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Tabel I Tabel Hasil Optimasi

Kondisi
Persentase RSD Standar Deviasi
Optimasi
Panjang
Flo Air:M Nilai Resolusi AuC Waktu AuC Waktu
Plate
w etano Retensi Retensi
Rat l
e
0.7 38:62 0.669 0.085 4,2 x 10- 0,407 0,9% 5,97%
5 3
1.0 38:62 0.78 0.011 10.03x1 0.452 30.03% 7.55%
0-2
0.7 30:70 0.78 0.065 0.04 0.01 2.2915 0.49%
5
1.0 30:70 0.955 0.116 0.105 0.0146 4.97% 0.1915%
0.7 30:70 0.08 0.194 0.3576 0.40 173.59% 0.38%
5
1.0 30:70 0.08 0.505 0.118 2.159 34.11% 17.16%
0.7 33:67 0.03 8.3 x 10-3 0.09 0.36 35.144% 4.14%
5
1.0 33:67 0.019 5.6 x 10-3 0.0876 0.537 41.24% 8.31%
0.7 35:65 1.73 - - - - -
5
Faktor Kapasitas Sampel Peak 1

TR 1T 0
K1 = T0

6.5201.593
K1 = 1.593

K1 = 3.09

Faktor Kapasitas Sampel Peak 2

TR 1T 0
K2 = T0

7.0971.593
K2 = 1.593

Pembuatan Larutan Sampel Stock 100ppm

Menimbang 2mg di larutkan larutan eluen 20ml. dilakukan pengenceran


- 100 ppm ke 80 ppm
100 x V1 = 80 x 5
V1 = 4mL add eluen sampai 5 ml
- 100 ppm ke 60 ppm
100 x V1 = 60 x 5
V1 = 3mL add eluen sampai 5 ml
- 100 ppm ke 40 ppm
100 x V1 = 40 x 5
V1 = 2mL add eluen sampai 5 ml
- 100 ppm ke 20 ppm
100 x V1 = 20 x 5
V1 = 1mL add eluen sampai 5 ml
- 100 ppm ke 10 ppm
100 x V1 = 10 x 5
V1 = 0.5mL (500 L add eluen sampai 5 ml)

Tabel II Tabel Pembakuan ( Pembuatan Kurva Kalibrasi)

Konsentrasi AuC
10ppm 0.3596
20ppm 1.3042
40ppm 2.7436
60ppm 3.8957
80ppm 5.7532

Gambar 1 Kurva Baku Asetosal

Kurva Baku
8

6
f(x) = 0.07x - 0.3 AUC
4
AuC R = 0.99 Linear (AUC)
2

0
0 10 20 30 40 50 60 70 80 90
Konsentrasi

Tabel III Tabel pengukuran Tablet Asetosal

Konsentrasi AuC
40 ppm 2.4358
40 ppm 2.3527
40 ppm 2.4080
Rata-Rata 2.3983

Perhitungan Kadar Tablet Asetosal

Y = 0.0741x 0.3011

2.3983 = 0.0741x - 0.3011

2.6994 = 0.0741x

X = 36.429 ppm

Persentase Kadar Tablet Asetosal

36.429
Persentase Kadar =
X 100
40

Persentase Kadar = 91.07%