NDT20
Contents
Section Subject
Preliminary pages
Contents
Standards and Associated Reading
COSHH, H&S, Cautions and Warnings
Introduction to NDT Methods
NDT Certification Schemes
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10 Radiographic Techniques (for Welds in Plate and Pipe)
10.1 IQI type and placement
10.2 Location markers
10.3 Identification of radiographs
10.4 Radiation energy
10.5 Source to film distance
10.6 SWSI techniques
10.7 Double wall single image
11 Interpretation of Radiographs
11.1 Introduction
11.2 Viewing conditions
11.3 Reporting
11.4 Film quality
11.5 Interpretation of radiographic images
11.6 Artefacts
11.7 Interpretation of weld radiographs
11.8 Interpretation of casting radiographs
12 Localisation
12.1 90method
12.2 Tube (source) shift method
12.3 Tube (source) shift method with lead markers
13 Units Used in Radiography
13.1 Ionisation (exposure)
13.2 Absorbed dose
13.3 Man mammal equivalent or radiobiological equivalent
13.4 Dose rate
13.5 Source strength or activity
13.6 Specific activity
13.7 Output
14 Radiation Monitoring Devices
14.1 Survey meters
14.2 Personal monitors
15 Radiation Safety
15.1 Precautions
15.2 Exposure limits for radiation workers
15.3 Permitted levels
15.4 Safe working distances
16 Glossary
Appendix
Product Technology Notes
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Preface
These notes are provided as training reference material and to meet the study
requirements for examination on the NDT course to which they relate.
They do not form an authoritative document, nor should they be used as a reference for
NDT inspection or used as the basis for decision making on NDT matters. The standards
listed are correct at time of printing and should be consulted for technical matters.
NOTE: These training notes are not subject to amendment after issue.
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Standards and Associated Reading
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EN ISO 10675-2 Non-destructive testing of welds Part 2: Evaluation of welded
joints in aluminium and its alloys by radiography Acceptance
levels
EN 12681 Founding Radiographic examination
Associated Reading
NDT Ed.org Introduction to radiographic testing
http://www.ndt-
ed.org/EducationResources/CommunityCollege/Radiography/cc_rad_index.htm
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COSHH, H&S, Caution and Warnings Relevant to TWI Training & Examination
Services
Introduction
The use of chemicals in NDT is regulated by law under the Control of Substances
Hazardous to Health (COSHH) Regulations 2005. These regulations require the School to
assess and control the risk of health damage from every kind of substance used in
training. Students are also required by the law to co-operate with the Schools risk
management efforts and to comply with the Control Measures adopted.
The School holds Manufacturers Safety Data Sheets for every substance in use. Copies
are readily available for students to read before using any product. The Data Sheets
contain information on:
What is Exposure?
Exposure to a substance is uptake into the body. The exposure routes are:
Many thousands of substances are used at work but only about 500 substances have
workplace exposure limits (WELs). Until 2005 it had been normal for HSE to publish a
new edition of EH40, or at least an amendment, each year. However, with increasing use
of the website facilities, the HSE no longer always publishes a revised hardcopy edition
or amendment.
The web-based list applicable from 1 October 2007 can now be found at
http://www.hse.gov.uk/coshh/table1.pdf
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Safety and Environmental Requirements
Ultrasonic testing requires the use of couplant and cleaning fluids, some of which may be
hazardous to health. Extended or repeated contact of such materials with the skin or
mucous membranes shall be avoided.
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Introduction to Non-Destructive Testing
Non-destructive testing (NDT) is the ability to examine a material (usually for
discontinuities) without degrading it or permanently altering the article being tested, as
opposed to destructive testing which renders the product virtually useless after testing.
Other advantages of NDT over destructive testing are that every item can be examined
with no adverse consequences, materials can be examined for conditions internally and
at the surface and, most importantly, parts can be examined whilst in service, giving a
good balance between cost effectiveness and quality control. NDT is used in almost
every industry with the majority of applications coming from the aerospace, power
generation, automotive, rail, oil & gas, petrochemical and pipeline markets, safety being
the main priority of these industries. When properly applied, NDT saves money, time,
materials and lives. NDT as it is known today has been developing since around the
1920s, with the methods used today taking shape later and vast technological
advancements being made during the Second World War. The basic principal methods
are:
In all NDT methods, the interpretation of results is critical. Much depends on the skill and
experience of the technician, although properly formulated test techniques and
procedures will improve accuracy and consistency.
Visual testing begins with the eye; however, the first boroscopes used a hollow tube and
a mirror with a small lamp at the end to investigate the bores of rifles and cannons for
problems and discontinuities. In the 1950s, the lamps were replaced by glass fibre
bundles which were used to transmit the light. These became known as fibrescopes
which were also less rigid, increasing the capabilities of testing. With usage expanding,
many users began to suffer from eye fatigue which led to the development of video
technology. This was first used in the 1970s and relies on electronics to transmit the
images rather than fibreoptics.
Further enhancements to video technology include pan, tilt and zoom lenses, and
mounting cameras to platforms and wheels, all allowing more parts to be tested and
better images for improved inspection. Video devices also allow recordings of inspections
to be taken, meaning permanent records can be kept. This has a number of advantages
such as enabling other inspectors to observe the test as it was performed and allowing
further review and evaluation.
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Advantages Disadvantages
Able to test large parts with a portable kit Careful surface preparation required
A different (though related) method was introduced in the 1940s. The surface under
examination was coated with a lacquer, and after drying, the sample was caused to
vibrate by the tap of a hammer. The vibration causes
the brittle lacquer layer to crack generally around
surface defects. The brittle lacquer (stress coat) has
been used primarily to show the distribution of
stresses in a part and not for finding defects.
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Magnetic particle testing (MT)
Magnetic particle testing is used to locate surface and slightly sub-surface discontinuities
in ferromagnetic materials by introducing a magnetic flux into the material.
Advantages Disadvantages
This form of NDT became much more common after the First World War, in the 1920s,
when William Hoke discovered that flaws in magnetised materials created distortions in
the magnetic field. When a fine ferromagnetic powder was applied to the parts, it was
observed that they built up around the defects, providing a visible indication of their
location.
Magnetic particle testing superseded the oil and chalk method in the 1930s as it proved
far more sensitive to surface breaking flaws. Today it is still preferred to the penetrant
method on ferromagnetic material and much of the equipment being used then is very
similar to that of today, with the only advances coming in the form of fluorescent coating
to increase the visibility of indications and more portable devices being used. In the early
days, battery packs and direct current were the norm and it was some years before
alternating current proved acceptable.
Magnetism
The phenomenon called magnetism is said to have been discovered in the ancient Greek
city of Magnesia, where naturally occurring magnets were found to attract iron.
The use of magnets in navigation goes back to Viking times or maybe earlier, where it
was found that rods of magnetised material, when freely suspended, would always point
in a north-south direction. The end of the rod which pointed towards the North Pole star
became known as the North Pole and consequently the other end became the South
Pole.
Hans Christian Oersted (1777-1851) discovered the connection between electricity and
magnetism, followed by Michael Faraday (1791-1867), whose experiments revealed that
magnetic and electrical energy could be interchanged.
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Historical perspective
Electromagnetic testing the interaction of magnetic fields with circulating electrical
currents - had its origin in 1831 when Michael Faraday discovered electromagnetic
induction. He induced current flow in a secondary coil by switching a battery on and off.
D E Hughes performed the first recorded eddy current test in 1879. He was able to
distinguish between different metals by noting a change in excitation frequency resulting
from effects of test material resistivity and magnetic permeability.
Advantages Disadvantages
Can detect through surface coatings Will not detect defects parallel to surface
Accurate conductivity measurements Not suitable for large areas and/or complex
geometries
Portability
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History of eddy current testing
The principles of eddy currents arose in 1831 with Faradays discovery of
electromagnetic induction; eddy current testing methods have their origins in a period
just after the First World War, when materials with a high magnetic permeability were
being developed for electrical power transformer cores and motor armatures. Eddy
currents are a considerable nuisance in electrical engineering they dissipate heat and
efforts to reduce their effect led to a discovery that they could be used to detect material
changes and cracks in magnetic materials. The first eddy current testing devices for NDT
were in 1879 by Hughes, who used the principles of eddy currents to conduct
metallurgical sorting tests and the stray flux tube and bar tests.
It was left to Dr Friedrich Frster in the late 1940s to develop the modern day eddy
current testing equipment and formulate the theories which govern their use. The
introduction by Frster of sophisticated, stable, quantitative test equipment and of
practical methods for analysis of quantitative test signals on the complex plane was by
far the most important factor contributing to the rapid development and acceptance of
electromagnetic induction and eddy current testing. Frster is rightly identified as the
father of modern eddy current testing.
By 1950, he had developed a precise theory for many basic types of eddy current tests,
including both absolute and differential or comparator test systems and probe or fork coil
systems used with thin sheets and extended surfaces.
Applications for microcomputer chips abound, from giving lift-off suppression in simple
crack detection to providing signal processing for immediate analysis of condenser tube
inspection. As with other testing methods, improvements to the equipment have been
made to increase its portability and computer-based systems now allow easy data
manipulation and signal processing. Eddy current testing is now a widely used and
understood inspection method for flaw detection as well as for thickness and conductivity
measurements.
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Advantages Disadvantages
The origin of modern ultrasonic testing (UT) is the discovery by the Curie brothers in
1880 that quartz crystals cut in a certain way produce an electric potential when
subjected to pressure - the piezo-electric effect, from the Greek piedzein (to press or
strike). In 1881 Lippman theorised that the effect might work in reverse, and that quartz
crystals might change shape if an electric current was applied to them. He found that
this was so and experimented further. Crystals of quartz vibrate when alternating
currents are applied to them. Crystal microphones in a modern stereo rely on this
principle.
When the Titanic sank in 1912, the Admiralty tried to find a way of locating icebergs by
sending out sound waves and listening for an echo. They experimented further with
sound to detect submarines during the First World War. Between the wars, marine echo
sounding was developed and in the Second World War ASDIC (Anti-Submarine Detection
Investigation Committee) was extensively used in the Battle of the Atlantic against the
U-boats.
In the years after the Second World War, researchers in Japan began to experiment on
the use of ultrasound for medical diagnostic purposes. Working largely in isolation until
the 1950s, the Japanese developed techniques for the detection of gallstones, breast
masses, and tumours. Japan was also the first country to apply Doppler ultrasound, an
application of ultrasound that detects internal moving objects such as blood coursing
through the heart for cardiovascular investigation.
The first flaw detector was made by Sproule in 1942 while he was working for the
Scottish firm Kelvin & Hughes. Similar work was carried out by Firestone in the USA and
by German physicists. Sproule went on to develop the shear-wave probe.
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Initially UT was limited to testing aircraft, but in the 1950s it was extensively used in the
building of power stations in Britain for examining thick steel components safely and
cheaply. UT was found to have several advantages over radiography in heavy industrial
applications:
No health hazards were associated with radiography, and a UT technician could work
next to welders and other employees without endangering them of holding up work.
It was efficient in detecting toe cracks in boilers a major cause of explosions and
lack of fusion in boiler tubes.
It could find planar defects, like laminations, which were sometimes missed by
radiography.
A UT check on a thick component took no more time than a similar check on a thin
component as opposed to long exposure times in radiography.
Over the next twenty years, improvements focused on accurate detection and sizing of
the flaws with limited success, until 1977 when Silk first discovered an accurate
measurement and display of the top and bottom edges of a discontinuity with the time-
of-flight diffraction (TOFD) technique. Advances in computing technology have now
expanded the use of TOFD as real time analyses of results are now available.
