Report Assignment 4
GROUP 14
GROUP PERSONNEL :
AGUS AMANDA TANOYO (1206254113)
CLAUDIA HARFIAN (1206239876)
DENA PRESTIA HALLATU (1206202141)
ERICCO JANITRA (1206249845)
ERWIN FIRMANSYAH (1206202053)
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LIST OF CONTENTS
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LIST OF TABLES
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CHAPTER 1
HSE MANAGEMENT
1.1.1 HAZID
Hazard Identification or commonly known as HAZID is an analysis of
hazard to prevent any of risk on industrial installation by observing some aspects.
In analyzing hazard identification aspect in industrial are information data,
location, risk, trigger factor of danger and hazard potential. Information data that
we needs are process flow diagram (PFD), piping and instrumentation diagram
(P&ID), equipment and building layout and record of events. Location analysis
includes operating facilities and supporting facilities. Trigger factor of danger
includes operation process, transportation, geography, meteorology and social
cultural. Hazard potential likes huge fire and explosion, drown and environmental
contaminant. For the risk analysis are consider from human resources,
environment and asset.
Identification of hazard in ethanol plant covers some aspects such as
environment, assets, and human resources. For this hazard identification we create
a reference parameter first and analyzing the impact of any risks and hazards.
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From those criteria, we can determine the hazard identification in our plan which
is tabulated in Table 1.3 below:
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Operating
Separation of Installingand monitoring
Distillation Fire and/or temperature
21 ethanol-water Severe Unlikely Pressure and
Column explosion and/or pressuree
(Purification temperature control
is too high
Ethanol)
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1.1.2 HAZOP
Hazard and Operability Study (HAZOP) is a systematic approach to investigating each element of a process. It have function
to identify all of the ways in which parameters can deviate from the intended design conditions and create hazards or operability
problem. HAZOP is also used for identify and evaluate problems that may pose a danger to the individual employees, equipment
operation, or efficiency of the process operation. The goals after doing HAZOP are:
1. Identify safety, hazard and operational problems that related with process which are immediately threatens workers
safety/operation.
2. Determine the severity of identified problem effect.
3. Identify and evaluate the engineering and procedural safeguards.
4. Recommend additional engineering and procedural safeguards if it is needed.
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Pressure testing
The purpose of pressure testing is to confirm that the mechanical
integrity of the plant, verifying capability of containing the pressures it
has been designed to hold, ensure there are no leaks and verify that the
plant can be reliably made leak free, identify any vulnerabilities well
before the plant is placed into service, and to meet the requirements of
legislation, local, international and industry standards.
Water for testing and flushing should contain a rust inhibitor - one
low in chloride content for stainless steel lines. After testing, water
should be drained completely from all lines that do not normally carry
water, steam or steam condensate. All low points should be checked
for presence of water. Lines should be dried by blowing hot air, dry
inert gas or instrument air. On the vacuum system, final checks are
best performed by pulling a vacuum and observing the rate of pressure
rise in the blocked in system. Excessive leaks can then be located by
applying a mild positive pressure and testing each flange with bubble
solution.
Isometric drawings of all systems to be tested should be displayed
on a board and marked up as each section is tested. Hydro testing of
piping and equipment according to code requirements to confirm
mechanical strength should be carried out on groups of equipment
naturally suggested by design pressure and function. All water, steam,
condensate, oil, gas and process steam piping should be hydro tested.
Major equipment that has already been tested as part of manufacturing
may be isolated by blanks.
Cleaning and flushing
Need to ensure no construction debris is left in pipes of vessels -
welding rods, bolts, gloves, rags etc. Before flushing is started, check
the process thoroughly to ensure screens have been installed in front of
pump suctions.
Regardless of whether pipes are cleaned with water, steam, air or
nitrogen, flow velocities should be high enough to ensure that pipes
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will be suitably scoured. Need to ensure that the debris from one piece
of equipment will not simply be flushed into another.
