PROPOSAL TESIS

Program Studi Magister

Jurusan Teknik Material dan Metalurgi
FTI - ITS
DAFTAR ISI

LEMBAR JUDUL........................................................................................... i
LEMBAR PENGESAHAN............................................................................. iii
ABSTRAK........................................................................................................v
ABSTRACT..................................................................................................... vii
DAFTAR ISI.................................................................................................... ix
DAFTAR GAMBAR....................................................................................... xi
DAFTAR TABEL........................................................................................... xiii

BAB 1 PENDAHULUAN................................................................................ 1
1.1 Latar Belakang Masalah................................................................. 1
1.2 Perumusan Masalah........................................................................ 2
1.3 Batasan Masalah............................................................................. 2
1.4 Tujuan Penelitian............................................................................ 3
1.5 Manfaat Penelitian.......................................................................... 3

BAB 2 TINJAUAN PUSTAKA....................................................................... 5

2.1 Baterai............................................................................................. 5
2.2 Jenis-jenis Baterai/sel..................................................................... 6
2.3Dasar-dasar Elektrokimia.................................................................9
2.3.1 Prinsip Mekanisme Reaksi Baterai Ion Lithium...................9
2.3.2 Sifat-sifat Dasar Elektroda....................................................11
2.4 Sifat-sifat Dasar Baterai.................................................................. 14
2.5 Material untuk Katoda.................................................................... 14
2.5.1 Katoda LiV3O8...................................................................... 15
2.6 Elektrolit......................................................................................... 16
2.7 Separator......................................................................................... 17
2.8 Carbamide/Urea............................................................................. 19
2.9 Proses Hidrotermal......................................................................... 19
2.10 Proses Kalsinasi................,........................................................... 20

ix
PROPOSAL TESIS
Program Studi Magister
Jurusan Teknik Material dan Metalurgi
FTI - ITS
2.11 Hasil Penelitian Sebelumnya........................................................ 21

BAB 3 METODE PENELITIAN......................................................................27

3.1 Diagram Alir Penelitian.................................................................. 27
3.2 Bahan Penelitian............................................................................. 28
3.3 Peralatan dan Pengujian.................................................................. 30
3.4 Metode Penelitian........................................................................... 30
3.4.1 Sintesis LiV3O8..................................................................... 30
3.4.2 Proses Kalsinasi.................................................................... 30
3.5 Pengujian Karakterisasi Material.................................................... 30
3.5.1 Scanning Electron Microscope (SEM)................................ 30
3.5.2 Transmission Electron Microscope (TEM).......................... 31
3.5.3 X-Ray Diffraction (XRD)......................................................33
3.5.4 Brauner Emmet Teller Analysis (BET Analysis).................. 36
3.6 Pengujian Performa Elektrokimia.................................................. 36
3.6.1 Galvanostatic Charge/Discharge......................................... 36
3.6.2 Electrochemical Impedance Spectroscopy (EIS)................. 37
3.6.3Cyclic Voltametry (CV)......................................................... 38
3.7 Pengambilan Data........................................................................... 38
3.8 Analisa Data.................................................................................... 39
DAFTAR PUSTAKA....................................................................................... 39

DAFTAR ISI | 10