TEXTILE DYEING

Experiment Name: Desizing of Cotton Fabric with Enzyme.

Recipe:

Rapidose 3x = 4gm/L

Acetic Acid = 3gm/L

Common salt (NaCl) = 0.5gm/L

Wetting Agent = 0.5gm/L

pH = 6-7

Time = 30-45 minutes

Temperature = 70c

Material: Liquor = 1:50

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Process Curve:

100

80

60

40

20

05 -10 30 - 45

TIME (MIN)
Rapidose 3x Cold wash
Wetting Agent
Acetic Acid
Common salt (NaCl)
Fabric

Figure: Process Curve of Desizing of Cotton Fabric with Enzyme.

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Experiment Name: Scouring and Bleaching of Cotton Yarn in Single

Stage.

Recipe:

NaOH = 2gm/L

H2O2 = 3gm/L

Stabilizer = 1cc/L

Wetting Agent = 1gm/L

Sequestering Agent = 1gm/L

pH = 9.5-11.5

Temperature = 90-100c

Time = 60 minutes

Material: Liquor = 1:50

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Process Curve:

100

80

60

40

20

05 -10 60

TIME (MIN)
Cold wash

NaOH
H2O2
Stabilizer
Wetting Agent
Sequestering Agent
Cotton yarns

Figure: Process Curve of scouring and bleaching of cotton yarn in single

stage.

Experiment Name: Dyeing of Cotton Fabric with Direct Dye.

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Recipe:

Dye = 2 % (On the of weight material)

Wetting Agent = 0.5gm/L

NaCl = 1gm/L

Temperature = (70-80) c

Time = 60 minutes

Material: Liquor = 1:50

Process Curve:

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100

80

60

40

20

05 -10 50 - 60

TIME (MIN)
Dye Cold wash
Wetting Agent
Fabric
NaCl

Figure: Process Curve of dyeing of cotton fabric with direct dye.

Experiment Name: Dyeing of nylon yarn with acid dye.

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Recipe:

Dye = 2% (On the weight of material)

Acetic acid = 0.5 gm/L

Wetting Agent = 1gm/L

Salt = 10 gm/L

Temperature = 100 C

Time = 60 minute

Material: Liquor = 1:50

Process Curve:

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120

100

80

60

40

20

05 -10 60

TIME (MIN)
Wetting Agent Cold wash
Dye
Acetic acid
Salt
Fabric

Figure: Process curve of dyeing of nylon yarn with acid dye.

Experiment Name: Dyeing of jute yearn with basic dye.

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TEXTILE DYEING

Recipe:

Dye = 1.5% (On the weight of material)

Acetic acid = 1 gm/L

Sodium acetate (Ch3COONa) = 1 gm/L

Wetting Agent = 1gm/L

pH = 5.6

Temperature = 80-90 C

Time = 45 minute

Material: Liquor = 1:50

Process Curve:

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100

80

60

40

20

20 -30 40 - 60

TIME (MIN)
Wetting Agent Cold wash
Dye
Acetic acid
Sodium acetate (Ch3COONa)
Fabric

Figure: Process Curve of dyeing of jute yarn with basic dye.

Experiment Name: Dyeing of cotton fabric with vat dye.

Recipe:

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Dye = 5% (On the weight of material)

Hydrose = 15% (On the weight of material)

NaOH = 20% (On the weight of material)

Wetting agent = 5% (On the weight of material)

Vatting temperature = 50 C

Vatting time = 20 minute

Dyeing temperature = 70-80 C

Dyeing time = 1 hours

Material: Liquor = 1:50

Process Curve:
80

70

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60

50

40

30

20

20 -30 40 - 60

TIME (MIN)
Dye Rest of Water
Cold wash

NaOH

Wetting Agent

Hydrose

Fabric

Half of Water

Figure: Process Curve of dyeing of jute yarn with basic dye.

Experiment Name: Printing of cotton fabric with direct dye with
block printing method.

Recipe:

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Dye = 4 parts

Glycerin = 5 parts

Thickener = 70 parts

Trisodium phosphate = 2 parts

Water = As required

TOTAL = 100 parts

Experiment Name: Printing of cotton fabric by vat dye in screen

printing method.

Recipe:

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TEXTILE DYEING

Dye = 4 parts

Glycerin = 4 parts

Na-hydrosulphite = 4 parts

K2CO3 = 6 parts

Thickener = 70 parts

Water = As required

TOTAL = 100 parts

Experiment Name: Dyeing of cotton fabric with sulphur

dye.