2. Utilities commissioning
Utilities commissioning usually represents the first phase of
commissioning, as these usually need to operational first, before the rest of
the plant can be commissioned. First of all, check supply pressures of all
services (steam, cooling water). At the most distant points, open drains,
vent valves or pipe flanges and purge until fluids come out clean and rust
free. Purge/blow out lines to each piece of equipment. Circulate water to
waste water system until water lines clear and clean. Flush waste water
and drain systems to ensure no blockages. Check operation of steam traps.
Drain condensate to waste water until it is clean.
3. Operational Testing
A period of 2-3 weeks is usually sufficient for operational testing, after the
mechanical dry running of individual pieces of equipment and hot testing
complete. Air and water tests should be set up in a closed loop with fluid
continuously recycled, with loops as large a possible. The loop should
ideally be the same loop that will be subject to solvent testing. Tests
should continue for several days in order to give all shifts a chance to
conduct the same tests. All shifts should be given the opportunity to start
up and shutdown each closed loop test.
4. Start Up Sequence
Following the proper start-up sequence also helps ensure that system
operating parameters conform to design conditions so that productivity
goals can be achieved. Measurement of initial system performance is an
important part of the start-up process. Documented results of this
evaluation serve as benchmarks against which ongoing system operating
performance can be measured.
Typical Start Up Sequence:
a. Check all valves to ensure that settings are correct. The feed pressure
control and concentrate control valves should be fully open.
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b. Use low pressure at a low flow rate to flush the air out of the elements
and pressure vessels. Flush at a gauge pressure of 30 to 60 psi (0.2
0.4 MPa.
c. During the flushing operation, check all pipe connections and valves
for leaks. Tighten connection where necessary.
d. After the system has been flushed for a minimum of 30 minutes, close
the feed pressure control valve.
e. Ensure that the concentrate control valve is open. Starting against a
closed or almost closed concentrate valve should cause the recovery to
be exceeded which may lead to scaling.
f. Slowly crack open the feed pressure control valve (feed pressure
should be less than 60 psi/0.4 MPa).
g. Start the high pressure pump.
h. Slowly open the feed pressure control valve, increasing the feed
pressure and feed flow rate until the design concentrate flow is
reached. The feed pressure increase to the elements should be less than
10 psi (0.07 MPa) per second to achieve a soft start. If the feed
pressure and/or the feed flow rate are ramped up too quickly, the
housing of the elements may be damaged by excessive forces in flow
direction and/or in radial direction - especially if air is in the system -
leading to telescoping and/or fiberglass shell cracking.
i. Slowly close the concentrate control valve until the ratio of concentrate
flow approaches, but does not exceed the design ratio (recovery).
Continue to check the system pressure to ensure that it does not exceed
the upper design limit. Repeat steps until the design concentrate flows
are obtained.
j. Calculate the system recovery and compare it to the system's design
value.
k. Allow the system to run for one hour.
l. Take the first reading of all operating parameters.
m. Check feed conductivity from each pressure vessel to verify that all
vessels conform to performance expectations.
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Knowing about those safety precautions, here is the procedure for shutting
down ethanol plant.
1. Stop biomass, water, air and MDEA stream by closing the lid stream
valve.
2. Stop each stream pump of biomass, water, and MDEA.
3. After the raw material stream being stopped, then we stop the heat
exchanger system of water stream through reactor.
4. After we stop the heat exchanger system, then we can stop scrubbing and
CO2 removal.
5. After all raw material reacted in the chamber reactor then the product
stream formed, we can start to stop separation/distillation unit process.
6. Stopping distillation unit process can be done by stopping the tray system
first then the upper and bottom stream include the arrangement to stop
reboiler and condenser temperature.
7. In the process to shut the system down, we have to maintain the change
of temperature to prevent its equipment to be broken or inaccurate.
8. Finally, the last instrument to be turned off are the regeneration and
recycle system of each stream to make sure all the last process is
correctly done. After this, the plant will be completely stopped.