It was also during the 1970s that industries focused on reducing the size and weight of
ultrasonic flaw detectors and making them more portable. This was achieved by using
semiconductor technology and during the 1990s microchips were introduced into the
devices to allow calibration parameters and signal traces to be stored. LCD display
panels and digital technology have also contributed to reducing the size and weight of
ultrasonic flaw detectors. With the development of ultrasonic phased array and increased
computing power, the future for ultrasonic inspection is very exciting.
In UT a sound pulse is sent into a solid object and an echo returns from any flaws in that
object or from the other side of the object. An echo is returned from a solid-air interface
or any solid-non-solid interface in the object being examined. We can send ultrasonic
pulses into material by making a piezo-electric crystal vibrate in a probe. The pulses can
travel in a compression, shear or transverse mode. This is the basis of ultrasonic testing.
However, the information from the returning echoes must be presented for
interpretation. It is for this purpose that the UT set, or flaw detector as it is frequently
called, contains a cathode ray tube.
In the majority of UT sets, the information is presented on the screen in a display called
the A Scan. The bottom of the CRT screen is a time base made to represent a distance -
say 100mm. An echo from the backwall comes up on the screen as a signal, the
amplitude of which represents the amount of sound returning to the probe. By seeing
how far the signal comes along the screen we can measure the thickness of the material
we are examining.
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If that material contains a flaw, sound is reflected back from the flaw and appears on the
screen as a signal in front of the backwall echo (BWE) as the sound reflected from the
flaw has not had so far to travel as that from the backwall.
BWE
BWE
BWE
BWE
Defect
Defect
Ultrasonic signals
Anything that sends back sound energy to a probe to cause a signal on the screen is
called a reflector. By measuring the distance from the edge of the CRT screen to the
signal, we can calculate how far down in the material the reflector lies.
Advantages Disadvantages
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History of radiographic testing
X-rays were discovered in 1895 by Wilhelm Conrad Roentgen
(1845-1923) who was a Professor at Wrzburg University in
Germany. Whilst performing experiments in which he passed an
electric current through a Crookes tube (an evacuated glass
tube with an anode and a cathode), he found that when a high
voltage was applied, the tube produced a fluorescent glow.
Roentgen noticed that some nearby photographic plates
became fogged. This caused Roentgen to conclude that a new
type of ray was being emitted from the tube. He believed that
unknown rays were passing from the tube and through the
plates. He found that the new ray could pass through most
substances. Roentgen also discovered that the ray could pass
through the tissue of humans, but not bones and metal objects.
One of Roentgen's first experiments late in 1895 was a film of
the hand of his wife.
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In 1898, the Curies discovered another radio-active element in pitchblende, and named
it polonium in honour of Maries native homeland. Later that year, the Curies discovered
another radioactive element which they named radium, or shining element. Both
polonium and radium were more radioactive than uranium. Due to her lifelong research
in this field, Marie Curie is widely credited with the discovery of gamma radiation and the
introduction of the new term: radio-active.
Since these discoveries, many other radioactive elements have been discovered or
produced. Radiography in the form of NDT took shape in the early 1920s when H H
Lester began testing on different materials. Radium became the initial industrial gamma
ray source. The material allowed castings up to 10 to 12 inches thick to be radiographed.
During the Second World War, industrial radiography grew tremendously as part of the
Navy's shipbuilding programme. In 1946, man-made gamma ray sources from elements
such as cobalt and iridium became available. These new sources were far stronger than
radium and much less expensive. The man-made sources rapidly replaced radium, and
the use of gamma rays increased quickly in industrial radiography.
Direct radiography (DR) systems are also used based upon complementary metal oxide
sensor (CMOS) technology and TFT (thin film transistors). These systems have the
ability to directly convert light into digital format; additionally, they may be coupled with
a scintillator which coats CMOS and charged couple device (CCD) sensors. The
scintillator converts photon energy to light before the sensor and ADC converts to digital
format. Systems which use scintillators in this way are often referred to as indirect
systems.
Quality issues of any digital system are based upon the effective pixel size and the
signal-to-noise ratio (SNR). The benefits of using digital systems are the speed of
inspection and the absence of chemical processing requirements and wet film; however,
the initial equipment costs will be high.
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NDT Certification Schemes
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PCN Personal Certification in Non-destructive testing
Managed and marketed by the British Institute of Non-Destructive
Testing (BINDT) which owns and operates the PCN Certification Scheme,
it offeres a UKAS accreditied certification of competence for NDT and
condition monitoring in a variety of product sectors.
Both schemes offer NDT certification conforming to BS EN ISO 9712; Qualification and
Certification of NDT personnel, this superseding EN473.
The points below cover extracts from this document which are major items, the full
document can be viewed on the BINDT website www.bindt.org/certification/PCN.
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References
PCN documents
PSL/4 Examination availability
PSL/8A PCN documents issue status
PSL/30 Log of pre-certification experience
PSL/31 Use of PCN & UKAS logo
PSL/42 Log of pre-certification on-the-job training
PSL/44 Vision requirements
PSL/49 Examination exemptions for holders of certification other than PCN
PSL/51 Acceptable certification for persons supervising PCN candidates gaining
experience prior to certification
PSL/57C Application for certification, experience gained post examination
PSL/67 Supplementary 56 day waiver
PSL/70 Request for L2 certificate issue to a L3 holder
CP9 Requirements for BINDT authorised qualifying bodies
CP16 Renewal and recertification of PCN Levels 1 & 2 certificates
CP17 Renewal and recertification of PCN Level 3 certificates
CP19 Informal access to authorised qualifying bodies by third parties
CP22 Marking and grading PCN examinations
CP25 Guidelines for the preparation of NDT procedures and instructions in PCN
examinations
CP27 Code of ethics for PCN certificate holders
Set up equipment.
Carry out the test.
Record and classify the results in terms of written criteria.
Report the results.
Level 1 personnel have not demonstrated competence in the choice of test method or
technique to be used, nor for the assessment, characterisation or interpretation of test
results.
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Level 2 personnel have demonstrated competence to perform and supervise non-
destructive testing according to established or recognised procedures. Within the scope
of the competence defined on the certificate, Level 2 personnel may be authorised by the
employer to:
Level 3 personnel are qualified to direct any NDT operation for which they are
certificated and may be authorised by the employer to:
Assume full responsibility for a test facility or examination centre and staff.
Establish, review for editorial and technical correctness and validate NDT instructions
and procedures.
Interpret codes, standards, specifications and procedures.
Designate the particular test methods, techniques and procedures to be used.
Within the scope and limitations of any certification held carry out all Level 1 and 2
duties and;
Provide guidance and supervision at all levels.
Level 3 certificated personnel may be authorised to carry out, manage and supervise
PCN qualification examinations on behalf of the British Institute of NDT.
Where Level 3 duties require the individual to apply routine NDT by a method(s) within a
particular product or industry sector, the British Institute of NDT strongly recommends
that industry demand that this person should hold and maintain Level 2 certification in
the applicable methods and sectors.
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Training
ET 40 40 40
PT 16 24 24
MT 16 24 32
RT 40 80 72
RI N/A 56 N/A
UT 40 80 72
VT 16 24 24
Note 1. Direct access to Level 2 requires the total number of hours shown in Table 1 for Levels 1
and 2, and direct access to Level 3 requires the total number of hours shown in Table 1 for
Levels 1-3. Up to one third of the total specified in this table may take the form of OTJ training
documented using form PSL/42 provided it is verifiable and covered practical application of the
syllabus detailed in CEN ISO/TR 25107:2006.
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Table 2 Minimum duration of experience for certification.
Experience, months
NDT method
Level 1
Level 2 Level 3
ET 3 9 18
MT 1 3 12
PT 1 3 12
RT 3 9 18
UT 3 9 18
RI N/A 6 N/A
VT 1 3 12
Work experience in months is based on a nominal 40-hour week or the legal week of work.
When an individual is working in excess of 40h/week, he may be credited with experience
based on the total hours, but he shall be required to produce evidence of this experience.
Direct access to Level 2 requires the total number of hours shown in Table 2 for Levels 1 and 2,
and direct access to Level 3 requires the total number of hours shown in Table 2 for Levels 1-3
Qualification examination
Table 3 Numbers of general questions.
NDT method Level 1 Level 2
ET 40 40
PT 30 40
MT 30 40
RT 40 40
RI N/A 40
UT 40 40
VT 30 40
BRS 30 N/A
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Re-examination
a A candidate who fails to obtain the pass grade for any examination part (general,
specific or practical) may be re-examined twice in the failed part(s), provided the re-
examination takes place not sooner than one month, unless further training
acceptable to BINDT is satisfactorily completed, nor later than twelve months after
the original examination.
b A candidate who achieves a passing grade of 70% in each of the examination parts
(general, specific or practical) but whose average score is less than the required 80%
may be re-examined a maximum of two times in any or all of the examination parts
in order to achieve an overall average score of 80%, provided the re-examination
takes place not sooner than one month, unless further training acceptable to BINDT
is satisfactorily completed, nor later than twelve months after the original
examination.
c A candidate who fails all permitted re-examinations shall apply for and take the initial
examination according to the procedure established for new candidates.
d A candidate whose examination results have not been accepted for reason of fraud or
unethical behaviour shall wait at least twelve months before re-applying for
examination.
Summary
The PCN scheme is managed and administered by the British Institute of NDT (BINDT)
on behalf of its stakeholders. It meets or exceeds the criteria of BS EN ISO 9712.
1 Aerospace.
2 Castings.
3 Welds.
4 Wrought Products and Forgings.
5 Pre and in-service inspection (multi sector).
6 Railway.
There are many additional supporting documents varying from vision requirements
PSL44 to renewal and recertification (Levels 1 and 2 CP16; Level 3 CP17) and so on.
The document defines many terms used in certification of NDT personnel (PCN Gen
Section 3)
The certification body (BINDT) meets the requirements of BS EN ISO 17024 (PCN Gen
section 5)
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BINDT approves authorised qualifying bodies (AQBs) to carry out the examinations (PCN
Gen Section 5)
a The document sets out the Levels of PCN certification and what each level of
personnel is qualified to do (PCN Gen section 6). There are 3 Levels of PCN
certification.
b Candidates for examination must have successfully completed a BINDT validated
course of training at a BINDT authorised training organisation (PCN Gen Section 7).
c Table 1 shows the minimum required duration of training for all Levels and methods
plus a section of notes.
d Table 2 gives the minimum duration of experience for each Level and method.
e A candidate is required to have a vision test of colour perception and a near vision
test (Jaeger Number 1 or N4.5). PCN Gen Section a the near vision test to be taken
annually.
f Examination applications are made directly with the AQB.
g PCN Level 1s and 2 initial exams comprise general; specific and practical parts.
h Table 3 shows the number of general questions at Levels 1 and 2 examinations.
i There are 30 specific questions on the Level 1 papers.
j There are 36 questions on the Level 2 specific papers.
k A variety of practical samples are tested depending on the method and sector.
l A Level 3 examination comprises a basic and a method examination however the
basic examination needs to be passed only once. Table 4 shows the number of basic
examination questions. Table 5 shows the number of Level 3 examination questions.
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Table 5 Main method examination.
m A pass is obtained where each part is 70% or over with an average grade of 80% or
over.
n A PCN certificate is valid for 5 years.
o Renewal and recertification requirements are covered in CP16 for Level 1 and Level 2
and CP17 for Level 3.
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Section 1
Properties of Penetrating Radiation
(X- and Gamma)
1 Properties of Penetrating Radiation (X- and Gamma)
Radiation has six basic properties:
Film
Object
Source
of radiation
Figure 1.1 Penetrating radiation passing through an object and the resulting
radiograph.
Note: In film radiography thin sections appear darker while thicker sections
appear lighter. The opposite is true if a fluorescent screen rather than a
photographic film is used as a radiation detector.
