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Tribology International 51 (2012) 3641

Contents lists available at SciVerse ScienceDirect

Tribology International
journal homepage: www.elsevier.com/locate/triboint

Analysis of stir die cast AlSiC composite brake drums based


on coefcient of friction
A. Rehman a,n, S. Das b, G. Dixit a
a
Department of Mechanical Engineering, M.A.N.I.T. Bhopal, India
b
A.M.P.R.I., Bhopal, India

a r t i c l e i n f o a b s t r a c t

Article history: The work reported here is to analyze the suitability of Aluminum alloySilicon Carbide MMC (AlSiC
Received 5 July 2011 MMC) in the automobile brake drum applications in comparison with cast iron (CI) brake drum. A brake
Received in revised form drum dynamometer test rig was developed for the purpose. AlSiC MMC was reinforced with 10% and
23 October 2011
15% SiC particle by weight. The effect of heat treatment of the AlSiC MMC brake drum was also
Accepted 15 February 2012
studied. Performance was mainly evaluated on the basis of brake drum coefcient of friction (m).
Available online 2 March 2012
Scanning electron microscope was also used to study the effect of braking on the sliding surface of the
Keywords: brake drum.
Coefcient of friction & 2012 Elsevier Ltd. All rights reserved.
Metalmatrix composites (MMCs)
Brakes
Scanning electron microscope

1. Introduction A material for a tribo component must possess a precise balance


of physical and mechanical properties such as thermal expansion,
The aluminum alloy composites are made by mixing the damping capacity, conformability, strength, stiffness and fatigue
particulate in a molten alloy. The composites are stronger, more life [2].
rigid, harder, and more wear- and abrasion-resistant. On the Signicant efforts to develop materials for brake drums are
other hand, their ductility and fracture toughness are less, and underway, however, available literature resources are still scarce.
machining typically requires the use of polycrystalline diamond These efforts are spread in many directions, namely: development
cutting tools for efcient production. In general, aluminum of Aluminum brake components, developing different testing
decreases electrical and thermal conductivity and the coefcient apparatus, characterization of different materials, analysis of
of thermal expansion where as silicon carbide increases thermal brake system and comparative study with cast iron brake com-
conductivity while decreasing electrical conductivity and thermal ponents apart from optimization of brake material formulation
expansivity [1]. [632]. Design optimization is essential as drums constitute
The properties of MMC materials have been widely examined major weight in brake assemblies.
and would appear to offer several major advantages over cast iron
like lower density, better resistance to corrosion, lower thermal
expansion, higher thermal conductivity and higher thermal diffu- 2. Development of the AlSiC metal matrix composite
sivity [26]. brake drums
When developing brakes and suitable friction partners, engi-
neers have to consider a variety of parameters like temperature at In the present work the emphasis has been on developing
braking interface, applied braking load, speed etc. which inuence affordable AlSiC MMC brake drum, reinforced with SiC. Fabrication
the friction process of the surfaces in abrasive contact [3,4]. The of AlSiC MMC brake drum was done by stir die casting technique as
important parameters to evaluate the brake drum material are also been undertaken by Natarajan et al. [9]. Different MMC brake
friction power, friction work, friction surface temperature, mate- drums casted with aluminum alloy ADC12 had 10 wt% SiC, 15 wt%
rial of the friction partners, wear, geometry of the friction SiC and they have been referred to as ADC12-10SiC, ADC12-15SiC,
partners, environmental inuences and local mechanism [3]. respectively. ADC12-10SiC and ADC12-15SiC were also heat treated
and were referred to as ADC12-10SiC (HT) and ADC12-15SiC (HT),
respectively. Brake drum with cast iron ring, as braking surface, was
n
Corresponding author. Tel.: 91 9826203022. used as baseline reference material and named as CI (Base). Brake
E-mail address: manitars@gmail.com (A. Rehman). drum with cast iron ring is normally used in scooter applications.

