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  • Cicac Informe CNEA316

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    gustavoesanchez
    9 tayangan10 halaman
    Preparatíon of Glutaraldehyde l,5 14 C Glutaraldehyde 1,5 14 C was prepared from 14 CNK. The method includes the following steps: a} preparation of glutaronitrile 1,5 14 C by means of the reaction of 14CNK with 1,3-dibromopropane; b) glutaric acid 1,5 14C was ob­ tained by hidrolysis of glutaronitrile; c) glutaric acid was con verted into glutaryl chloride 1,5 14 C with thionyl bromide, and d) glutaraldehyde 1,5 1•c was obtained by hídrogenation of glutaryl chloride 1,5 14C. Glutaraldehyde 1,5 14C was controlled by infrared spectrum and X-ray diffaction of the 2,4-dinitrophenylhydrazone.

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    Preparatíon of Glutaraldehyde l,5 14 C Glutaraldehyde 1,5 14 C was prepared from 14 CNK. The method includes the following steps: a} preparation of glutaronitrile 1,5 14 C by means of the reaction of 14CNK with 1,3-dibromopropane; b) glutaric acid 1,5 14C was ob­ tained by hidrolysis of glutaronitrile; c) glutaric acid was con verted into glutaryl chloride 1,5 14 C with thionyl bromide, and d) glutaraldehyde 1,5 1•c was obtained by hídrogenation of glutaryl chloride 1,5 14C. Glutaraldehyde 1,5 14C was controlled by infrared spectrum and X-ray diffaction of the 2,4-dinitrophenylhydrazone.

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    9 tayangan10 halaman

    Cicac Informe CNEA316

    Diunggah oleh

    gustavoesanchez
    Preparatíon of Glutaraldehyde l,5 14 C Glutaraldehyde 1,5 14 C was prepared from 14 CNK. The method includes the following steps: a} preparation of glutaronitrile 1,5 14 C by means of the reaction of 14CNK with 1,3-dibromopropane; b) glutaric acid 1,5 14C was ob­ tained by hidrolysis of glutaronitrile; c) glutaric acid was con verted into glutaryl chloride 1,5 14 C with thionyl bromide, and d) glutaraldehyde 1,5 1•c was obtained by hídrogenation of glutaryl chloride 1,5 14C. Glutaraldehyde 1,5 14C was controlled by infrared spectrum and X-ray diffaction of the 2,4-dinitrophenylhydrazone.

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    © All Rights Reserved
    Unduh sebagai PDF, TXT atau baca online dari Scribd
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    dari 10

    http://www2.cnea.gov.ar/cac/ci/CICACInformes/cicacInformeCNEA316.

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