SEMESTER IV

Theory:
1. AM2202A: Mathematical Methods

It gives idea of differential equations, integral transforms and their application,

complex variable and probability and statistics. More generally it describes us
about Bessel functions, Legendre and Hermite polynomials, Laplace
transformation, Fourier transformation, conformal mapping, Laplace equation in
Cartesian and polar forms, probability distributions and their application.

2. EE2202A: Electrical Engineering

This course incorporates a brief discussion about electrical circuits, electrical

machines, distribution of power and electrical measurement instruments. It
basically discusses the circuit solving techniques, transformer, DC machines,
induction and synchronous machines, tariff calculation, energy meter, ammeter,
wattmeter and voltmeter.

3. CH2201: Physico-Chemical Principles

This course includes phase stability, simple mixtures, ionic equilibria, electrokinetic phenomena, colloids, adsorption and spectroscopy. These topics help in
understanding different phase equilibria, partial molar quantities,
electrochemical cells, chromatography, NMR spectroscopy and Raman
spectroscopy.

4. CH2202: Fluid Particle Mechanics & Mechanical Operations

This course has been designed for giving insight of different characteristics of
solid particles like shape, size, size reduction, separation, handling etc. In detail it
discusses about screening, crushing, sedimentation, thickeners, flow through
porous media, fluidization, flow through packed bed, solid storage and transport
and mixing of solids and pastes.

5. CH2203: Mass Transfer Operations- I

This is an introductory course for mass transfer which basically discusses about
molecular and eddy diffusion, interphase mass transfer, gas-liquid contactors,
gas absorption and stripping, humidification and dehumidification, drying and
crystallisation.

6. CH2204: Heat Transfer Operations

It describes about mechanism of heat transfer like conduction, convection and

radiation, heat transfer with phase change (condensation, boiling, reboilers and
vaporisers), heat exchangers and evaporators.

Practical:
7. EE2402A: Electrical Engineering Laboratory

(i) Measurement of internal resistance of voltmeter: In this experiment we

calculated internal resistance by measuring the current and voltage (dc).

(ii) Open and short circuit test: These two tests are performed on a transformer
to determine (a) equivalent circuit of transformer (b) voltage regulation of
transformer (c) efficiency of transformer.
(iii) Verification of maximum power transfer theorem: In this experiment current
voltages are calculated for different values of impedance and plotted.
(iv) Load test on a single phase transformer: The experiment is performed & seen
that as load current increases voltage drop in transformer winding is also
increases, voltage and hence voltage regulation is increased. Also we increase
the load current the efficiency is also increase up to certain limit after this
efficiency decreases with increase load current
(v) Study of the characteristics of a separately excited DC generator: In
a separately excited DC generator, the field winding is excited by an external
independent source.
(vi) Study of the characteristics of a DC motor: There are two types of characteristics:
speed v/s load characteristics and torque v/s load characteristics

(vii) Study of methods of speed control of DC motor: Speed control of dc series

motor can be done either by armature control or by field control.
(viii) Study of the characteristics of a compound DC generator: This type of
generators can be used as either long shunt or short shunt compound wound
generators.
(ix) Measurement of speed of DC series motor as a function of load torque: Since
the torque produced by the motor is proportional to the product of the armature
current and the magnetic field in the armature, the series motor under heavy
load at low speed will produce a very large amount of torque. Thus the series
motor is very useful for starting large, high-inertia loads.
(x) Three phase power measurement by two wattmeter method: This method
enables the user to utilise the third phase of a 3 phase power analyser for a DC
bus for example, yet the user is still able to make 3 phase measurements with
only the first two channels of the power analyser .
(xi) R-L-C circuit: We observed the relationships between the voltage and current
across resistors, inductors, and capacitors in series combinations as the
frequency of the source was varied and resonance in the R-L-C circuit.
(xii) Star and delta connection: It helps in validating the theoretical correlation.

