. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.

65 8. Nozzle sizes shown are for one exchanger. Two exchangers are required for this service.
0
REVISION NO:
66
INITIAL / DATE
AJ
1/27/11
67 PROCESS ENGINEER

W/m2C

Sketch (Pass Arrangement / Nozzle Orientation)

Design / Test Pressure


(Note 2)
kPa (g)
Design/ MDMT Temperature
(Note 2)
C
No Passes/ No. Channels per pass
Corrosion Allowance
in
Connection
16 / 150#
18 / 150#
In
(Note 7,8) in
18 / 150#
16 / 150#
Size &
Out
(Note 7,8) in
2 / 150#
2 / 150#
Rating
Vent & Drain (Note 7,8) in
Tube No.
OD
mm
Thk.
mm
m
Pitch
Layout
Tube Type
Stainless Steel (Note 3)
Material
Shell
Shell Cover
Stainless Steel (Note 3)
ID
inch
Channel or Bonnet
Channel Cover
Carbon Steel (Note 3)
Tubesheet-Stationary
Tubesheet-Float
Stainless Steel (Note 3)
Floating Head Cover
Impingement Plate
Baffles-Cross
%Cut (Area)
Spacing(c/c)
Inlet
Baffles-Long
Seal Type
Supports-Tube
U-Bend
Type
Bypass Seal Arrangement
Tube-Tubesheet Joint
Expansion Joint
Type
2
Bundle Entrance
Bundle Exit
Rho-V -Inlet Nozzle
Gaskets-Shell Side
Floating Head
Tube Side

5
6
7
8

lb

55
56
57
58
59
60
61
62
63
64
65
66
67

SHELL GLOBAL SOLUTIONS (US)


PLATE & FRAME HEAT EXCHANGER DATA SHEET
1
2
3
4
5
6
7

Customer
Project
Plant Location

Job No:
Requisition No:
Page No:
No. of Units Req'd:
Item No:
Frames per Unit
Surface Area / Frame

Shell Canada Limited


HMU CO2 Capture Project
Scotford

Lean Amine Trim Cooler


Service of Unit
Frame Size (LxWxH)
Surface Area / Unit

m
m2

8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32

33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72

1 of 1
1
E-8 A/B
Parallel

Series

PERFORMANCE OF ONE UNIT


Fluid Allocation
Fluid Name
(Note 8)
kg/h
Fluid Quality, Total
kg/h
Vapor (In/Out)
kg/h
Liquid
kg/h
Steam
kg/h
Water
kg/h
Non-Condensable
C
Temperature (In/Out)
Density,
Liquid / Vapor
kg / m3
cP
Viscosity,
Liquid / Vapor
Molecular Weight, Liquid / Vapor
Molecular Weight, Non-Condensable
kJ / kgC
Specific Heat, Liquid / Vapor
W/m-C
Thermal Cond., Liquid / Vapor
kJ / kg @C
Latent Heat
kPa (g)
Inlet Pressure
m/s
Velocity
kPa
Pressure Drop, Allowable / Calc
% Excess Area
Overall Fouling Allowance
Fouling Resistance (min)
m2-C/W
kPa
Wall Shear Stress
29,520
Heat Exchanged
Transfer Rate, Service

1029.1
3.02
29.06
3.62
0.391

1,495,800

1,475,491

50.0
/
/
/
/
/
/

1040.3
5.46
29.06
3.57
0.378

30.0
/
/
/
/
/
/

996.5
0.91
18.02
4.18
0.606

25.0
/
/
/
/
/
/

4.18
0.628

42.0
/
/
/
/
/
/

420 (Note 1)

140

140
0.000009 (Note 2)

kW
Dirty

1,495,800

990.7
0.65
18.02

863

(Note 8)

9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32

Cold Side
Cooling Water
1,495,800

Hot Side
Lean Amine
1,475,491
1,475,491

0.000009 (Note 2)

MTD (Corrected)

Hot Side
1530 (Note 5) / HV (Note 7)
150
/
150

C
Clean

CONSTRUCTION OF ONE UNIT

1
2
3
4
5
6
7

W/m2C

Sketch (Pass Arrangement / Nozzle Orientation)

Cold Side
800 (Note1) /
60
/

(Note 6)
kPa (g)
Design / Test Pressure
(Note 6)
C
Design/ MDMT Temperature
No Passes/ No. Channels per pass
in
Corrosion Allowance
16 / 150#
14 / 150#
In
(Note 4,9) in
Connection
16 / 150#
14 / 150#
Size &
Out
(Note 4,9) in
2 / 150#
2 / 150#
Rating
Vent & Drain (Note 4,9) in
Pass No.
No. of Channels per Fluid
No. of Plates
Plate Model
Chevron Angle
Surface Area Enhancement Factor
Note 3
Note 3
Plate Materials
Plate Thickness
Place Spacing
Area per Plate
Port Diameter
Vertical Distance between Port Centers
Horizontal Distance between Port Centers
Gaskets
Gasket Type
Connections
Frame
Bolts/Nuts
Nozzle Lining
Materials
(Note 3)
Tie Bars
Surface Finish
Shroud
Spare Plates
Maximum No. Plates per Frame
Stamp
Other
Code
Dry
kg
Weights per FrameFlooded
NOTES:
1. Cooling water design conditions per utilities design data.
2. To be verified during detailed engineering. This fouling resistance is equivalent to 0.00036 m2-C/W for shell and tube exchangers.
3. See Materials Section in the BDP for details. General Materials: Titanium R50400 Plates; EPDM Gaskets
4. Inlet and outlet nozzle details to be confirmed during detailed design in coordination with exchanger vendor.
5. Design pressure to be set by pump shut-off head - estimated at 1530 kPa(g).
6. Design temperature and pressure conditions to be confirmed in detailed engineering.
7. HV stands for half vacuum.
8. Duty and flow given are for both exchangers combined. Each exchanger will be deisgned for 50% of the total duty.
9. Nozzle sizes shown are for one exchanger. Two exchangers are required for this service.
REVISION NO:
0
PROCESS ENGINEER
INITIAL / DATE
AJ
1/27/11

kg

33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
68
69
70
71
72

SR.11.10343

73

APPENDIX D3- VESSELS

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT. - CLASS 1

AJ

ORIG. BY

DOCUMENT No.

REVIEWED

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1 of 12

OPERATING / MECHANICAL DATA


Description

GAS SCRUBBER

Contents

Hydrogen / Water

Case

Units

DESIGN
32

39

Working Temperature, max. / normal / min.


- normal / min. vac. conditions
Design temperature, upper / lower
Design pressure, internal / external

3014

Working Pressure - max. / normal / min.

kPa
N/A

N/A

kPa
C

95
(Note 2)

3500

HV @ 150 C

kPa (g)

Test pressure, hydrostatic / pneumatic


Feed Gas

Circ Water In

Makeup Water

Treated Gas

Circ Water Out

kPa
32259

Quantity

kg / h

Molecular Weight

5.3

kg / kg mol

Density at working temperature

6.01

kg / m

38873

kg / h

Quantity

Molecular Weight

18.1

kg / kg mol

Density at working temperature

994.3

kg / m

Quantity

4509

kg / h

Molecular Weight

18.0

kg / kg mol

Density at working temperature

993.7

kg / m

Quantity

32206

kg / h

Molecular Weight

5.25

kg / kg mol

Density at working temperature

6.03

kg / m

43436

kg / h

Quantity

Molecular Weight

18.1

kg / kg mol

Density at working temperature

992.7

kg / m

Vessel Orientation

Vertical

Overall Tangent - Tangent Length

10.50

Description - Section 1 / Section 2

Lower Section

Upper Section

Tray Numbers -

Section 1 / Section 2

1-6

7-9

Inside Diameter of Shell -

Section 1 / Section 2

1.80

1.80

Total Packed Height -

Section 1 / Section 2

NA

0.42

Number of Packed Beds -

Section 1 / Section 2

NA

Size and Type of Packing -

Section 1 / Section 2

NA

Mellapak 250Y

Number Trays Required -

Section 1 / Section 2

Type of Trays -

Section 1 / Section 2

Valve

Bubble Cap

Tray Spacing -

Section 1 / Section 2

450

600

Number of Tray Downcomers

mm
m

Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm

Type of heads

Semielliptical

Minimum skirt height


Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:
1) Detailed drawings to be reviewed by Shell Global Solutions (US) Inc
2) HV stands for half vacuum.

Relief valve(s)

Earthquake factor

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
2 of 12

NOZZLE DATA
Service

NPS / Flange Class

Internal(s)

NPS 14" / 300

Half Open Pipe Internal

Mark

Number

N1

Vapor Feed

N2

Circ Water Inlet

NPS 4" / 300

Branched Pipe Distributor

N3

Makeup Water Inlet

NPS 3" / 300

Elbow into False Downcomer

N4

Vapor Outlet

NPS 12" / 300

N5

Circ Water Outlet

NPS 6" / 300

N6

Drain

NPS 2" / 300

N7

Steam Out

NPS 3" / 300

Final Sizing by EPC Contractor

N8

Vent

NPS 6" / 300

Final Sizing by EPC Contractor

N9

Relief

TBD / 300

Final Sizing by EPC Contractor

Remarks

Vortex Breaker
Final Sizing by EPC Contractor

INSTRUMENT CONNECTIONS
K1 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

K2 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

K3 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P1

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

MANHOLES
A1

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A2

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A3

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A4

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

Material Note:

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

Part

Material
Carbon Steel

Shell

SS (Note 1)

Cladding/lining of shell

Carbon Steel

Heads

SS (Note 1)

Cladding/lining of heads

Part

Material
316 SS

Trays
Distributors

316 SS

Downcomers

316 SS

Baffles

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

3 of 12

Nuts, internal
Note 2

Nozzles (line pipe/plate)


Liner of nozzles and manholes

Gaskets, external
Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
Internal parts
FABRICATION AND INSPECTION REQUIREMENTS
Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS internal cladding required on entire vessel
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer is responsible for ensuring
that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to the manufacturer are for information and tendering
purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to all the applicable codes and national statutory regulations, and he shall
obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1) Drawings to be reviewed by Shell Global Solutions (US) Inc


2) Dimensions are in meters

DOCUMENT No.
4 of 12

TRAY LOADING SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

ITEM No:

V-1

Absorber #1 Water Wash Vessel

SERVICE:
REVISION
DATE

0
27-Jan-11

DOC. CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

Section (Name/Description)
LOWER
Design Case
DESIGN
Tray number included (Note 1)
1-6
Loading on Actual Tray No.
1
Number of Trays Required
6
NORMAL VAPOR TO:
Flow Rate, kg/hr
32259
Density, kg/m3
6.01
Flow Rate, m3/s
1.49
Molecular Weight
5.3
Viscosity, Pa s
1.0E-05
Pressure, kPa
3014
Temperature, C
39
NORMAL LIQUID FROM:
Flow Rate, kg/hr
43436
3
Density, kg/m
992.7
3
0.012
Flow Rate, m /s
Molecular Weight
18.1
Surface Tension, N/m
0.070
Viscosity, Pa s
7.0E-04
Temperature, C
38
PERFORMANCE REQUIREMENTS:
Max. delta P per tray, kPa
Max. % Jet Flood
80
Max. DC inlet velocity, m/s
Max.
Backup, mm clear liquid
225
Max DC Backup
Derating Factor
1.00
Purpose for Derating (Foaming, System, Safety)
NA
MECHANICAL REQUIREMENTS:
Tower Diameter, m
1.80
Tray Arrangement
1 pass
Tray Spacing, mm
450
valve
Type of Tray
Hole/Bubble Cap Diameter, mm
SS / 2 mm
Deck Material/Thickness
316 SS
Valve/Bubble Cap Material
Weir Height
75 mm
Maximum allowable DP per tray
1450 Pa
Support Material/Thickness
Total Corrosion Allowance
24
Nominal Vessel Manhole Size, NPS
MISCELLANEOUS:
NA
Solids Present
Design Load
not req'd
Anti-Jump Baffles
Note 3
Special Features:
NOTES:
1) Tray Number 1 = Bottom Tray.

DOCUMENT No.

UPPER
DESIGN
7-9
7
3
32253
6.07
1.47
5.3
1.2E-05
3007
35
4558
993.3
0.0013
18.0
0.071
7.4E-04
35

80
300
1.00
NA
1.80
1 pass
600
bubble cap
SS / 2 mm
316 SS
100 mm
1450 Pa

24
NA
not req'd
Notes 4,5

2) Tray Design is based upon 100 % of the stated vapor and 100 % of the stated liquid flow rates.
3) Valves to be Sulzer Type "RC-1" or equivalent.
4) Picket fence weirs required
5) Inlet weirs required
6) Drawings to be reviewed by Shell Global Solutions (US) inc

5 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

HALF PIPE DISTRIBUTOR AT NOZZLE N1

1) END OF DISTRIBUTOR TO BE ATTACHED TO VESSEL SHELL


2) DRAWINGS TO BE REVIEWED BY SHELL GLOBAL SOLUTIONS (US) INC

DOCUMENT No.
6 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DISTRIBUTOR AT NOZZLE N2

1) ENDS OF BRANCHES OF TEE TO BE CLOSED


2) DISTRIBUTOR BRANCHES TO BE ATTACHED TO VESSEL SHELL
3) DRAWINGS TO BE REVIEWED BY SHELL GLOBAL SOLUTIONS (US) INC

DOCUMENT No.
7 of 12

PACKING / MESH PAD SPECIFICATIONS

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

ITEM No:

V-1

Absorber #1 Water Wash Vessel

SERVICE:
REVISION
DATE

0
27-Jan-11

DOC. CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

DOCUMENT No.

INTERNAL

Packing

Mesh Pad

Case

DESIGN

DESIGN

32206

32206

Vapor Density, kg/m3

6.03

6.03

Design Liquid Load, kg/hr

902

45

Liquid Density, kg/m3

993.7

993.7

Liquid Viscosity, Pa s

0.0007

0.0007

Surface Tension, N/m

0.0708

0.0708

Vapor Flow Rate to Mesh Pad, kg/hr

PACKING
Tower Inside Diameter, m
Packing
Packed Bed Height, m
Sheet Thickness, mm
# of packing layers

1.80
Mellapak 250Y
0.42
0.20
4 half layers

Support Grid Required?

YES

Hold Down Grid Required?

YES

MESH PAD
Tower Inside Diameter, m

1.80

Diameter of mesh pad, m

1.40

Mesh Pad thickness, m

0.15

Minimum Surface Area, 1/m

350

Minimum free volume of mat

97%

Wire thickness, mm
Hold down grid required?
Mesh
M h Material
M t i l

0.23 - 0.28
YES
316 SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be places between two grids with free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

8 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.028

DOCUMENT No.
9 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.030

DOCUMENT No.
10 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.029

DOCUMENT No.
11 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #1 Water Wash Vessel

ITEM No:

V-1

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
12 of 12

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:

PROJECT No:

REVISION

27-Jan-11

DATE

DOCUMENT CAT. - CLASS 1

AJ

ORIG. BY

DOCUMENT No.

REVIEWED

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1 of 12

OPERATING / MECHANICAL DATA


Description

GAS SCRUBBER

Contents

Hydrogen / Water

Case

Units

DESIGN
32

39

Working Temperature, max. / normal / min.


