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Data Series Information

Name: o1
Number of Intervals: 1
Application: RHEOPLUS/32 V3.61 21005948-33024
Device: MCR52 SN81069040; FW3.65; Slot(3,-1); Adj(612,0)d
Measuring Date/Time: 1/27/2014; 3:25 PM
Measuring System: DG35.12/PR; d=60 mm
Accessories: TU1=C-LTD180-SN81018062; ADV1=PA-23S/400bar

Interval: 1
Number of Data Points: 25

Time Setting: 25 Meas. Pts., Reset Strain


Meas. Pt. Duration 5 s
Measuring Profile:
Shear Rate d(gamma)/dt = 1 ... 6,000 1/s log

Meas. Pts. Shear RateShear StresPressure Pressure TemperaturViscosity Speed


[1/s] [Pa] [bar] [psi] [C] [Pas] [1/min]
1 0.99 1.47 1.86 27 25.8 1.49 0.232
2 1.44 1.34 1.86 27 25.8 0.931 0.336
3 2.06 1.32 1.86 27 25.8 0.642 0.481
4 2.96 1.32 1.86 27 25.8 0.447 0.693
5 4.23 1.52 1.86 27 25.8 0.359 0.989
6 6.11 1.73 1.86 27 25.8 0.283 1.43
7 8.83 1.76 1.86 27 25.8 0.199 2.07
8 12.6 1.99 1.86 27 25.9 0.157 2.95
9 18.2 2.49 1.86 27 25.9 0.137 4.25
10 26.2 2.51 1.86 27 25.9 0.0958 6.12
11 37.5 2.82 1.87 27.1 25.9 0.0751 8.77
12 53.9 3.06 1.85 26.9 25.9 0.0568 12.6
13 77.5 3.27 1.86 26.9 25.9 0.0422 18.1
14 111 3.68 1.86 27 25.9 0.0331 26
15 160 4.09 1.86 27 25.9 0.0255 37.4
16 230 4.69 1.86 27 25.9 0.0204 53.8
17 330 5.69 1.86 27 25.9 0.0172 77.2
18 474 6.67 1.86 27 25.9 0.0141 111
19 682 7.99 1.86 27 25.9 0.0117 159
20 980 9.67 1.87 27.1 25.9 0.00987 229
21 1,410 12.2 1.87 27.1 25.9 0.00868 329
22 2,020 15.4 1.86 27 25.9 0.00762 473
23 2,910 21.5 1.86 27 25.9 0.00742 680
24 4,180 34.6 1.86 27 25.9 0.0083 977
25 5,130 44.6 1.86 26.9 25.9 0.0087 1,200
ETA, TAU - LOG

10 1

Pas

1 P

0.1 1

0.01

0.001 1
1 10 100 1,000 1/s 10,00
.
Shear Rate
Torque Status
[Nm] []
353 Dy_accu
320 Dy_accu
316 Dy_accu
318 Dy_accu
364 Dy_accu
415 Dy_accu
421 Dy_accu
476 Dy_accu
597 Dy_accu
601 Dy_accu
675 Dy_accu
734 Dy_accu
783 Dy_accu
883 Dy_accu
980 Dy_accu
1,120 Dy_accu
1,360 Dy_accu
1,600 Dy_accu
1,920 Dy_accu
2,320 Dy_accu
2,930 Dy_accu
3,700 Dy_accu
5,170 Dy_accu
8,310 Dy_accu
10,700 n+ ,WMa
ETA, TAU - LOG

100

Pa

o1

DG35.12/PR; d=60 mm
10
Viscosity

Shear Stress

1
1,000 1/s 10,000
CSD

1 0
10 10

Pa

G' 0
10 Pa

G''

-1 -1
10 10
10 % 100
Strain
Anton Paar GmbH

Data Series Information


Name:
Number of Intervals:
Application:
Device:
Measuring Date/Time:
Measuring System:
Accessories:
Calculating Constants:
- Csr [min/s]:
- Css [Pa/mNm]:
- Start Delay Time [s]:
- Substance Density [rho]:
- Measurement Type:
- Axial Compliance [m/N]:
- Position [m]:

Interval:
Number of Data Points:

Time Setting:

Measuring Profile:
#NAME?