8. CH2401: Chemical & Instrumental Analysis Laboratory

(i) To determine the available chlorine in Bleaching powder by iodometric

titration method
(ii) To determine the the Vitamin C in Vitamin C tablet by iodometric titration
method
(iii) To determine the amount of nitrite in waste water by Spectrophometric
method

(iv) To determine the amount of sulphate in sample by naphelometric method

(v) To determine the percentage of manganese dioxide in Pyrolusite by redox
titration method
(vi) To determine the percentage of sodium hydroxide and sodium carbonate in
the commercial caustic soda by Acid-Base titration method
(vii) To determine the amount of dissolved oxygen in waste water by iodometric
titration method
(viii) To determine the total, temporary (carbonate) and permanent (noncarbonates) hardness of water by complexometric titration (EDTA) method
(ix) To determine the amount of glucose in the given sample by Dinitrosalicylic
acid reagent (DNS) method
(x) To determine the point of zero charge of activated charcoal by solid activation
method
9. CH2402: Fluid Flow & Mechanical Operations Laboratory
1. (a) Orifice meter: We drew a calibration curve for the orifice meter, Cd vs. Re
and calibrated the Rotameter.
(b) Venturimeter: We drew a calibration curve for the venturimeter, Cd vs. Re
and calibrated the venturimeter.
2. Frictional loss for flow through straight pipe fittings: We determined the
equivalent lengths for different pipe fittings and plotted f vs. Re for straight
pipes.
3. Characteristics of Centrifugal Pump: We plotted the following characteristics of
the centrifugal pipe head vs. discharge, input power vs. discharge and pump
efficiency vs. discharge
4. (a) Water Fluidized Bed: We plotted P and Void fraction vs. superficial
velocity, determined the minimum fluidization velocity and compared with
standard value. Also we determine the free settling velocity.
(b) Air fluidized bed: We plotted P and Void fraction vs. superficial velocity. Also
we determined the minimum fluidization velocity and compared with standard
value.
5. Jar Mill: We plotted cumulative mass fraction vs. log of particle size,
determined the overall energy efficiency and theoretical effectiveness of Jar mill.
6. Screen Analysis: We performed and reported the screen analysis for the given
sample and plotted log-log graph of mass fraction vs. avg. particle diameter and
cumulative mass fraction vs. screen aperture. Also we calculated Specific
surface, mean surface diameter and Mean volume diameter.

7. Plate and Frame Filter: For the Plate and frame filter press we determined filter
medium resistance and specific cake resistance for constant pressure runs. Also
we determine optimum filtration time.
8. Sparkler Filter: For the Sparkler filter press we determined filter medium
resistance and specific cake resistance for constant pressure runs.
9. Sweatland Filter: For the sweatland filter press we determined filter medium
resistance and specific cake resistance for constant pressure/ Volume runs.
10. (a) Sedimentation: We studied the sedimentation of the given sample and
showed the different zones of settling and calculated the terminal velocity of the
particles.
(b) Reynolds Experiments: Through visual observation of laminar and turbulent
flow, we determined the lower and upper critical Reynolds number.
SEMESTER V

Theory:
1. CH3101: Process Instrumentation
This course has incorporated the discussions about the process variables,
process instrumentation diagrams and symbols, static and dynamic
characteristics of instruments, signal transmission, converter, transducers, data
acquisition system etc. Beside these it also discusses about the principles,
construction
of
instruments
for
the
measurement,
transmission,
control/indication/ recording of process variables, final control element, and
transducer.
2. CH3102: Process Dynamics and Control
In this course, there is an account of basic theory underlying the various
processes in transient and different types of controllers. It also discusses about
various stability criteria and the design of controllers based on different models.
3. CH3103: Energy Resources and Utilization
It discusses different types of fuels (solid, liquid and gaseous), nuclear energy,
hydrogen production and storage, solar, wind, tidal and geothermal energies. It
also includes energy conservation, energy audits and several environmental
issues.
4. CH3104: Chemical Reaction Engineering I
This course includes the analyses of batch reactor and flow reactors. It also
discusses about non-isothermal operation, non-ideal flow and corresponding
models.
5. CH3105: Chemical Technology I

