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Process Condensate Treatment in Distilleries.

ACOPTM Advanced Catalytic Oxidation Process.

AIDA & NSI Seminar

Hotel Katriya, Hyderabad.
17th 18th October 2016

By:
Lijo T Jacob & Nandni Joshi

C 77 Sector 65, NOIDA 201307 NCR INDIA

Environmental | Energy | Analytical Services | Water & Waste Water | Process & Chemicals I Civil & Infra
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EWE Consulting Engineers - ACOP for Evaporator Condensate at AIDA NSI Seminar Hyderabad dated 17 18 October 2016
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EWE Operating Horizons

Environment Water & Waste Water Energy MEP Services

Analytical Process Chemicals Civil & Infra

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Sources of Waste Water in a Distillery

Waste Water sources from Molasses / Grain Based Distillery

Spent lees from Primary Distillation
High BOD,COD,TDS, VA & TOC Low TSS
DM Plant / Softener Regeneration
High TDS Low BOD COD TSS
Evaporator / Process Condensate.
Low TSS TDS Medium BOD COD TOC High VA
Dryer Vapor Condensate.
RO Plant Reject.
Sealing Water.
Filter Backwash.
Floor Washings.
CIP Water.
Cooling Tower Blowdown.
Boiler Blowdown.
Bottle wash.

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EWE Consulting Engineers - ACOP for Evaporator Condensate at AIDA NSI Seminar Hyderabad dated 17 18 October 2016
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Major Problems - Condensate & CIP Water

Pain points / Pollutants in Process Condensate.

TDS.
TSS.
pH
BOD
COD
VA Volatile Acids
TOC / DOC Organic Carbon
Ammonia.

Available Technologies:
Biological Aeration.
Anaerobic Digestion followed by Biological Aeration.
Catalytic Oxidation.
Advanced Catalytic Oxidation Process ACOPTM.

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Basics of Degradation

Carbonaceous Matter (C,H and/or O) degradation in absence of Oxygen.

Anaerobic digesters can be categorized as :

The biomass is fixed to a surface ("attached growth")
freely mix type with the reactor liquid ("suspended growth")
Hybrid Types.

There are about 20 variants of anaerobic digesters.

CSTR
Anaerobic contact process
Anaerobic expanded-bed reactor
Anaerobic filter
Anaerobic fluidized bed One format is UASB
Anaerobic lagoon
ECFB Recirculatory Anaerobic Boreactor.

C6H12O6 ------ > CO2 + CO + H2O + CH4 + H2S + Energy

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CPU Conventional Treatment

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Enhaned Recirculator Anaerobic Metabolic Path

Any Matter having high C & H content. Stage 6 Gas liquid

Sepration

Objective Maximum generation of CH4

Stage 5
(upto 76% CH4 has been obtained by us
Methnogenisis

Greater than 97 % CH4 after purification) Stage 4

Minimizing Water Carryover.
Acetogenesis

Estimation of H2S generation. Stage 3 Acedogenisis

Steps in Anaerobic Digestion: Stage 2 Hydrolysis

Dispersion.
Hydrolysis Stage 1 Distribution

Complex Organics ----- Monosacharides, Amino Acids, Fatty Acids & Alcohol
Acidogenesis
Monosacharides, Amino Acids, Fatty Acids & Alcohol ----- to Volatile Acids
Acetogenesis
Volatile acids ------ Acetates, H2, CO2.
Methanogenesis.
Acetate ----- CH4 & CO2.
Gas Liquid Separation Reduction in carry over of solids & water.
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ACOP the Five Phase Process

Objective Degradation of Low molecular weight organics.
Different with Grain, Beet, Molasses etc. VA & DOC
Presence of Heavy Metals
Different from Photo Catalysis.

Stages of ACOP 5 Stage

- Liquid Initiator OH
- Gaseous Progresso.
- Solid Catalyst Granular / Beed / Powder form
- Vapor Phase Oxidation Sonification / Cavitation.
- Ultraviolet Light.

Typical Generation for Process / Evaporator Condensate:

Parameter Grain Molasses Treated
BOD (ppm) 1500 2500 2500 3500 < 20
COD (ppm) 3000 4000 4000 5000 < 150
VA (ppm) 2000 - 2500 3000 4000 < 30
DOC (ppm) 500 1500 1500 2500 < 10
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EWE Consulting Engineers - ACOP for Evaporator Condensate at AIDA NSI Seminar Hyderabad dated 17 18 October 2016
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ACOP Process

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EWE Consulting Engineers - ACOP for Evaporator Condensate at AIDA NSI Seminar Hyderabad dated 17 18 October 2016