Working Pressure - max. / normal / min.
- normal / min. vac. conditions

kPa
N/A

N/A

kPa

95

Design temperature, upper / lower


Design pressure, internal / external

3014

(Note 2)

3500

HV @ 150 C

kPa (g)

Test pressure, hydrostatic / pneumatic


Feed Gas

Circ Water In

Makeup Water

Treated Gas

Circ Water Out

kPa
32259

Quantity

kg / h

Molecular Weight

5.3

kg / kg mol

Density at working temperature

6.01

kg / m

38873

kg / h

Quantity

Molecular Weight

18.1

kg / kg mol

Density at working temperature

994.3

kg / m

Quantity

4509

kg / h

Molecular Weight

18.0

kg / kg mol

Density at working temperature

993.7

kg / m

Quantity

32206

kg / h

Molecular Weight

5.25

kg / kg mol

Density at working temperature

6.03

kg / m

43436

kg / h

Quantity

Molecular Weight

18.1

kg / kg mol

Density at working temperature

992.7

kg / m

Vessel Orientation

Vertical
10.50

Overall Tangent - Tangent Length


Description - Section 1 / Section 2

Lower Section

Upper Section
7-9

Tray Numbers -

Section 1 / Section 2

1-6

Inside Diameter of Shell -

Section 1 / Section 2

1.80

1.80

Total Packed Height -

Section 1 / Section 2

NA

0.42

Number of Packed Beds -

Section 1 / Section 2

NA

Size and Type of Packing -

Section 1 / Section 2

NA

Mellapak 250Y

Number Trays Required -

Section 1 / Section 2

Type of Trays -

Section 1 / Section 2

Valve

Bubble Cap

Tray Spacing -

Section 1 / Section 2

450

600

Number of Tray Downcomers

mm
m

Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm
Semielliptical

Type of heads
Minimum skirt height
Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:
1) Detailed drawings to be reviewed by Shell Global Solutions (US) Inc
2) HV stands for half vacuum.

Relief valve(s)

Earthquake factor

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
2 of 12

NOZZLE DATA
Service

NPS / Flange Class

Internal(s)

NPS 14" / 300

Half Open Pipe Internal

Mark

Number

N1

Vapor Feed

N2

Circ Water Inlet

NPS 4" / 300

Branched Pipe Distributor

N3

Makeup Water Inlet

NPS 3" / 300

Elbow into False Downcomer

N4

Vapor Outlet

NPS 12" / 300

N5

Circ Water Outlet

NPS 6" / 300

N6

Drain

NPS 2" / 300

Final Sizing by EPC Contractor

N7

Steam Out

NPS 3" / 300

Final Sizing by EPC Contractor

N8

Vent

NPS 6" / 300

Final Sizing by EPC Contractor

N9

Relief

TBD / 300

Final Sizing by EPC Contractor

Remarks

Vortex Breaker

INSTRUMENT CONNECTIONS
K1 A/B

Level Transmitter

NPS 2" / 300

K2 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor


Final Sizing by EPC Contractor

K3 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P1

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

MANHOLES
A1

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A2

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A3

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A4

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

Material Note:

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

Part

Material
Carbon Steel

Shell

SS (Note 1)

Cladding/lining of shell

Carbon Steel

Heads

SS (Note 1)

Cladding/lining of heads

Part

Material

Trays

316 SS

Distributors

316 SS

Downcomers

316 SS

Baffles

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

3 of 12

Nuts, internal
Note 2

Nozzles (line pipe/plate)


Liner of nozzles and manholes

Gaskets, external
Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
Internal parts
FABRICATION AND INSPECTION REQUIREMENTS
Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS internal cladding required on entire vessel
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer is responsible for ensuring
that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to the manufacturer are for information and tendering
purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to all the applicable codes and national statutory regulations, and he shall
obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1) Drawings to be reviewed by Shell Global Solutions (US) Inc


2) Dimensions are in meters

DOCUMENT No.
4 of 12

TRAY LOADING SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

ITEM No:

V-2

Absorber #2 Water Wash Vessel

SERVICE:
REVISION
DATE

0
27-Jan-11

DOC. CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

Section (Name/Description)
LOWER
Design Case
DESIGN
Tray number included (Note 1)
1-6
Loading on Actual Tray No.
1
Number of Trays Required
6
NORMAL VAPOR TO:
Flow Rate, kg/hr
32259
3
Density, kg/m
6.01
Flow Rate, m3/s
1.49
Molecular Weight
5.3
Viscosity, Pa s
1.0E-05
Pressure, kPa
3014
Temperature, C
39
NORMAL LIQUID FROM:
Flow Rate, kg/hr
43436
3
Density, kg/m
992.7
Flow Rate, m3/s
0.012
Molecular Weight
18.1
Surface Tension, N/m
0.070
Viscosity, Pa s
7.0E-04
Temperature, C
38
PERFORMANCE REQUIREMENTS:
Max. delta P per tray, kPa
Max. % Jet Flood
80
Max. DC inlet velocity, m/s
Max.
Backup, mm clear liquid
225
Max DC Backup
Derating Factor
1.00
Purpose for Derating (Foaming, System, Safety)
NA
MECHANICAL REQUIREMENTS:
1.80
Tower Diameter, m
1 pass
Tray Arrangement
450
Tray Spacing, mm
Type of Tray
valve
Hole/Bubble Cap Diameter, mm
SS / 2 mm
Deck Material/Thickness
316 SS
Valve/Bubble Cap Material
Weir Height
75 mm
Maximum allowable DP per tray
1450 Pa
Support Material/Thickness
Total Corrosion Allowance
Nominal Vessel Manhole Size, NPS
24
MISCELLANEOUS:
Solids Present
NA
Design Load
Anti-Jump Baffles
not req'd
Special Features:
Note 3
1) Tray Number 1 = Bottom Tray.
NOTES:

DOCUMENT No.

UPPER
DESIGN
7-9
7
3
32253
6.07
1.47
5.3
1.2E-05
3007
35
4558
993.3
0.0013
18.0
0.071
7.4E-04
35

80
300
1.00
NA
1.80
1 pass
600
bubble cap
SS / 2 mm
316 SS
100 mm
1450 Pa

24
NA
not req'd
Notes 4,5

2) Tray Design is based upon 100 % of the stated vapor and 100 % of the stated liquid flow rates.
3) Valves to be Sulzer Type "RC-1" or equivalent.
4) Picket fence weirs required
5) Inlet weirs required
6) Drawings to be reviewed by Shell Global Solutions (US) inc

5 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

HALF PIPE DISTRIBUTOR AT NOZZLE N1

1) END OF DISTRIBUTOR TO BE ATTACHED TO VESSEL SHELL


2) DRAWINGS TO BE REVIEWED BY SHELL GLOBAL SOLUTIONS (US) INC

DOCUMENT No.
6 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DISTRIBUTOR AT NOZZLE N2

1) ENDS OF BRANCHES OF TEE TO BE CLOSED


2) DISTRIBUTOR BRANCHES TO BE ATTACHED TO VESSEL SHELL
3) DRAWINGS TO BE REVIEWED BY SHELL GLOBAL SOLUTIONS (US) INC

DOCUMENT No.
7 of 12

PACKING / MESH PAD SPECIFICATIONS

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

ITEM No:

V-2

Absorber #2 Water Wash Vessel

SERVICE:
REVISION
DATE

0
27-Jan-11

DOC. CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

DOCUMENT No.

INTERNAL

Packing

Mesh Pad

Case

DESIGN

DESIGN

32206

32206

Vapor Density, kg/m3

6.03

6.03

Design Liquid Load, kg/hr

902

45

Liquid Density, kg/m3

993.7

993.7

Liquid Viscosity, Pa s

0.0007

0.0007

Surface Tension, N/m

0.0708

0.0708

Vapor Flow Rate to Mesh Pad, kg/hr

PACKING
Tower Inside Diameter, m
Packing
Packed Bed Height, m
Sheet Thickness, mm
# of packing layers

1.80
Mellapak 250Y
0.42
0.20
4 half layers

Support Grid Required?

YES

Hold Down Grid Required?

YES

MESH PAD
Tower Inside Diameter, m

1.80

Diameter of mesh pad, m

1.40

Mesh Pad thickness, m

0.15

Minimum Surface Area, 1/m

350

Minimum free volume of mat

97%

Wire thickness, mm
Hold down grid required?
Mesh
M h Material
M t i l

0.23 - 0.28
YES
316 SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be places between two grids with free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

8 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.028

DOCUMENT No.
9 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.030

DOCUMENT No.
10 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.029

DOCUMENT No.
11 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #2 Water Wash Vessel

ITEM No:

V-2

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
12 of 12

Shell Global Solutions (US) Inc.

COLUMN PROCESS SPECIFICATION

CUSTOMER NAME:

Shell Canada

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:

PROJECT No:

REVISION

27-Jan-11

DATE

DOCUMENT CAT. - CLASS 1

AJ

ORIG. BY

DOCUMENT No.

REVIEWED

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1 of 12

OPERATING / MECHANICAL DATA


Description

GAS SCRUBBER

Contents

Hydrogen / Water

Case

Units

DESIGN
32

39

Working Temperature, max. / normal / min.

kPa
N/A

N/A

- normal / min. vac. conditions


Design temperature, upper / lower
Design pressure, internal / external

3054

Working Pressure - max. / normal / min.

kPa
C

95
(Note 2)

3500

HV @ 150 C

kPa (g)

Test pressure, hydrostatic / pneumatic


Feed Gas

Circ Water In

Makeup Water

Treated Gas

Circ Water Out

kPa
50531

Quantity

kg / hr

Molecular Weight

5.69

kg / kg mol

Density at working temperature

6.60

kg / m

56041

kg / hr

Quantity

Molecular Weight

18.1

kg / kg mol

Density at working temperature

994.3

kg / m

Quantity

6527

kg / hr

Molecular Weight

18.0

kg / kg mol

Density at working temperature

993.7

kg / m

Quantity

50458

kg / hr

Molecular Weight

5.68

kg / kg mol

Density at working temperature

6.62

kg / m

62641

kg / hr

Quantity

Molecular Weight

18.1

kg / kg mol

Density at working temperature

992.7

kg / m

Vessel Orientation

Vertical

Overall Tangent - Tangent Length

10.70

Description - Section 1 / Section 2

Lower Section

Upper Section

Tray Numbers -

Section 1 / Section 2

1-6

7-9

Inside Diameter of Shell -

Section 1 / Section 2

2.10

2.10

Total Packed Height -

Section 1 / Section 2

NA

0.42

Number of Packed Beds -

Section 1 / Section 2

NA

Size and Type of Packing -

Section 1 / Section 2

NA

Mellapak 250Y

Number Trays Required -

Section 1 / Section 2

Type of Trays -

Section 1 / Section 2

Valve

Bubble Cap

Tray Spacing -

Section 1 / Section 2

450

600

Number of Tray Downcomers

mm
m

Wall thickness - shell / head

mm

Corrosion allowance

mm

Insulation thickness

mm

Type of heads

Semielliptical

Minimum skirt height


Total Volume (T/T)

- Type / size

Normal liquid volume

- Set pressure

Volume range required for level control

- Number required

Wind pressure

kPa

Notes:
1) Detailed drawings to be reviewed by Shell Global Solutions (US) Inc
2) HV stands for half vacuum.

Relief valve(s)

Earthquake factor

kPa

COLUMN PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
2 of 12

NOZZLE DATA

Service

NPS / Flange Class

Internal(s)

NPS 18" / 300

Half Open Pipe Internal

Mark

Number

N1

Vapor Feed

N2

Circ Water Inlet

NPS 6" / 300

Branched Pipe Distributor

N3

Makeup Water Inlet

NPS 3" / 300

Elbow into False Downcomer

N4

Vapor Outlet

NPS 16" / 300

N5

Circ Water Outlet

NPS 8" / 300

N6

Drain

NPS 2" / 300

Final Sizing by EPC Contractor

N7

Steam Out

NPS 3" / 300

Final Sizing by EPC Contractor

N8

Vent

NPS 6" / 300

Final Sizing by EPC Contractor

N9

Relief

TBD / 300

Final Sizing by EPC Contractor

Remarks

Vortex Breaker

INSTRUMENT CONNECTIONS
K1 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

K2 A/B

Level Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor


Final Sizing by EPC Contractor

K3 A/B

Level Transmitter

NPS 2" / 300

P1

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

P2

Pressure Transmitter

NPS 2" / 300

Final Sizing by EPC Contractor

MANHOLES
A1

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A2

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A3

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

A4

Manhole

NPS 24" / 300

Include Blind (Manway Cover)

Material Note:

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMERS NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
0

REVISION

27-Jan-11

DATE

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

Part

Material
Carbon Steel

Shell

SS (Note 1)

Cladding/lining of shell

Carbon Steel

Heads

SS (Note 1)

Cladding/lining of heads

Part

Material

Trays

316 SS

Distributors

316 SS

Downcomers

316 SS

Baffles

Reinforcing rings

Internal pipe fittings

Skirt, base plate, etc.

Stud bolts, external

Saddles

Nuts, external

Jacket

Bolts, internal

Shell flanges

3 of 12

Nuts, internal
Note 2

Nozzles (line pipe/plate)


Liner of nozzles and manholes

Gaskets, external
Gaskets, internal

Flanges (ANS)
Flanges (Non-ANS)
Welding fittings
Stiffening rings
Insulation support rings
Cleats for platforms, etc.
Internal parts
FABRICATION AND INSPECTION REQUIREMENTS
Construction in accordance with:

Inspection

full/limited

Inspection authority
Stress relieving
Special heat treatment
Radiography
Other non-destructive testing
Chemical analysis
Manufacturer's certificate

- chemical analysis
- mechanical data
WEIGHTS

Erection weight (shipping weight)

kg Weight of internals

kg

Total weight, operating

kg Weight of insulation

kg

Total weight, full of water

kg Weight of fireproofing

kg

REFERENCE DRAWINGS/LISTS
Arrangement - construction - outline
Standard vessel
Additional drawings
Welding electrodes, rods, etc.

See DEP 30.10.60.18-Gen.

General remarks for vessels

Anchor bolt ring and base plate

Flanged pipe nozzles

Lifting lug

Thermowell nozzles

Name plate

Carbon steel flanges

Support ring for insulation

Vortex breaker

Inspection hole/handhole/

Skirt/saddles/brackets
Note 1: 3 mm (min) SS internal cladding required on entire vessel
Note 2: Inlet nozzles connected to stainless steel pipe should be internally SS clad
Note 3: Refer to the Materials Section of the BDP for details

The manufacturer is responsible for ensuring that the equipment is designed and constructed in accordance with the specifications and codes referred to on the requisition and/or drawings. Furthermore, the manufacturer is responsible for
ensuring that the design, including thicknesses of pressure parts, is satisfactory for the design conditions indicated on the requisition and/or drawings. Calculations and thicknesses of material supplied to the manufacturer are for information and
tendering purposes only. The manufacturer shall make his own calculations for which he is fully responsible. The manufacturer shall ensure that the equipment supplied conforms to all the applicable codes and national statutory regulations,
and he shall obtain all necessary approvals from statutory authorities.

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

1) Drawings to be reviewed by Shell Global Solutions (US) inc


2) Dimensions are in meters

DOCUMENT No.
4 of 12

TRAY LOADING SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
REVISION
DATE

0
27-Jan-11

DOC. CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

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APP. BY

RR

DOC.SEQUENCE No.