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Film
Object
Source
of radiation
Two important points to keep in mind when viewing a radiographic image are:
2 The lack of side fusion will not appear as an image on the radiograph
because 0.01 which is much too small to be detected by
the technique used.
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Set-up
Resultant
radiograph
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Section 2
The Electromagnetic Spectrum
2 The Electromagnetic Spectrum
From the early part of the nineteenth centrury it was understood that light was
a waveform. Light, however, was well known to be capable of passing through a
vacuum. Scientists of the day puzzled long and hard as to how it could be
possible that a waveform could travel without some form of matter to support
it, therefore the concept of a substance called ether, which filled otherwise
apparently empty space, was postulated and a lot of research time was
expended in trying to isolate this mysterious substance. The search continued
until around 1865 when a scientist called James Maxwell predicted the
existence of electromagnetic waves. Such waves, he said, would be capable of
passing through a vacuum, since they were supported by oscillating magnetic
and electrical fields mutually at right angles to each other and to the direction
of propagation. Moreover, using mathematics, Maxwell predicted a speed of
travel for such waves that was equal to the then known speed of light. It soon
became clear that light was in itself a form of electromagnetic radiation.
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Wave length in nanometres
The electron volt (eV) is a unit of energy equal to the kinetic energy that an
electron obtains when it accelerates through an electric field of 1V. One electron
volt is equal to 1.6 x 10-19 Joules. A Mega electron volt (MeV) is equal to the
kinetic energy of an electron that has accelerated through an electric field of 1
million volts (see Figure 2.1).
From Figure 2.1 also outcomes that as wavelength increase the energy
decreases and vice versa. This relation reflects the formula .
Note: The relationship between wavelength and photon energy on which the
diagram above has been based is approximate.
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Section 3
Simple Atomic Theory
3 Simple Atomic Theory
To understand how X- and gamma rays are produced it is necessary to have a
basic understanding of atomic theory. An atom is the smallest part of any
chemical element. Atoms are known to consist of three basic types of particle,
these being the positively charged proton, the neutron (which has no electrical
charge) and the negatively charged electron. The electrical charge on the
proton and electron are equal in magnitude but opposite in polarity. The atomic
mass of a proton is, by definition, equal to 1 atomic mass unit (abbreviation:
amu; 1 amu = 1.6725 x 10-27kg). The electron has a tiny mass, around 1/1836
that of a proton (0.000545 amu or about 9.11 x 10-31kg), while that of a
neutron is very slightly greater than that of a proton at 1.0014 amu (or 1.6748
x 10-27kg). The atom is thought to consist of a positively charged nucleus
(which consists of protons and neutrons) surrounded by a cloud of orbiting
negatively charged electrons.
In the equilibrium state the number of orbital electrons is equal to the number
of protons and there is no net electrical charge. When there is inequality
between the number of protons and electrons then there is a net electrical
charge and the atom is said to be ionised. Ions may be negatively charged if
the number of electrons exceeds the number of protons or positively charged if
the converse is true. So called electropositive elements, a group which includes
all metals, like to form positive ions while the electronegative elements such as
oxygen, phosphorus, chlorine and sulphur like to form negative ions.
The orbital electrons exist in fixed energy levels or shells. Each shell can contain
a fixed maximum number of electrons. The shells are identified by letters K,
L, M, N and so on. The lowest energy level is represented by the K-shell; this is
the innermost of the electron shells and it can contain a maximum of two
electrons. The L-shell can contain up to eight electrons while the M-shell
contains a maximum of 18 and the N-shell contains a maximum of 32. The
maximum total number of electrons in each shell is equal to 2n2 where n is the
shell number counting the K-shell as one, L-shell as two, etc. Within the M, N
and other shells certain groupings of electrons produce greater stability,
elements having an even number of electrons tend to less chemically reactive
than those which have an odd number. A group of eight electrons in the M or N
shells produces an element which is the most chemically inert of all elements
an inert gas. In electropositive elements the orbital electrons are relatively
loosely bound and there is a tendency to form positive ions. In electronegative
elements the orbital electrons are relatively tightly bound and there is a
tendency to form negative ions. The inert gases such as neon, argon, xenon
and krypton either have an outer shell that is completely full or one which
contains a very stable grouping of electrons. Based on their chemical properties
the elements can be organised into a periodic table as shown below. Elements
falling in the same vertical column share very similar chemical properties.
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1 2
H He
1.008 4.003
3 4 5 6 7 8 9 10
Li Be B C N O F Ne
6.940 9.012 10.81 12.01 14.01 16.00 19.00 20.17
11 12 13 14 15 16 17 18
Na Mg Al Si P S Cl Ar
22.99 24.30 26.98 28.09 30.97 32.06 35.45 39.95
19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36
K Ca Sc Ti V Cr Mn Fe Co Ni Cu Zn Ga Ge As Se Br Kr
39.10 40.08 44.96 47.90 50.94 52.00 54.94 55.85 58.93 58.71 63.55 65.38 69.74 72.59 74.92 78.96 79.90 83.80
37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54
Rb Sr Y Zr Nb Mo Tc Ru Rh Pd Ag Cd In Sn Sb Te I Xe
85.47 87.62 88.91 91.22 92.91 95.94 98.91 101.1 102.9 106.4 107.9 112.4 114.8 118.7 121.8 127.6 126.9 131.3
55 56 57 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86
Cs Ba La Hf Ta W Re Os Ir Pt Au Hg Tl Pb Bi Po At Rn
132.9 137.3 138.9 178.5 181.0 183.9 186.2 190.2 192.2 195.1 197.0 200.6 204.4 207.2 209.0 (209) (210) (222)
87 88 89
Fr Ra Ac
(223) 226.0 (227)
58 59 60 61 62 63 64 65 66 67 68 69 70 71
Lanthanide Series Ce Pr Nd Pm Sm Eu Gd Tb Dy Ho Er Tm Yb Lu
140.1 140.9 144.2 (145) 150.4 152.0 157.3 158.9 162.5 164.9 167.3 168.9 173.0 175.0
The numbers above and below each chemical symbol are the atomic number
and the atomic weight of each element. Note: That the atomic weight differs
slightly from the atomic mass number.
Each element has its own characteristic number of protons in the nucleus. This
number is the atomic number, usually abbreviated as Z. It is the atomic
number that determines the chemical properties of a given substance. However,
each element can exist as any one of a number of nuclides or isotopes. Each
isotope of a given element has the same atomic number, number of protons
and chemical properties, but each isotope has a different atomic mass number.
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The difference in atomic mass number is due to a difference in the number of
neutrons in the nucleus. The atomic mass number is equal to the total of
protons + neutrons in the nucleus. Most elements can exist in nature as any
one of several stable isotopes. Some isotopes, however, are not stable these
are the so called radioactive isotopes. The following notation is typically used,
for example:
Where:
59 is the number of protons + neutrons (the atomic mass number).
27 is the number of protons (the atomic number).
is the chemical symbol, in this case cobalt.
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Section 4
Ionising Radiation
4 Ionising Radiation
The two types of penetrating radiation most used in industrial radiography, X-
and gamma rays, are often referred to as ionising radiation. This is because the
nature of their interaction with matter is to cause ionisation. Ionisation is
caused by loss of an orbiting electron which leaves the atom in an
electrically positively charged state (+ ion). Alpha and beta particles,
which are products of radioactive fission also cause ionisation and are therefore
included within the term ionising radiation. Neutron radiation is a hazard in the
nuclear power industry, it can [indirectly] cause ionisation, and it is therefore
often included within this group of types of radiation referred to as ionising.
Alpha and beta particle radiation are covered in greater detail in Sections 6 and
7.
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Section 5
X-Rays or Bremsstrahlung
5 X-Rays or Bremsstrahlung
The term X-ray is applied to ionising radiation produced when a beam of high
velocity (ie high kinetic energy) electrons collides with the atoms of a target
material. The photon energy of the X-radiation thereby produced depends on
two factors:
X-ray photon
(low energy)
Deflected electron
Captured electron
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Characteristic radiation peaks
[nanometers]
The maximum intensity (the number of photons per square metre) in the
continuous spectrum produced occurs at approximately2 .
The ability of the X-rays to penetrate matter depends on their photon energy,
the shorter the wavelength, the higher the photon energy, the more
penetrating the radiation. The penetrating power of the X-rays can be controlled
by increasing or decreasing the accelerating voltage, the greater the
accelerating voltage, the more penetrating the radiation. In an X-ray set the
accelerating voltage is the tube voltage.
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The two characteristic peaks shown in Figure 5.2 are caused by target material
inner shell electrons jumping to a higher energy level, and then falling back to
their equilibrium state. Characteristic radiation generally occurs at relatively low
energy, long wavelength and is of no great importance in the industrial
radiography of metallic components although it can cause a problem known as
diffraction mottling (see the section on artefacts). As the name suggests, each
element produces its own specific characteristic peaks, and measurement of
these can be used to perform chemical analysis (X-ray fluoroscopy). Low
energy X-rays can be diffracted by crystalline materials such as metals. In the
diffraction process radiation is deflected from its original path at an angle that is
determined by its wavelength and the spacing of the atoms in the crystalline
material. This effect can be used to produce the mono-wavelength X-rays that
are used in X-ray crystallography.
1 Source of electrons.
2 Target, constructed from a suitable high melting point material.
3 Means of accelerating electrons toward the target.
High velocity electrons cannot travel far in air, therefore the process of
acceleration must take place in a high vacuum.
Tungsten filament
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The target material is usually tungsten because this has a very high melting
point (above 3400 C). This reduces the chances it will be vaporised by the
large amount of heat generated. Tungsten has a high atomic number and
therefore a large number of electrons, this makes it a relatively efficient
material for converting kinetic energy to X-ray energy which in turn helps to
reduce the amount of heat produced as a proportion of the total output of
energy. Sometimes the target is constructed from tantalum (melting point
3000C) and less frequently from other refractory metals.
Nearly all anodes are hooded (see Figures 5.4 and 5.5). The hood is a high
conductivity copper shroud which is designed to intercept stray electrons and
prevent them from hitting the tube walls. The hood has a window in the form of
a beryllium insert or a thinned section of copper which permits X-rays to exit
without unduly increasing inherent filtration. Inherent filtration is the term used
to describe removal of X-rays from the primary beam due to absorption by the
materials used in X-ray head construction. The reason that a beryllium window
is used in many X-ray heads is that beryllium has a very low absorption factor
and this minimises inherent filtration whilst still affording the tube walls
protection from stray electrons.
High conductivity
copper
Hood
Electrons
Cooling fins
Beryllium
window
Tungsten target
Useful X-rays
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High conductivity hood
Hood
Electrons
Cooling fins
Beryllium
window
Tungsten target
Useful X-rays
Effective focus
size viewed
from
B = 4 x 3.8mm Actual focus size
viewed from
A = 4 x 11mm
Target
Electrons
70o
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5.1.3 X-ray tubes
The cathode and anode are mounted in an evacuated glass (or in modern tubes
metal-ceramic) envelope (Figure 5.7). The tube may be provided with shielding
to absorb any unwanted radiation that is not already shielded out by the natural
geometry of the anode. Directional type tubes produce a useful beam of
radiation that is usually in the form of a cone with a dihedral angle of around
40. X-ray tubes fitted with a panoramic anode produce a useful beam of
radiation through an angle of 360 about the tube axis.
Aluminium shell
Ceramic
insulator
Cathode Anode
Electrons
X-rays
Evacuated
chamber
Ceramic
insulator
The X-ray beam produced is filtered by the wall of the glass (or metal-ceramic)
envelope. This reduces the useful quantity of X-rays produced, with the low
energy components of the spectrum being particularly affected. Therefore it is
common in glass tubes that the tube wall is ground thinner in the region of the
useful beam in order to minimise the X-ray energy lost due to self-filtration.
