TITLE PAGE
GROUP 22
GROUP PERSONNEL:
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We have nine needs that have been interpreted from 12 respondents that
we had. Based on the consumer requirements, the insulation product should be
able to meet the following criteria: have low thermal conductivity, able to
withstand thermal expansion, pressure, hit or crash, and is easy for maintenance
and services.
After collecting needs and specification, the result shows that the costumer
are satisfied enough with the existing insulation except for several problems. For
developing the existing product, they want insulation that having low thermal
conductivity as low as 0.03 W/mK, insulation that can be placed at hinges, joint,
cable holes, and at top of the storages, also insulation that able to withstand
thermal expansion, hit, pressure or crash, and is easy for maintenance.
After benchmark to several existing products Aspen Aerogels, Rockwool,
and Arabian Fiberglass we obtain their specifications. The existing products
thermal conductivity are sequentially 0,021; 0,038; 0,028 W/m.K. The service
temprature range are consecutively -156 6 oC; 0 250 oC; -18 450 oC. Their
durability are in sequence 80 years, 60 years, and 50 years. So, current best
existing product is Aspen Aerogels.
The shortage of existing product are could cause skin irritation due to, lung
and respiratory problems due to inhaling material dust, still vulnerable to
condensation, freezing, and even corrosion, the existing product not really durable
due to extreme temperature difference and quiet pricey for a low thermal
conductivity value. Although we have such a big obstacles, we offer insulation
that is low pricey with high specifications so those two points will be out main
features on our product.
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PREFACE
Praise to Allah, the Cherisher and Sustainers of the world; God who has
been giving all His Blessing and Mercy for writer to complete this Assignment 1
Report of Chemical Product Design entitled Insulation in Cryogenic, Pipelines,
Storage and Air-conditioning.
This final report is submitted to fulfill one of the requirements in Chemical
Product Design Class as capstone course of Chemical Engineering Major in
Universitas Indonesia.
In the completion this report, the writer really gives his regards and thanks
for people who has given guidance and help, they are:
1. Prof. Dr. Ir. Widodo Wahyu Purwanto, DEA., Dr. rer. nat. Ir. Yuswan
Muharam M.T. , Dr. Ing. Ir. Misri Gozan M.Tech., Ir. Dewi Tristantini,
M.T., PhD., and others Lecturers, who has given their best guidance to the
writer in writing a great quality report and well developed chemical
product.
2. The informant and respondent of our questionnaire that helps indirectly to
begin this report
3. Imas Mega Pratiwi, Giovanni Anggasta, Raden M. Fatih, Nugrahirani
Hijrianti as the lecturer assistants of Chemical Product Design 2017 who
gives suggestion and guidance to the writer in writing this final report.
4. Our Parents, who always give their supports, prayers, and blessing.
5. Our beloved friends in Chemical Engineering Department batch 2014 who
always give their supports.
6. All of our correspondents who spend their time to fill our questionnaire.
Finally, the writer realizes there are unintended errors in writing this final
report. The writer really appreciates all readers giving their suggestion to improve
its content in order to be made as one of the good examples for the next report.
Depok, February 2017
Writer team
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LIST OF GROUP MEMBERS
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TABLE OF CONTENTS
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3.2. Consumer Requirement ...............................................................................23
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TABLE OF FIGURES
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LIST OF TABLES
Table 2.1 Dew Point for Relative Humidities for Ambient Still Air Temperatures
from -20C to + 50C with Standard Barometric Pressure ....................8
Table 2.2 Water vapour permeance for different plant cold surface .....................11
Table 2.3 Thermal conductivity cellular glass at density indicated ......................14
Table 2.4 Thermal conductivity cork at density indicated ....................................15
Table 2.5 Thermal conductivity glass mineral at density indicated ......................16
Table 2.6 Thermal conductivity phenolic foam at density indicated ....................17
Table 2.7 Thermal conductivity polystyrene at density indicated .........................19
Table 3.1 Consumer needs interpretation ..............................................................25
Table 3.2 List of needs ..........................................................................................28
Table 3.3 List of tidy up needs ..............................................................................29
Table 3.4 Groups of need ......................................................................................29
Table 3.5 Groups of needs with its rank ................................................................30
Table 4.1 List of metrics ........................................................................................32
Table 4.2 The needs-metric matrix ........................................................................33
Table 4.3 Competitive benchmarking chart based on metrics ..............................33
Table 4.4 The target specifications ........................................................................34
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CHAPTER 1
INTRODUCTION
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CHAPTER 2
REVIEW OF LITERATURE
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makes for the best insulation for low to medium temperatures where compression
and/or vibration is not a factor.