1.2.2 PPE
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dangerously exposed. It may not provide the level of protection desired and may
discourage employee use. Personal protection equipment can be divided into:
1. Eye and Face Protection
Eye protection is suggested to be routinely considered for use by
carpenters, electricians, machinists, mechanics, millwrights, plumbers and
pipefitters, sheetmetal workers and tinsmiths, assemblers, sanders,
grinding machine operators, sawyers, welders, laborers, chemical process
operators and handlers, and timber cutting and logging workers.
Employers of workers in other job categories should decide whether there
is a need for eye and face PPE through a hazard assessment. Examples of
potential eye or face injuries include:
Dust, dirt, metal or wood chips entering the eye from activities such as
chipping, grinding, sawing, hammering, the use of power tools or even
strong wind forces.
Chemical splashes from corrosive substances, hot liquids, solvents or
other hazardous solutions.
Objects swinging into the eye or face, such as tree limbs, chains, tools
or ropes.
Radiant energy from welding, harmful rays from the use of lasers or
other radiant light (as well as heat, glare, sparks, splash and flying
particles).
The eye and face protection selected for employee use must clearly
identify the manufacturer. Any new eye and face protective devices must
comply with ANSI Z87.1-1989 or be at least as effective as this standard
requires. This include goggles and the mask.
2. Head Protection
Employers must ensure that their employees wear head protection if any of
the following apply:
Objects might fall from above and strike them on the head;
They might bump their heads against fixed objects, such as exposed
pipes or beams; or
There is a possibility of accidental head contact with electrical hazards.
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Hard hats must have a hard outer shell and a shock-absorbing lining that
incorporates a headband and straps that suspend the shell from 1 to 1 1/4
inches (2.54 cm to 3.18 cm) away from the head. This type of design
provides shock absorption during an impact and ventilation during normal
wear.
3. Foot and Leg Protection
Safety footwear must meet ANSI minimum compression and impact
performance standards in ANSI Z41-1991 (American National Standard
for Personal Protection-Protective Footwear) or provide equivalent
protection. This kind of protection will include the safety shoes. Safety
shoes have impact-resistant toes and heat-resistant soles that protect the
feet against hot work surfaces common in roofing, paving and hot metal
industries. The metal insoles of some safety shoes protect against puncture
wounds. Safety shoes may also be designed to be electrically conductive to
prevent the buildup of static electricity in areas with the potential for
explosive atmospheres or nonconductive to protect workers from
workplace electrical hazards.
4. Hand and Arm Protection
If a workplace hazard assessment reveals that employees face potential
injury to hands and arms that cannot be eliminated through engineering
and work practice controls, employers must ensure that employees wear
appropriate protection. Potential hazards include skin absorption of
harmful substances, chemical or thermal burns, electrical dangers, bruises,
abrasions, cuts, punctures, fractures and amputations. Protective
equipment includes gloves, finger guards and arm coverings or elbow-
length gloves. Gloves made from a wide variety of materials are designed
for many types of workplace hazards. In general, gloves fall into four
groups:
Gloves made of leather, canvas or metal mesh;
Fabric and coated fabric gloves;
Chemical- and liquid-resistant gloves;
Insulating rubber gloves
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5. Body Protection
Employees who face possible bodily injury of any kind that cannot be
eliminated through engineering, work practice or administrative controls,
must wear appropriate body protection while performing their jobs. In
addition to cuts and radiation, the following are examples of workplace
hazards that could cause bodily injury:
Temperature extremes;
Hot splashes from molten metals and other hot liquids;
Potential impacts from tools, machinery and materials;
Hazardous chemicals.
Protective clothing comes in a variety of materials, each effective against
particular hazards, such as:
Paper-like fiber, used for disposable suits provide protection against
dust and splashes.
Treated wool and cotton, adapts well to changing temperatures, is
comfortable, and fire-resistant and protects against dust, abrasions and
rough and irritating surfaces.
Duck, is a closely woven cotton fabric that protects against cuts and
bruises when handling heavy, sharp or rough materials.
Leather, is often used to protect against dry heat and flames.
Rubber, rubberized fabrics, neoprene and plastics, protect against
certain chemicals and physical hazards. When chemical or physical
hazards are present, check with the clothing manufacturer to ensure
that the material selected will provide protection against the specific
hazard.