Section (Name/Description)
Design Case
Tray number included (Note 1)
Loading on Actual Tray No.
Number of Trays Required
NORMAL VAPOR TO:
Flow Rate, kg/hr
Density, kg/m3
Flow Rate, m3/s
Molecular Weight
Viscosity, Pa s
Pressure, kPa
Temperature, C
NORMAL LIQUID FROM:
Flow Rate, kg/hr
Density, kg/m3
Flow Rate, m3/s
Molecular Weight
Surface Tension, N/m
Viscosity, Pa s
Temperature, C
PERFORMANCE REQUIREMENTS:
Max. delta P per tray, kPa
Max. % Jet Flood
Max. DC inlet velocity, m/s
Max. DC Backup,
mm clear
M
B k
l
liliquid
id
Derating Factor
Purpose for Derating (Foaming, System, Safety)
MECHANICAL REQUIREMENTS:
Tower Diameter, m
Tray Arrangement
Tray Spacing, mm
Type of Tray
Hole/Bubble Cap Diameter, mm
Deck Material/Thickness
Valve/Bubble Cap Material
Weir Height
Maximum Allowable Tray Pressure Drop
Total Corrosion Allowance
Nominal Vessel Manhole Size, NPS
MISCELLANEOUS:
Solids Present
Design Load
Anti-Jump Baffles
Special Features:
NOTES:
1) Tray Number 1 = Bottom Tray.

DOCUMENT No.

LOWER
DESIGN
1-6
1
6

UPPER
DESIGN
7- 9
9
3

50531
6.60
2.13
5.7
1.0E-05
3054
39

50524
6.58
2.13
5.7
1.2E-05
3046
35

62641
992.7
0.018
18.1
0.070
7.0E-04
38

6593
993.3
0.0018
18.0
0.071
7.4E-04
35

80

80

225
1.00
NA

300
1.00
NA

2.10
1 pass
450
valve

2.10
1 pass
600
bubble cap

SS / 2 mm
316 SS
75 mm
1450 Pa

SS / 2 mm
316 SS
100 mm
1450 Pa

24

24

NA

NA

Not req'd
Note 3

Not req'd
Note 4,5

2) Tray Design is based upon 100 % of the stated vapor and 100 % of the stated liquid flow rates.
3) Valves to be Sulzer Type "RC-1" or equivalent.
4) Picket Fence Weirs required
5) Inlet Weirs required
6) Drawings to be reviewed by Shell Global Solutions (US) Inc

5 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.

HALF PIPE DISTRIBUTOR AT NOZZLE N1

N1

1) End of distributor to be supported on clips on vessel wall


2) Drawings to be reviewed by Shell Global Solutions (US) Inc

6 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

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RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
7 of 12

DISTRIBUTOR AT NOZZLE N2

NPS 6 header
1.65

slots on 45 deg angle

N2
45

Diverting baffle

1) Ends of branches to be supported on clips on vessel wall


2) Drawings to be reviewed by Shell Global Solutions (US) Inc
3) Ends of branches to be closed

MESH PAD SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
0

REVISION
DATE

27-Jan-11

DOC. CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOC.SEQUENCE No.

DOCUMENT No.

INTERNAL

Packing

Mesh Pad

Case

DESIGN

DESIGN

50458

50458

Vapor Density, kg/m3

6.62

6.62

Design Liquid Load, kg/hr

1305

65

Liquid Density, kg/m3

993.7

993.7

Liquid Viscosity, Pa s

0.0007

0.0007

Surface Tension, N/m

0.0708

0.0708

Vapor Flow Rate to Mesh Pad, kg/hr

PACKING
Tower Inside Diameter, m
Packing

2.10
Mellapak 250Y

Packed Bed Height, m

0.42

Sheet Thickness, mm

0.20

# of packing layers

4 half layers

Support Grid Required?

YES

Hold Down Grid Required?

YES

MESH PAD
Tower Inside Diameter, m

2.10

Diameter of mesh pad, m

1.70

Mesh Pad thickness, m

0.15

Minimum Surface Area, 1/m

350

Minimum free volume of mat

97%

Wire thickness, mm
Hold down grid required?
Mesh Material

0.23 - 0.28
YES
316 SS

NOTES:
1) Design and constructon to be in accordance with Shell DEP 31.22.05.11-Gen
2) Mat to be made of knitted wire formed to the correct shape and not cut so as to leave edges and/or loose wires which could become detached
3) Mat shall be places between two grids with free area of 97%.
4) Mat shall be fastened in such a way that it cannot be compressed when mounted
5) Refer to standard drawings S20.028/29/30 for mounting details

8 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.028

DOCUMENT No.
9 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.030

DOCUMENT No.
10 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
0

REVISION
DATE

27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DWG S 20.029

DOCUMENT No.
11 of 12

VESSEL PROCESS SPECIFICATION

Shell Global Solutions (US) Inc


CUSTOMER NAME:

Shell Canada

PROJECT No:

LOCATION:

Scotford, AB

UNIT No:

HMU

Absorber #3 Water Wash Vessel

ITEM No:

V-3

SERVICE:
REVISION
DATE

0
27-Jan-11

DOCUMENT CAT.-CLASS 1

ORIG. BY

AJ

REVIEW

BKK

SHEET

APP. BY

RR

DOCUMENT SEQUENCE No.

DOCUMENT No.
12 of 12

SHELL GLOBAL SOLUTIONS (US)


Vessel Data Sheet
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60

CLIENT:
PROJECT:
LOCATION:
ITEM NO.:
SERVICE:

JOB/REQ:

Shell Canada
HMU CO2 Capture Project
Scotford
V-4
Reflux Drum
VESSEL DESIGN DATA

BY:

CODE:

AJ
PAGE:
1 of 2
QUANTITY:
One (1)
SIZE:
3658 mm ID x 6900 mm T/T
MATERIAL SPECIFICATIONS
Stainless Steel (Note 1)
Stainless Steel (Note 1)

HEAD:

STAMP:

NATIONAL BOARD:

DESIGN

INTERNAL:

PRESSURE

EXTERNAL:

(Note 2)

OPERATING PRESSURE:

350
FV
50

MDMT:

KPAG

AT

KPAG

AT

KPAG

AT

LIQ SP GR:

PWHT:

No

JOINT EFF:

SHELL:

CORR ALLOW: VESSEL:

SHELL:

150
150
36
0.994

DEG C

SADDLES:

DEG C

NOZZLE NECKS:

DEG C

FLANGES:
COUPLINGS:

RADIOGRAPHY:

FIXED INTERNALS:

HEADS:

REMOVABLE INTERNALS:

SADDLES:

GASKETS:

WIND DESIGN:

Stainless Steel (Note 1)


Stainless Steel (Note 1)

ACCESSORIES SUPPLIED BY VENDOR

SEISMIC DESIGN:

MANWAY:

NOZZLE RATING: CLASS:

150#

TYPE:

PROJ FROM CL: NOZZLES:

MANWAYS:

INSULATION (BY OTHERS):

THICKNESS:

FIREPROOFING:

THICKNESS:

RF

SUPPORTS:
NUMBER:

SIZE:

LADDER/PLATFORM CLIPS:
PIPE SUPPORT CLIPS:

MAWP (NEW & COLD):

SURFACE PREP:

HYDROTEST PRESSURE:

PAINT:

NOTES
1. See Materials Section of the BDP for additional details.
2. Design pressure to be confirmed and verified by others during
the next phase.
3. Additional slug volume equivalent to 1 sec of design volumetric
gas
g flow is considered between NLL and HLL.
4. Vessel has a demister mat. Size to be determined.

LIFTING LUGS:

DFT:
TRAILING LUG:

VESSEL

FAB:

EMPTY:

WEIGHT

OPER:

TEST:

FLANGE FINISH:

NOZZLE SCHEDULE
MARK

NUMBER

SIZE (in)

RATING

TYPE

N1
N2
N3
N4
N5
N6
N7
N8

1
1
1
1
1
1
1
1

42
36
6
2
2
HOLD
2
2

150#
150#
150#
150#
150#
150#
150#
150#

RF
RF
RF
RF
RF
RF
RF
RF

Vapor / Liquid Inlet


Vapor Outlet
Liquid Outlet
Water make-up inlet
Drain
Relief Valve
Vent
Steam Out

K1A/B
K2A/B

2
2

2
2

150#
150#

RF
RF

Level Gage
Level Transmitter

M1
M2

1
1

24
24

150#
150#

RF
RF

Manway
Manway

REVISION
ENGINEER / DATE

0
AJ

01/27/11

DESCRIPTION

REMARKS

With Half-Pipe Distributor


With vortex breaker
With inlet baffle
Blinded off, outside skirt
Sized during detailed design.

Include blind
Include blind

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60

SHELL GLOBAL SOLUTIONS (US)


Generic Data Sheet
1 CLIENT:
2 PROJECT:
3 LOCATION:
4 ITEM NO.:
5 SERVICE:

JOB/REQ:

Shell Canada
HMU CO2 Capture Project
Scotford
V-4
Reflux Drum

BY:
PAGE:
QUANTITY:

AJ
2 of 2

2
3
4
5

10

10

11

Elevations from b.t.l.

11

12

LLLL

300 mm

12

13

LLL

420 mm

13

14

NLL

530 mm

14

15

HLL

2300 mm

15

16

HHLL

2420 mm

16

17

17

18

18

19

19

20

20

21

21

22

22

23

23

24

24

25

Dimensions

26

27

25
26

3658 mm
6900 mm

28

2420 mm

28

29

X1

4480 mm

29

27

30

30

31

31

32

32

33

33

34

34

35

35

36

36

37

37

38

38

39

39

40

40

41

41

42

42

43

Notes:

43

44

1. Inlet is a half-pipe distributor.

44

45

2. Actual number of instrument connections and their locations to be confirmed during detailed design.

45

46

3. Centerline of nozzle N4 to be 300 mm above HHLL.

46

47

47

48

48

49

49

50

50

51

51

52

52

53

53

54

REVISION

55

Engineer / DATE

54

0
AJ

01/27/11

55

SR.11.10343

74

APPENDIX D4- ROTATING EQUIPMENT

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-1 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

REVISION NO.
PAGE

PURCHASE

AS BUILT

1/27/2011

BY

PUMP CLASS:

PUMP SIZE

TYPE

5 MANUFACTURER

API

NON-API

Lean Amine Booster Pumps


NO. STAGES

Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

BY PURCHASER

SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-1 A/B

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

SITE AND UTILITY DATA (CONT)

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

1236

(kPag)

19

DIFFERENTIAL PRESSURE

1139

(kPa)

TYPE OR NAME OF LIQUID

20

DIFF. HEAD

(m)

PUMPING TEMPERATURE

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:
24

1510.6 (m3/hr) RATED

119.1

CONT.

(m)

NPSHA

1661.7

(m3/hr)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(3.5.2.6)

97

(kPag)

INSTRUMENT AIR: MAX/MIN PRESS

(kPag)

1.7

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

25

LIQUID

119

45 wt% ADIP-X Solvent (Lean Amine)


(C) MAX.

HYD P

kW

525.8

NORMAL

(kJ/kg-C)

(cP) @

0.75

27

INDOOR

HEATED

UNDER ROOF

MAX. VISCOSITY

28

OUTDOOR

UNHEATED

PARTIAL SIDES

CORROSIVE/EROSIVE AGENT

29

GRADE

MEZZANINE

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)

(cP)
(2.11.1.8)

CO2

GR

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

38

OTHER

THERMAL

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

39

40 STEAM:

(C)

119

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)

MIN

3.87

VISCOSITY

CL

(C)

119

MAX

0.98

SPECIFIC HEAT, Cp

SITE AND UTILITY DATA

31

(C) MIN.
(kPaA) @

175

RELATIVE DENSITY (SPECIFIC GRAVITY):

26 LOCATION: (2.1.29)

32

AJ

UNIT
SERVICE

4 NO. REQ 2 (1Oper + 1Spare)

DATE

OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(2.1.9)

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-1 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

PAGE

DATE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

24

300#

RF

SPACER LENGTH

15 DISCHARGE

24

300#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-2 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

REVISION NO.
PAGE

PURCHASE

AS BUILT

1/27/2011

BY

PUMP CLASS:

PUMP SIZE

TYPE

5 MANUFACTURER

API

NON-API

Stripper Reflux Pumps


NO. STAGES

Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

BY PURCHASER

SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-2 A/B

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

SITE AND UTILITY DATA (CONT)

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

580

(kPag)

19

DIFFERENTIAL PRESSURE

514

(kPa)

TYPE OR NAME OF LIQUID

20

DIFF. HEAD

(m)

PUMPING TEMPERATURE

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:
24

36.4

(m3/hr) RATED
/

(m)

52.8

CONT.

NPSHA

41.9

(m3/hr)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(3.5.2.6)

67

(kPag)

INSTRUMENT AIR: MAX/MIN PRESS

(kPag)

1.7

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

25

HYD P

kW

6.0

CORROSIVE/EROSIVE AGENT

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


CL

(kJ/kg-C)

(cP) @

0.71

PARTIAL SIDES

UNHEATED
MEZZANINE

(cP)
(2.11.1.8)

CO2

GR

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

38

OTHER

THERMAL

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

39

40 STEAM:

(C)

36

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)

MIN

4.18

MAX. VISCOSITY

OUTDOOR

(C)

36

MAX

0.99

UNDER ROOF

GRADE

31

NORMAL

HEATED

29

(C) MIN.
(kPaA) @

144

VISCOSITY

28

32

(C) MAX.

36

SPECIFIC HEAT, Cp

SITE AND UTILITY DATA

INDOOR

LIQUID

Reflux Water (with dissolved CO2)

RELATIVE DENSITY (SPECIFIC GRAVITY):

26 LOCATION: (2.1.29)
27

AJ

UNIT
SERVICE

4 NO. REQ 2 (1Oper + 1Spare)

DATE

0
OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(2.1.9)

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-2 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

DATE

PAGE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

150#

RF

SPACER LENGTH

15 DISCHARGE

150#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-3 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

REVISION NO.
PAGE

PURCHASE

AS BUILT

1/27/2011

BY

PUMP CLASS:

PUMP SIZE

TYPE

5 MANUFACTURER

API

NON-API

Lean Amine Charge Pumps


NO. STAGES

Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

BY PURCHASER

SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-3 A/B

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

SITE AND UTILITY DATA (CONT)

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

3617

(kPag)

19

DIFFERENTIAL PRESSURE

3211

(kPa)

20

DIFF. HEAD

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:
24

1418.4 (m3/hr) RATED

315.2

CONT.

(m)

NPSHA

1560.2

(m3/hr)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(3.5.2.6)

406

(kPag)

INSTRUMENT AIR: MAX/MIN PRESS

(kPag)

Ample (m)

HYD P

1392.0 kW

NORMAL

PARTIAL SIDES

CORROSIVE/EROSIVE AGENT

UNHEATED
MEZZANINE

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


CL

(kJ/kg-C)

(cP) @

5.44

MAX. VISCOSITY

OUTDOOR

(cP)
(2.11.1.8)

CO2

GR

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

38

OTHER

THERMAL

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

39

40 STEAM:

(C)

30

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)

MIN

3.57

UNDER ROOF

GRADE

(C)

30

MAX

1.04

HEATED

29

(C) MIN.
(kPaA) @

5.8

VISCOSITY

28

31

(C) MAX.

30

SPECIFIC HEAT, Cp

26 LOCATION: (2.1.29)

32

45 wt% ADIP-X Solvent (Lean Amine)

RELATIVE DENSITY (SPECIFIC GRAVITY):

SITE AND UTILITY DATA

INDOOR

LIQUID
TYPE OR NAME OF LIQUID
PUMPING TEMPERATURE

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

25
27

AJ

UNIT
SERVICE

4 NO. REQ 2 (1Oper + 1Spare)

DATE

0
OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(2.1.9)

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-3 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

DATE

PAGE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

20

600#

RF

SPACER LENGTH

15 DISCHARGE

20

600#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-4 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

REVISION NO.
PAGE

PURCHASE

0
1

AS BUILT

1/27/2011

BY

PUMP CLASS:

PUMP SIZE

TYPE

5 MANUFACTURER

API

BY PURCHASER

NO. STAGES
SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-4 A/B

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

43.7

SITE AND UTILITY DATA (CONT)

(m3/hr) RATED

43.7

(m3/hr)

2937

(kPag)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(kPag)

3185

DIFFERENTIAL PRESSURE
DIFF. HEAD

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:

248
(m)

CONT.