However, where higher temperatures are encountered, the air or gas voids
need to be reduced in size to minimize the convection within the voids and this is
achieved by increasing the density of the insulation (TIASA, 2001). Density may
be increased to a point where the solids content of the insulation is such that the
heat bridge of the solids overcomes the insulating effect of the voids. It follows
therefore, that by encasing a container of heat with thermal insulation material the
reverse heat flow will be retarded with resultant reducing energy loss and cost.
The word retarded is important because no matter how much insulation
is applied, the reverse flow of heat to ambient can never be stopped. The primary
reasons for insulation are many and varied, the main ones being (TIASA, 2001):
To conserve energy
To reduce heat loss or gain
To maintain a temperature condition
To maintain the effective operation of equipment or chemical reaction
To assist in maintaining a product at a constant temperature
To prevent condensation
To create a comfortable environmental condition
To protect personnel
The type and thickness of insulation depend on the foregoing primary
reasons together with the parameters of the specific conditions. Economic
thickness is the thickness of insulation, which will result in minimum total cost of
energy losses plus the cost of the erected insulation. The calculation of economic
thickness is complex and in some cases is overruled by the other listed primary
reasons, which can make the calculation unnecessary. The exception is when retro
fitting of insulation is envisaged. Retro fitting is the application of additional
insulation to existing insulation to further reduce heat loss or gain in order to
reduce the cost of energy losses.
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Table 2.1 Dew Point for Relative Humidities for Ambient Still Air Temperatures
from -20C to + 50C with Standard Barometric Pressure
(Source : Thermal Insulation Handbook, The Thermal Insulation Association of Southern Africa,
2001)
Many materials, which are moisture-resistant, are not necessarily vapour-
resistant. All insulation materials are susceptible to water vapour penetration to
various degrees. If penetration is not prevented, the water vapour condenses to
moisture or ice when its temperature reaches the dew point. This will, in time,
saturate the insulation thereby rendering it useless. To prevent this from taking
place, a vapour barrier is applied on the warm side of the insulation (TIASA,
2001).
In selecting a vapour barrier, material comparisons should be made
between the various permeability ratings as supplied by manufacturers as there
may be vast differences between materials. Care should be taken to ensure that the
choice of vapour barriers does not affect the fire performance of the whole
assembly of insulating and finishing materials. The design of the cold insulation
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system should assume that at some time a breakdown of the vapour barrier might
occur (TIASA, 2001).
In such an event, and in the case of cold rooms, it is better that the water
vapour has an unhindered path to the cold surface to enable it to be drawn off by
the refrigeration equipment. In the case of pipe work and vessels, it is preferable
that the water vapour has free passage to the cold surface where the resultant
water or ice will be encased by the insulation. A break in the vapour barrier of the
insulation system will eventually cause the system to fail but its effective life will
have been prolonged by a design which permits the through transmission of water
vapour.
Whatever the primary reason for cold insulation, it should be designed to
prevent condensation. Condensation occurs when water vapour in the atmosphere
comes in contact with a surface at a temperature of less or equal to the dew point.
Therefore, if the surface temperature is less than the dew point, condensation will
occur. The presence of condensation on the warm side of the vapour barrier has no
detrimental effect on the insulation but, nevertheless, it is a condition, which has
to be avoided. To prevent condensation, the insulation thickness should be so
designed that temperature on the warm side of the vapour barrier is above the dew
point (TIASA, 2001).