Recipe:

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TEXTILE DYEING

Dye = 10% (On the weight of material)

Na2S = 15% (On the weight of material)

Wetting agent = 10% (On the weight of material)

Na2Co3 = 10% (On the weight of material)

NaCl = 20 %( On the weight of material)

Temperature = 90 C

pH = 9-11

Time = 60 minutes

Material: Liquor = 1:50

Process Curve:

100

80

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60

40

20

05 -10 10 50-
60

TIME (MIN)
Dye
Na2S
NaCl
Wetting Agent Cold wash
Fabric

Figure: Process curve of Dyeing of cotton fabric with sulphur

dye.

Experiment Name: Dyeing of cotton fabric with azoic colour.

Recipe:
For Naphtholation:
Naphthol = 2% (On the weight of material)

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TEXTILE DYEING

NaOH = 3 gm/L

Salt = 20 gm/L

T.R.Oil = 2 cc/L

Temperature = Room

Time = 20-25 minute

Material: Liquor = 1:25

For Base:
Base = 2% (On the weight of material)

HCl = 5 cc/L

Na2No2 = 2 gm/L

CH3COONa = 0.5 gm/L

Temperature = 0-5 C

Time = 20-25 minutes

Material: Liquor = 1:25

Process Curve:

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Experiment Name: Dyeing of cotton fabric with reactive dye (cold

brand).

Recipe:

Dye = 2% (On the weight of material)

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Red=1%,
Yellow=0.5%,
Blue=0.5%

NaCl =40 gm/l

NaCO3 = 15 gm/l

Wetting agent = 1 cc/l

Temperature = 40 C

Time = 60 minutes

pH = 9-11

Material: Liquor = 1:50

Process Curve:

60

50

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TEXTILE DYEING

40

30

20

05 -10 60

TIME (MIN)
Dye
NaCl
Cold wash
NaCO3
Wetting Agent
Fabric

Figure: Process curve of dyeing of cotton fabric with reactive

dye (cold brand).

Experiment Name: Dyeing of cotton fabric with reactive dye (hot

brand).

Recipe:

Dye = 2% (On the weight of material)

Red=1%,
Yellow=0.5%,

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TEXTILE DYEING

Blue=0.5%

Common salt = 30 gm/L

Soda ash = 15 gm/L

Wetting Agent = 1gm/L

Time = 60 minute

Temperature = 80-90 C

pH = 9-11

Material: Liquor = 1:50

Process Curve:

100

80

60

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TEXTILE DYEING

40

20

05 -10 60

TIME (MIN)
Dye
Wetting Agent Cold wash
Common salt
Soda Ash
Fabric

Figure: Process curve of dyeing of cotton fabric with reactive dye (hot brand).

Experiment Name: Dyeing of polyester fabric with disperse dye by

HTP method.

Recipe:

Dye = 2% (On the weight of material)

Red=1%,
Blue=1%

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Dispersing agent = 1 cc/L

Acetic acid = 1 cc/L

pH = 4.5-5.5

Temperature = 130 C

Time = 30 minutes

Material: Liquor = 1:50

Process Curve:
140

120

100

80

60

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40

20

5 -10 30

TIME (MIN)
Dye
Dispersing agent Cold wash
Acetic acid
Fabric

Figure: Process curve of dyeing of polyester fabric with disperse dye by HTP
method.

Experiment Name: Printing on cotton fabric with reactive dye by

screen printing method.

Recipe:

Dye = 3 parts

Thickener = 66 parts

Soda ash = 6 parts

Urea = 8 parts

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Water = As per required

TOTAL =100 parts

Experiment Name: Printing on polyester fabric with disperse dye

by block printing method.

Recipe:

Dye = 4 parts

Thickener = 83 parts

Dispersing agent = 2 parts

H 4 2 O4 H4
(N S /N Cl = 7 parts

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Water = As per required

TOTAL =100 parts

Experiment Name: Determination of water hardness.

Recipe:

Buffer solution = 2-3drops

Eriochroma black-T = 2-3drops (2ml)

(0.02ml) EDTA = (amount is given below)

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TEXTILE DYEING

Amount of EDTA(Burette reading):

SL NO Initial reading Final reading Difference (ml)
(ml) (ml)
01 x x x
02 x x x
03 x x x

Experiment Name: Tie Dyeing of Cotton Fabric with Reactive Dye.