It comprises the discussion of different industrial products as industrial gases

(H2, O2, N2 and Inert gases), sulphur chemicals, fertilisers, marine chemicals,
chlor alkalis, ceramics, industrial carbon and inorganic pigments. It
simultaneously discusses about various advances and challenges related to that
industry.
6. CH3106: Mass Transfer Operations II
Mass Transfer-II gives insight of various separation processes as distillation,
leaching, liquid-liquid extraction, adsorption and ion-exchange. It also gives
details of equipments of these processes.

Practicals:
7. CH3301: Heat Transfer Laboratory
(i) Double pipe heat exchanger: In this experiment we need to calculate the
overall heat transfer coefficient both clean and dirt.
(ii) Shell and tube heat exchanger: In this experiment we need to calculate the
overall heat transfer coefficient both clean and dirt.
(iii) Single effect evaporator: In this experiment we need to calculate overall heat
transfer coefficient for condenser and evaporator.
(iv) Open pan evaporator: In this experiment we need to calculate the overall
heat transfer coefficient of it.
(v) U-tube heat exchanger: In this experiment we need to calculate the overall
heat transfer coefficient of it.
(vi) Coil heater: In this experiment we need to calculate the overall heat transfer
coefficient of it.
8. CH3302-Energy Resources Laboratory
(i) Determination of calorific value by Bomb method: In this experiment we need
to calculate calorific value of an oil sample.
(ii) Proximate analysis of coal: In this experiment we need to calculate moisture
content, ash content, fixed carbon content and volatile matter.
(iii) Determination of water content of oil sample by Dean Stark method: In this
experiment with the help of distillation we separate water and oil and measured
the impurity.
(iv) Determination of Reid vapour pressure of an oil sample: In this experiment
vapour pressure was calculated with the help of standard instrument.
(v) Determination of kinematic viscosity by Redwood viscometer No.-1: Viscosity
of low viscous sample was calculated by measuring the time taken to empty the
vessel.

(vi) Determination of carbon residue of given oil sample by Rams Bottom

Apparatus: The remained carbon was calculated by burning in the apparatus.
(vii) Evaluation of UL , FR , and in thermosymphonic mode of flow with fixed
input parameters using solar flat plate collector: In this experiment water was
heated with help of halogens and temperature was noted down to calculate the
above mentioned parameters.
(viii) Flash point and fire point: An oil sample was heated and flame was
introduced and thus the fire and flash point was calculated.
(ix) ASTM Distillation: An oil sample was heated in flask and the vapour was
condensed. At every 5ml of distillate temperature was measured.
(x) Cloud point and pour point: Oil sample was cooled with the help of ice and the
temperature was noted when cloudiness formed. Further it was cooled until
waxes gets forms.
9. CH3303-Mass Transfer laboratory
(i) Solubility of Ternary Liquid System: In this experiment we calculated the
solubility and drawn triangular and rectangular diagrams.
(ii) Equilibrium and tie-line data for Ternary Liquid System: In this experiment tielines compostions were found.
(iii) Vapour Liquid Equilibrium: In this experiment vapour composition and residue
composition was calculated with help of refractometer.
(iv) Solubility of Organic Compound: The solubility was found out by mixing and
then titrating the mixture.
(v) Packed Distillation Column: The HETP was calculated with help of distillate
and residue composition
(vi) Batch Distillation-Verification of Rayleigh Law: In this experiment we did
batch distillation of a mixture and found the moles of distillate and residue
theoretically and experimentally.
(vii) Steam Distillation: In this experiment a high boiling point liquid was
evaporated with the help of carrier steam.
(viii) Drying Characteristics: Samples were dried and the drying rate was
calculated.