In calculating the thickness of insulation required to prevent condensation,
it is prudent to know or assume conditions of high relative humidity. If the fluid
inside the pipe or vessel is likely to remain static for long periods when the
ambient temperature is below the freezing point of the fluid, it is important that
this shall be stated. Also, the fluid in small diameter pipes may be especially
susceptible to freezing, particularly if the rate of flow is intermittent or slow, it
may be necessary to consider the use of supplementary means of heating, possibly
only in local areas, like heat tracing.
2.2.1 Application of Cold Insulation
All insulation should fit snugly around piping and equipment. On low
temperature insulation work all attachments to the piping or equipment and
projecting through the insulation should also be insulated for a distance of four
times the thickness of the basic insulation from the point where the projection is
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exposed. All the insulation and the vapour barrier should be continuous at pipe
supports. Where metal cradles preformed to the outside diameter of the insulation
are provided at the pipe supports the cradle should be designed to prevent undue
compression of the insulation due to the weight of the insulated pipe (TIASA,
2001).
Joint Sealers and Adhesives
All materials intended for use for cryogenic insulation of pipes and vessels
should be checked for their suitability at low temperatures and if, for example, no
acceptable joint mastic is available for -196C (liquid oxygen, nitrogen, etc) then
only the joints on the outer layer on a multi-layer system should be sealed. Joint
sealers and adhesives should be completely compatible with the insulation, vapour
barrier and the item being insulated (refer manufacturers recommendations).
When insulating low temperature pipe work, it is advisable to create
circumferential vapour dams extending from the bare pipe to the vapour seal on
the warm side of the insulation. The longitudinal spacing of the dams is arbitrary
and as a guide, 2m, for very low temperatures to 10m for, say chilled water,
should be considered. The purpose of the dams is to prevent the failure of long
sections of pipe insulation should the warm side vapour seal be ruptured in any
way.
Support For Insulation
The following can support insulation:
Adhesive
Pins plastic or nylon
Strapping bands for large cylindrical surfaces
Pressure-sensitive tape for small diameter surfaces
Pre-installed insulation support rings, normally used on large vertical
vessels.
Vapour Barriers
The following tables provides a guideline for the required water vapour
permeance for different plant cold surface temperatures:
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Table 2.2 Water vapour permeance for different plant cold surface temperatures
(Source : Thermal Insulation Handbook, The Thermal Insulation Association of Southern Africa,
2001)
Structural Barriers
Often prefabricated to exact dimensions required and ready to install, these
are rigid sheets of reinforced plastic, galvanized, aluminium or stainless steel
jacketing - flat, corrugated or embossed.
Membran Barriers
Metal foils, laminated foils and treated papers, plastic films and sheets,
and coated felts and paper - these are either part of the insulation as supplied or
can be supplied separately.
Coating Barriers
In fluid form as a paint or mastic (or semi-fluid of the hot-melt variety) the
material can be asphaltic, resinous or polymeric. These provide a seamless coating
but require time to dry and are normally reinforced with a membrane sandwiched
between layers. Special attention must be given to vapour sealing of protrusions,
joints or any other discontinuities such as glands, local to valve spindles or
mechanical drives, etc.
Protection of Insulation
Protection of the insulation may consist of metal cladding or a coating
system. Metal and non-metallic finishes should generally be as per the insulation
guideline for hot insulation. However, care should be taken where piping and
equipment is being clad; the cladding should be manufactured and installed so as
to prevent the vapour barrier being punctured. Cushioning material applied
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between screws or rivets and vapour barrier, or other suitable means, would be a
normal practice.
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a. Cellular Glass
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For cold insulation, we can replace heat loss with heat gain.
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should be coated with a suitable paint. It has been found that below this
temperature corrosion conditions can occur.
Pre-Installation support, Insulation supports shall be installed prior to the
application of the insulation.