Meas. Pts. Strain


[%]
1 19.9
2 17.4
3 18.2
4 18.4
5 19
6 19.8
7 19.3
8 19.5
9 19.8
10 19.8
11 19.6
12 19.4
13 19.8
14 19.4
15 19.2
16 18.9
17 19.2
18 19.5
19 20.3
20 20.4
21 21.4
22 31.7
23 46.5
24 68.2
25 100
0
10

71

DG35.12/PR; d=60 mm

G' Storage Modulus


Pa
G'' Loss Modulus

Shear Stress

-1
10
100

Information
71
1
RHEOPLUS/32 V3.61 21005948-33024
MCR52 SN81069040; FW3.65; Slot(3,-1); Adj(612,0)d
Date/Time: 1/27/2014; 3:43 PM
DG35.12/PR; d=60 mm
TU1=C-LTD180-SN81018062; ADV1=PA-23S/400bar
Constants:
4.274725
4.169975
y Time [s]: 9.972
Density [rho]: 1,000
7
pliance [m/N]: 1.00E-06
1.00E-06

1
Data Points: 25

25 Meas. Pts.
Meas. Pt. Duration 5 s

Amplitude gamma = 0.01 ... 100 % log


Angular Frequency omega = 10 rad/s

Shear StresStorage MoLoss ModulDamping FaDeflection Torque Status


[Pa] [Pa] [Pa] [1] [mrad] [Nm] []
3.30E-01 1.17E+00 1.18E+00 1.01 4.88 79.1 M- ,WE-
3.00E-01 1.19E+00 1.26E+00 1.06 4.25 71.9 M- ,WE-
2.97E-01 1.16E+00 1.14E+00 0.981 4.47 71.2 M- ,WE-
3.07E-01 1.20E+00 1.16E+00 0.969 4.5 73.6 M- ,WE-
3.09E-01 1.18E+00 1.11E+00 0.939 4.66 74 M- ,WE-
3.19E-01 1.17E+00 1.10E+00 0.938 4.85 76.5 M- ,WE-
3.14E-01 1.21E+00 1.08E+00 0.896 4.74 75.2 M- ,WE-
3.17E-01 1.19E+00 1.11E+00 0.934 4.77 75.9 M- ,WE-
3.22E-01 1.21E+00 1.09E+00 0.903 4.85 77.2 M- ,WE-
3.19E-01 1.21E+00 1.07E+00 0.88 4.84 76.6 M- ,WE-
3.17E-01 1.21E+00 1.07E+00 0.882 4.79 76 M- ,WE-
3.18E-01 1.22E+00 1.09E+00 0.891 4.76 76.4 M- ,WE-
3.27E-01 1.24E+00 1.09E+00 0.874 4.85 78.5 M- ,WE-
3.24E-01 1.25E+00 1.10E+00 0.882 4.76 77.7 M- ,WE-
3.23E-01 1.27E+00 1.10E+00 0.87 4.7 77.4 M- ,WE-
3.22E-01 1.29E+00 1.11E+00 0.864 4.63 77.2 M- ,WE-
3.26E-01 1.28E+00 1.11E+00 0.863 4.71 78.2 M- ,WE-
3.25E-01 1.27E+00 1.09E+00 0.858 4.77 78 M- ,WE-
3.38E-01 1.26E+00 1.09E+00 0.864 4.97 81 M- ,WE-
3.48E-01 1.30E+00 1.10E+00 0.848 5 83.4 M- ,WE-
3.60E-01 1.27E+00 1.10E+00 0.863 5.25 86.3 M- ,WMa
4.24E-01 8.43E-01 1.04E+00 1.23 7.76 102 M- ,WMa
4.58E-01 4.44E-01 8.79E-01 1.98 11.4 110 M-
5.36E-01 1.37E-01 7.75E-01 5.66 16.7 129 M-
6.93E-01 0 6.93E-01 ### 24.5 166 M- ,ME-
CSD