6. Hearing Protection
Some types of hearing protection include:
Single-use earplugs, are made of waxed cotton, foam, silicone rubber
or fiberglass wool. They are self-forming and, when properly inserted,
they work as well as most molded earplugs.
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The National Fire Protection Association (NFPA) has developed a system for
indicating the health, flammability, reactivity and special hazards for many
common chemicals through use of the NFPA 704 Diamond. The hazard rating for
the laboratory is determined by looking at all the chemicals, gases and special lab
uses in the laboratory and coming up with a rating for each hazard category based
on criteria established below. The rating summary are as follows:
Health (Blue) Detailed Description of Health Rating
4: Danger May be fatal on short exposure. Specialized protective
equipment required
3: Warning Corrosive or toxic. Aviod skin contact or inhalation
2: Warning May be harmful if inhaled or absorbed
1: Caution May be irritating
0: No unusual hazard
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possible, and the last, evacuate if necessary.The plan works best when expressed
as an easily recalled acronym, such as SAFE:
a. S Sound the alarm
Either sound it yourself or call out to someone else to sound it. This allows
the fire department to be on its way while other activities are being
performed.
b. A Alert others
Quickly tell others in the area of the fire. Do this in a calm, firm manner.
Do not cause a panic. Secure the area for the fire department. Close all
doors and windows to prevent the spread of smoke and flames. Call
security to give verification and information about location of fire.
c. F Fight the fire
Do this only in the case of a manageable fire, one that you have the
training and experience to fight. For example, fire in a wastebasket. If it
possible two employeesshould fight the fire together using two fire
extinguishers. If you have any doubt about your ability to fight the fire,
then do not attempt to combat it.
d. E Evacuate the area
If necessary.
Alarm which used for evacuation system is an alarm system standard from
OSHA. It applies to provide an early warning for emergency actions or reaction
time for employees to safely escape the work place, the immediate work area, or
both. Type of alarms which used in this plant is:
1. Audible Alarm
Audible alarm which used consists of horn and sirens. Horns produce a
very loud distinctive sound that immediately attracts attention. Horns can
be useful to call attention to critical situations. Signals other than those
used for evacuation purposes do not have to produce the temporal coded
signal. Thus, sirens produce a loud piercing wail that makes them ideally
suitable for initiating a site-wide evacuation
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2. Visible Alarm
Visual alarm which used consists of flashing/steady lights and strobe
lights. Steady lights are well suited for areas where ambient noise makes
audible signals difficult to hear, for an example in area where the
compressor is in. These types of lights come with different colored covers
for increased attention and can be ordered with rotating or flashing lights.
Strobe lights use high intensity flash tubes that are ideally suited for areas
where high ambient light levels make traditional rotating or flashing lights
difficult to distinguish or where ambient noise makes audible signals
difficult to hear.
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a. Dial the plant infirmary and inform the nurse of emergency and its
location in the plant.
b. If the nurse cannot be reached, dial emergency call, and inform any
hospital or fire department of the medical emergency. Give the dispatcher
the nature and location in the plant of medical emergency.
c. Unless you have been designated by management to be a first aid
responder, do not provide first aid. Make the victim as comfortable as
possible until medical help arrives
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b. Fire Hydrant
Fire hydrant is a permanent system that is used to extinguish the fire. It
uses pressurized water which flowed through pipes and fire hose to
extinguish the fire. In our plant, there are class 2 of building hydrant
system. This type has 1,5 inch diameter of a hose. This type usually used
for untrained people.
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CO2
Char
Ash
Waste Water
Household waste
Sound (noise)
All of these wastes can be directly discarded, recycled, or used again to
main process. Government gives boundary for every industrial to process their
waste based in Human Safety Environment. We have grouped all of the waste
based on the type or phase. There are such as solid waste, liquid waste, gas waste,
and sound (noise) waste. Management for the waste will be explained below:
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emission can be directly discharge into the air because it is not dangerous
emission. The hydrogen will also be sold to our plant costumer.