2.6.2 Designing Insullation Systems
Factors, which influence the design of an insulation system, are (TIASA,
2001):
Location of Plant
Indoors
Outdoors protected from the weather
Outdoors exposed to the weather
Shape, size and elevations all need to be taken into consideration
Temperature Condition
The normal operating temperatures
The extreme temperature if other than normal operating
temperature
Any fluctuating temperature
Duration of extreme or fluctuating temperatures
Surrounding Atmospheric Condition
Ambient temperature
Relative humidity to establish dew point for cold insulation
Flammable conditions
Potentially corrosive atmosphere
Acidic conditions in atmosphere
Air flow over insulated surface (wind velocity)
Special or Service Conditions Requirements
Resistance to compression, for example, foot traffic
Resistance to fire
Resistance to vibration
Resistance to mechanical damage
Resistance to corrosive fluids or gases
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1. CHAPTER 3
NEEDS AND IDEAS
3.1.Needs
Since heat always flow from a higher temperature region to one at a lower
temperature, there is a continuous flow of heat from outside to the refrigerated
space, whether it is through walls or floor. To limit the amount of such heat flow,
it becomes necessary to use good insulating material for the system. In this case,
the temperature difference between the outside and the refrigerated space is large.
Thus it becomes essential to use insulation.
Heat transfer, as we have studied, occurs due to conduction, convection
and radiation. For reducing the heat flow through the walls and roofs of cold
storages, the heat flow due to conduction and convection has to be reducted. The
heat flow due to conduction can be reduced by the use of materials having a low-
heat conductivity. The heat transfer through convection can be reduced by having
very small closed air cells in the insulation material. Based on this theory, we
conclude that the basic needs is that an insulating material should have a low-heat
conductivity and a number of small closed air cells for good insulation.
The insulation strategy is to minimize radiative heat transfer, minimize
convective heat transfer, and introduce a minimum of solid conductance media.
Factors considered in the selection of the most suitable insulation include it
ruggedness, convenience, volume, weight, ease of fabrication and handling, and
of course thermal effectiveness and cost.
The existing insulation product hasnt been able to answer the needs of
consumers yet who are well marked by complaints regarding the operational
costs, and performances.However, we can meet consumer expectations related to
this product by listen to their voices at the beginning of this project.Thus, we do
survey in orderto identify the needs of existing consumers.
3.2. Consumer Requirement
Consumer requirement is consumer ideas that have been surveyed,
analyzed, and examined where those consumer voices are affecting the
sustainability of product design and development.
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Based on Figure 3.1 which is extracted from the survey, it can be seen that
from we got 12 respondentswhich comes from PT Pagoda Sakti, Air Liquide, and
Huntsman Indonesia as producing company of insulation, and also several user
companies such as Saudi Aramco, Schlumberger, Energi Mega Persada, PT
Perusahaan Gas Negara, Vico Indonesia, and Mr. Nelson Saksono as cryogenic
expert.
3.3. Consumer Needs Interpretation
The results of interviews obtained is then converted into a list of
consumers needs which is used as a standard of design concept for new insulation
for low-temperature product. Table below describes consumer needs from the
interpretation based on the answer of interviews.
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Micro fiberglass
Insulation that is
How your company We should know the temprature
easily installed to
7 determine/select we want to maintain, the size of
every length and size
insulation product? the system
of the system
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and make it easier to classify so we can categorize them into several categories.
This category used as reference for developing insulation for low-temperature
system.
Here is the result of tidy up needs.
Table 3.3.List of tidy up needs
No. List of Tidy Up Needs
Insulation that has thermal conductivity minimum as low as 0.03
1
W/m.K
2 Insulation that is able to withstand thermal expansion
3 Insulation that is able to withstand wear or pressure
4 Insulation that is able to withstand extreme external condition
5 Insulation that is firm and ductile enough to withstand hit or crash
6 Insulation with a competitive price
Insulation that is easily installed to every length and size of the
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system
8 Insulation that is easy to maintain
9 Insulation that can withstand water absorbtion
Need
Needs
Number
A RETAILING
6. Insulation with a competitive price
B PRODUCT PERFORMANCE
Insulation that has thermal conductivity minimum as low as
1.