Metal-ceramic X-ray tubes (and low kilovoltage glass tubes) may have beryllium
inserts (usually called windows) in order to minimise the filtration effect of the
tube wall. Beryllium is used because it has a very low X-ray absorption
coefficient and it is mechanically strong enough to contain the necessary
vacuum.
X-ray tubes are invariably mounted inside some form of tank. This is usually a
metal cylinder that may be fitted with a beryllium or plastic window to minimise
self-filtration of the X-rays produced. The tank contains a coolant which may be
oil or some type of gas. It provides high voltage insulation and mechanical
protection. In portable equipment the high voltage transformer is mounted
inside the tank.
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5.1.4 X-ray tube power supply
In order to produce a beam of electrons from the filament in the tube it is
necessary to make the anode positive with respect to the cathode. If an AC
supply is connected across the tube then the beam of electrons will pass only
when the anode is positive and the tube will act as a half-wave rectifier.
Older type portable X-ray sets were half-wave self-rectified. This produced a
considerable weight-saving compared with the earlier types of constant
potential unit. Most modern portable units are constant potential and use
lightweight solid state rectifiers to produce what is effectively DC current.
Water is a very efficient coolant and direct water-cooling of the anode permits
operation at greatly increased tube currents. For example, the maximum tube
current for an older type 200kV oil-cooled head was typically 5mA self-rectified.
With modern portable equipment maximum constant potential tube currents of
15 or 30 mA are not unusual for a 200kV head.
Older type constant potential industrial X-ray units were extremely heavy, bulky
and suitable for use only in fixed installations. Much of the weight and bulk
came from the rectification circuitry used, the so called Greinacher Circuit and
the large external oil-cooling system necessary to dissipate the large amount of
heat generated.
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Single phase
AC voltage
Greinacher circuit
Self-rectified
Constant potential
Wavelength
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5.1.5 X-ray tube controls
The radiation produced by the X-ray tube can be varied in quantity and
penetrating power (or quality) by controlling the electrical supplies to the tube.
Some recognised codes and standards such as ASME BPVC V/2 and
EN ISO 17636-1 relate the maximum kilovoltage which may be used to the
material thickness which is to be examined. Table 1 gives the approximate
limiting maximum economically penetrable thicknesses of steel for various
kilovoltages. The figures given are typical for film radiography using lead
intensifying screens and portable self-rectified equipment. Constant potential
units can be used economically on greater thicknesses than can self-rectify
units.
Figure 5.11 EN ISO 17636-1 maximum permissible X-ray tube voltage for
various materials.
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Occasionally penetrating radiation is referred to as being either hard or soft.
These terms are relative, but hard radiation is produced by high tube voltages
(above 150kV) whilst soft radiation is produced at lower tube voltage.
Penetrating power,
Kilovolts mm of steel
120 6
160 20
200 30
250 45
300 60
The total quantity of radiation produced by the X-ray set is directly proportional
to the product of the exposure time (ie the time for which the X-ray tube is
energised) and the tube current; therefore X-ray exposures are usually given in
milliampere minutes (mA.min) at a given tube voltage.
Voltage control: This alters the tube voltage (kV) by varying the low voltage
supply to the high voltage transformer. Note: That high voltage is not
generated in the control panel, this minimises the hazard to personnel.
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As explained above it is convenient to refer to X-ray exposures in terms of
milliampere minutes. For example an exposure which produces an acceptable
radiograph may have been determined to be, 36mAmins at 200kV. If this was
the case then any of the following exposures should give an identical acceptable
result:
This is because the amount of radiation produced is the same in each case.
Obviously it would be desirable to use a high value of mA, in order to reduce
the exposure time, but as explained above the use of high tube currents can
severely damage the anode of the X-ray tube and thus reduce its service life.
Therefore it is usual to operate at a value of mA which is well within the tubes
specified capabilities.
Linear accelerators
Linear accelerators (often called linacs) accelerate electrons to very high
velocities along a straight path by means of an electromagnetic waveform
generated by a device called a magnetotron. The particle velocities are similar
to those achieved in betatrons but a much higher output of radiation is
achievable. For radiation energies above 10MeV linear accelerators are
generally the preferred solution.
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5.1.7 Special types of X-ray unit
Microfocus X-ray sources
Standard X-ray equipment has an effective focus size usually in the range 0.8 -
4 mm. This is small enough to provide adequate image quality for most
standard techniques. Micro-focus X-ray equipment may have an effective focus
size as small as 0.1mm. Using such a small focus size geometric enlargement
techniques is possible whilst still producing an adequately sharp image.
Focus
Object
Image
Umbra
Penumbra
Aluminium
X-rays
Cathode tube
Electron Anode
X-rays
Evacuated
chamber
Ceramic Aluminium
insulator shell
Figure 5.13 Rod anode X-ray tube.
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Rotating anode X-ray equipment
In medical radiography a very large tube current is generally desirable as this
permits a very short exposure time which in turn helps to eliminate or reduce
unsharpness caused by relative movement during exposure. To maximise tube
current some medical equipment is fitted with a rotating anode, where the
anode rotates at high speed and the focus area of the target is therefore
constantly changing. Each section of the tungsten target is in use for a short
time followed by a slightly longer period of resting. This helps to prevent
overheating so the tube current can be greatly increased.
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Section 6
Gamma Rays
6 Gamma Rays
Gamma () ray is the term applied to the electromagnetic radiation which is
sometimes produced when the atomic nuclei of a radioactive isotope
disintegrate in the process known as atomic fission. Alpha () and beta ()
particles may also be produced during the disintegration process; in fact
gamma emission is always a by-product of alpha or beta emission. Of the three
main types of radiation produced by fission alpha is by far the most hazardous
to health; alpha and beta radiation must be taken into consideration when
assessing safety. Except as a health hazard, alpha and beta particle radiation
have no significance for industrial radiography since they are easily absorbed by
very thin materials.
The disintegration process is fixed for each radioactive isotope and as a result
the gamma ray energies produced are also fixed.
60
27 Co 28
60
Ni
0.31 MeV 1.17 MeV 1.33 MeV
The spectra produced are line or discrete spectra as opposed to the continuous
spectra produced by X-ray equipment. Table 6.1 lists the principal gamma
emissions for various commonly used isotopes. Figure 6.1 shows the line
spectrum for Iridium 192.
For example:
239
94 Pu 235
92 U 2 He
4
Thus in alpha emission there is a loss of 4amu from the nucleus and a reduction
in atomic number of 2 (see the example above). Alpha particle radiation cannot
penetrate more than a thin sheet of paper or a few centimetres of air, it is,
however, very strongly ionising. The great danger to health with alpha emitters
is that they may be ingested radioactive contamination. Once within the
human body they will in most cases cause cancer.
For example:
14
6 C 147 N E
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Thus in beta emission there is no loss from the atomic mass number whilst the
atomic number increases by 1 (see the example above). Beta radiation is more
penetrating than alpha. It can penetrate the outer layers of the skin and lead to
fatal skin burns. The damage caused is very similar to sunburn, but much more
severe. Many of the early victims of the Chernobyl disaster died as a result of
skin burns caused by exposure to high intensities of beta radiation. If beta
emitters are ingested they will often lead to cancer.
All gamma sources in use today are man-made. They are manufactured by
neutron bombardment of non-radioactive raw materials in the core of a small
nuclear reactor. The sources in use are all beta emitters, gamma rays being
produced as a by-product of beta emission. In order to prevent beta emission
or contamination hazard the sources used in industrial radiography are
invariably sealed sources. The fissile material is encapsulated in a high integrity
titanium or stainless steel shell. Beta radiation is not capable of penetrating the
walls of the capsule, and the capsule further precludes any possible
contamination hazard so long as it remains intact.
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Table 6.1 Gamma emissions for commonly used isotopes.
Penetrating
Principal Equivalent X-ray power in mm
Isotope Half-life emissions, MeV kilovoltage, kV of steel
Iridium (Ir) 74.4 days 0.31, 0.47, 0.60 400 - 600 20 - 100
192
Cobalt (Co) 5.3 years 1.17, 1.33 2000 - 2500 40 - 200
60
Thulium (Tm) 127 days 0.052, 0.084 80 up to 5
170
Ytterbium 32 days 0.17, 0.20 145 1 - 15
(Yb) 169
Selenium 118.5 days 0.121, 0.136, 320 - 450 10 - 40
(Se) 75 0.265, 0.28,
0.401
Isotope
Connection device
(stainless steel)
Figure 6.2 shows the typical encapsulation arrangement for iridium 192 and
cobalt 60. Some isotopes such as caesium 137 are double encapsulated. In the
case of caesium 137 this is because it is in the form of caesium chloride which
is highly corrosive and highly water soluble (but this is still an improvement on
caesium metal which causes an explosion on contact with water).
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6.5 Radiation intensity
The amount of gamma radiation, the number of photons, produced by an
isotope is controlled by the number of disintegrations (atomic fissions) per unit
time. The source strength of an isotope is usually expressed in curies (Ci) or
Becquerels (Bq). Source strength may also be referred to as source activity.
The Becquerel, which is the SI unit of radioactivity, is a very small unit in terms
of what is required for industrial radiography. The Curie is therefore generally
preferred. If the Becquerel is used at all then it is usually in the form of
gigabecquerels (GBq). One gigabecquerel is equal to one thousand million (109)
becquerels. One curie is equal to 37 gigabecquerels (37GBq). In the majority of
cases gamma ray exposures are expressed in curie-hours, curie-minutes or
curie-seconds; this in each case being the product of source strength measured
in curies multiplied by exposure time measured in hours, minutes or seconds.
Example:
All other factors being equal the exposure time would therefore be either:
The half-life of various commonly encountered isotopes are given in Table 6.1.
If the half-life of an isotope is known then the source activity at a given time
can be calculated if the source activity had previously been measured.
Then at time t, the source strength or activity St, can be calculated using:
St = S0 2-(t/h)
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Figure 6.3 Iridium 192 decay.
Uranium shielded isotope containers are much lighter and more portable than
their lead shielded counterparts. A uranium shielded container having a weight
of about 20kg can safely store 100 Ci of iridium 192. A lead shielded container
of the same weight would be capable of safely containing only 20 Ci of iridium
192.
1 Contain the radioactive isotope and reduce the emitted intensity of radiation
to a level which allows for safe transportation and storage.
All modern isotope containers are designed to be operated by cable (see Figure
6.6). They are of two basic types, (Figures 6.4 and 6.5). Of the two types
depicted the S tube type is intrinsically safer but around 30% heavier than the
equivalent shutter type. Older types of isotope container did not provide for
remote operation.
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Sealed
source Locking device
Connector for
delivery tube Connector for
wind-out
Projection tube
Isotope container
Wind-out
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Figure 6.7 Sealed source with flexible cable (pigtail) attached.
The output of radiation per unit time is variable for X-ray equipment up to the
maximum mA rating of the tube. The output of radiation from a radioactive
isotope is fixed by the source activity. The output of radiation produced by X-
ray equipment is generally much greater than that produced by radioactive
isotopes.
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Table 6.2 Useful thickness range for various sources of radiation
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Table 6.3 Specific activity for common radioisotopes
Note:
1 Density is for compressed caesium chloride (CsCl).
2 Density is for thulium oxide (Tm2O3).
Note: That the maximum activity of a gamma ray source is limited by its
physical size. The most useful isotopes are those which have a high value of
practically achievable specific activity. In an iridium 192 source at the maximum
achievable activity, about 2.5 atoms per 100 million are radioactive. In a cobalt
60 source the figure is only about 1 atom in every 10,000 million.