0301-679X/$ - see front matter & 2012 Elsevier Ltd. All rights reserved.
doi:10.1016/j.triboint.2012.02.007
A. Rehman et al. / Tribology International 51 (2012) 3641 37

2.1. Matrix alloy for composite brake drums A higher magnication micrograph Fig. 1(d) shows good
interface bonding between aluminum and SiC particles and also
Aluminumsilicon alloy (ADC-12) was used as the metal depicts eutectic Silicon around the SiC particles.
matrix alloy. ADC-12 alloy has 10.29% Si, 0.12% Mn, 0.47% Mg,
1.98% Cu, 0.75% Fe and 0.80% Ni in aluminum. AlSi alloy has high
resistance to corrosion, is easy to weld and has lower coefcient 2.4. AlSiC MMC preparation and brake drum casting
of thermal expansion.
The composite melt was prepared by dispersing the second
phase SiC particles on to the vortex of the molten alloy. The speed
2.2. Size distribution of silicon carbide particles of rotation was maintained around 500 to 600 rpm. The second
phase dispersoid particles (10 wt% and 15 wt%) were heated to
The particles are sieved using standard sieving practice with 1000 1C in graphite crucibles in a mufe furnace. Magnesium metal
an aim to get particles within the size range of 4080 mm. Grading ( 1.0%wt) of the melt weight was also added to the melt during
of the particles shows that 3035% of the SiC particles are in the dispersing the SiC particles to induce wettability between the SiC
range of 5055 mm sizes and 25% of the SiC particles are in the particles and the melt. After the complete addition of SiC particles,
range of 4560 mm sizes. the speed of the stirrer was brought down to 200400 rpm and the
stirring continued for 35 min after which the stirrer was with-
drawn from the melt. In continuation to the above sequence and
2.3. Microstructure of AlSiC MMC materials with the mixing of SiC particles, the composite melt was poured and
solidied in the hot cast iron die, which was designed and developed
Microstructure of cast aluminum silicon ADC-12 alloy and its to cast the AlSiC MMC brake drums. Fig. 2 shows the photograph of
composites is studied in scanning electron microscopes. Fig. 1 (a) to various machined MMC brake drums along with a CI brake drum.
(c) show that the distribution of SiC particles throughout the matrix is Comparative analysis of AlSiC MMC brake drums with com-
fairly uniform for both ADC-12 SiC composites and heat treated mercially used two wheeler CI braking ring brake drum was done.
ADC-12 SiC composites samples. Fig. 1(a) Shows a typical micro- The CI brake drum was cut across to understand its constructional
structure of ADC12 alloy which consists of aluminum dendrites and details and its casting technique. Sectional view of the CI drum is
eutectic silicon in the inter-dendritic regions and around the den- shown in Fig. 3. which clearly shows the CI braking ring.
drites some inter metallic phases were also observed. Fig. 1(b) shows
a typical scanning electron micrograph of ADC-12 SiC composite
sample which clearly depicts uniform distribution of SiC particles in 2.5. Heat treatment of the AlSiC metal matrix composite
aluminum matrix. The composites were heat treated using T6 heat brake drum
treatment cycle. Fig. 1(c) shows a typical microstructure of heat
treated alloy clearly depicts the alteration of silicon morphology from The alloy and composites were heat treated in a mufe
needle shape to more or less spherical in nature. electric furnace. Following three stages were involved during

Fig. 1. Typical scanning electron micrograph. (a) ADC12 Alloy, (b) ADC12 Composite, (c) Heat Treated Composite and (d) Aluminum and SiC Interphase Particles.
38 A. Rehman et al. / Tribology International 51 (2012) 3641

heat treatment of the materials: 3. Test rig for brake drum performance evaluation