NPSHA

1.7

25

(kPa)

TYPE OR NAME OF LIQUID

(m)

PUMPING TEMPERATURE

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

Circulating Water (with dissolved CO2 and Amine)


(C)

38

kW

3.0

NORMAL

0.99

SPECIFIC HEAT, Cp

26 LOCATION: (2.1.29)

VISCOSITY

38

(C) MIN.

(kPaA) @
MAX

MIN
(kJ/kg-C)

(cP) @

0.70

INDOOR

HEATED

UNDER ROOF

MAX. VISCOSITY

28

OUTDOOR

UNHEATED

PARTIAL SIDES

CORROSIVE/EROSIVE AGENT

29

GRADE

MEZZANINE

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


GR

(cP)
(2.11.1.8)

CO2

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5
/

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

OTHER

THERMAL

39

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

38

40 STEAM:

(C)

38

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)
(C)

38

4.17

27

CL

MAX.

3014

RELATIVE DENSITY (SPECIFIC GRAVITY):

HYD P

SITE AND UTILITY DATA

31

(kPag)
LIQUID

19

25.5

(3.5.2.6)

INSTRUMENT AIR: MAX/MIN PRESS

20

32

NON-API

Absorber #1 Circulating Water Wash Pumps


Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

24

AJ

UNIT
SERVICE

4 NO. REQ 2 (1Oper + 1Spare)

DATE

OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

(m3/hr)

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

(2.1.9)

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-4 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

PAGE

DATE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

300#

RF

SPACER LENGTH

15 DISCHARGE

300#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-5 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

REVISION NO.
PAGE

PURCHASE

0
1

AS BUILT

1/27/2011

BY

PUMP CLASS:

PUMP SIZE

TYPE

5 MANUFACTURER

API

BY PURCHASER

NO. STAGES
SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-5 A/B

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

43.7

SITE AND UTILITY DATA (CONT)

(m3/hr) RATED

43.7

(m3/hr)

2937

(kPag)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(kPag)

3185

DIFFERENTIAL PRESSURE
DIFF. HEAD

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:

248
(m)

CONT.

NPSHA

1.7

25

(kPa)

TYPE OR NAME OF LIQUID

(m)

PUMPING TEMPERATURE

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

Circulating Water (with dissolved CO2 and Amine)


(C)

38

kW

3.0

NORMAL

0.99

SPECIFIC HEAT, Cp

26 LOCATION: (2.1.29)

VISCOSITY

38

(C) MIN.

(kPaA) @
MAX

MIN
(kJ/kg-C)

(cP) @

0.70

INDOOR

HEATED

UNDER ROOF

MAX. VISCOSITY

28

OUTDOOR

UNHEATED

PARTIAL SIDES

CORROSIVE/EROSIVE AGENT

29

GRADE

MEZZANINE

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


GR

(cP)
(2.11.1.8)

CO2

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5
/

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

OTHER

THERMAL

39

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

38

40 STEAM:

(C)

38

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)
(C)

38

4.17

27

CL

MAX.

3014

RELATIVE DENSITY (SPECIFIC GRAVITY):

HYD P

SITE AND UTILITY DATA

31

(kPag)
LIQUID

19

25.5

(3.5.2.6)

INSTRUMENT AIR: MAX/MIN PRESS

20

32

NON-API

Absorber #2 Circulating Water Wash Pumps


Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

24

AJ

UNIT
SERVICE

4 NO. REQ 2 (1Oper + 1Spare)

DATE

OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

(m3/hr)

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

(2.1.9)

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-5 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

PAGE

DATE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

300#

RF

SPACER LENGTH

15 DISCHARGE

300#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-6 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

REVISION NO.
PAGE

PURCHASE

0
1

AS BUILT

1/27/2011

BY

PUMP CLASS:

PUMP SIZE

TYPE

5 MANUFACTURER

API

BY PURCHASER

NO. STAGES
SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-6 A/B

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

63.1

SITE AND UTILITY DATA (CONT)

(m3/hr) RATED

63.1

(m3/hr)

2977

(kPag)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(kPag)

3230

DIFFERENTIAL PRESSURE
DIFF. HEAD

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:

253
(m)

CONT.

NPSHA

1.7

25

(kPa)

TYPE OR NAME OF LIQUID

(m)

PUMPING TEMPERATURE

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

Circulating Water (with dissolved CO2 and Amine)


(C)

38

kW

4.4

NORMAL

0.99

SPECIFIC HEAT, Cp

26 LOCATION: (2.1.29)

VISCOSITY

38

(C) MIN.

(kPaA) @
MAX

MIN
(kJ/kg-C)

(cP) @

0.70

INDOOR

HEATED

UNDER ROOF

MAX. VISCOSITY

28

OUTDOOR

UNHEATED

PARTIAL SIDES

CORROSIVE/EROSIVE AGENT

29

GRADE

MEZZANINE

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


GR

(cP)
(2.11.1.8)

CO2

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5
/

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

OTHER

THERMAL

39

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

38

40 STEAM:

(C)

38

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)
(C)

38

4.17

27

CL

MAX.

3054

RELATIVE DENSITY (SPECIFIC GRAVITY):

HYD P

SITE AND UTILITY DATA

31

(kPag)
LIQUID

19

26.1

(3.5.2.6)

INSTRUMENT AIR: MAX/MIN PRESS

20

32

NON-API

Absorber #3 Circulating Water Wash Pumps


Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

24

AJ

UNIT
SERVICE

4 NO. REQ 2 (1Oper + 1Spare)

DATE

OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

(m3/hr)

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

(2.1.9)

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-6 A/B

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

PAGE

DATE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

300#

RF

SPACER LENGTH

15 DISCHARGE

300#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-7

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

4 NO. REQ

REVISION NO.
PAGE

PURCHASE

AS BUILT

1/27/2011

BY

PUMP CLASS:
SERVICE
TYPE

5 MANUFACTURER

API

NON-API

Amine Make-Up Tank Pump


NO. STAGES

Centrifugal Electric Drive

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

BY PURCHASER

SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-7

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

SITE AND UTILITY DATA (CONT)

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

339

(kPag)

19

DIFFERENTIAL PRESSURE

338

(kPa)

TYPE OR NAME OF LIQUID

20

DIFF. HEAD

(m)

PUMPING TEMPERATURE

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:
24

10.0

(m3/hr) RATED
/

(m)

33.3

CONT.

NPSHA

10.0

(m3/hr)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(3.5.2.6)

(kPag)

INSTRUMENT AIR: MAX/MIN PRESS

(kPag)

8.7

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

25

HYD P

kW

0.9

CORROSIVE/EROSIVE AGENT

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


CL

(kJ/kg-C)

(cP) @

5.31

PARTIAL SIDES

UNHEATED
MEZZANINE

(cP)
(2.11.1.8)

CO2

GR

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

38

OTHER

THERMAL

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

39

40 STEAM:

(C)

30

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)

MIN

3.61

MAX. VISCOSITY

OUTDOOR

(C)

30

MAX

1.04

UNDER ROOF

GRADE

31

NORMAL

HEATED

28

(C) MIN.
(kPaA) @

5.8

VISCOSITY

29

32

(C) MAX.

30

SPECIFIC HEAT, Cp

SITE AND UTILITY DATA

INDOOR

LIQUID

45 wt% ADIP-X Solvent (Lean Amine)

RELATIVE DENSITY (SPECIFIC GRAVITY):

26 LOCATION: (2.1.29)
27

AJ

UNIT
PUMP SIZE

DATE

OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(2.1.9)

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-7

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

PAGE

DATE

/
OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

150#

RF

SPACER LENGTH

15 DISCHARGE

150#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-8

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1 APPLICABLE TO:

BDP

2 FOR

Shell Canada Limited

3 SITE

Scotford

4 NO. REQ

REVISION NO.
PAGE

PURCHASE

AS BUILT

1/27/2011

BY

PUMP CLASS:
SERVICE
TYPE

5 MANUFACTURER

API

NON-API

Closed Drain Amine Pump


NO. STAGES

Submerged Centrifugal

MODEL

6 NOTES: INFORMATION BELOW TO BE COMPLETED:

BY PURCHASER

SERIAL NO.

BY MANUFACTURER

BY MANUFACTURER OR PURCHASER

GENERAL (3.1.1)

8 PUMPS TO OPERATE IN (PARALLEL)

NO. MOTOR DRIVEN

9 (SERIES) WITH

PUMP ITEM NO.

NO. TURBINE DRIVEN

PUMP ITEM NO.

P-8

10 GEAR ITEM NO.

MOTOR ITEM NO.

TURBINE ITEM NO.

11 GEAR PROVIDED BY

MOTOR PROVIDED BY

TURBINE PROVIDED BY

12 GEAR MOUNTED BY

MOTOR MOUNTED BY

TURBINE MOUNTED BY

13 GEAR DATA SHT. NO.

MOTOR DATA SHT. NO.

14

TURBINE DATA SHT. NO.

OPERATING CONDITIONS

SITE AND UTILITY DATA (CONT)

15

CAPACITY, NORMAL

16

OTHER

17

SUCTION PRESSURE MAX./RATED

18

DISCHARGE PRESSURE

477

(kPag)

19

DIFFERENTIAL PRESSURE

474

(kPa)

TYPE OR NAME OF LIQUID

20

DIFF. HEAD

(m)

PUMPING TEMPERATURE

21

PROCESS VARIATIONS

(3.1.2)

NORMAL

22

STARTING CONDITIONS

(3.1.3)

VAPOR PRESSURE

23 SERVICE:
24

10.9

(m3/hr) RATED
/

(m)

46.5

CONT.

NPSHA

10.9

(m3/hr)

WATER SOURCE
CHLORIDE CONCENTRATION (PPM)

(3.5.2.6)

(kPag)

INSTRUMENT AIR: MAX/MIN PRESS

(kPag)

0.3

INTERMITTENT (STARTS/DAY)

PARALLEL OPERATION REQ'D (2.1.11)

25

HYD P

kW

1.4

CORROSIVE/EROSIVE AGENT

30

ELECTRIC AREA CLASSIFICATION (2.1.22 / 3.1.5)


CL

(kJ/kg-C)

(cP) @

5.46

PARTIAL SIDES

UNHEATED
MEZZANINE

(cP)
(2.11.1.8)

CO2

GR

(3.5.2.6)

H2S CONCENTRATION (PPM)

DIV

LIQUID (2.1.3)

TROPICALIZATION REQ'D.

(2.11.1.11)

HAZARDOUS

FLAMMABLE

OTHER

33 SITE DATA (2.1.29)

PERFORMANCE

34

ALTITUDE

35

RANGE OF AMBIENT TEMPS: MIN/MAX.

36

RELATIVE HUMIDITY:

(m)

BAROMETER

93.5

-43

MIN / MAX

37 UNUSUAL CONDITIONS: (2.1.23)

40

/
DUST

(kPa)

PROPOASAL CURVE NO.

RPM

(C)

IMPELLER DIA. RATED

MAX.

(%)

RATED POWER

(kW) EFFICIENCY

FUMES

MIN.

38

OTHER

THERMAL

UTILITY CONDITIONS:

PREFERRED OPERATING REGION

TO

ALLOWABLE OPERATING REGION

TO

41

MIN

42

MAX

43 ELECTRICITY

DRIVERS

HEATING

(kPag)

(C)

(kPag)
DRIVERS

(kPag)

(C)
HEATING

(kPag)
CONTROL

(mm)
(%)

MINIMUM CONTINUOUS FLOW:

39

40 STEAM:

(C)

30

CHLORIDE CONCENTRATION (PPM)

WINTERIZATION REQ'D

(C)

MIN

3.57

MAX. VISCOSITY

OUTDOOR

(C)

30

MAX

1.04

UNDER ROOF

GRADE

31

NORMAL

HEATED

28

(C) MIN.
(kPaA) @

94

VISCOSITY

29

32

(C) MAX.

30

SPECIFIC HEAT, Cp

SITE AND UTILITY DATA

INDOOR

LIQUID

45 wt% ADIP-X Solvent (Lean Amine)

RELATIVE DENSITY (SPECIFIC GRAVITY):

26 LOCATION: (2.1.29)
27

AJ

UNIT
PUMP SIZE

DATE

0
OF

(C)

MAX HEAD @ RATED IMPELLER

(C)

MAX POWER @ RATED IMPELLER

SHUTDOWN

(m3/hr)

STABLE

NPSHR AT RATED CAPACITY

(m3/hr)
(m3/hr)
(m3/hr)
(m)
(BHP)
(m) (2.1.8)

44

VOLTAGE

SUCTION SPECIFIC SPEED

45

HERTZ

MAX. SOUND PRESS. LEVEL REQ'D

(dBA) (2.1.14)

46

PHASE

EST MAX SOUND PRESS. LEVEL

(dBA) (2.1.14)

47 COOLING WATER: (2.1.17)

REMARKS:

48

TEMP. INLET

(C)

MAX. RETURN

49

PRESS. NORM

(kPag)

DESIGN

50

MIN RETURN

51
52

(2.1.9)

(kPag)

MAX ALLOW DP

(C)
(kPag)
(kPa)

1. Pump hydraulic requirements to be confirmed during detailed design when


detailed piping configuration is available.
2. NPSHa and NPSHr to be confirmed during detailed design.

JOB NO.

Shell Global Solutions (US)

ITEM NO.

P-8

PURCHASE ORDER NO.


REQUISITION NO.

CENTRIFUGAL PUMP
DATA SHEET
METRIC UNITS
1

REVISION NO.

DATE

PAGE

OF

CONSTRUCTION

1/27/2011

BY

AJ

CONSTRUCTION (CONT)

2 APPLICABLE STANDARD:

SHAFT DIAMETER BETWEEN BEARINGS

(mm)

API 610 8TH EDITION

SPAN BETWEEN BEARING CENTERS

(mm)

OTHER

SPAN BETWEEN BEARING & IMPELLER

(mm)

(SEE REMARKS)

5 PUMP TYPE: (1.1.2)

REMARKS

OH2

BB1

VS1

VS6

OH3

BB2

VS2

VS7

OH6

BB3

VS3

OTHER

BB4

VS4

MAKE

BB5

VS5

MODEL

9
10
11

RATING (HP/100 RPM)

NOZZLE CONDITIONS: (2.3.2)

12

DRIVER - PUMP

COUPLINGS: (3.2.2)

SIZE (in)

FLANGE
RATING (lb)

FAC'G

14 SUCTION

150#

RF

SPACER LENGTH

15 DISCHARGE

150#

RF

SERVICE FACTOR

13

POSITION

LUBRICATION
LIMITED END FLOAT REQUIRED

16 BALANCE DRUM

(mm)

DRIVER HALF COUPLING MOUNTED BY: (3.2.11)

17 PRESSURE CASING CONNECTIONS: (2.3.3)


NO.

18

PUMP MFR.
SIZE (in)

TYPE

DRIVER MFR.