1 0
10 10

Pa

G' 0
10 Pa

G''

-1 -1
10 10
10 % 100
Strain
Anton Paar GmbH

Data Series Information


Name: 41
Number of Intervals: 1
Application: RHEOPLUS/32 V3.61 2100
Device: MCR52 SN81069040; FW3
Measuring Date/Time: 1/27/2014; 3:56 PM
Measuring System: DG35.12/PR; d=60 mm
Accessories: TU1=C-LTD180-SN810180
Calculating Constants:
- Csr [min/s]: 4.274725
- Css [Pa/mNm]: 4.169975
- Start Delay Time [s]: 9.004
- Substance Density [rho]: 1,000
- Measurement Type: 7
- Axial Compliance [m/N]: 1.00E-06
- Position [m]: 1.00E-06

Interval: 1
Number of Data Points: 25

Time Setting: 25 Meas. Pts.


Meas. Pt. Duration 5 s
Measuring Profile:
#NAME? Amplitude gamma = 0.01
Angular Frequency omega

Meas. Pts. Strain Shear StresStorage Mo


[%] [Pa] [Pa]
1 32.2 3.03E-01 0
2 31.5 2.81E-01 0
3 32.8 2.86E-01 0
4 32.1 2.78E-01 0
5 32.4 2.76E-01 0
6 32.6 2.74E-01 0
7 32.5 2.74E-01 0
8 32.6 2.73E-01 0
9 32.1 2.70E-01 0
10 30.6 2.66E-01 0
11 31.6 2.63E-01 0
12 31.3 2.61E-01 0
13 31.5 2.63E-01 0
14 11.8 1.53E-01 3.09E-01
15 32 2.68E-01 0
16 31.2 2.61E-01 0
17 31.9 2.62E-01 0
18 32.1 2.63E-01 0
19 35.5 2.87E-01 0
20 37 2.95E-01 0
21 36.7 2.95E-01 0
22 36 2.88E-01 0
23 46.4 3.81E-01 0
24 68.1 6.46E-01 0
25 100 9.94E-01 0
0
10

41

DG35.12/PR; d=60 mm

G' Storage Modulus


Pa
G'' Loss Modulus

Shear Stress

-1
10
100

HEOPLUS/32 V3.61 21005948-33024


MCR52 SN81069040; FW3.65; Slot(3,-1); Adj(612,0)d
/27/2014; 3:56 PM
G35.12/PR; d=60 mm
U1=C-LTD180-SN81018062; ADV1=PA-23S/400bar
5 Meas. Pts.
Meas. Pt. Duration 5 s