0.03 W/m.K
2. Insulation that is able to withstand thermal expansion
3. Insulation that is able to withstand wear or pressure
Insulation that is firm and ductile enough to withstand hit or
5.
crash
8. Insulation that is easy for maintenance and services
9. Insulation that can withstand water absorbtion
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C PRODUCT PERCEPTION
Insulation that is able to withstand extreme external
4.
condition
Insulation that is easily installed to every length and size of
7.
the system
After grouping has been done, grading or ranking is done to know how
important these needs for insulation for low-temperature product. Needs rank
consists of :
1 undesirable needs
2 not important needs
3 nice to have needs
4 highly desirable needs
5 essential needs
Need
Needs Rank
Number
A RETAILING
6. Insulation with a competitive price 4
B PRODUCT PERFORMANCE
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2. CHAPTER 4
3. SPECIFICATION
4.
4.1. List of Metrics
The focus in this chapter is translating what customer needs from the previous
chapter into product specification. This chapter, we define the specification of the
product to all of needs which has been grouped and given rank into dimension and
then giving unit based on the specification. By changing the qualitative form into
the quantitative one, it helps us to determine what we should do in the future to
reach our goal to produce the desirable product.
5. Table 4.1 List of Metrics
Metric Need
Metric Rank. Units
No. Nos.
1 1 Thermal conductivity 5 W/mK
o
2 2 Service temperature range 5 C
3 3 Durability 4 Year
4 3,8 Combustibility 3 Combustible/Non
5 3,9 Water vapour transmission 4 gm/Nh
6 4 Density 4 kg/m3
7 4,5 Thickness range 2 Mm
8 6 Unit manufacturing cost 5 US$/m2
9 7,8 Time to assamble 1 S
10 8,9 Surface spread to flame 3 Class
6. (Source: Reproduce from the literature)
4.2. Metrics & Needs
The next step is making a matrix of needs and metrics. This step will help us to
see if there are some needs which have a same metric units. If there are some
needs that have same metric unit, that doesnt mean we have to erase one or some
of it. Because therere some needs that has subjective specification, its possible to
have needs that have same metric.
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10
1
2
3
4
5
6
7
8
9
Water vapour transmission
Metric
Time to assamble
Thickness range
Combustibility
Durability
Density
Need
1 Insulation that has thermal conductivity minimum as low 0.03 W/m.K
2 Insulation that is able to withstand thermal expansion
3 Insulation that is able to withstand wear or pressure
4 Insulation that is able to withstand extreme external condition
5 Insulation that is firm and ductile enough to withstand hit or crash
6 Insulation with a competitive price
7 Insulation that is easily installed to every length and size of the system
8 Insulation that is easy to maintain
9 Insulation that can withstand water absorbtion
9. (Source: Reproduce from the interview & literature)
10.
4.3. Benchmarking Existing Product
As conceptual product that will move forward to its production scale, our product
needs benchmarking. Benchmarking is a way to determine the superiority of our
products to be the production of other products that similar and have been
producing in the market. The necessity to conduct benchmarking is vital, because
we will produce a product that must be able to compete with existing products in
the market overally.
The result from benchmarking also help us to project the market segment for our
product, so we can analyze which variable require to scale up, and or further
modification so it will meet both the market share and customer needs.
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Service
o
2 2 temperature 5 C (-56) 6 0 250 (-18) 450
range
3 3 Durability 4 year 80 60 50
Combust-
4 3,8 Combustibility 3 Non Non Non
ible/Non
Water vapour
5 3,9 4 gm/Nh Zero N/a N/a
transmission
6 4 Density 4 kg/m3 160 120 64
Thickness
7 4,5 2 Mm 5-10 20 120 12.7 650
range
Unit
8 6 manufacturing 5 US$/m2 25 5.5 0.58
cost
Time to
9 7,8 1 s 7200 N/a 10800
assamble
Surface spread
10 8,9 3 Class N/a 1 1
to flame
12. (Source: Reproduce from the interview & literature)
13.