(i) Solution treatment: the alloy or composite are heated for Friction material manufacturers and researchers around the
8 h at a temperature of 490 1C until the alloying solute world have explored various methods to predict the performance
elements are completely dissolved in Al solid solution, of a friction material in a specic vehicle braking system [29].
(ii) Quenching: the solution treated material is cooled rapidly in Important test results of different materials for brake applications
the water to prevent the precipitation of the solute elements and their analysis with their tribological behavior were reported
and to obtain a super saturated solid solution and by Sallit et al. [5], Mosleh et al. [7], Natarajan et al. [10], Uyyuru
(iii) Articial aging: hardening can be done by reheating the et al. [14], Shorowordi et al. [16], Cueva et al. [25], Daoud et al.
quenched alloy to a temperature of 180 1C for 8 h in order to [26], Kennedy et al. [27] and Gomes et al. [31] using a pin on disk
get improved properties. machine. A sub-scale disk brake testing (SSBT) system was built
to enable instrumented tests to be performed on candidate truck
brake materials by Blau et al. [6]. A brake drum test rig was
developed to test brake drums by Natarajan et al. [9]. Fash et al.
developed a small specimen testing apparatus to characterize the
friction behavior of the braking pairs [11]. Wear processes at the
interfaces of the specic rotor-pad combinations have been
studied through the analysis of friction and the use of electron
microscopy by Howell et al. [13] on a test setup. Laden et al. [15]
tested frictional characteristics of AlSiC MMC brake disk on a
specially designed braking stand. Shaoyang et al. [17] developed
a chase machine to test and compare the performance of two
AlSiC MMC brake drums each reinforced with different SiC
particle size. In order to simulate the heating produced during
braking, an apparatus was developed to evaluate the effect of
thermal stresses with SiC reinforced AlSiC MMC brake drum by
Marco et al. [18]. Straffelini et al. used block on disk machine to
study the inuence of load and temperature on the sliding
behavior of AlSiC MMC material against friction material [20].
Fig. 2. Brake drums made up of different materials.
Comparison of Chase and inertial brake Dynamometer testing
of automotive friction materials was done by Tsang et al. [23].
Greening et al. [29] used dual dynamometer differential effec-
tiveness to predict the whole vehicle braking performance.
Kuroda et al. [30] developed a scale dynamometer testing facility
for observing rapid performance characteristic. Ramachandra Rao
et al. [32] used an inertia dynamometer with a data-logging
system. In the light of the study of test setups used by various
researchers and on the basis of their reported performance of
various materials a brake drum test rig was designed and
developed to compare the performance of brake drums casted
with different AlSiC MMC materials with that of CI brake drum.
Fig. 4 shows the test rig developed for testing brake drums of
Fig. 3. Sectioned view of CI brake drum. two wheelers. All the parts of the setup are placed coaxial to each

Fig. 4. Brake drum test rig.