mplitude gamma = 0.01 ... 100 % log


ngular Frequency omega = 10 rad/s

Loss ModulDamping FaDeflection Torque Status


[Pa] [1] [mrad] [Nm] []
9.41E-01 ### 7.88 72.6 M- ,WE-
8.93E-01 ### 7.71 67.4 M- ,WE-
8.74E-01 ### 8.03 68.7 M- ,WE-
8.66E-01 ### 7.86 66.6 M- ,WE-
8.52E-01 ### 7.94 66.2 M- ,WE-
8.42E-01 ### 7.98 65.8 M- ,WE-
8.44E-01 ### 7.96 65.8 M- ,WE-
8.36E-01 ### 8 65.5 M- ,WE-
8.41E-01 ### 7.87 64.8 M- ,WE-
8.69E-01 ### 7.49 63.7 M- ,WE-
8.32E-01 ### 7.74 63 M- ,WE-
8.34E-01 ### 7.66 62.5 M- ,WE-
8.33E-01 ### 7.72 63 M- ,WE-
1.26E+00 4.1 2.89 36.8 M- ,WE-
8.37E-01 ### 7.83 64.2 M- ,WE-
8.37E-01 ### 7.64 62.6 M- ,WE-
8.22E-01 ### 7.8 62.8 M- ,WE-
8.20E-01 ### 7.86 63.1 M- ,WE-
8.10E-01 ### 8.69 68.9 M- ,WE-
7.98E-01 ### 9.07 70.8 M- ,WE-
8.02E-01 ### 9 70.7 M- ,WE-
8.00E-01 ### 8.83 69.1 M- ,WE-
8.21E-01 ### 11.4 91.4 M- ,ME-
9.49E-01 ### 16.7 155 M- ,ME-
9.93E-01 ### 24.5 238 M- ,ME-
ETA, TAU - LOG

0.6 100

Pas

0.5 Pa

0.45

0.4 10

0.35

0.3

0.25

0.2 1

0.15

0.1

0.05

0 0.1
1 10 100 1,000 1/s 10,000
.
Shear Rate

Data Series Information


Name:
Number of Intervals:
Application:
Device:
Measuring Date/Time:
Measuring System:
Accessories:

Interval:
Number of Data Points:

Time Setting:

Measuring Profile:
Shear Rate

Meas. Pts. Shear RateShear Stres


[1/s] [Pa]
1 1.06 0.538
2 1.48 0.33
3 2.1 0.328
4 2.96 0.554
5 4.25 0.832
6 6.13 1.16
7 8.85 1.57
8 12.7 1.32
9 18.2 0.925
10 26.2 0.927
11 37.5 0.984
12 53.9 1.18
13 77.5 1.27
14 111 1.36
15 160 1.47
16 230 1.63
17 330 1.97
18 474 2.48
19 682 3.11
20 980 4.01
21 1,410 5.28
22 2,020 7.82
23 2,910 12.3
24 4,180 19.5
25 5,130 24.7
TAU - LOG

100

Pa

10
11

DG35.12/PR; d=60 mm

Viscosity

Shear Stress

0.1
000 1/s 10,000

11
1
RHEOPLUS/32 V3.61 21005948-33024
MCR52 SN81069040; FW3.65; Slot(3,-1); Adj(612,0)d
1/27/2014; 3:50 PM
DG35.12/PR; d=60 mm
TU1=C-LTD180-SN81018062; ADV1=PA-23S/400bar

1
25

25 Meas. Pts., Reset Strain


Meas. Pt. Duration 5 s

d(gamma)/dt = 1 ... 6,000 1/s log

Viscosity Speed Torque Status


[Pas] [1/min] [Nm] []
0.509 0.247 129 M- ,Dy_
0.222 0.347 79.1 M- ,Dy_
0.156 0.491 78.7 M- ,Dy_
0.187 0.692 133 M- ,Dy_
0.196 0.994 200 M- ,Dy_
0.19 1.43 279 Dy_accu
0.178 2.07 377 Dy_accu
0.104 2.96 317 Dy_accu
0.0509 4.25 222 M- ,Dy_
0.0354 6.12 222 M- ,Dy_
0.0262 8.77 236 M- ,Dy_
0.0218 12.6 282 Dy_accu
0.0164 18.1 304 Dy_accu
0.0122 26 326 Dy_accu
0.00921 37.4 353 Dy_accu
0.00709 53.8 391 Dy_accu
0.00596 77.2 472 Dy_accu
0.00522 111 594 Dy_accu
0.00456 159 746 Dy_accu
0.0041 229 962 Dy_accu
0.00375 329 1,270 Dy_accu
0.00387 473 1,880 Dy_accu
0.00424 680 2,950 Dy_accu
0.00468 977 4,680 Dy_accu
0.00481 1,200 5,910 n+ ,WMa