19

DRAIN

20

VENT

API BASEPLATE NUMBER

21

PRESSURE GAUGE

NON-GROUT CONSTRUCTION: (3.3.13/5.3.7.3.5)

BASEPLATES:

22

TEMP GAUGE

23

WARM-UP

24

BALANCE / LEAK-OFF

25

CYLINDRICAL THREADS REQUIRED (2.3.3)

(APPENDIX M)

REMARKS:

26 CASING MOUNTING:

MATERIAL

( SEE SEPARATE SHEET FOR VERTICLES)

APPENDIX H CLASS

(2.11.1.1)

27

CENTERLINE

NEAR CENTERLINE

MIN DESIGN METAL TEMP (2.11.4.5)

28

FOOT

SEPARATE MOUNTING PLATE

BARREL/CASE

29

IN-LINE

SHAFT

AXIAL

RADIAL

SS

COUPLING SPACER/HUBS

33

SINGLE VOLUTE

MULTIPLE VOLUTE

DIFFUSER

34

OVERHUNG

BETWEEN BEARINGS

BARREL

COUPLING DIAPHAGMS (DISKS)


REMARKS:

35 CASE PRESSURE RATING:

37

38

HYDROTEST PRESSURE

39

SUCT'N PRESS. REGIONS MUST BE DESIGNED FOR MAWP (2.2.4)

41
42

1. See the Materials Section of the BDP for additional details


2. Nozzle size and flange rating to be finalized by vendor.

MAX ALLOWABLE WORKING PRESSURE

(kPa g)

(C)

40 ROTATION:
CW

SS

DIFFUSERS

32 CASING TYPE:

36

(C)
IMPELLER

SS

CASE/IMPELLER WEAR RINGS

30 CASING SPLIT:
31

PURCHASER

COUPLING PER API 671 (5.2.7)

BEARINGS AND LUBRICATION


(kPa g)

(VIEWED FROM COUPLING END)


CCW

BEARING (TYPE/NUMBER):
RADIAL

THRUST

REVIEW AND APPROVE THRUST BEARING SIZE (5.2.5.2.4)

IMPELLERS INDIVIDUALLY SECURED (5.2.2.2)

LUBRICATION: (2.10)

43 REMARKS:

GREASE

FLOOD

RING OIL

44

FLINGER

PURGE OIL MIST

PURE OIL MIST

45

BOLT OH3 PUMP TO PAD/FOUNDATION (5.1.2.4)

CONSTANT LEVEL OILER PREFERENCE (SEE REMARKS) (2.9.2.2)

46 SHAFT:
47

SHAFT DIAMETER AT COUPLING

48 REMARKS:
49
50
51
52
53
54
55
56
57
58

PRESSURE LUBE SYS (5.2.6)


(mm)

OIL VISC. ISO GRADE (5.2.6.5)

API-610

API-614

SR.11.10343

75

APPENDIX D5- FILTERS

SHELL GLOBAL SOLUTIONS (US)


Filter Data Sheet
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

CLIENT:

Shell Canada Limited


PROJECT:
HMU CO2 Capture Project
LOCATION:
Scotford
ITEM NO.:
F-1
SERVICE:
Lean Amine Filter
OPERATING CONDITIONS
FLUID FILTERED:
ADIP-X Amine Solvent
FLOW RATE: NORMAL:
355
(Note 3)
MAXIMUM:
INLET TEMPERATURE:

30
709
1.04
5.46

INLET PRESSURE:
SPEC GRAV @ TEMP:
VISCOSITY @ TEMP:
MAX ALLOW DP:

JOB/REQ:
BY:
PAGE:
QUANTITY:

DESIGN PRESSURE:
M3/HR

DESIGN TEMPERATURE:

M3/HR

CODE:

DEG C

CORROSION ALLOWANCE:

KPAG
CP

DEG C

KG

Cartridge

COVER TYPE: [ ] SINGLE BOLT [ ] MULTIPLE BOLT [ ] SWING BOLT


[ ] LIFTING SCREW [ ] HANDWHEEL

KPA

103

KPAG

MM

WEIGHT:

KPA

DIRTY:

DESIGN CONDITIONS
1530 (Note 1) / HV (Note 5)
150 / 150

STAMP?

FILTER TYPE:

CLEAN:

AJ
1 of 1
One (1)

FILTRATION REQUIRED:

99% to 10 micron absolute

TYPE OF SOLIDS:

CONNECTIONS
INLET
OUTLET

NUMBER

SIZE (in)

RATING

FACING

1
1

10
10

150#
150#

RF
RF

CASE:
COVER:
GASKETS:

DRAINS

FILTER MEDIA:

VENTS

CARTRIDGE CORE:

PRESSURE GAUGES
RELIEF VALVE
OTHER
REMARKS

1. Design pressure to be set by pump shut-off head - estimated at 1530 kPag


2. See the Materials Section of the BDP for additional details.
3. Sized for 25% of Lean Amine Flow.
4. Nozzle details to be determined during detailed design.
5. HV stands for half vacuum.

REVISION
ENGINEER / DATE

0
AJ

1/27/11

MATERIALS OF CONSTRUCTION
Carbon Steel (PWHT)
(Note 2)

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

SHELL GLOBAL SOLUTIONS (US)


Filter Data Sheet
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

CLIENT:

Shell Canada Limited


PROJECT:
HMU CO2 Capture Project
LOCATION:
Scotford
ITEM NO.:
F-2
SERVICE:
Lean Amine Post Filter
OPERATING CONDITIONS
FLUID FILTERED:
ADIP-X Amine Solvent
FLOW RATE: NORMAL:
75
(Note 3)
MAXIMUM:
INLET TEMPERATURE:

30
537
1.04
5.46

INLET PRESSURE:
SPEC GRAV @ TEMP:
VISCOSITY @ TEMP:
MAX ALLOW DP:

JOB/REQ:
BY:
PAGE:
QUANTITY:

DESIGN PRESSURE:
M3/HR

DESIGN TEMPERATURE:

M3/HR

CODE:

DEG C

CORROSION ALLOWANCE:

KPAG
CP

DEG C

KG

Cartridge

COVER TYPE: [ ] SINGLE BOLT [ ] MULTIPLE BOLT [ ] SWING BOLT


[ ] LIFTING SCREW [ ] HANDWHEEL

KPA

103

KPAG

MM

WEIGHT:

KPA

DIRTY:

DESIGN CONDITIONS
1530 (Note 1) / HV (Note 5)
150 / 150

STAMP?

FILTER TYPE:

CLEAN:

AJ
1 of 1
One (1)

FILTRATION REQUIRED:

99% to 10 micron absolute

TYPE OF SOLIDS:

CONNECTIONS
INLET
OUTLET

NUMBER

SIZE (in)

RATING

FACING

1
1

6
6

150#
150#

RF
RF

CASE:
COVER:
GASKETS:

DRAINS

FILTER MEDIA:

VENTS

CARTRIDGE CORE:

PRESSURE GAUGES
RELIEF VALVE
OTHER
REMARKS

1. Design pressure to be set by pump shut-off head - estimated at 1530 kPag


2. See the Materials Section of the BDP for additional details.
3. Sized for approximately 5% of Lean Amine Flow.
4. Nozzle details to be determined during detailed design.
5. HV stands for half vacuum.

REVISION
ENGINEER / DATE

0
AJ

1/27/11

MATERIALS OF CONSTRUCTION
Carbon Steel (PWHT)
(Note 2)

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

SHELL GLOBAL SOLUTIONS (US)


Filter Data Sheet
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

CLIENT:

JOB/REQ:

Shell Canada Limited


PROJECT:
HMU CO2 Capture Project
LOCATION:
Scotford
ITEM NO.:
F-3
SERVICE:
Closed Amine Drain Collection Filter
OPERATING CONDITIONS
FLUID FILTERED:
ADIP-X Amine Solvent
FLOW RATE: NORMAL:
11

BY:
PAGE:
QUANTITY:

DESIGN PRESSURE:

MAXIMUM:
INLET TEMPERATURE:

30
477
1.04
5.46

INLET PRESSURE:
SPEC GRAV @ TEMP:
VISCOSITY @ TEMP:
MAX ALLOW DP:

M3/HR

DESIGN TEMPERATURE:

M3/HR

CODE:

DEG C

CORROSION ALLOWANCE:

KPAG
CP

KG

Cartridge

COVER TYPE: [ ] SINGLE BOLT [ ] MULTIPLE BOLT [ ] SWING BOLT


[ ] LIFTING SCREW [ ] HANDWHEEL

KPA

138

DEG C
MM

WEIGHT:

KPA

DIRTY:

KPAG
STAMP?

FILTER TYPE:

CLEAN:

DESIGN CONDITIONS
600 (Note 1) / HV (Note 4)
150 / 150

AJ
1 of 1
One (1)

FILTRATION REQUIRED:

99% to 10 micron absolute

TYPE OF SOLIDS:

CONNECTIONS
INLET
OUTLET

NUMBER

SIZE (in)

RATING

FACING

1
1

3
3

150#
150#

RF
RF

CASE:
COVER:
GASKETS:

DRAINS

FILTER MEDIA:

VENTS

CARTRIDGE CORE:

PRESSURE GAUGES
RELIEF VALVE
OTHER
REMARKS

1. Design pressure to be set by pump shut-off head - estimated at 600 kPag


2. See the Materials Section of the BDP for additional details.
3. Nozzle details to be determined during detailed design.
4. HV stands for half vacuum.

REVISION
ENGINEER / DATE

0
AJ

1/27/11

MATERIALS OF CONSTRUCTION
Carbon Steel (PWHT)
(Note 2)

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

SHELL GLOBAL SOLUTIONS (US)


Vessel Data Sheet
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62

CLIENT:
PROJECT:
LOCATION:
ITEM NO.:
SERVICE:

JOB/REQ:

Shell Canada Limited


HMU CO2 Capture Project
Scotford
D-1
Lean Amine Carbon Filter
VESSEL DESIGN DATA

BY:

CODE:

HEAD:

STAMP:

NATIONAL BOARD:

DESIGN

INTERNAL:

PRESSURE

EXTERNAL:

OPERATING PRESSURE:
FLOW RATE:

1530
HV (Note 5)
606

NORMAL:

KPAG

AT

KPAG

AT

KPAG

AT

75

SHELL:

150
150
30
(Note 4)

MAXIMUM:
LIQ SP GR:

PWHT:

Yes
SHELL:

CORR ALLOW: VESSEL:

DEG C

SADDLES:

DEG C

NOZZLE NECKS:

DEG C

FLANGES:

M3/HR
M3/HR

MDMT:
JOINT EFF:

AJ
PAGE:
1 of 2
QUANTITY:
One (1)
SIZE:
3200 mm ID x 6000 mm T/T
MATERIAL SPECIFICATIONS
Carbon Steel (PWHT) (Note 1)
Carbon Steel (PWHT) (Note 1)

3 mm

COUPLINGS:

1.04

RADIOGRAPHY:

FIXED INTERNALS:

HEADS:

REMOVABLE INTERNALS:

SADDLES:

GASKETS:

WIND DESIGN:

Stainless Steel (Note 1)


Stainless Steel (Note 1)

ACCESSORIES SUPPLIED BY VENDOR

SEISMIC DESIGN:

MANWAY:

NOZZLE RATING: CLASS:

TYPE:

150#

PROJ FROM CL: NOZZLES:

MANWAYS:

INSULATION (BY OTHERS):

THICKNESS:

FIREPROOFING:

THICKNESS:

SUPPORTS:

RF

NUMBER:

SIZE:

LADDER/PLATFORM CLIPS:
PIPE SUPPORT CLIPS:

MAWP (NEW & COLD):

SURFACE PREP:

HYDROTEST PRESSURE:

PAINT:

NOTES
1. See Materials Section of the BDP for additional details.
2. Design Pressure to be set by pump shut-off head
estimated at 1530 kPag.
3. 38 m3 of activated carbon. Sized for 75 m3/hr amine flow
4. 75 m3/hr is approximately 5% of lean amine flow.
5. HV stands for half vacuum.

LIFTING LUGS:

DFT:
TRAILING LUG:

VESSEL

FAB:

EMPTY:

WEIGHT

OPER:

TEST:

FLANGE FINISH:

NOZZLE SCHEDULE
MARK

NUMBER

SIZE (in)

RATING

TYPE

N1
N2
N3

1
1
1

6
6
3

150#
150#
150#

RF
RF
RF

Liquid Inlet
Liquid Outlet
Drain

N4
N5

1
1

3
4

150#
150#

RF
RF

Utility / Steam Out


Vent

Inlet deflector plate required.


Outlet deflector plate required.
Blinded off, outside skirt (Final sizing by
EPC Contractor)
Final sizing by EPC Contractor
Final sizing by EPC Contractor

K1A/B

150#

RF

Differential Pressure

Final sizing by EPC Contractor

M1
M2

1
1

24
24

150#
150#

RF
RF

Manway
Manway

Include blind.
Include blind.

REVISION
ENGINEER / DATE

0
AJ

1/27/11

DESCRIPTION

REMARKS

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62

SHELL GLOBAL SOLUTIONS (US)


Generic Data Sheet
1 CLIENT:
2 PROJECT:
3 LOCATION:
4 ITEM NO.:
5 SERVICE:

JOB/REQ:

Shell Canada Limited


HMU CO2 Capture Project
Scotford
D-1
Lean Amine Carbon Filter

BY:
PAGE:
QUANTITY:

AJ
2 of 2
One (1)

2
3
4
5

10

10

11

11

12

12

13

13

14

14

15

15

16

16

17

17

18

18

19

19

20

20

21

21

22

22

23

23

24

24

25

25

26

26

27

27

28

28

29

29

30

30

31

31

32

32

33

33

Dimensions

34

34

35

3200

mm

35

36

6000

mm

36

37

X1

600

mm

37

X2
X3

4800
600

mm
mm

38
39

38
39

40

40

41

41

42

42

43

Notes:

43

44

1. Maximum allowable pressure drop is 70 kPa.

44

45

2. Top and bottom bed screens are required. Mesh size to be set during detailed design in coordination with

45

47

activated carbon supplier.


3. Vessel internals (screens / deflector plates) to be stainless steel.

48

4. Actual number of instrument connections to be confirmed during detailed design.

48

49

5. Diameter of inlet and outlet deflector plates to be approximately 4 times the diameter of the associated nozzle.

49

46

50
51

6. Inlet deflector to be perforated with 21 (twenty one) , 25 mm diameter holes (open area of approximately 55% of inlet pipe area).
7. Additional height of 600 mm added above and below the actual bed to be confirmed based on supports selected.