A. Rehman et al. / Tribology International 51 (2012) 3641 39

other in such a fashion that the driving element of the test rig, an the contact surface, rather, because of their angular shape,
AC motor (A), is connected to a ywheel shaft (B) through an scratches the counter surface material which is oxidized during
electromagnetic clutch (C). The ywheel shaft on the other end is the sliding process because of higher degree of localized heating.
overhung and is mounted with a chuck (D) to hold the brake SiC particles increase the surface to surface friction due to their
drum to be tested. Chuck is placed coaxial to a tailstock (E) which inherent property of hardness. The brake drum test samples of
is mounted so as to align the brake shoe plate (F) with the brake ADC12-10SiC (HT) and ADC12-15SiC (HT) have further higher
drum. Brake shoe plate also holds a high precision load cell such coefcient of friction at all applied brake force and speeds as
that it records the tangential load on the braking surface. This compared to the values obtained with ADC12-10SiC, ADC12-
tangential load is used to calculate the braking torque and 15SiC and CI. Heat treatment of the composite material further
coefcient of friction of the braking surface. Speed is measured hardens the aluminum alloy and makes the SiC particles more
by an electromagnetic pickup. Gravity braking mechanism (G) has rm in the matrix which results in increased coefcient of
been designed to maintain a uniform braking load during all the friction. Hence, in application heat treated composite material
tests. The brake drum is driven by an electric motor which is brake drum would need less effort to stop the vehicle in
controlled by a variable frequency drive for speed variation. One comparison to other test materials. The material pair used for
thermocouple was embedded in the stationary friction liner to brake drum applications should have higher and stable coefcient
record the dynamic changes in liner temperature during braking. of friction [10]. However, very high coefcient of friction has its
A data acquisition card on the computer acquires real time own disadvantages in automotive applications [26]. Results
data and displays it on a computer display screen and also on the shown here can be used as a reference data to tailor a material
analog display panel (H). Performance is then calculated and then for specic application other than the automotives. The wear and
displayed on the result screen. frictional behavior of the material pairs is complex due to
additional factors like contact asperities, wear debris, surface
contact percentage of drum and liner rubbing surface [22].
4. Results and discussion
4.2. Coefcient of friction and inuence of transfer layer
Each new pair of brake shoes and drum was operated with
about 250 brakes to stop the drum at medium speeds and loads so
The results shown in Fig. 5 for coefcient of friction need to be
as to wear off the mating surfaces to ensures more than 90%
understood in the light of transfer of layer from one surface to the
surface to surface contact. The burnishing process helps in
other surface during rubbing/sliding. The formation of third body
repeatability of results. However, each test was repeated three
or tribo induced lms as a result of sliding between a pair of
times and average values of the performance parameters are
contacting surfaces has a role in reducing friction and wear.
reported here. Tests at three different operational speeds were
During sliding contact, transfer and back transfer of material
conducted and on each speed six braking forces were applied.
between contacting sliding surfaces can occur [2]. The transfer
Testing sequences were intended to create actual operating
layer is a body composed of various elements of different sizes. If
conditions by implementing user dened braking forces, and
the hardness of the transfer layer is greater than that of the
speeds. The test speed has been shown on the graph in kilometer
matrix, meaning that it acts as a protection as well as a semi-
per hour (km/h) in place of revolutions per minute (rpm) so as to
lubricant. The transfer layer does not have a regular thickness and
show the on road test speed for the brake drum.
is composed of various elements whether it is stratied or
fragmented [5]. The lms tend to have complex, heterogeneous
4.1. Effect of braking load and speed on coefcient of friction microstructures since the friction materials from which they form
may contain in excess of 15 different additives [6]. Uyyuru et al.
Fig. 5 shows that the coefcient of friction of the brake drums reported transfer of the pin material occurs because of ploughing
varies in a narrow scatter band for brake drums of different action of the hard asperities of disk material against the relatively
materials which is according to the fundamentals of dry sliding soft pin material [14]. Laden et al. has also reported that under
solids under dry lubrication. The coefcient of friction for CI brake certain operating conditions the transfer layer breaks which again
drum is minimum under all speeds and braking force and lower affects coefcient of friction [15]. The fall in coefcient of friction
than ADC12-10SiC and ADC12-15SiC brake drums. The SiC parti- for CI after 540 N and for heat treated composite after 720 N can
cles are considerably harder and are not plastically deformed at be attributed to the phenomena of transfer layer making and

Fig. 5. Trend of coefcient of friction with increasing order of brake load at different speeds.
40 A. Rehman et al. / Tribology International 51 (2012) 3641