The noise levels that exceed the threshold may cause disruption to the
workforce and this limit is called critical level of intensity. The disorder may
include:
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Hearing Problem
The immediate and acute effect of noise pollution to a person, over a
period of time, is impairment of hearing. Prolonged exposure to impulsive
noise to a person will damage their eardrum, which may result in a
permanent hearing impairment.
Effects on general health
Health effects of noise include anxiety and stress reaction and in extreme
cases fright. The physiological manifestations are headaches, irritability
and nervousness, feeling of fatigue and decreases work efficiency. For
example, being pounded by the siren of fire fighters, police or ambulance
in your city all night everyday leave people (especially elderly people)
stresses and tired in the morning.
To overcome this problem, we must control the noise effect on the
workers by:
1. Reduce the noise transmission to workers
This can be done by insulating the noisy equipments or insulate the
workers workplace to prevent high noise transmission.
2. Eliminate noise directly from the source
This can be done by not using noisy equipments from the first place. But,
since this method is nearly impossible because the need of rotating
equipments we can do the third method below,
3. Personal Protection
Efforts to protect employees from noise in the work environment can
applied by wearing ear protection devices or personal protective
equipment, in the form of ear plugs and ear muffs
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CHAPTER 2
PLANT LAYOUT
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Our plant has a total area of 3 hectares. In this plant, the area are divided
into two big groups which are inside battery limit and outside battery limit.
Battery limit are the area that are related with the plant process such as the main
processes and water treatment. Outside battery limit are the area that is not related
with the main processes of the plant, such as the office, canteen, and others. The
main process is located in the middle of the factory area. It is because the main
process needs a lot of space, and for the safety reason the office that contain lots
of person need to be located near the exit door so if there are some explosion the
worker can leave the area immidiately
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2.3.2 3D Picture
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2.4 Utilities
Utlilities are section or equipments that can improve of support the works
of main equipments. The layout of our plant utilities can be seen in Figure 2.3
which surround by a red dot lines. Our plant utilities consist of cooling tower,
high pressure steam, and generator set for electricity.
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CHAPTER 3
CONCLUSION
1. The most dangerous area is in the ractor area, due to the flammable material
inside reactors.
2. There are several equipments which needs more attention due to its severe
hazard effects, such as crusher, gasification reactor, char combustor,
condenser, reboiler, distillation column, reflux drum, sorage ethanol, also
laboratory area.
3. In HSE management, our plant has our own start up system and shut dwon
system to prevent accidents while starting up or shutting down thee plant.
4. Every employees must wear full PPE to enter the plant area, which is goggles,
helmet, ear plug, mask (if needed), gloves, coverall, safety shoes, and ID card
to plant.
5. Our plant slogan in emergency operation is SAFE (Sound the alarm, Alert
others, Fight the fire, Evacuate the area).
6. If medical emergency occurs, employee can be take to clinic. If they need
further checkup, then they will be take to the nearest hospital.
7. Out plant have a solid waste, liquid waste, gas waste that will be treated in
waste treatment area. For sound pollution, to reduce the noise level, performed
regular maintenance and replacing parts causing noise.
8. Our plant location is in Losarang, Indramayu, which is the biggest rice
producer in Indonesia. Also, Losarang is an industrial estate in Indramayu.
9. The area of our plant is 3 hectares, which include the plant area, office area,
and other additional areas. The plant area about 100 x 60 meters.
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REFERENCES
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APPENDIX
1. ETHANOL MSDS
Product Name : Ethanol
CAS : 64-17-5
Chemical Formula : C2H6O
Hazard Identification
- Eye Contact: Irritating to eyes.
- Skin Contact: May cause skin irritation. Prolonged and/or repeated contact
may cause defatting of the skin and dermatitis. May be absorbed through the
skin.
- Serious Skin Contact: Not available.
- Inhalation: Irritating to nose & throat.
