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    Sequence File C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-4.

    S t a t i s t i c R e p o r t

    Sequence table: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-


    4.S
    Data directory path: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\
    Operator: FMT

    Method file name: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPROFENO.M

    Run Location Inj Inj. Date/Time File Name Sample Name


    # #
    ---|--------|---|------------------------|-----------------|----------------
    1 Vial 31 1 2/22/2014 2:05:15 AM IBUPRO0000004.D ST1 IBUPROFENO
    2 Vial 31 1 2/22/2014 2:25:15 AM IBUPRO0000005.D ST1 IBUPROFENO
    3 Vial 31 2 2/22/2014 2:45:13 AM IBUPRO0000006.D ST1 IBUPROFENO
    4 Vial 31 3 2/22/2014 3:05:10 AM IBUPRO0000007.D ST1 IBUPROFENO
    5 Vial 31 4 2/22/2014 3:25:08 AM IBUPRO0000008.D ST1 IBUPROFENO

    Compound: BENZOFENONA (Signal: VWD1 A, Wavelength=220 nm)

    Run Type RetTime Amount Area Height Width Symm.


    # [min] [mg/5mL] [mAU*s] [mAU] [min]
    ---|----|-------|----------|----------|----------|-------|-----
    1 VBA 11.435 1.00000 2020.97131 79.98344 0.3892 0.96
    2 BBA 11.522 1.00000 2013.03625 80.28480 0.3858 0.95
    3 VBA 11.616 1.00000 2011.99524 79.16714 0.3917 0.95
    4 VBA 11.615 1.00000 2013.92517 78.74802 0.3942 0.96
    5 VBA 11.619 1.00000 2011.57458 78.61407 0.3942 0.96

    --------|-------|----------|----------|----------|-------|-----
    Mean: 11.561 1.00000 2014.30051 79.35949 0.3910 0.96
    S.D.: 0.082 0.00000 3.84004 7.43647e-1 3.56e-3 5e-3
    RSD : 0.706 0.00000 1.90639e-1 9.37061e-1 0.9092 0.55
    95% CI: 0.101 0.00000 4.76804 9.23360e-1 4.41e-3 6e-3

    Compound: IBUPROFENO (Signal: VWD1 A, Wavelength=220 nm)

    Run Type RetTime Amount Area Height Width Symm.


    # [min] [mg/5mL] [mAU*s] [mAU] [min]
    ---|----|-------|----------|----------|----------|-------|-----
    1 BV 15.352 1.09382e-1 2064.09790 53.60612 0.5900 0.98
    2 BV 15.401 1.09202e-1 2052.20117 54.25457 0.5800 0.98
    3 BBA 15.535 1.09823e-1 2063.15942 53.93253 0.5867 0.99
    4 BBA 15.530 1.09676e-1 2062.52588 54.01070 0.5858 0.98
    5 BBA 15.538 1.09834e-1 2063.34253 53.97802 0.5867 0.98

    --------|-------|----------|----------|----------|-------|-----
    Mean: 15.471 1.09584e-1 2061.06538 53.95639 0.5858 0.98
    S.D.: 0.088 2.80532e-4 4.98683 2.32156e-1 3.63e-3 4e-3
    RSD : 0.572 2.55998e-1 2.41954e-1 4.30266e-1 0.6200 0.41
    95% CI: 0.110 3.48326e-4 6.19196 2.88260e-1 4.51e-3 5e-3

    BELOFARM HPLC 1260 VWD-1 2/24/2014 10:21:18 AM FMT Page 1 of 3


    Sequence File C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-4.S

    S t a t i s t i c R e p o r t

    Sequence table: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-


    4.S
    Data directory path: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\
    Operator: FMT

    No (or not enough) sample runs with cal. compounds available!

    BELOFARM HPLC 1260 VWD-1 2/24/2014 10:21:18 AM FMT Page 2 of 3


    Sequence File C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-4.S

    S a m p l e S u m m a r y

    Sequence table: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-


    4.S
    Data directory path: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\
    Logbook: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPIROL DI 23-
    4.LOG
    Sequence start: 2/22/2014 2:05:15 AM
    Statistic report on calibration runs: 1
    Statistic report on sample runs: 2
    Operator: FMT

    Method file name: C:\CHEM32\1\DATA\PP PT 2014\IBUPROFENO\2014-02-22 02-00-36\IBUPROFENO.M

    Run Location Inj Sample Name Sample Amt Multip.* File name Cal # Page
    # # [mg/5mL] Dilution Cmp #
    ---|--------|---|----------------|----------|--------|-----------------|-|---|----
    1 Vial 31 1 ST1 IBUPROFENO - 1.0000 IBUPRO0000004.D * 2 -
    2 Vial 31 1 ST1 IBUPROFENO - 1.0000 IBUPRO0000005.D * 2 -
    3 Vial 31 2 ST1 IBUPROFENO - 1.0000 IBUPRO0000006.D * 2 -
    4 Vial 31 3 ST1 IBUPROFENO - 1.0000 IBUPRO0000007.D * 2 -
    5 Vial 31 4 ST1 IBUPROFENO - 1.0000 IBUPRO0000008.D * 2 -

    BELOFARM HPLC 1260 VWD-1 2/24/2014 10:21:18 AM FMT Page 3 of 3

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