52

46
47

50
51
52

53

53

54

REVISION

55

Engineer / DATE

54

0
AJ

1/27/11

55

SR.11.10343

76

APPENDIX D6- TANKS

SHELL GLOBAL SOLUTIONS (US)


Tank Data Sheet
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

CLIENT:
PROJECT:
LOCATION:
ITEM NO.:
SERVICE:

JOB/REQ:

Shell Canada
HMU CO2 Capture Project
Scotford
T-1
Amine Make-up Tank
TANK DESIGN DATA

STANDARD:

BY:

AJ
PAGE:
1 of 1
QUANTITY:
One (1)
SIZE:
2150 mm ID x 3700 mm High
MATERIAL SPECIFICATIONS

APPENDIX:

NOM. / WORKING CAPACITY:


DESIGN

INTERNAL:

PRESSURE

EXTERNAL:

ROOF:

10 /
ATM

OPERATING PRESSURE:
MDMT:

KPAG

AT

KPAG

AT

KPAG

AT

LIQ SP GR:

PWHT:
CORR ALLOW: TANK:

Yes
3 mm

ROOF LOAD:

150

m3

SHELL:

DEG C

BOTTOM:

DEG C

NOZZLE NECKS:

DEG C

FLANGES:

1.035

Carbon Steel (Note 1)


ANNULAR RING:

COUPLINGS:

RADIOGRAPHY:

HEATING COIL:

STRUCT:

STRUCTURAL:

RAIN:

GASKETS:

Required
ANCHOR BOLTS:

WIND DESIGN:

ACCESSORIES SUPPLIED BY VENDOR

SEISMIC DESIGN:

MANWAY:

NOZZLE RATING: CLASS:

150#

TYPE:

RF

INSUL SUPPORTS: NUMBER:

SIZE:

PROJ FROM CL: NOZZLES:

MANWAYS:

STAIRWAY: TYPE:

INSULATION (BY OTHERS):

THICKNESS:

LADDER:

PUMPING RATE: IN:

OUT:

DRAW-OFF SUMP:

HEATING COIL:

ROOF: TYPE:

WELD:

ROOF DRAIN: TYPE:

SIZE:

SHELL: METHOD:

FRANGIBLE ROOF:

CLEANOUT: TYPE:

SIZE:

BOTTOM: TYPE:

WELD:

PIPE SUPPORT CLIPS:

ANCHOR BOLTS: QTY:

SIZE:

SURFACE PREP:

HYDROTEST:

VACUUM BOX TEST:

NOTES
1. See Materials Section of BDP for additional details.
2.
Tank
dimension
be verif
ified
during
dettail
iled
desiign.
2 T
k di
i
to b
i dd
i
d
dd
3. Pump rate out is 10 m3/h
4. Fluid is 45 wt% ADIP-X amine solvent; for higher strength
tank design should be re-evaluated.

HANDRAIL:
PLATFORM:

PAINT:

CLIPS:

DFT:

LIFTING LUGS:
TANK
WEIGHT

FAB:

EMPTY:

OPER:

TEST:

FLANGE FINISH:

NOZZLE SCHEDULE
MARK

NUMBER

SIZE (in)

RATING

TYPE

Nozzle details to be determined during detailed design.

REVISION
ENGINEER / DATE

0
AJ

1/27/11

DESCRIPTION

REMARKS

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58

SR.11.10343

Appendix E:

77

Material Selection Guide

Included in this section is a copy of the Materials Selection Guide for Amine Units (Update 2004). This
is report number OG.04.20821.

Material Selection.pdf

SR.11.10343

78

Material Selection Guide - Appendix E

OP.99.20651

Materials Selection for Amine Units

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

10

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

11

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

12

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

13

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

14

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

15

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

16

OP.99.20651

Shell ADIP & Sulfinol Process Design Manual

17

SR.11.10343

Appendix F:

79

Material Safety Data Sheets

Piperazine, Hexahydrate (DEDA)


SECTION 1 CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
MDL INFORMATION SYSTEMS, INC.
EMERGENCY TELEPHONE NUMBER:
1281 Murfreesboro Road, Suite 300
1-800-424-9300 (NORTH AMERICA)
Nashville, TN 37217-2423
1-703-527-3887 (INTERNATIONAL)
1-615-366-2000
SUBSTANCE: PIPERAZINE, HEXAHYDRATE
TRADE NAMES/SYNONYMS:
ARPEZINE; ARTHRITICINE; PARID; VERMISOL; PIPERAZINE; OHS18935; RTECS TM0850000
CHEMICAL FAMILY: heterocyclic, nitrogen
CREATION DATE: Feb 19 1987
REVISION DATE: Sep 19 2000
SECTION 2 COMPOSITION, INFORMATION ON INGREDIENTS
COMPONENT: PIPERAZINE, HEXAHYDRATE
CAS NUMBER: 142-63-2
EC NUMBER: Not assigned.
PERCENTAGE: 100.0
SECTION 3 HAZARDS IDENTIFICATION
NFPA RATINGS (SCALE 0-4): HEALTH=3 FIRE=1 REACTIVITY=0
EC CLASSIFICATION (CALCULATED):
Xi Irritant
R 37-38-41
EMERGENCY OVERVIEW:
COLOR: white
PHYSICAL FORM: crystals
MAJOR HEALTH HAZARDS: harmful if inhaled, eye burns, respiratory tract irritation, skin irritation,
central nervous system depression
PHYSICAL HAZARDS: Dust/air mixtures may ignite or explode.

SR.11.10343

80

POTENTIAL HEALTH EFFECTS:


INHALATION:
SHORT TERM EXPOSURE: irritation, lung congestion
LONG TERM EXPOSURE: no information on significant adverse effects
SKIN CONTACT:
SHORT TERM EXPOSURE: irritation
LONG TERM EXPOSURE: same as effects reported in short term exposure
EYE CONTACT:
SHORT TERM EXPOSURE: irritation (possibly severe)
LONG TERM EXPOSURE: same as effects reported in short term exposure
INGESTION:
SHORT TERM EXPOSURE: rash, nausea, vomiting, diarrhea, headache, symptoms of drunkenness,
hyperactivity, blurred vision, nerve damage, convulsions
LONG TERM EXPOSURE: irregular heartbeat, drowsiness, dilated pupils, blood disorders, kidney
damage, liver damage, coma
CARCINOGEN STATUS:
OSHA: N
NTP: N
IARC: N
SECTION 4 FIRST AID MEASURES
INHALATION: If adverse effects occur, remove to uncontaminated area. Give artificial respiration if not
breathing. If breathing is difficult, oxygen should be administered by qualified personnel. Get
immediate medical attention.
SKIN CONTACT: Wash skin with soap and water for at least 15 minutes while removing contaminated
clothing and shoes. Get immediate medical attention. Thoroughly clean and dry contaminated
clothing and shoes before reuse. Destroy contaminated shoes.
EYE CONTACT: Immediately flush eyes with plenty of water for at least 15 minutes. Then get
immediate medical attention.
INGESTION: If a large amount is swallowed, get medical attention.
NOTE TO PHYSICIAN: For inhalation, consider oxygen.
SECTION 5 FIRE FIGHTING MEASURES
FIRE AND EXPLOSION HAZARDS: Slight fire hazard. Dust/air mixtures may ignite or explode.
EXTINGUISHING MEDIA: regular dry chemical, carbon dioxide, water, regular foam
Large fires: Use regular foam or flood with fine water spray.

SR.11.10343

81

FIRE FIGHTING: Move container from fire area if it can be done without risk. Do not scatter spilled
material with high-pressure water streams. Dike for later disposal. Use extinguishing agents
appropriate for surrounding fire. Avoid inhalation of material or combustion by-products. Stay upwind
and keep out of low areas.
SECTION 6 ACCIDENTAL RELEASE MEASURES
OCCUPATIONAL RELEASE:
Collect spilled material in appropriate container for disposal. Keep out of water supplies and sewers.
Keep unnecessary people away, isolate hazard area and deny entry.
SECTION 7 HANDLING AND STORAGE
Store and handle in accordance with all current regulations and standards.
SECTION 8 EXPOSURE CONTROLS, PERSONAL PROTECTION
EXPOSURE LIMITS:
PIPERAZINE, HEXAHYDRATE:
No occupational exposure limits established.
VENTILATION: Provide local exhaust or process enclosure ventilation system.
Ventilation equipment should be explosion-resistant if explosive concentrations of material are
present. Ensure compliance with applicable exposure limits.
EYE PROTECTION: Wear splash resistant safety goggles. Provide an emergency eye wash fountain and
quick drench shower in the immediate work area.
CLOTHING: Wear appropriate chemical resistant clothing.
GLOVES: Wear appropriate chemical resistant gloves.
RESPIRATOR: Under conditions of frequent use or heavy exposure, respiratory protection may be
needed. Respiratory protection is ranked in order from minimum to maximum.
Consider warning properties before use. Any supplied-air respirator with a full facepiece that is
operated in a pressure-demand or other positive-pressure mode.
Any self-contained breathing apparatus that has a full facepiece and is operated in a pressure-demand
or other positive-pressure mode.
For Unknown Concentrations or Immediately Dangerous to Life or Health Any supplied-air respirator with full facepiece and operated in a pressure-demand or other positivepressure mode in combination with a separate escape supply.
Any self-contained breathing apparatus with a full facepiece.

SR.11.10343

82

SECTION 9 PHYSICAL AND CHEMICAL PROPERTIES


PHYSICAL STATE: solid
COLOR: white
PHYSICAL FORM: crystals
ODOR: Not available
MOLECULAR WEIGHT: 194.19
MOLECULAR FORMULA: C4-H10-N2 . 6(H2O)
BOILING POINT: 257 F (125 C)
MELTING POINT: 111 F (44 C)
VAPOR PRESSURE: Not applicable
VAPOR DENSITY: Not applicable
SPECIFIC GRAVITY: Not available
WATER SOLUBILITY: soluble
PH: 10-11 (10% solution)
VOLATILITY: Not applicable
ODOR THRESHOLD: Not available
EVAPORATION RATE: Not applicable
COEFFICIENT OF WATER/OIL DISTRIBUTION: Not available
SOLVENT SOLUBILITY:
Soluble: alcohol
Insoluble: ether
SECTION 10 STABILITY AND REACTIVITY
REACTIVITY: Stable at normal temperatures and pressure.
CONDITIONS TO AVOID: Avoid heat, flames, sparks and other sources of ignition. Avoid contact with
incompatible materials.
INCOMPATIBILITIES: metals, cyanides, acids
PIPERAZINE:
ALUMINUM: Solutions are corrosive.
DICYANOFURAZAN: Mixture is instantly explosive.
STRONG ACIDS: Solutions react violently.
ZINC: Solutions are corrosive.
HAZARDOUS DECOMPOSITION:
Thermal decomposition products: oxides of nitrogen
POLYMERIZATION: Will not polymerize.
SECTION 11 TOXICOLOGICAL INFORMATION
PIPERAZINE, HEXAHYDRATE:

SR.11.10343

83

TOXICITY DATA:
500 mg/kg oral-rat LDLo; 11200 mg/kg oral-mouse LD50; 300 mg/kg intraperitoneal-mouse LD50
LOCAL EFFECTS:
Irritant: inhalation, skin
Corrosive: eye
ACUTE TOXICITY LEVEL:
Slightly Toxic: ingestion
TARGET ORGANS: nervous system
MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE: convulsive disorders, kidney disorders
HEALTH EFFECTS:
INHALATION:
ACUTE EXPOSURE:
PIPERAZINE: Piperazine is a strong organic base; inhalation of vapors may cause irritation to the nose
and throat. It may cause pulmonary edema which manifests a few hours after exposure. Mice inhaling
5400 mg/m3 for 2 hours exhibited excitement and changes in motor activity and coordination; half of
them died. 6 rats inhaling a saturated vapor of piperazine for 8 hours survived.
CHRONIC EXPOSURE:
PIPERAZINE: Sensitization may occur; rare cases of ashtma have beenobserved following industrial use
of piperazine. No adverse effects were detected when guinea pigs were exposed to a 100 ppm
concentration for 3 hours a day 7 times in 11 days.
SKIN CONTACT:
ACUTE EXPOSURE:
PIPERAZINE: May cause irritation. Cases of dermatitis have occurred. Application of 4000 mg/kg to the
skin of rabbits for an unreported period
of time killed half of the rabbits. Application of 500 mg
to the skin of rabbits caused irritation.
CHRONIC EXPOSURE:
PIPERAZINE: Repeated or prolonged exposure may cause irritation or dermatitis.
EYE CONTACT:
ACUTE EXPOSURE:
PIPERAZINE: May cause irritation or burns to eyes. 750 ug full strengthpiperazine on rabbit's eyes
caused severe injury; applications of 0.2 molar solution for 10 minutes produced no effects.
CHRONIC EXPOSURE:
PIPERAZINE: Systemic poisoning may cause difficulty in focusing, a
flashes upon closing the eyes at night.

disturbance of color vision, and

INGESTION:
ACUTE EXPOSURE:
PIPERAZINE: May cause vomiting, giddiness, blurred vision, diarrhea, urticaria, tremors, and collapse.
Neurological disorders and subnormal kidney function may occur. Doses of 75 to 3500 mg/kg in
humans produced headache, nausea, vomiting, lethargy, tremor, incoordination, muscular weakness,

SR.11.10343

84

utricaria and ocular disturbance. Reports of abnormal pain, confusion, convulsions, central nervous
system depression with reduced activity, emotional quieting, affective indifference, periods of
agitation, and hyperactivity prior to depression have been reported. It may cause extrapyramidal
symptoms, torticollis, body stiffness, and impaired speech. A 10 year old girl who ingested 4.8 grams
had purpura with epistaxis and bleeding gums 8 days after treatment. Rats fed 1900 mg/kg showed
excitement and neurological and muscular disorders; the dose was lethal to 50% of the rats tested.
CHRONIC EXPOSURE:
PIPERAZINE: Symptoms of neurotoxicity reported with several fatalities of young children who
received dosages ranging from 75 to 155 mg/kg for 3 or more days include dizziness, urticaria,
vomiting, hypotonia, impairment of gait, blurred vision, weakness, and convulsions. Prolonged
treatment may cause sedation, drowsiness, apathy, anticholinergic dilated pupils, coma, dry mouth,
nausea, gastrointestinal upset, constipation, urinary retention, chilliness, fever, tachycardia, ventricular
arrhythmias, hypotension, changes in EEG, respiratory depression, stuffy nose, ataxia, tarsive
dyskinesia and involuntary muscle spasms. Prolonged treatment may cause bone marrow depression,
with agranulocytosis, parkinsonism, gastrointestinal upset, and transient neurological effects. Rats fed
a diet containing 0.1% piperazine for 90 days exhibited no effects in appearance, behavior, growth,
mortality, food consumption, final body or organ weights or gross and microscopic tissue examination.
1% to 3% in the diet caused moderate liver and kidney damage. When rats were fed 750 mg/kg daily
for 30 days, the lipid level in their liver, kidneys and lungs was lower than in animals not fed piperazine.
Ingestion of piperazine, or its salts, is especially dangerous to persons with a history of convulsive
disorders, or impaired kidney function.
SECTION 12 ECOLOGICAL INFORMATION
Not available
SECTION 13 DISPOSAL CONSIDERATIONS
Dispose in accordance with all applicable regulations.
SECTION 14 TRANSPORT INFORMATION
U.S. DOT 49 CFR 172.101 SHIPPING NAME-UN NUMBER:
Piperazine-UN2579
U.S. DOT 49 CFR 172.101 HAZARD CLASS OR DIVISION:
8
U.S. DOT 49 CFR 172.101 PACKING GROUP:
III
U.S. DOT 49 CFR 172.101 AND SUBPART E LABELING REQUIREMENTS:
Corrosive
U.S. DOT 49 CFR 172.101 PACKAGING AUTHORIZATIONS:

SR.11.10343

85

EXCEPTIONS: 49 CFR 173.154


NON-BULK PACKAGING: 49 CFR 173.213
BULK PACKAGING: 49 CFR 173.240
U.S. DOT 49 CFR 172.101 QUANTITY LIMITATIONS:
PASSENGER AIRCRAFT OR RAILCAR: 25 kg
CARGO AIRCRAFT ONLY: 100 kg
LAND TRANSPORT ADR/RID:
SUBSTANCE NAME: Piperazine
UN NUMBER: UN2579
ADR/RID CLASS: 8
ITEM NUMBER: 52(c)
WARNING SIGN/LABEL: 8
HAZARD ID NUMBER: 80
AIR TRANSPORT IATA/ICAO:
CORRECT TECHNICAL NAME: Piperazine
UN/ID NUMBER: UN2579
IATA/ICAO CLASS: 8
PACKAGING GROUP: III
LABEL: Corrosive
MARITIME TRANSPORT IMDG:
CORRECT TECHNICAL NAME: Diethylenediamine, solid or solution
UN/ID NUMBER: UN2579
IMDG CLASS: 8
PACKAGING GROUP: III
EmS No.: 8-05
MFAG Table No.: 320
MARINE POLLUTANT: N
SECTION 15 REGULATORY INFORMATION
U.S. REGULATIONS:
TSCA INVENTORY STATUS: N
TSCA 12(b) EXPORT NOTIFICATION: Not listed.
CERCLA SECTION 103 (40CFR302.4): N
SARA SECTION 302 (40CFR355.30): N
SARA SECTION 304 (40CFR355.40): N
SARA SECTION 313 (40CFR372.65): N
SARA HAZARD CATEGORIES, SARA SECTIONS 311/312 (40CFR370.21):
ACUTE: Y
CHRONIC: Y
FIRE: N

SR.11.10343

86

REACTIVE: N
SUDDEN RELEASE: N
OSHA PROCESS SAFETY (29CFR1910.119): N
STATE REGULATIONS:
California Proposition 65: N
EUROPEAN REGULATIONS:
EC NUMBER: Not assigned.
EC RISK AND SAFETY PHRASES:
R 37
Irritating to respiratory system.
R 38
Irritating to skin.
R 41
Risk of serious damage to eyes.
S2
S 24
S 25
S 26
S 39
S 46

Keep out of reach of children.