The output of radiation from a typical X-ray machine is much greater than from
a typical gamma source. This means that in X-radiography the use of long focal
to film distances is more economically feasible than in gamma radiography.
Thus, even though the focus is similar in physical size when compared with the
average gamma source, it is generally the case that geometric unsharpness is
better for X-ray techniques than for gamma.
The exposure time for gamma radiography tends to be longer. This is because
the output of radiation (in photons per second) is generally much less. Gamma
ray exposure times are usually in the range from about 30 seconds to 1 hour,
but exposure times exceeding 24 hours are not unheard of. The required
exposure time for a gamma ray source increases as the source activity reduces
with time.
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6.7.6 Physical size and weight
An iridium 192 isotope with a source activity of up to 100 curies can safely be
stored in a container weighing 15-20kg which has outside dimensions of
approximately 200 x 400 x 100mm. Such isotopes are useful for the
radiography of steel sections of up to 75mm thick. Gamma ray sources can be
used to make exposures in situations where access is extremely limited.
A typical self-rectified 300kV rated X-ray set (which is useful for the
radiography of steel sections of up to 60mm thickness) is on the other hand
considerably less portable and less manoeuvrable. A typical 300kV self-rectified
tube head could weigh 55kg and measure 300 x 300 x 750mm while the
associated control panel might weigh as much as 30 kg and measure 450 x 350
x 250mm. Low kilovoltage equipment offers improved portability and
manoeuvrability but this has to be offset against the reduced penetrating
power.
X-ray exposures tend to be shorter so there can be a cost saving with X-ray
equipment if the setting-up time between successive exposures is minimised.
Overall gamma radiography tends to be the most cost effective solution for
construction site work but X-radiography may provide the cheapest option
where are large number of similar radiographs are required (such as may be
the case in pipeline or mass production environments).
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Section 7
Methods of Producing a Radiographic Image
7 Methods of Producing a Radiographic Image
7.1 Radiographic film
Radiographic film is essentially the same as that used in photography in that it
consists of a suspension of silver halide grains in a gelatine binder on an
acetate or polyester base. Radiographic film, however, differs from
photographic film in that the:
Direct type film: Where the principal cause of image formation is the ionising
radiation itself. This may be coupled with the effect of secondary electrons
emitted from metallic foil intensifying screens.
Screen type film: Where the principal cause of image formation is light
emitted from fluorescent image intensifying screens under the action of
ionising radiation.
Super-coat
Emulsion
Subbing
0.2mm
Base
Subbing
Emulsion
Super-coat
Some radiographic film will produce good results either as a direct type or as a
screen type film. The film emulsion in screen type films usually has a matt
finish so as to avoid reflecting the light produced by fluorescence.
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Table 7.1 Classification of radiographic films
EN ISO ASTM E
AGFA CF KODAK CF FUJI CF FOMA CF
11699-1 1815
Note: Not all film categories are suitable for given purpose. Therefore for
example standard EN ISO 17636-1 lists only 3 classes (C3 to C5).
On the other hand fine grain film is offering better resolution of radiograph and
also better contrast.
From this we can say that fine grain film = slow film and coarse grain film
= fast film. The designation fast and slow is typical for US standards and
codes while EN ISO rather speaks about film factor CF.
Because film AGFA D7 is classified as film class C5, all other films classified in
this class are said to has same film factor CF = 1. There may be small variation
in speed of particular forms in given film class due to fact that class represents
some band of film speed values.
Advantage of film factor (against film speed) is that film factor is represented
by numerical value which can be used for recalculation of exposure time when it
is necessary to interchange given film by another.
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7.3.1 Latent image formation
When film is exposed to X-rays, gamma rays, or light, an invisible change called
a latent image is produced in the film emulsion. The areas exposed become
dark when the film is immersed in a developing solution, the degree of
darkening depending on the amount of exposure.
Photography utilising film emulsion similar to that in use today has been with us
since around 1839 but the mechanisms involved in latent image formation
remained a mystery until 1938 when the Gurney-Mott theory was first put
forward. Although this theory is now generally accepted there remain areas of
speculation.
Formation of a latent image involves a very subtle change in the silver halide
grain. It is known to involve the absorption of only one or a few photons of
radiation. Because of the small amount of energy involved it is obvious that
only a few atoms, out of the ten thousand million or so atoms in a typical silver
halide grain, can actually be affected. To date it has proved impossible to detect
either the physical or the chemical nature of the tiny changes involved. Against
this, however, much can be deduced about what the physical nature of these
changes must be. For one thing we know that the substance which forms the
radiographic image must be metallic silver.
We also know that the latent image is localised at certain discrete sites within
the silver halide grain. The evidence for this is shown in Figure 7.2 an electron
micrograph of a section of film emulsion that has been exposed to light followed
by brief contact with developer. Note how tiny amounts of silver (the dark
areas) have appeared (the dark areas) within each grain of silver halide.
Further it is known that prolonged exposure to light will darken the film
emulsion even without development. Therefore the mechanism of latent image
formation will by itself cause the release of silver from a silver halide grain
under extreme conditions (see Figure 7.3).
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Figure 7.3 Electron micrograph of the release of silver in a grain of silver halide
caused by very intense exposure to light.
Film cassettes must be handled with care, as they are particularly easy to
rupture during loading and unloading of the film. Cassettes which leak light can
add considerably to the cost of radiography if they lead to a radiograph having
to be retaken. Therefore it is good practice to inspect cassettes prior to use.
Leaky cassettes can often be satisfactorily repaired using opaque adhesive tape.
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Metallic foil intensifying screens
At first it may seem to be a little paradoxical that metallic (nearly always lead
but occasionally copper, steel or tantalum) foil screens can produce an
intensifying effect. All metals are good absorbers of ionising radiation so one
would naturally expect that the film density would be reduced rather than
increased. In practice however, lead or copper foil screens brought into close
contact with direct type radiographic film reduce the required exposure for
radiation energies in excess of 120keV by a factor of about two. The reason for
this is that under the action of ionising radiation of energy 120keV or greater
metals produce secondary electrons which have kinetic energy sufficient to
cause the sensitisation of the grains of silver halide which they strike. Metallic
foil screens further add to the quality of the radiograph by filtering out a large
proportion of the scattered radiation which is of lower energy (and therefore
more easily absorbed) than the primary beam.
For most purposes lead foil screens of thickness 0.03 to 0.125 mm are used but
thicker screens are used for high energy radiography. Copper screens tend to
be used only for extremely high energy techniques (above 1MeV). The lead
screens found in pre-packed film are only a few microns thick, they produce a
strong intensifying effect but have a much reduced effect on the scattered
radiation as compared with standard re-useable lead screens. Pre-packed film is
available either in individual disposable cassettes or as rollpack where a long
narrow length of film is supplied complete with lead screens in a protective light
proof sheath. Rollpack film can be cut to any desired length. The cut ends have
to be light sealed with suitable adhesive tape. Rollpack is commonly used on
pipelines in conjunction with the panoramic technique.
EN ISO 17636-1 specifies metallic screens of lead, copper, steel and tantalum
and the specified thickness range and screen material change for different X-ray
tube voltages and different isotopes.
Salt screens
Salt screens consist of a layer of calcium tungstate (or other fluorescent
material), attached using a suitable binding material, to a sheet of cardboard.
While salt screens can produce a dramatic reduction in exposure time when
used with screen type film they are seldom used in industrial radiography
because they produce an image of inferior quality, are expensive and very
easily damaged.
Fluorometallic screens
These screens, which attempt to combine the advantages of lead screens with
those of salt screens, are occasionally used in industrial radiography when there
are strong financial pressures for a reduction in exposure time. One such
application is on offshore pipe laying barges. They are even more expensive
than salt screens at around 70 for a pair of 10 x 40cm screens and they are
just as easily damaged. They do not provide quite the same reduction in
exposure time as do salt screens but the image quality is considerably improved
(although still inferior to that produced using lead screens). Fluorometallic
screens consist of a cardboard backing material with a layer of lead foil
attached, a layer of calcium tungstate or other fluorescent crystalline material
suspended in a suitable binding material.
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7.3.4 Film processing
Radiographic film forms a latent image during exposure to ionising radiation,
light or secondary electrons. By a process which is not fully understood, silver
halide grains become sensitised during exposure (see Section 7.3.1). To make
the latent image formed by the sensitised grains visible it is necessary to
chemically process the film. Films can be processed either manually or
automatically but the chemical processes involved are the same. Radiographic
film must not be exposed to light except that from darkroom safe-lamps; even
this exposure must be minimised as prolonged exposure can result in film
fogging. Extreme care must be exercised during film processing because the
wet film emulsion is extremely fragile.
Velcro fastening
Lead screen
Black PVC
Film cassette
Cardboard
backing of
screen
Velcro fastening
Development
The first stage in film processing is development. During this stage a reducing
agent such as hydroquinone or metol reduces the sensitised silver halide grains
in the film emulsion to metallic silver. Development, whether manual or
automatic, must be carried out within the temperature range recommended by
the developer manufacturer otherwise image quality will be severely impaired.
Developers for manual processing are usually designed for use at 20C, for
automatic processing this will usually be increased to around 27C. Films should
always be developed for the optimum processing time of about five minutes for
manual and fewer than two minutes for automatic development.
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Stop bath
The stop bath serves two purposes: (1) Curtail the action of the developer and
(2) Protects the fixer by reducing carry-over of developer solution. It is not
essential to use a stop bath but it is desirable because it will considerably
extend the life of the fixer. It will also help to avoid possible film artefacts,
dichroic fogging in particular. Two types of stop bath may be used, an acid or
running water. In either case the stop bath must be maintained at a
temperature which is comparable to that of the developer otherwise reticulation
may result. The developer operates in an alkaline buffer solution. Acid stop
baths neutralise the alkalinity of the developer and stop the development
process almost immediately. It is normal to allow the film to remain in such a
stop bath for 10-30 seconds. Running water stop baths quickly dilute the
developer solution thus rapidly slowing the development reaction and
minimising the damage to the fixer. It is normal to allow a time of 2-3 minutes
when using running water stop baths.
The process of removing excess silver halides is called fixing. The chemical used
to achieve this is sodium (or ammonium) thiosulphate (sometimes called hypo).
The gelatine binder which holds the silver and silver halides becomes soft and
spongy in the developer. Hardening the film serves to get rid of some of this
sponginess and gives the film better resistance to the formation of water marks
during drying. Hardening of the film emulsion, although desirable, is not
absolutely necessary if the films are subsequently washed at a temperature of
less than 25C and dried manually If automatic dryers are to be used, however,
the film emulsion will be badly damaged by the rollers if the film has not been
properly hardened.
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Washing
After fixing the film must be thoroughly washed so as to remove all traces of
the fixer chemicals from the emulsion. Insufficient washing will result in the
formation of brownish yellow stains while over-washing can cause water marks
or even frilling (see above). Adequate wash times in a running water wash vary
from 10 minutes at 30C to 30 minutes at 10C. Most film manufacturers
recommend that the wash temperature should not be more than 25C. Film can
be washed successfully in a still water bath provided that the water is changed
regularly.
Drying
The application of a wetting agent to the film prior to drying will help the film to
dry quickly/evenly without watermarks. If the films are to be dried using a
warm air draught then care must be taken to ensure that dust is not blown onto
the wet films. Warm air dryers with a downward draught dry the film more
quickly.
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7.4.3 Real-time radiography (fluoroscopy)
Real-time radiography (RTR), or real-time radioscopy, is NDT method whereby
an image is produced electronically, rather than on film, so that very little lag
time occurs between the item being exposed to radiation and the resulting
image. In most instances, the electronic image that is viewed results from the
radiation passing through the object being inspected and interacting with a
screen of material that fluoresces or gives off light when the interaction occurs.