breaking. Experimental results of Shorowordi et al. [16] also show


that a mixed layer is formed on the worn surface of MMCs. The
layer mostly contained the constituents of the brake pad which
act as counter body. Straffelini et al. [20] reported presence of
transfer layer on the basis of SEM micrograph and reported that
the layer contained friction material on the basis of EDXS analysis.
Straffelini et al. also reported that increase in contact temperature
decreases coefcient of friction. The paper also states the fact that
friction coefcient is in general determined by two phenomena,
rstly due to the adhesive interaction between the contacting
asperities and secondly due to the ploughing contribution due to
abrasion. Further, it reports that one of these two dominates the
other depending upon the SiC weight percentage in the aluminum
composite material. Higher SiC in the aluminum composite
results in adhesive interaction rather than abrasive one [20].
At low applied braking force and speed the friction coefcient
is observed to be less due to less formation of transfer lm at the
interface [10]. Critically examining the trends of the coefcient of
friction curves, in Fig. 5, against braking force it can be suggested
that with increasing order of braking force from 180 N to 540 N Fig. 6. Overall average coefcient of friction for different brake drums.
the coefcient of friction increased marginally and then decreased
for cast Iron at all speeds. Similar trends were observed with
AlSiC MMC brake drums with the coefcient of friction getting
maximum at slightly higher braking force of 720 N. The coef-
cient of friction response with CI and AlSiC MMC brake drums
can also be understood in the light of the explanation presented
by Howell et al. and Uyyuru et al. [13,14]. During light braking
force, the product of specic heat and density signicantly affects
the peak disk temperature than does the thermal conductivity.
Uyyuru et al. reported that during moderate to heavy braking,
thermal conductivity plays a predominant role in determining
peak disk temperatures [14]. Howell et al. reported that during
light braking, cast iron rotors will run cooler than aluminum MMC
rotors but as the applied pressure increases, aluminum MMC
rotors with their high thermal conductivity will run cooler and
should show superior frictional stability over cast iron rotors [13].
Also it has been reported that temperature under certain range
slightly increases coefcient of friction while excessively high
temperature has a fading effect and coefcient of friction falls
[3,32]. The excessively high temperature were not encountered in
the present work. However, making and breaking aspect of Fig. 7. Maximum temperature at the braking interface.
transfer layer may have played a very important role in the
nominal uctuations observed during drum testing. As reported
by Osterle et al. [8] the coefcient of friction decreased with speeds and braking force. The gure has been included so that the
increasing braking stress. It was reported that during the run in values reported here can be used for brake drum design purposes.
period the coefcient of friction increases steadily from 0.4 to As shown in the gure overall average coefcient of friction for CI,
0.7 at the low contact pressure and from 0.3 to 0.5 from the high ADC12-10SiC, ADC12-15SiC, ADC12-10SiC (HT) and ADC12-15SiC
contact pressure, respectively. Osterle et al. points out that, (HT) brake drums was 0.56, 0.78, 0.80, 0.90 and 0.93, respectively.
though this behavior can be explained by the formation and Higher coefcient of friction with composite material can be
growth of contact areas, chemical and microstructural changes attributed to the hard SiC particles which penetrate deep into
may play an important role as well. In fact, the material formed the counter surface leading to formation of microchips from
during the run in period at the surface, the so called friction layer, counter surface. As a result greater amount of frictional force is
differs considerably from the original pad material. required for sliding of composite over the counter surface. As the
Straffelini et al. reported increase in the contact temperature SiC content increases number of SiC particles penetrating to the
produced a decrease in the coefcient of friction [20]. Rhee et al. counter surface increases and thus the coefcient of friction in
[3] has investigated that the frictional force during sliding, is to be composites increases with increase in SiC content.
the power function of applied load and sliding velocity at a
particular temperature. Under heavy braking conditions, the 4.4. Braking surface interface temperature
value of frictional force reduces due to rise in temperature and
result in brake fade [10]. Fig. 7 shows the maximum interface temperature recorded at
maximum braking force and speed for all brake drums. Braking
4.3. Overall average coefcient of friction of all brake drums interface temperature with CI brake drum was 205 1C followed by
ADC12-15SiC (HT), ADC12-10SiC (HT), ADC12-15SiC and ADC12-
Fig. 6 shows overall average coefcient of friction of different 10SiC which was 184, 175, 125 and 120 1C, respectively, during
AlSiC MMC and CI brake drums for all speeds and braking force. braking. The results are in agreement with Howell et al. who
Overall average coefcient of friction was calculated at all test suggested that as the applied braking force increases, aluminum
A. Rehman et al. / Tribology International 51 (2012) 3641 41

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