Avoid contact with skin.
Avoid contact with eyes.
In case of contact with eyes, rinse immediately with plenty of water and seek medical
advice.
Wear eye/face protection.
If swallowed, seek medical advice immediately and show this container or label.

GERMAN REGULATIONS:
WATER HAZARD CLASS (WGK): 2 (Self Classification by Manufacturers and Distributors)
SECTION 16 OTHER INFORMATION
COPYRIGHT 1984-2000 MDL INFORMATION SYSTEMS, INC. ALL RIGHTS RESERVED.

SR.11.10343

87

Methyldiethanolamine (MDEA)
SECTION 1 CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
MDL INFORMATION SYSTEMS, INC.
14600 CATALINA STREET
SAN LEANDRO, CA 94577

EMERGENCY TELEPHONE NUMBER:


1-800-424-9300 (NORTH AMERICA)
1-703-527-3887 (INTERNATIONAL)
1-800-738-4765 OR 1-615-366-2000

SUBSTANCE: N-METHYLDIETHANOLAMINE
TRADE NAMES/SYNONYMS:
N-METHYLIMINODIETHANOL; N-METHYL-2,2'-IMINODIETHANOL;
2,2'-(METHYLIMINO)DIETHANOL; 2,2-(METHYLIMINO)BIS-ETHANOL;
METHYLDIETHANOLAMINE; METHYL DIETHANOLAMINE; MDEA; C5H13NO2; HYSOL HD3410;
OHS15750; KL7525000
CHEMICAL FAMILY: amines, alcohols, aliphatic
CREATION DATE: May 28 1986
REVISION DATE: Jun 30 1997
SECTION 2 COMPOSITION, INFORMATION ON INGREDIENTS
COMPONENT: N-METHYLDIETHANOLAMINE
CAS NUMBER: 105-59-9
EC NUMBER (EINECS): 203-312-7
EC INDEX NUMBER: 603-079-00-5
PERCENTAGE: 100
SECTION 3 HAZARDS IDENTIFICATION
NFPA RATINGS (SCALE 0-4): HEALTH=2 FIRE=1 REACTIVITY=0
EC CLASSIFICATION (ASSIGNED): Xi Irritant R 36
EC Classification may be inconsistent with independently-researched data.
EMERGENCY OVERVIEW:
COLOR: colorless
PHYSICAL FORM: liquid
ODOR: fishy odor
MAJOR HEALTH HAZARDS: respiratory tract irritation, skin irritation, eye irritation

SR.11.10343

88

POTENTIAL HEALTH EFFECTS:


INHALATION:
SHORT TERM EXPOSURE: irritation.
LONG TERM EXPOSURE: no information is available.
SKIN CONTACT:
SHORT TERM EXPOSURE: irritation.
LONG TERM EXPOSURE: same as effects reported in short term exposure.
EYE CONTACT:
SHORT TERM EXPOSURE: irritation.
LONG TERM EXPOSURE: same as effects reported in short term exposure.
INGESTION:
SHORT TERM EXPOSURE: no information on significant adverse effects.
LONG TERM EXPOSURE: no information is available.
CARCINOGEN STATUS:
OSHA: N
NTP: N
IARC: N
SECTION 4 FIRST AID MEASURES
INHALATION: Remove from exposure immediately. Use a bag valve mask or similar device to perform
artificial respiration (rescue breathing) if needed. Get medical attention.
SKIN CONTACT: Remove contaminated clothing, jewelry, and shoes immediately.
Wash with soap or mild detergent and large amounts of water until no evidence of chemical remains
(at least 15-20 minutes). Get medical attention, if needed.
EYE CONTACT: Wash eyes immediately with large amounts of water or normal saline, occasionally
lifting upper and lower lids, until no evidence of chemical remains.
Get medical attention immediately.
INGESTION: If vomiting occurs, keep head lower than hips to help prevent aspiration.
Get medical attention, if needed.
SECTION 5 FIRE FIGHTING MEASURES
FIRE AND EXPLOSION HAZARDS: Slight fire hazard.
EXTINGUISHING MEDIA: regular dry chemical, carbon dioxide, water, regular foam
Large fires: Use regular foam or flood with fine water spray.

SR.11.10343

89

FIREFIGHTING: Move container from fire area if it can be done without risk.
Do not scatter spilled material with high-pressure water streams. Dike for ater disposal.
Use extinguishing agents appropriate for surrounding fire.
Aoid inhalation of material or combustion by-products. Stay upwind and keep out of low areas.
FIREFIGHTING PROTECTIVE EQUIPMENT: Full firefighting turn-out gear (bunker gear).
Any supplied-air respirator with full facepiece and operated in a pressure-demand or other positivepressure mode in combination with a separate escape supply. Any self-contained breathing apparatus
with a full facepiece.
FLASH POINT: 259 F (126 C) (OC)
SECTION 6 ACCIDENTAL RELEASE MEASURES
OCCUPATIONAL RELEASE:
Stop leak if possible without personal risk. Small spills: Absorb with sand or other non-combustible
material. Collect spilled material in appropriate container for disposal.
Keep unnecessary people away, isolate hazard area and deny entry.
SECTION 7 HANDLING AND STORAGE
Store and handle in accordance with all current regulations and standards.
Keep separated from incompatible substances.
SECTION 8 EXPOSURE CONTROLS, PERSONAL PROTECTION
EXPOSURE LIMITS:
N-METHYLDIETHANOLAMINE:
No occupational exposure limits established.
VENTILATION: Provide local exhaust ventilation system.
Ensure compliance with applicable exposure limits.
EYE PROTECTION: Wear splash resistant safety goggles.
Provide an emergency eye wash fountain and quick drench shower in the immediate work area.
CLOTHING: Wear appropriate chemical resistant clothing.
GLOVES: Wear appropriate chemical resistant gloves.
RESPIRATOR: Under conditions of frequent use or heavy exposure, respiratory protection may be
needed. Respiratory protection is ranked in order from minimum to maximum.
Consider warning properties before use. Any chemical cartridge respirator with organic vapor
cartridge(s). Any chemical cartridge respirator with a full facepiece and organic vapor cartridge(s).
Any air-purifying respirator with a full facepiece and an organic vapor canister.
For Unknown Concentrations or Immediately Dangerous to Life or Health -

SR.11.10343

90

Any supplied-air respirator with full facepiece and operated in a pressure-demand or other positivepressure mode in combination with a separate escape supply. Any self-contained breathing apparatus
with a full facepiece.
SECTION 9 PHYSICAL AND CHEMICAL PROPERTIES
PHYSICAL STATE: liquid
COLOR: colorless
ODOR: fishy odor
MOLECULAR WEIGHT: 119.16
MOLECULAR FORMULA: C5-H13-N-O2
BOILING POINT: 475-478 F (246-248 C)
FREEZING POINT: -5.8 F (-21.0 C)
VAPOR PRESSURE: <0.01 mmHg @ 20 C
VAPOR DENSITY: Not available
SPECIFIC GRAVITY (water=1): 1.04 @ 20 C
WATER SOLUBILITY: soluble
PH: Not available
VOLATILITY: Not available
ODOR THRESHOLD: Not available
EVAPORATION RATE: Not available
COEFFICIENT OF WATER/OIL DISTRIBUTION: Not available
SOLVENT SOLUBILITY:
Soluble: benzene
SECTION 10 STABILITY AND REACTIVITY
REACTIVITY: Stable at normal temperatures and pressure.
CONDITIONS TO AVOID: Avoid heat, flames, sparks and other sources of ignition.
Avoid contact with incompatible materials.
INCOMPATIBILITIES: oxidizing materials
N-METHYLDIETHANOLAMINE:
OXIDIZERS (STRONG): Fire and explosion hazard.
HAZARDOUS DECOMPOSITION: Thermal decomposition products: oxides of nitrogen, carbon.
POLYMERIZATION: Will not polymerize.
SECTION 11 TOXICOLOGICAL INFORMATION
N-METHYLDIETHANOLAMINE:
IRRITATION DATA:

SR.11.10343

91

10 mg/24 hour(s) open skin-rabbit mild; 502 mg open skin-rabbit mild; 20 mg open eyes-rabbit.
TOXICITY DATA:
4780 mg/kg oral-rat LD50; 500 mg/kg intraperitoneal-mouse LD50; 5990 ul/kg skin-rabbit LD50.
LOCAL EFFECTS:
Irritant: inhalation, skin, eye.
ACUTE TOXICITY LEVEL:
Moderately Toxic: ingestion.
Slightly Toxic: dermal absorption.
HEALTH EFFECTS:
INHALATION:
ACUTE EXPOSURE:
N-METHYLDIETHANOLAMINE: May cause irritation to the mucous membranes.
CHRONIC EXPOSURE:
N-METHYLDIETHANOLAMINE: No data available.
SKIN CONTACT:
ACUTE EXPOSURE:
N-METHYLDIETHANOLAMINE: May cause irritation. 10 mg applied to the skin of rabbits caused mild
irritation.
CHRONIC EXPOSURE:
N-METHYLDIETHANOLAMINE: May cause dermatitis after repeated or prolonged exposure.
EYE CONTACT:
ACUTE EXPOSURE:
N-METHYLDIETHANOLAMINE: May cause irritation. 20 mg applied to the eyes of rabbits caused
irritation.
CHRONIC EXPOSURE:
N-METHYLDIETHANOLAMINE: May cause conjunctivitis after repeated or prolonged exposure.
INGESTION:
ACUTE EXPOSURE:
N-METHYLDIETHANOLAMINE: The lethal dose reported in rats was 4780 mg/kg.
CHRONIC EXPOSURE:
N-METHYLDIETHANOLAMINE: No data available.
SECTION 12 ECOLOGICAL INFORMATION
Not available.

SR.11.10343

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SECTION 13 DISPOSAL CONSIDERATIONS


Dispose in accordance with all applicable regulations.
SECTION 14 TRANSPORT INFORMATION
No classification assigned.
SECTION 15 REGULATORY INFORMATION
U.S. REGULATIONS:
TSCA INVENTORY STATUS: Y
TSCA 12(b) EXPORT NOTIFICATION: Not listed.
CERCLA SECTION 103 (40CFR302.4): N
SARA SECTION 302 (40CFR355.30): N
SARA SECTION 304 (40CFR355.40): N
SARA SECTION 313 (40CFR372.65): N
SARA HAZARD CATEGORIES, SARA SECTIONS 311/312 (40CFR370.21):
ACUTE: Y
CHRONIC: N
FIRE: N
REACTIVE: N
SUDDEN RELEASE: N
OSHA PROCESS SAFETY (29CFR1910.119): N
STATE REGULATIONS:
CALIFORNIA PROPOSITION 65: N
EUROPEAN REGULATIONS:
EC NUMBER (EINECS): 203-312-7
EC RISK AND SAFETY PHRASES:
R 36
Irritating to eyes.
S2
Keep out of reach of children.
S 24
Avoid contact with skin.
SECTION 16 OTHER INFORMATION
MSDS SUMMARY OF CHANGES
SECTION 1
CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
SECTION 2
COMPOSITION, INFORMATION ON INGREDIENTS
SECTION 3
HAZARDS IDENTIFICATION
SECTION 5
FIRE FIGHTING MEASURES
SECTION 6
ACCIDENTAL RELEASE MEASURES
SECTION 8
EXPOSURE CONTROLS, PERSONAL PROTECTION
SECTION 9
PHYSICAL AND CHEMICAL PROPERTIES
SECTION 10 STABILITY AND REACTIVITY

SR.11.10343

SECTION 11
SECTION 12
SECTION 14
SECTION 15

93

TOXICOLOGICAL INFORMATION
ECOLOGICAL INFORMATION
TRANSPORT INFORMATION
REGULATORY INFORMATION

COPYRIGHT 1984-1997 MDL INFORMATION SYSTEMS, INC. ALL RIGHTS RESERVED.

SR.11.10343

94

Carbon Dioxide (CO2)


SECTION 1 CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
MDL INFORMATION SYSTEMS, INC.
14600 CATALINA STREET
SAN LEANDRO, CA 94577

EMERGENCY TELEPHONE NUMBER:


1-800-424-9300 (NORTH AMERICA)
1-703-527-3887 (INTERNATIONAL)
1-800-738-4765 OR 1-615-366-2000

SUBSTANCE: CARBON DIOXIDE, GAS


TRADE NAMES/SYNONYMS:
CARBONIC ACID GAS; CARBONIC ANHYDRIDE; CARBON DIOXIDE; CARBON OXIDE; CARBON DIOXIDE
GAS; CARBON DIOXIDE, CARBONIC ANHYDRIDE; UN 1013; STCC 4904535; CO2; OHS04260; FF6400000
CHEMICAL FAMILY: oxides of carbon
CREATION DATE: Feb 11 1985
REVISION DATE: Jun 30 1997
SECTION 2 COMPOSITION, INFORMATION ON INGREDIENTS
COMPONENT: CARBON DIOXIDE, GAS
CAS NUMBER: 124-38-9
EC NUMBER (EINECS): 204-696-9
PERCENTAGE: 100
SECTION 3 HAZARDS IDENTIFICATION
NFPA RATINGS (SCALE 0-4): HEALTH=1 FIRE=0 REACTIVITY=0
EC CLASSIFICATION (CALCULATED): No classification assigned.
EMERGENCY OVERVIEW:
COLOR: colorless
PHYSICAL FORM: gas
ODOR: odorless
MAJOR HEALTH HAZARDS: difficulty breathing
PHYSICAL HAZARDS: Containers may rupture or explode if exposed to heat.
POTENTIAL HEALTH EFFECTS:
INHALATION:

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95

SHORT TERM EXPOSURE: ringing in the ears, nausea, irregular heartbeat, headache, drowsiness,
dizziness, tingling sensation, visual disturbances, suffocation, convulsions, coma.
LONG TERM EXPOSURE: no information on significant adverse effects.
SKIN CONTACT:
SHORT TERM EXPOSURE: no information on significant adverse effects.
LONG TERM EXPOSURE: no information on significant adverse effects.
EYE CONTACT:
SHORT TERM EXPOSURE: irritation.
LONG TERM EXPOSURE: no information on significant adverse effects.
INGESTION:
SHORT TERM EXPOSURE: ingestion of a gas is unlikely.
LONG TERM EXPOSURE: ingestion of a gas is unlikely.
CARCINOGEN STATUS:
OSHA: N
NTP: N
IARC: N
SECTION 4 FIRST AID MEASURES
INHALATION: When safe to enter area, remove from exposure. Use a bag valve mask or similar device
to perform artificial respiration (rescue breathing) if needed. Keep warm and at rest.
Get medical attention immediately.
SKIN CONTACT: Wash if needed. If frostbite, freezing, or cryogenic burns occur, warm affected area in
warm water. If this is not available, gently wrap affected parts in blankets.
Allow circulation to return naturally.
Get medical attention immediately.
EYE CONTACT: It is unlikely that emergency treatment will be required. Wash with large amounts of
water or normal saline until no evidence of chemical remains (at least 15-20 minutes).
Get medical attention immediately.
INGESTION: It is unlikely that emergency treatment will be required. Get medical attention, if needed.
NOTE TO PHYSICIAN: For inhalation, consider oxygen.
SECTION 5 FIRE FIGHTING MEASURES
FIRE AND EXPLOSION HAZARDS: Negligible fire hazard.
EXTINGUISHING MEDIA: carbon dioxide, regular dry chemical

SR.11.10343

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Large fires: Use regular foam or flood with fine water spray.
FIREFIGHTING: Move container from fire area if it can be done without risk.
Cool containers with water spray until well after the fire is out. Stay away from the ends of tanks.
Withdraw immediately in case of rising sound from venting safety device or any discoloration of tanks
due to fire. For tank, rail car or tank truck, evacuation radius: 800 meters (1/2 mile).
Use extinguishing agents appropriate for surrounding fire. Cool containers with water spray until well
after the fire is out. Apply water from a protected location or from a safe distance.
Do not get water directly on material. Reduce vapors with water spray. Avoid inhalation of material or
combustion by-products. Stay upwind and keep out of low areas.
Consider downwind evacuation if material is leaking.
FIREFIGHTING PROTECTIVE EQUIPMENT: Full firefighting turn-out gear (bunker gear).
Any supplied-air respirator with full facepiece and operated in a pressure-demand or other positivepressure mode in combination with a separate escape supply. Any self-contained breathing apparatus
with a full facepiece.
SECTION 6 ACCIDENTAL RELEASE MEASURES
OCCUPATIONAL RELEASE:
Stop leak if possible without personal risk. Keep unnecessary people away, isolate hazard area and
deny entry. Stay upwind and keep out of low areas.
SECTION 7 HANDLING AND STORAGE
Store and handle in accordance with all current regulations and standards.
Subject to storage regulations: U.S. OSHA 29 CFR 1910.101.
Keep separated from incompatible substances.
SECTION 8 EXPOSURE CONTROLS, PERSONAL PROTECTION
EXPOSURE LIMITS:
CARBON DIOXIDE, GAS:
CARBON DIOXIDE:
5000 ppm (9000 mg/m3) OSHA TWA
10000 ppm (18000 mg/m3) OSHA TWA (vacated by 58 FR 35338, June 30, 1993)
30000 ppm (54000 mg/m3) OSHA STEL (vacated by 58 FR 35338, June 30, 1993)
5000 ppm (9000 mg/m3) ACGIH TWA
30000 ppm (54000 mg/m3) ACGIH STEL
5000 ppm (9000 mg/m3) NIOSH recommended TWA 10 hour(s)
30000 ppm (54000 mg/m3) NIOSH recommended STEL
MEASUREMENT METHOD: Gas collection bag; Gas chromatography with thermal conductivity
detector; NIOSH III # S249

SR.11.10343

97

VENTILATION: Provide local exhaust ventilation system. Ensure compliance with applicable exposure
limits.
EYE PROTECTION: Eye protection not required, but recommended.
CLOTHING: For the gas: Protective clothing is not required. For the liquid:
Wear appropriate protective, cold insulating clothing.
GLOVES: Protective gloves are not required, but recommended.
RESPIRATOR: The following respirators and maximum use concentrations are drawn from NIOSH
and/or OSHA.
40,000 ppm
Any supplied-air respirator.
Any self-contained breathing apparatus with a full facepiece.
Escape Any appropriate escape-type, self-contained breathing apparatus.
For Unknown Concentrations or Immediately Dangerous to Life or Health Any supplied-air respirator with full facepiece and operated in a pressure-demand or other positivepressure mode in combination with a separate escape supply.
Any self-contained breathing apparatus with a full facepiece.
SECTION 9 PHYSICAL AND CHEMICAL PROPERTIES
PHYSICAL STATE: gas
COLOR: colorless
ODOR: odorless
TASTE: acid taste
MOLECULAR WEIGHT: 44.01
MOLECULAR FORMULA: C-O2
BOILING POINT: Not available
FREEZING POINT: -71 F (-57 C) @ 4000 mmHg
SUBLIMATION POINT: -110 F (-79 C)
VAPOR PRESSURE: 43700 mmHg @ 21 C
VAPOR DENSITY (air=1): 1.5
SPECIFIC GRAVITY (water=1): 1.522 @ 21 C
WATER SOLUBILITY: soluble
PH: acidic in solution
VOLATILITY: Not applicable
ODOR THRESHOLD: Not available
EVAPORATION RATE: Not applicable
COEFFICIENT OF WATER/OIL DISTRIBUTION: Not applicable
SOLVENT SOLUBILITY:
Soluble: alcohol, acetone, hydrocarbons, organic solvents

SR.11.10343

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SECTION 10 STABILITY AND REACTIVITY


REACTIVITY: Stable at normal temperatures and pressure.
CONDITIONS TO AVOID: Protect from physical damage and heat.
Containers may rupture or explode if exposed to heat.
INCOMPATIBILITIES: combustible materials, oxidizing materials, metal salts, reducing agents, metal
carbide, metals, bases
CARBON DIOXIDE:
ACRYLALDEHYDE: Exothermic polymerization.
BARIUM PEROXIDE: Incandescent reaction.
CESIUM OXIDE: Ignition.
DIETHYL MAGNESIUM: Ignition.
ETHYLENEIMINE: Explosive polymerization.
HYDRAZINE: Decomposition.
METAL ACETYLIDES: Ignition or incandescence.
METAL HYDRIDES: Reduction reaction.
METALS: Dusts of many metals suspended in carbon dioxide atmospheres are ignitable and explosive;
some bulk metals will burn in the gas at elevated temperatures.
POTASSIUM: Mixtures of the solids are impact-sensitive.
POTASSIUM-SODIUM ALLOY: Mixtures of the solids are impact-sensitive.
SODIUM: Mixtures of the solids are impact-sensitive.
SODIUM PEROXIDE: Highly exothermic reaction; may be explosive in the presence of metals.
POLYMERIZATION: Will not polymerize.
SECTION 11 TOXICOLOGICAL INFORMATION
CARBON DIOXIDE, GAS:
TOXICITY DATA:
9 pph/5 minute(s) inhalation-human LCLo; 90000 ppm/5 minute(s)
inhalation-mammal LCLo; 10000 ppm/24 hour(s)-30 day(s) continuous
inhalation-rat TCLo; 27000 ppm/24 hour(s)-30 day(s) continuous
inhalation-rabbit TCLo.
ACUTE TOXICITY LEVEL: Insufficient Data.
MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE: heart or cardiovascular disorders, respiratory
disorders.
REPRODUCTIVE EFFECTS DATA:
6 pph inhalation-rat TCLo/24 hour(s) 10 day(s) pregnant female continuous;
6 pph inhalation-rat TCLo/24 hour(s) 10 day(s) pregnant female continuous;
55 pph inhalation-mouse TCLo/2 hour(s) 3 day(s) male; 55 pph
inhalation-mouse TCLo/4 hour(s) 6 day(s) male;
2 pph inhalation-mouse TCLo/8 hour(s) 10 day(s) pregnant female continuous;
13 pph inhalation-rabbit TCLo/4 hour(s) 9-12 day(s) pregnant female continuous.

SR.11.10343

99

HEALTH EFFECTS:
INHALATION:
ACUTE EXPOSURE:
CARBON DIOXIDE: In the solid or liquid form carbon dioxide is very volatile, readily releasing the gas. At
concentrations from 2-10% it may cause acidic taste, dyspnea, headache, vertigo, nausea, labored
breathing, weakness, drowsiness, mental confusion, and increase in blood pressure, pulse, and
respiratory rate. Exposure to 10% for a few minutes has been reported to cause visual disturbances,
tinnitus, tremors, profuse perspiration, restlessness, paresthesias, general feeling of
discomfort, loss of consciousness, and coma.
Concentrations of 25-30% may cause coma and convulsions within one minute. Tachycardia and
arrhythmias are possible. Concentrations of 50% may cause symptoms of hypocalcemia including
carpopedal spasms. Excessive carbon dioxide for a time period of not more than 5 minutes was
reported to cause effects on vision with constriction of visual fields, enlargement of blind spots,
photophobia, loss of convergence and accommodation, and deficient dark adaptation as well as
headache, insomnia, and personality changes, largely depression and irritability.
Even when there is sufficient oxygen present to prevent simple asphyxiation by carbon dioxide,
high concentrations may cause adverse effects by interfering with its normal
elimination from the body. Initially, exposure to increased carbon dioxide concentrations results in a
compensatory increase in both rate and depth of ventilation. Beyond a certain point, however, this
may reverse to hypoventilation resulting in respiratory acidosis. Death from asphyxia may occur if the
concentration and duration of exposure are sufficient. Reproductive effects have been reported in
animals.
CHRONIC EXPOSURE:
CARBON DIOXIDE: It has been reported that persons may tolerate 1.5% in inhaled air for prolonged
periods without adverse effects, but calcium/phosphorus metabolism may be affected with serum
levels of calcium and urinary phosphorus progressively falling.
At 2% concentration, deepened respiration may occur. At 3% impairment of performance has been
noted. It has, however, been demonstrated that the development of tolerance may occur during
prolonged exposure to low levels. Reproductive effects have been reported in animals.
SKIN CONTACT:
ACUTE EXPOSURE:
CARBON DIOXIDE: No adverse effects have been reported from exposure to the gas. Due to rapid
evaporation, the liquid or solid may cause frostbite with redness, tingling and pain or numbness. In
more severe cases, the skin may become hard and white and develop blisters.
CHRONIC EXPOSURE:
CARBON DIOXIDE: No adverse effects are expected from exposure at low levels.
EYE CONTACT:
ACUTE EXPOSURE:
CARBON DIOXIDE: At high concentrations in air, carbon dioxide may cause a stinging sensation of the
eyes. 200,000 ppm of the gas may cause irritation. Due to rapid evaporation, the liquid or solid may
cause frostbite with redness, pain, and blurred vision.

SR.11.10343

100

CHRONIC EXPOSURE:
CARBON DIOXIDE: No adverse effects are expected from exposure to low levels.
INGESTION:
ACUTE EXPOSURE:
CARBON DIOXIDE: Ingestion of a gas is unlikely. If the liquid or solid is swallowed, frostbite damage to
the lips, mouth and mucous membranes may occur.
CHRONIC EXPOSURE:
CARBON DIOXIDE: No data available.
SECTION 12 ECOLOGICAL INFORMATION
ECOTOXICITY DATA:
FISH TOXICITY: 150000 ug/L 48 day(s) (Mortality) Brown trout (Salmo trutta).
SECTION 13 DISPOSAL CONSIDERATIONS
Dispose in accordance with all applicable regulations.
SECTION 14 TRANSPORT INFORMATION
U.S. DOT 49 CFR 172.101 SHIPPING NAME-UN NUMBER: Carbon dioxide-UN1013
U.S. DOT 49 CFR 172.101 HAZARD CLASS OR DIVISION: 2.2
U.S. DOT 49 CFR 172.101 AND SUBPART E LABELING REQUIREMENTS:
NONFLAMMABLE GAS
U.S. DOT 49 CFR 172.101 PACKAGING AUTHORIZATIONS:
EXCEPTIONS: 49 CFR 173.306
NON-BULK PACKAGING: 49 CFR 173.302, 304
BULK PACKAGING: 49 CFR 173.302, 314, 315
U.S. DOT 49 CFR 172.101 QUANTITY LIMITATIONS:
PASSENGER AIRCRAFT OR RAILCAR: 75 kg
CARGO AIRCRAFT ONLY: 150 kg
SECTION 15 REGULATORY INFORMATION
U.S. REGULATIONS:
TSCA INVENTORY STATUS: Y
TSCA 12(b) EXPORT NOTIFICATION: Not listed.
CERCLA SECTION 103 (40CFR302.4): N
SARA SECTION 302 (40CFR355.30): N

SR.11.10343

101

SARA SECTION 304 (40CFR355.40): N


SARA SECTION 313 (40CFR372.65): N
SARA HAZARD CATEGORIES, SARA SECTIONS 311/312 (40CFR370.21):
ACUTE: Y
CHRONIC: N
FIRE: N
REACTIVE: N
SUDDEN RELEASE: Y
OSHA PROCESS SAFETY (29CFR1910.119): N
STATE REGULATIONS:
CALIFORNIA PROPOSITION 65: N
EUROPEAN REGULATIONS:
EC NUMBER (EINECS): 204-696-9

SR.11.10343

102

Bibliographic Information

Report Number

: SR.11.10343

Title

: QUEST CO2 Capture Project - Amine Unit

Subtitle

: Basic Design Package

Author(s)

: R. Rangi
A. Joura

PTU/TDUA
PTU/TDUA

Contributor(s)

: B. Kruelskie

PTD/TDSA

Reviewed by

: P. Nasir

PTU/TDUA

Approved by

: P. Nasir

PTU/TDUA

Content Owner

: P. Nasir

PTU/TDUA

Issue Date

: February 2011

Activity Code

: ZZPT/010252/010104

Project Number

: ZZPT/010252/010104

Sponsor

: Shell Canada Limited, Anita Spence

Keywords

: Amine, MDEA, ADIP-X, Carbon Dioxide, CO2 capture

Electronic file

: SR.11.10343.pdf

Issuing Company

: Shell International Exploration and Production Inc.,


Woodcreek, 200 North Dairy Ashford,
Houston, Texas 77079-1197
Tel. +1 281 544 6251

SR.11.10343

103

Report distribution
Outside Shell Global Solutions
Company name and address

E or P

No. of
paper
copies

Shell Canada Ltd.


400 4th Avenue SW
Calgary, Alberta T2P 2H5
Attn: Mr. Manoj Dharwadkar

E and P

Shell Canada Ltd.


400 4th Avenue SW
Calgary, Alberta T2P 2H5
Attn: Jeffrey Leontowich

E and P

Shell Canada Ltd.


400 4th Avenue SW
Calgary, Alberta T2P 2H5
Attn: Anita Spence

Within Shell Global Solutions


Name

Ref. Ind.

Location

E or P

No. of
paper
copies

R. Rangi

SIEPPTU/TDUA

HOU-WTC R-2180

E and P

A. Joura

GSUSIPTU/TDUA

HOU-WTC R-2140

E and P

B. Kruelskie

GSUSIPTD/TDSA

HOU-WTC T-2171

P. Nasir

SIEPPTU/TDUA

HOU-WTC R-2150

Petro-Chemical Knowledge Center, Westhollow Technology Center 3333


Highway 6 South, PO Box 1380 Houston, Texas 77082

E and P

Shell International Exploration and Production Inc., Woodcreek, 200


North Dairy Ashford, Houston, Texas 77079-1197

E and P

This report can be freely shared with all Shell Global Solutions employees.

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