14. 4.4 Target Value for Each Metric
15. After we listed competitors specifications, we need to make the
specification for our product. The specification of our product is based on
ideal value and marginal value. Ideal value is a value we hope our product
could be reach while marginal value is an acceptable value. Marginal
value is obtained based on the interview toward the respondents and the
expertise. Ideal values are obtained by selecting the ideal specification
from the best product. We use the specification from the existing product
as reference because we could not find it from any literature. Own values
are obtained by discussing together with all of our members to select the
minimum value that our product should have.
16.
17. Table 4.4 The Target Spesification
Metric Need Marginal Ideal
Metric Rank. Units
No. Nos. Value Value
Thermal 0.021
1 1 5 W/mK 0.023 0.03
conductivity 0.03
Service temperature o (-200)
2 2 5 C (-180) 20
range 5
3 3 Durability 4 Year 15 60 90 100
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20. CHAPTER 5
CONCLUSION
The use of thermal insulation is to prevent heat gain which cause energy
consumption to skyrocket by simply providing resistance to heat flow
during heat transfer mechanisms.
Basic requirement for insulation system is due to their thermal
conductivity. The lower the number of thermal conductivity the less the
flow of heat is.
The insulation strategy is to minimize radiative heat transfer, minimize
convective heat transfer, and introduce a minimum of solid conductance
media.
Based on the consumer requirements, the insulation product should be
able to meet the following criteria: have low thermal conductivity, able to
withstand thermal expansion, pressure, hit or crash, and is easy for
maintenance and services.
After benchmark to several existing products Aspen Aerogels,
Rockwool, and Arabian Fiberglass we obtain their specifications. The
existing products thermal conductivity are sequentially 0,021; 0,038;
0,028 W/m.K. The service temprature range are consecutively -156 6
o
C; 0 250 oC; -18 450 oC. Their durability are in sequence 80 years,
60 years, and 50 years. So, current best insulation product is Aspen
Aerogels.
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1. REFERENCES
2.
3. Ulric, Karl T., Eppinger, Steven D. 2000. Product Design and
Development. United States of America:McGraw-Hill Companies, Inc.
4. Aspen Aerogels, Inc. 2013. PIPE INSULATION FOR COLD SERVICE.
Northborough: Aspen Aerogels, Inc.
5. Arabian Fiberglass Insulation Co., Ltd. 2015. Heavy Density Pipe
Insulation Product. Dammam: AFICO
6. Cengel, Yunus A. 2008. Thermodynamics An Engineering Approach. 7 th.
Edition, McGraw-Hill Comp: New Jersey
7. Van ness, Smith and Abbott. 2005. An Introduction to Chemical
Engineering Thermodynamics 7th Edition. Mc-Graw Hill Comp: Cambridge
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[2]Holman, J. P. "Introduction." Heat Transfer. New York: McGraw Hill,
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[3]Zakaria, MS, Osman, K, Yusof, AA, Mohd Hanafi, MH, Saadun, MNA
& Manaf, MZA 2014, 'Parametric analysis on boil-off gas rate inside liquefied
natural gas storage tank' Journal of Mechanical Engineering and Sciences, vol 6,
pp. 845-853.
[4]"Shell Launches First LNG Outlook." Shell Global. N.p., n.d. Web. 9
Feb. 2017.
[5]Bahadori, Alireza. Thermal Insulation Handbook for the Oil, Gas, and
Petrochemical Industries. Oxford: Gulf Professional, 2014. Print.
[6]"Asbestos Exposure and Cancer Risk." National Cancer Institute. N.p.,
n.d. Web. 9 Feb. 2017.
[7]"Potential Chemical Exposures From Spray Polyurethane Foam." EPA.
Environmental Protection Agency, 02 Feb. 2017. Web. 9 Feb. 2017.
8.
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