Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
1 +, 1 +
01 ' 5
Jawaharlal Nehru
! $ ' +-
Satyanarayan Gangaram Pitroda
! > 0 B
BharthariNtiatakam
IS: 144s[P:30]-I970
A&d. 28 lkrradrr 1970
Indian Standard
( Reaffirmed 2003 )
First Revision)
UDC
665.5 : 543.86
Designation 0473-65
and IP
in crude
OF THE MElTIOD
2.1 The sample is taken in a refractory thimble and is extracted with hot
toluene until the residue reaches constant weight.
The weight of residue,
calculated in percent is reported as sediment by extraction .
3. APPARATUS
A wide-mouthed
the following
parts assembled
as
43 1
INDIAN
STANDARDS
6EuB
BNiADUR
Z&PAP
INSTITUTION
MAttO,
NRW
DELHI
IlOO@
August 1971
The coil shall be formed of metal or alloy tubing having an outside diameter of 8 mm and wall thickness of 1.5 mm and composed of tin or tincoated copper or brass.
The tin-coating
shall have a minimum-thickness
of 0.075 mm.
The exposed surface of the coil for cooling purposes is
about 115 sq cm.
EXTRACTION
FIG. 1
Fra.
EXTRACTION
APPARATUS
SHOWING
2
WATERCUP IN POSITION
1970
CAUTION:
Toluene is toxic. Take precautions
toluene vapours ( see also IS : 4644-1968:
).
to avoid breathinK
5. PROCEDURE
5.1 Before using a new thimble, rub its outer surface with fine sandpaper
and remove all loosened material with a stiff brush. Give thimble a
preliminary extraction with toluene allowing the solvent to drip from the
thimble for at least one hour. Then dry the thimble for one hour at a
for to&e,
I970
AND
for
the
the
two
REPORTING
6.1 Calculate
7.1 Results
of duplicate
tests shall
than
the following
amounts:
Repeatability
Rqkducibility
O-017 + O-2554
0.033 + 0.255A
where
A = average
result in percent
weight.
4
Printed. at Offset Printing Centre, New Delhi, India