Recipe:

Dye = 3 % (on the weight of fabric)

Salt = 60gm/L

Soda = 15gm/L

Sequestering Agent = 1gm/L

Leveling Agent = 1gm/L

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Anti-foaming Agent = 1gm/L

Material: Liquor = 1:30

Time = 45minutes

Temperature = 60c

pH = > 10

Process Curve:

60

50

40

30

20

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TEXTILE DYEING

05 -10 20
30-45

TIME (MIN)
Dye Soda ash 1% of Cold

Sequestering Agent Acetic wash

Salt Acid

Leveling Agent wash

Anti-Foaming Agent

Fabric

Figure: Process curve of tie dyeing of cotton fabric with reactive dye

Experiment Name: Batik Printing of Cotton Fabric with Reactive

Dye.

Recipe for Wax Solution:

White Wax = 50%

Honey Wax = 40%

Roson (Adhesive) = 10%

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TEXTILE DYEING

Recipe for Dyeing:

Dye = 3 %( On the weight of fabric)

Salt = 60gm/L

Soda = 15gm/L

Wetting Agent = 1gm/L

Sequestering Agent = 1gm/L

Leveling Agent = 1gm/L

Material: Liquor = 1:50

Time = 45minutes

Temperature = 40c

Process Curve:
50

40

30

20

30
TEXTILE DYEING

0 05-10 10 30-45

TIME (MIN)

Dye Soda Ash Cold

Sequestering Agent wash

Salt

Leveling Agent

Fabric

Figure: Process Curve of batik printing of cotton fabric with reactive dye.
Experiment Name: Dyeing of Cotton Fabric with Pigment Color in a
Padding Mangle.

Recipe:

Pigment = 50gm/L

Binder = 150gm/L

Wetting Agent = 1gm/L

Anti-roller depositor = 2gm/L

Anti-migrating Agent = 2gm/L

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DAP (Diamino phosphate) = 1gm/L

Machine speed = 50m/min

pH = 4.5-5

Experiment Name: Dyeing of Polyester Fabric with Pigment Color

in a Padding Mangle.

Recipe:

Pigment = 50gm/L

Binder = 150gm/L

Wetting Agent = 1gm/L

Anti-roller depositor = 2gm/L

Anti-migrating Agent = 2gm/L

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TEXTILE DYEING

DAP (Diamino phosphate) = 1gm/L

Machine speed = 50m/min

pH = 4.5-5

Experiment Name: Preparation of Flat Screen for Screen Printing.

Recipe:
Autosol = 99%

Sensitizer = 1%

TOTAL = 100% (On the weight of material)

Experiment Name: Screen Printing on Cotton Fabric with Reactive

Dye.

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TEXTILE DYEING

Recipe:

Reactive Dye = 50 parts

Urea = 100 parts

Thickener = 500 parts

Resist Salt = 15 parts

NaHCO3 = 10 parts

Warm Water = As required to make 1000parts

Total = 1000 parts

Experiment Name: Application of Softener on Cotton Fabric by

Padding Mangle.

Recipe:

Softener (Anionic) = 80gm/L

Acetic Acid = 1gm/L

pH = 4.5-5

Experiment Name: Application of Anti-crease on Cotton Fabric by

Padding Mangle.

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TEXTILE DYEING

Recipe:

Anti-crease Agent = 80gm/L

Catalyst = 20gm/L

Acetic Acid = 1gm/L

pH = 4.5-6

Experiment Name: Application of Anti-microbial on Cotton Fabric

by Padding Mangle.

Recipe:

Anti-microbial Finish = 80gm/L

Acetic Acid = 1gm/L

pH = 4.5-5

Experiment Name: Printing with Cibacron Dyes.

Recipe:

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Cibacron Dye = 50gm

Urea = 200gm

Hot water = 203gm

Sodium alginate = 407gm

K2CO3 = 60gm

Sodium hydroxide = 2gm

Albatex BD/Ludigol = 15gm

Total = 1Kg

Experiment Name: Printing with Remazol Dyes.

Recipe:

Remazol dye = 30 t0 70gm

Urea = 50gm

Hot water = 300gm

Sodium alginate paste = 400gm

Ludigol = 15gm

Acetic acid = 10gm

Water = 155 195gm

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Total = 1Kg

CALCULATION

Total liquor = [Sample weight liquor amount] cc

Dye:
If
liquid
Required Dye = [(Sample weight Sade %) Stock solution] cc

If
solid
Required Dye = [Sample weight Sade%] gm

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Chemical:
If
liquid
Required chemical = [(Total liquor Recipe amount) (1000Stock solution)] cc

If
solid
Required chemical = [(Total liquor Recipe amount) 1000] gm

If
liquid
&%
Required chemical = [(Total liquor Recipe %) Stock solution] cc

If
solid &
%
Required chemical = (Total liquor Recipe %) gm

Water:

Required additional water =[

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39