- Serious Inhalation: Chronic inhalation and ingestion may cause effects similar
to those of acute inhalation and ingestion. Prolonged or repeated skin contact
may cause defatting and dermatitis. Prolonged or repeated exposure may
cause adverse reproductive effects. May cause fetal effects.
- Ingestion: May be fatal or cause blindness if swallowed. May cause systemic
toxicity with acidosis. May cause liver and kidney damage. May cause central
nervous system depression, characterized by excitement, followed by
headache, dizziness, drowsiness, and nausea. Advanced stages may cause
collapse, unconsciousness, coma and possible death due to respiratory failure.
- Serious Ingestion: Not available.
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- Ingestion: If victim is conscious and alert, give 2-4 cupfuls of milk or water.
Never give anything by mouth to an unconscious person. Get medical aid.
Induce vomiting by giving one teaspoon of Syrup of Ipecac.
- Inhalation: Get medical aid immediately. Remove from exposure to fresh air
immediately. If not breathing, give artificial respiration. If breathing is
difficult, give oxygen.
- Notes to Physician: Treat symptomatically and supportively.
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2. WATER MSDS
Product Name : Water
CAS : 7732-18-5
Chemical Formula : H2O
Hazard Identification
- Non Toxic
Hazard Identification
- Eye Contact: Not applicable.
- Skin Contact: Not applicable.
- Serious Skin Contact: Not available.
- Inhalation: Not applicable.
- Serious Inhalation: Not available.
- Ingestion: Not Applicable
- Serious Ingestion: Not available.
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3. MEA MSDS
Product Name : Monoethanolamine
CAS : 141-43-5
Chemical Formula : NH2CH2CH2OH
Hazard Identification
- Eye Contact: Vapors and contact may cause severe irritation, burns, redness,
pain, and blurred vision.
- Skin Contact: May cause irritation, redness, burns, and pain. May be absorbed
through the skin; symptoms may parallel inhalation. .
- Serious Skin Contact: Not available.
- Inhalation: Vapor may cause irritation to the respiratory tract. Symptoms may
include sore throat, coughing, respiratory distress, headache, lethargy, and
narcosis. Exposure to higher concentrations may cause pulmonary irritation,
and kidney and liver damage. .
- Serious Inhalation: Not available.
- Ingestion: May cause mucosal burns of the mouth and esophagus, abdominal
pain, nausea, and vomiting. May cause systemic poisoning with symptoms
paralleling inhalation.
- Serious Ingestion: Not available.
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4. CuO MSDS
Product Name : Copper(II) Oxide
CAS : 1317-38-0
Chemical Formula : CuO
Hazard Identification
- Eye Contact: Causes eye irritation. May result in corneal injury. May cause
conjunctivitis.
- Skin Contact: Causes skin irritation. May cause skin discoloration. .
- Serious Skin Contact: Not available.
- Inhalation: Causes respiratory tract irritation. May cause ulceration and
perforation of the nasal septum if inhaled in excessive quantities. Inhalation of
fumes may cause metal fume fever, which is characterized by flu-like
symptoms with metallic taste, fever, chills, cough, weakness, chest pain,
muscle pain and increased white blood cell count.
- Ingestion: May cause central nervous system depression, kidney damage, and
liver damage. May cause gastrointestinal irritation with nausea, vomiting and
diarrhea. May cause circulatory system failure. May cause vascular collapse
and damage.
- Serious Ingestion: Not available.
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- Odor: odorless
- pH: Not available.
- Vapor Pressure: Not applicable.
- Vapor Density: Not available.
- Evaporation Rate:Not applicable.
- Viscosity: Not applicable.
- Boiling Point: Not available.
- Freezing/Melting Point:1326 deg C
- Autoignition Temperature: Not applicable.
- Flash Point: Not applicable.
- Decomposition Temperature:Not available.
- NFPA Rating: (estimated) Health: 2; Flammability: 0; Reactivity: 0
- Explosion Limits, Lower:Not available.
- Upper: Not available.
- Solubility: Insoluble in water
- Specific Gravity/Density: 6.3-6.5
- Molecular Formula:CuO
- Molecular Weight:79.5454
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