The fluorescent elements of the screen form the image much as the grains of
silver form the image in film radiography. The image formed is a positive image
since brighter areas on the image indicate where higher levels of transmitted
radiation reached the screen. This image is the opposite of the negative image
produced in film radiography. In other words, with RTR, the lighter, brighter
areas represent thinner sections or less dense sections of the test object.
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Section 8
Production of a Radiograph
(Film Radiography)
8 Production of a Radiograph (Film Radiography)
A radiograph is a record of the way in which a beam of radiation has been
differentially absorbed by an object stored on photographic film. In order to
produce good quality radiographs economically numerous factors have to be
taken into account. First it is necessary to understand what is meant by
radiographic quality.
Radiographic sensitivity
Contrast Definition
8.1.1 Contrast
Contrast can be defined as the ease with which it is possible to distinguish
between two adjacent areas of different film density. The chief factor which
determines whether or not the two areas will be clearly defined is the degree of
difference in film density.
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Subject contrast can be defined as the degree of difference in transmitted
radiation intensity produced by a given change in subject thickness. This is
primarily a function of the type of material from which the subject is made. For
instance a 1mm step in a 10mm section of lead will produce a much greater
change in transmitted radiation intensity than would the same step in a similar
section of aluminium (assuming that the energy of the incident radiation was
the same in both cases).
The factors affecting film and subject contrast are discussed below.
The gradient of a film characteristic curve represents the change in film density
produced by a small change in subject thickness. Figure 8.3 shows how the
gradient of the film characteristic curve varies with film density. Note: The
curve for Kodak MX125, an ultrafine grain film, has the steepest gradient. The
Agfa D7 curve is in turn steeper than that of Kodak CX. D7 and CX are both
class C5 fine grain film, but CX is slightly faster film than D7. Thus MX125 will
provide the best film contrast, whilst D7 should produce contrast better than
that of CX.
The logarithm to the base 10 of a number is just the power of 10 that will
produce the number itself.
For example:
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Film density
Figure 8.2 Film characteristic curves Kodak CX, AGFA D7 and Kodak MX125
(direct type film/lead screens).
8.0
Gradient of film characteristic curve
increasing gradient = increasing film
MX
6.0
D7
CX
contrast
4.0
2.0
0.0
Figure 8.3 Gradient of the film characteristic curve versus film density for
Kodak MX125, Agfa D7 and Kodak CX.
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Thus a film having a density of 2.0 transmits 1% of the incident light intensity
while a film with a density of 3.0 transmits only 0.1%. A film with a density of
0.3 would transmit about 50% of the incident light intensity.
Figures 8.2 and 8.3 show how film density affects film contrast. Film density
does not affect subject contrast. The gradient of the film characteristic curve is
a good measure of film contrast. The gradient for all films increases with
increasing film density. If the gradient is steep then a small change in radiation
intensity or exposure time will produce a large change in film density. The
gradient of all of the film characteristic curves becomes shallow at film densities
of less than 1.5, indicating that film contrast will be poor at low film densities.
In view of this all relevant industrial standards stipulates a minimum film
density for industrial radiography.
The dotted lines show the average gradient between film densities 1.5 and 2.5
for film having a base fog level of 0.1 and 0.5 respectively. The average
gradient with a base fog level of 0.1 is about 3.6 while that for a base fog level
of 0.5 is about 2.7. This decrease in average gradient is indicative of a
reduction in film contrast.
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Film processing (affects film contrast)
Radiographic film should always be processed in accordance with the
manufacturers recommendations. Any deviation from these will result in a
lowering of film contrast and hence sensitivity.
The film attains about 80% of its final density in the first 30 seconds of
development. During the remaining 3-5 minutes of the standard
development time radiographic developers are designed to increase film
contrast. The developer works more vigorously in areas where a lot of metallic
silver has already been released. Thus film contrast gradually improves during
the final minutes of the development process. This is why radiographs which
have been pulled intentionally underdeveloped in an effort to produce
acceptable film density invariably show poor film contrast. If the film is allowed
to remain in the developer for too long, however, the developer will begin to
attack all areas of the film and contrast will begin to suffer.
It is useful to talk about different radiation energy in terms of its half value
layer. The half value layer can be defined as the thickness of any particular
material which will reduce the intensity of the incident radiation by a factor of
two. The thickness of the half value layer for any material increases with
increasing radiation energy. Examples of half value layers for various materials
and radiation energies are given in Table 8.1.
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Scatter (affects film and subject contrast)
As ionising radiation passes through any material it undergoes a process known
as scattering. Scattering occurs due to various mechanisms (the principal cause
varies with the radiation energy) all of which occur due to the way in which
radiation photons interact with atoms. When an X-ray photon strikes an atom it
will cause the atom to lose one or more electrons, so that the affected atom
becomes positively charged. Such electrically charged atoms are normally
referred to as ions. Ions, by their nature, are not stable, they will try to attract
electrons into their empty energy shells in order to achieve a zero electrical
charge. As electrons are captured from free space by ions they give up part of
their kinetic energy as a photon of radiation. These photons will radiate in all
directions from the affected atoms. Such radiation is known as scattered
radiation and can lead to an overall fogging of the film emulsion. This reduces
film contrast.
8.1.2 Definition
Definition is a measure of the sharpness of the images on the radiograph. It can
be defined as the width of the boundary between two areas of different density
on a film. The opposite of definition is unsharpness.
Increasing unsharpness
Figure 8.5 Unsharpness: The unsharpness of the boundary between light and
dark increases from left to right.
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Geometric unsharpness
A major factor affecting definition on a radiograph is geometric unsharpness.
This can be defined as the width of the penumbra. Penumbra is the word used
in physics to describe the lack of sharpness at the edge of a shadow. Umbra
means full shadow and penumbra means half shadow. So long as the source of
radiation is not a true point source (and it never is a true point source) there
will be a penumbral area at the edge of any shadow. A radiographic image is
basically just a shadow.
The focal spot of an X-ray tube and a radioactive isotope always have finite
physical dimensions so a penumbra is always produced. Once the achieved
penumbra falls below about 0.2mm the unaided human eye ceases to perceive
any further improvement in definition. For very high quality radiographic
techniques geometric unsharpness is therefore generally kept to a value of less
than 0.2mm. To achieve this, the object to film distance is kept short and the
radiation source to film distance is made as long as necessary depending upon
the radiation source dimensions.
f OFD
Ug
FOD
Figure 8.6 Geometric unsharpness.
Inherent unsharpness
Inherent unsharpness depends on three factors: the type film, the type of
intensifying screen and the quality (or photon energy) of the radiation.
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Each silver halide grain in a fine grain film is around 1m in size. To give an
idea of just how small this is, the pixel size on a computer screen at a
resolution of 1024 x 768 is in excess of 40m.
It is now known that most silver bromide grains in a direct type radiographic
film are not sensitised directly by the penetrating radiation itself. They are for
the most part sensitised by the secondary electrons released by the intensifying
screens and by secondary electrons generated within the film emulsion itself.
The greater the distance the secondary electrons are able to travel within the
emulsion the greater the resulting unsharpness.
Salt screens fluoresce strongly under the influence of X-rays and produce very
large increases in film speed. They are not generally used in industrial
radiography due to the large increase in inherent unsharpness associated with
their use.
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8.2 Radiation scattering and scatter control
Matter which has absorbed ionising radiation and which has therefore reached
an unstable energy state will emit energy in the form of radiation as it returns
to a stable energy state. Some of this radiation will be in the form of heat, in a
few specialised cases it will be in the form of light and in many cases X-rays will
be produced. Such X-rays are termed scattered radiation and they can very
adversely affect radiographic quality. Control of scattered radiation is therefore
essential if high quality radiographs are to be produced.
Source
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E0
E 0 - Eb
Ee
E0
E e E0
Pair production
The predominant scattering mechanism above 6MeV is pair production. In this
the incident X- or gamma ray photon collides either with the nucleus or an inner
shell electron. The incident photon then converts to an electron - positron pair.
A positron is a particle having the same size and mass as an electron but
opposite electrical charge. Pair production cannot occur below a threshold
photon energy of 1.02MeV. The electron-positron pair is ejected at high velocity
but the positron has a very short life. It quickly meets a free electron and
annihilation occurs - the positron and electron cease to exist and 2 photons of
0.51MeV radiation are emitted. The ejected electron emits X-rays as it collides
and interacts with the atoms in its path.
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E0
2X0.51MeV
E+
E-
Photoelectric
Compton
Pair production
Total
Figure 8.11 shows how scatter is a greater problem at low incident radiation
energy. Scatter as a percentage of the total radiation is at a minimum at
around 2MeV, however, as radiation energy increases through the threshold
photon energy of 1.02MeV pair production within the film emulsion begins to
increase inherent unsharpness resulting in poor image quality.
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8.2.2 Types of scatter
Several types of scatter cause problems in radiography side, back and
internal scatter (self-scatter). The angle formed between the direction of travel
of the primary beam and the scattered radiation (reaching the film) is called the
scattering angle or angle of scatter. Side and internal scatter have an angle
which is less than or equal to 90 while for back scatter the angle exceeds 90.
Side scatter
Radiation may be scattered by parts of the object that are not within the
diagnostic area of the radiograph or by the walls of the exposure room. This is
termed side scatter.
This type of scatter can be reduced by collimating the beam such that only the
area to be examined is subjected to the primary beam and by the use of lead
masking, diaphragms or grids. In X-radiography the use of a filter may help to
reduce side scatter.
Side scatter causes undercutting of the radiographic image around the edges of
a component where these can be seen on the radiograph or at any site where
there is a large change in section thickness (eg a bolt hole). Undercutting
causes a lack of sharpness and may mask possible defect indications.
Back scatter
Back scatter is caused by the primary beam striking an object behind the film
and scattering back.
It can easily be reduced by shielding the back of the film cassette with a sheet
of lead, approximately 2mm thick is adequate for most applications. In X-
radiography the use of a filter may help to reduce back scatter.
The presence of excessive back scatter may be detected by placing a lead letter
B on the back surface of the cassette (ie the cassette surface furthest from the
source of radiation). If there is excessive back scatter then a light image of the
letter B will be seen on the developed film. The use of a lead letter B is
mandatory when working in accordance with the ASME code and is required for
each new technique by EN ISO 17636-1 (ie not for production radiography). In
accordance with EN ISO 17636-1 the lead letter B shall be a minimum of 10mm
high and 1.5mm thickness.
Note: If a dark image of the letter B appears this is not excessive back scatter.
It merely indicates characteristic radiation caused by the letter B itself.
Should back scatter be detected then the thickness of the lead sheet shielding
the back of the film cassette must be increased.
Self-scatter
Self-scatter is scattered radiation originating from within the test component.
The detrimental effect on film quality can be reduced by the use of lead
intensifying screens placed in contact with the film and, in X-radiography, by
the use of filters.
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If the radiation source is an X-ray tube then the use of a copper filter can help
to reduce the effects of this type of scatter. A copper filter significantly reduces
the proportion of low energy radiation within the primary beam. Since it is the
low energy radiation which is chiefly responsible for scatter the use of such a
filter can reduce the overall amount of scatter occurring and in this way
improve image quality. Filters made from lead, steel or other metals may be
used in a similar way.
Metallic foil intensifying screens made from lead or other metals reduce the
effects of self-scatter for both X- and gamma ray radiography as they filter out
the low energy scattered radiation and prevent it from reaching the film.
The principle of collimation is simply that if there is less radiation then there will
be proportionally less scatter.
Diaphragms
Diaphragms take collimation a step further. They consist of a sheet of lead
which has a hole cut in it the same shape as the object which is being
radiographed. Using a diaphragm the radiographer is attempting to shield out
all unwanted radiation, the set up for radiography must however, be extremely
accurate if it is to be successful. Diaphragms are therefore more likely to be
seen where a fully automated technique is in use that allows for a very high
degree of repeatability in the set-up accuracy.
Masking or blocking
Masking or blocking consists of placing sheets of lead, bags of lead shot or
barium putty or any other radiation absorbing material around the object which
is being radiographed to reduce the undercutting effect of side scatter. Figure
8.13 below shows the benefits of blocking.
Focus or
source
Diaphragm
Object
Film
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3mm lead Undercutting
blocking
Grids
The use of a grid is generally limited to medical radiography. It consists of a
matrix of parallel metal bars set in oscillation during exposure such that the grid
itself does not produce a radiographic image. It grid is a very effective method
of reducing the effects of side scatter, but grids are very rarely a practical
option for industrial situations. In order to be effective the grid must be placed
as close as possible to the film and microfocus X-radiography it may be placed
between the film and the object.
Filters
Figure 8.11 shows how the percentage of scattered radiation is high when the
radiation energy is low. Placing a thin sheet (typically 1 to 2mm) of copper or
other metal in the primary beam, close to the source of radiation, greatly
reduces the amount of low energy radiation while permitting most of the higher
energy radiation to pass through. If there is less low energy radiation there will
be less scatter, although it is possible that film contrast will be reduced. The
use of a filter to reduce scatter is limited to X-radiography because gamma ray
sources do not produce long wavelength low energy radiation.
Oscillating
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Figure 8.15 The effect of filtration on a typical X-ray spectrum.
In addition to this both screens intensify the effect of radiation, the energy of
which exceeds 120keV. The screens do this by producing secondary electrons to
which the film emulsion is sensitive. Most of the radiation exceeding 120keV will
be part of the primary beam. Thus the effect of the primary beam is amplified
at the expense of the unwanted scattered radiation.
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Reducing focus or source to film distance
The use of a source to film distance that will produce a value of geometric
unsharpness which is less than the inherent unsharpness for the film-screen
combination in use is therefore not recommended.
In gamma radiography the number of photons produced per unit time is directly
proportional to the source activity. Source activity is usually measured in curies
(Ci) or, less commonly in gigabecquerels (GBq). Therefore gamma ray
exposures are usually expressed in curie-minutes (Ci-min) or curie-hours (Ci-h)
but may also be expressed in gigabecquerel-minutes (GBq-min) or
gigabecquerel-hours (GBq-h).
The factors listed in Table 8.2 will affect either the film speed or the amount of
radiation reaching the film and have to be taken into account when determining
the correct exposure for film radiography. In addition to these factors the
required film density obviously has an impact upon the required exposure time.
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Table 8.2 Factors affecting radiographic exposure (film radiography)
Factor Comments
Coarse grained films are fast and require a short exposure while fine
Film type
grained films are slow and require a long exposure.
The effect of intensifying screens varies with the incident radiation
energy. Metallic foil intensifying screens reduce the required exposure
time by a factor of about 2 or 3 at radiation energies of 120keV or more.
Intensifying screen
Fluorometallic screens reduce the exposure time by a factor of about 50
type
with films designed for use with such screens. Salt screens can reduce
the required exposure time by a factor of 500 but are seldom used for
industrial radiography.
Developer type and concentration together with the development
temperature can affect the film speed. Automatic processing usually
Film processing
gives a slight increase in film speed when compared with manual
processing.
Fairly minor compared with other factors. Can affect the efficiency of the
Radiation energy intensifying screens, and to a lesser extent the film speed.
Factors affecting the intensity of radiation reaching the film (Table 8.2 Part 2)
Factor Comments
The amount of radiation absorbed by a material increases with
Material type
increasing density and atomic number.
The amount of radiation absorbed by an object rises exponentially with
increasing material thickness.
Material thickness
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Steel thickness/mm
Exposure/mAmins
Exposure/mAmins
Andrex 140kV
Kodak CX
FFD 914mm
Lead screens 0.125mm
Density 2.0
Steel thickness/mm
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Steel thickness/mm
Exposure/mAmins
Exposure/mAmins
Philips 300kV X4
Kodak CX
FFD 1000mm
Pb screens 0.125mm
Standard development
Density
Steel thickness/mm
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Steel thickness/mm
Exposure/mAmins
Exposure/mAmins
Pantak 200kV
Kodax CX
FFD 914mm
Lead screens
Density 2.2
Steel thickness/mm
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Steel thickness, mm
Exposure/curie hours
Steel thickness.mm
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8.3.2 Using exposure charts (X-ray)
Focus to film distance
Two factors affect the choice of focus to film distance, geometric unsharpness
(Ug) requirements and the desired diagnostic film length (DFL).
EN ISO 17636-1 does not directly specify geometric unsharpness, but controls it
by specifying a minimum value of focus to film distance for a given effective
focus size and object to film distance, see Figures 8.22 and 8.23 below.
Example:
Figure 8.21 Butt weld in 15mm plate. Radiograph of a butt weld in 15mm
thickness steel plate (allows for a weld reinforcement of 3mm).
Taking the example given in Figure 8.21 above lets suppose that we wish to
achieve a geometric unsharpness of 0.25mm or better. This would be sufficient
to satisfy the requirements of most national codes or standards including EN
ISO 17636-1 class A.
f OFD
Ug
FOD
but the OFD can be taken as being equal to the material thickness, in this case
18mm, and the FFD is equal to the FOD plus the material thickness so:
f 18
0.25
FFD 18
If we choose to use the Pantak 200 CP the effective focus size on the broad
focus setting is about 4mm, so:
4 18
Minimum FFD 18 306mm
0.25
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Object to film distance, mm
Note: This diagram is
for an effective source
Source size: 3mm size of 3mm.
f (d-OFD)+OFD
Object to film distance, mm
Note: EN ISO 17636-1 standard (basic) techniques are Class A, while enhanced
(improved) techniques are Class B.
Geometric unsharpness at minimum
source to film distance, mm
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So a focus to film distance of 306mm will achieve the required value of
geometric unsharpness. However if we use this minimum FFD the diagnostic
film length (DFL) will be rather short due to fade off. EN ISO 17636-1 has a
requirement for Class B techniques that the penetrated thickness (based on the
nominal thickness) at the ends of the DFL shall not exceed 110% of the nominal
thickness. For Class A the requirement is that the penetrated thickness shall not
exceed 120% of the nominal thickness at the end of the DFL. This translates to
a DFL that is approximately 0.9 x FFD for Class B and 1.3 x FFD for Class A. In
this case lets apply the EN ISO 17636-1 Class A requirement. If we want to
achieve a DFL of 450mm the minimum FFD based on this will be 450/1.3 =
346. For convenience we can round this up to say 400mm.
Tube voltage
After deciding on an appropriate value for focus to film distance the next thing
to consider when determining an exposure time for an X-ray technique is what
tube voltage will be appropriate. Some standards specify the maximum tube
voltage which may be used for a given thickness of material. EN ISO 17636-1
requirements, the maximum tube voltage in our case would be about 245 kV.
However, common good practice, which is to choose a tube voltage which will
produce an exposure time of between 1 and 5 minutes at around 75-100% of
the maximum tube current, will, in nearly all cases, satisfy such codes and
standards.
The exposure chart for the Pantak 200 CP is drawn for a source to film distance
of 914mm. The maximum tube current is 14mA. Lets use 10mA. We would like
to achieve an exposure time of between 1 and 5 minutes, giving an exposure of
between 10 and 50mA.mins. The focus to film distance that we wish to use is
400mm. The exposure chart has been constructed using FFD = 914. Using the
inverse square law (see Figure 8.24) we can see that an exposure of 10 to
50mA-mins at 400mm FFD is equivalent to an exposure at 914mm FFD of
between 10 x 9142/4002 = 52.2mA-mins and 50 x 9142/4002 = 261mA-mins.
Looking at the exposure chart (see Figure 8.19) a density of 2.2 will be
achieved using Kodak CX with an exposure of about 150mA-mins at 120kV or
with an exposure of about 40mA-mins at 140kV. These values are for an FFD of
914mm. The equivalent exposures at an FFD of 400mm will be:
Thus for Kodak CX and a film density of 2.2 these exposures should work:
The 120kV exposure should produce the best film contrast while the 140kV
exposure will be more economic.
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Figure 8.24 The inverse square law.
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Changing the film density
If a film density of 2.2 was thought too light, then the film characteristic curve
(Figure 8.2) can be used to find the correct amount of exposure compensation.
Lets say that we wanted to achieve a film density of 2.5.
Using Figure 8.2 logarithm (relative exposure) for a film density of 2.2 on
CX = 1.3 while for a film density of 2.5 logarithm (relative exposure) = 1.38
Thus if we use Kodak CX film the following exposures should achieve a film
density of 2.5:
or
EN ISO ASTM E
AGFA CF KODAK CF FUJI CF FOMA CF
11699-1 1815
Note: The film factors given in Table 8.3 are approximately correct for radiation
energy in the range 0.1 to 1.0MeV. Film factors can vary with radiation energy.
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Suppose that we wish to change from film A to film B:
Old exp osure
Film factor A
Thus to change from CX to MX125 we divide exposure time by the film factor
for CX (CF = 0.7) and multiply the result by the film factor for MX125 (CF =
2.8).
Original radiograph (with density 2.5) was exposed for time 1 minute. If we
wish to produce radiograph with same density on film Kodak MX125, than the
exposure time shall be ca. 4 minutes (considered that other parameters are
constant.
Radiation energy/isotope
Material 100keV 150keV 220keV 400keV Ir192
Steel 1.0 1.0 1.0 1.0 1.0
Copper 1.5 1.6 1.4 1.4 1.1
Aluminium 0.08 0.12 0.18 - 0.35
Al alloy 4.5% Cu 0.13 0.16 0.22 - 0.35
Titanium 0.5 0.45 0.35 - -
From the table it can be seen that at 150kV the copper equivalence factor is
probably about 1.6, while that for steel is 1.0, so 18mm copper is
radiographically equivalent to 18 1.0 x 1.6 = 28.8mm steel.
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Compensating for the use of a filter
If problems arise with scattered radiation one possibility in X-radiography is to
use a filter. Typically filters made from 1 or 2mm thickness copper sheet are
used, filters made from other metals such as lead may also be used. The
difference which the use of a filter will make to the exposure time for the steel
weld in the example can be calculated using the equivalence factors in Table
8.4.
Suppose that we wish to radiograph our 18mm thickness steel weld using the
Pantak 200 at 140kV with a focus to film distance of 400mm. The exposure
required for a film density of 2.5 without a filter was calculated above as
9.2mA-mins if using CX film. The equivalence factor for copper at 140kV is
about 0.64. Therefore 1mm of copper will be radiographically equivalent to 1
0.64 x 1 = 1.6mm of steel. To find the correct exposure (for a copper filter
thickness of 1mm) we simply need to add this amount to the steel thickness
which is being radiographed:
18 + 1.6 = 19.6mm
Gamma-ray exposures
The method used to establish gamma-ray exposures from an exposure chart is
similar to that used for X-rays except that the possibility to change the radiation
energy has been removed. Before carrying out gamma radiography it will be
necessary to establish the source activity at the time of exposure. This is done
by reference to the decay chart supplied by the source manufacturer.
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Section 9
Sensitiviy
9 Sensitivity
9.1 Radiographic sensitivity
Radiographic sensitivity is the ability of radiographic system to reveal
discontinuity of certain size on the radiographic image. It can also be defined as
a measure of quality of radiographic image. True radiographic sensitivity is
difficult quantity to measure.
These days the type of IQI most commonly in use is the wire type but other
types exist, two examples being the plaque and the step hole types.
XX=
Designation
Of
XX=
Material group
Designation
(Fe, Cu, Al or Ti)
Of thickest wire
(1, 6, 10 or 13)
7 consequently
Designated wires
(1-7, 6-12, 10-16 or 13-19)
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Table 9.1 EN ISO 19232-1 wire diameters.
Designation Diameter [mm]
W1 3.2
W2 2.5
W3 2.0
W4 1.6
W5 1.25
W6 1.0
W7 0.8
W8 0.63
W9 0.5
W10 0.4
W11 0.32
W12 0.25
W13 0.2
W14 0.16
W15 0.125
W16 0.1
W17 0.08
W18 0.063
W19 0.05
Note: It is fairly easy to remember the wire diameters: if you can remember
the diameters of the first three, 3.2, 2.5 and 2mm you can arrive at all other
wire diameters by halving as shown below in Figure 9.2.
Looking along each row the wire diameters are successively halved, eg 3.2, 1.6,
0.8.
The EN ISO 19232-1 material groupings are as follows: the Fe designated IQIs
(made from low alloy steel) cover all ferrous materials; the Cu (made from
copper) cover copper, tin, zinc and their alloys; the Al (made from aluminium)
cover aluminium and its alloys; the Ti (made from titanium) cover titanium and
its alloys. Special IQIs can be used for materials lying outside these four
groups, or the contracting parties could agree to use one of the four normal
designations.
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9.5 EN ISO 19232-2 step-hole type IQIs
BS EN 19232-2 IQIs consist of stepped blocks of material with each step having
one or a pair of through drilled holes. Step thicknesses of 0.8 mm or less have
two drilled holes, while the thicker steps have a single hole. In each case the
step thickness and the hole diameter are equal.
These IQIs are supplied encased in plastic complete with lead number
identification similar to that used in EN ISO 19232-1 wire type IQIs.
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9.6 ASTM E 1025 plaque type (flat-hole type) penetrameters
ASTM E 1025 describes plaque type penetrameters (penetrameter is just
another word meaning IQI).
This type of IQI has usually three holes The 1T hole has a diameter equal to
the plaque thickness, 2T two times and 4T four times. Penetrameters up to 160
thousandths of an inch thick are rectangular and contain 1T, 2T and 4T holes.
Thicker penetrameters are circular and contain 1T and 2T holes, and hole 4T is
substituted by rounded outline of IQI.
When using this type of IQI the image quality level is typically specified as
2-2T ocationally also as 1-2T or perhaps 2-4T. If image quality 2-2T is required,
than IQI plaque 2 % is required (first digit 2) and on image of IQI shall be
visible hole 2T.
A total of eight material groups are identified by adding notches to the edges of
the penetrameter. Where the component is a weld the reinforcement should be
taken into consideration when choosing the IQI.
It used to be common good practice to place the IQI in the least favourable
position within the diagnostic area of the radiograph. This would usually have
meant placing the IQI on the source side of the specimen and towards the
extremities of the diagnostic area because this is where the contrast and
definition would tend to be at their least favourable (highest value of geometric
unsharpness and lowest film density).
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Nowadays, when performing radiography of a weld in accordance with
EN ISO 17636-1 the IQI shall be placed preferably source side, possibly film
side, in an area of uniform optical density. This usually means on the parent
material and at the centre of the area of interest. The wires may or may not be
visible in the image of the weld for double wall single image (DWSI) or single
wall single image (SWSI) radiography but they shall be placed at 90 to the
weld axis and at least a 10mm length of wire shall appear on the parent
material in an area of uniform film density. The IQI shall be placed with its
wires parallel to the weld axis on the parent material adjacent to the weld. The
requirement for visible wire length remains unchanged.
In the past it was not uncommon for national codes or standards to specify an
overall requirement for a radiographic sensitivity of 2 % or better. This was
easy to achieve on thicker sections but often impossible to achieve on thinner
sections of material. Modern radiographic standards take account of the fact
that the best achievable sensitivity for a given situation and technique is not a
fixed quantity but a variable which depends upon such factors as the type of
radiation source, the technique and the thickness of the specimen. Such
standards specify a minimum sensitivity which should be achievable using a
good quality radiographic technique. One such standard is EN ISO 17636-1.
Table 9.4 below gives some EN ISO 17636-1 requirements for SWSI
radiography with source side IQI placement, DWSI radiography with film side
IQI placement and DWDI radiography with source side IQI placement.
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Table 9.4 EN ISO 17636-1 sensitivity requirements for wire type IQIs.
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9.8 Duplex wire IQI
Duplex wire type IQI as specified by EN ISO 19232-5 consists of set of 13
element (duplexes) placed in rigid plastic holder. It is used to assess total
image unsharpness of radiographic image.
Each element consist of pair of wires with equall circular cross-section. Its
separation equals to wire diameter. Duplexes D1, D2 and D3 are made of
tungsten, the rest of duplexes is made of platinum.
The largest element in which the image of wire has just merged without an
identifiable soace between the images of two wires defines the limit of
perceptibility The total imabe usnharpness is twice the diameter of wire in the
element and diameter is considered to be a spatial resoluteion of image.
Table 9.5 Duplex wire type IQI - Unsharpness and basic spatial resolution read-
out:
Wire diameter Achieved basic spatial resolution Achieved geometrical
Duplex identification unsharpness [mm]
[mm] [mm]
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Section 10
Radiographic Techniques
(For Welds in Plate and Pipe)
10 Radiographic Techniques (for Welds in Plate and Pipe)
Three basic techniques are used for the radiography of butt welds in pipe, these
being the single wall single image (SWSI), double wall single image (DWSI) and
double wall double image DWDI techniques. All radiographs of butt welds in
plate will, in general, be SWSI.
As a general rule, wherever possible, the IQI should be placed source side. As
then they are affected both by radiographic contrast and geometric
unsharpness. Film side IQIs indicate radiographic contrast only, thus source
side IQIs give a more accurate measure of the overall radiographic quality.
It used to be standard good practice to place wire type IQIs towards the end of
the diagnostic area, with the thinner wires toward the outside of the DFL; the
wires were invariably placed across the weld and sensitivity was assessed on
the weld allowing for any weld reinforcement present. This way of working
would still meet ASME V article 2 requirements, although this document does
not specify where within the DFL the IQI should be placed. In Europe matters
are different; when working in accordance with EN ISO 17636-1 sensitivity
should generally be assessed at the centre of the DFL on the parent material.
Plaque and step hole type IQIs should, preferably, always be placed at the
centre of the diagnostic area on the parent material. Should the image of these
IQI types encroach on the weld area the radiograph should be re-taken.
If working with a wire type IQI in accordance with ASME V/2 sensitivity would
probably be measured on the weld. ASME V article 2 then has a requirement
that the film density through the diagnostic length shall not vary by more than
+30 or -15% from that measured at the IQI. The same allowable density
variation applies to plaque type IQIs, but these, of course, must be placed
alongside, not on the weld. Plaque type IQIs may be shimmed to compensate
for any weld reinforcement. If a technique produces a wide range of film density
the placement of several IQIs may be necessary in order to meet the allowable
density variation requirement.
EN ISO 17636-1 limits the diagnostic film length (DFL) by specifying that the
penetrated thickness at the ends of the DFL shall not exceed 110% (Class B
techniques) or 120% (Class A techniques) of the thickness penetrated at the
centre of the DFL.
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10.2 Location markers
All national codes and standards require the use of location markers, usually in
the form of lead letters or numbers that appear in the radiograph as a
radiographic image. It is very important that the markers are placed in such a
way as to prove coverage of the weld where a multiple exposure technique is
used. Three general rules apply:
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10.3 Identification of radiographs
All national codes and standards require unique and permanent identification of
radiographs. In general this can be applied by any suitable means although in
some cases identification using lead numbers that appear as radiographic
images is required. Where not prohibited by the contract specification-flashing
the radiographic identification is a good method. The required identification is
written on a scrap of white paper, the radiograph is suitably masked and the
scrap of paper is placed on the unmasked area. The radiograph is then flashed
with a suitable light source and the identification becomes visible during
subsequent film processing. Exactly what constitutes an acceptable unique
identification varies widely from specification to specification, but the minimum
is a unique number. ASME V article 2 requires a unique weld number, the date
and the manufacturers name or symbol. Most codes require radiographs of
repair welds to be marked with R1, R2 and R3 etcetera depending on the
number of repair attempts. RW is commonly used to identify a complete re-
weld. Items such as heat treatment condition, welder number and welding
procedure reference may also be required.
Table 10.1 EN ISO 17636-1 applicable thickness ranges for gamma ray sources
and high energy X-rays.
Penetrated thickness, w, mm
Radiation source Class A Class B
Thulium 170 w5 w5
Ytterbium 169 (1) 1 w 15 2 w 12
Selenium 75 (2) 10 w 40 14 w 40
Iridium 192 20 w 100 20 w 90
Cobalt 60 40 w 200 60 w 150
X-ray equipment, 1-4MeV 30 w 200 50 w 180
X-ray equipment, 4-12MeV w 50 w 80
X-ray equipment, 12MeV and above w 80 w 100
(1) For aluminium and titanium, the penetrated material thickness is 10 w 70 for
Class A and 25 w 55 for Class B.
(2) For aluminium and titanium, the penetrated material thickness is 35 w 120
for Class A.
ASME V/2 requires that the radiation energy employed for any radiographic
technique shall achieve the density and IQI image requirements Standard
ASTM E 94 may provide some additional guidance.
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10.5 Source to film distance
The minimum source to film distance for EN ISO 17636-1 is calculated using the
formula: where is the minimal required source to object
distance, is the effective source or focus size, is the object to film distance
and is a constant equal to 7.5 for Class A techniques and 15 for Class B.
EN ISO 17636-1 also includes a nomogram for the less mathematically minded.
ASME V/2 limits the minimum source or focus to film distance by specifying
maximum geometric unsharpness, 0.51mm for component thickness up to 50.8
mm, 0.76 mm for greater than 50.8 and up to 76.2 mm, 1.0 mm for greater
than 76.2 and up to 101.6 mm and 1.78 mm for component thickness
exceeding 101.6 mm
Figure 10.2 shows a typical set-up for exposure of a butt weld in flat plate. The
annotations refer to EN ISO 17636-1 requirements.
The source should be positioned on the centre line of the weld, directly above
the centre of the diagnostic area.
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10.6.2 SWSI technique: source internal, placed centrally
(panoramic technique)
This technique is commonly used for pipeline welds where specially designed,
remotely operated, devices known as crawlers are often used. These machines
can travel up to several kilometres along the inside of the pipeline in order to
reach the desired position to radiograph a particular weld. The typical battery
life for an X-ray crawler will usually allow about 100 exposures to be made
between successive battery charges. Gamma ray crawlers are also used.
This technique may also be used for examining girth welds in cylindrical
pressure vessels. Using thulium 170 isotopes boiler tube welds, which may have
an outside diameter of only 40mm, are occasionally examined by this
technique.
The major advantage of this technique is that it can radiograph an entire girth
weld in a single exposure. With this technique location marker placement is not
critical, but it is usually more convenient to place the markers film side. In most
cases it will be impractical to place the IQI source side for this technique,
although source side IQIs would be preferred if access is not a problem, film
side IQIs are therefore generally used. Comparator radiographs having IQIs
placed source and film side can be used to establish sensitivity requirements for
film side IQIs. In most cases three IQIs are placed at 120 intervals around the
circumference, although some specifications require more or fewer than this.
The radiograph may consist of a number of overlapping films or it may be a
single length of rollpack film. Identification of the film may be included as a
radiographic image but it may also be added later. Where several overlapping
films are used each film must be uniquely and permanently identified.
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10.6.3 SWSI technique: source internal, offset
Figure 10.4 SWSI source internal and offset technique (EN ISO 17636-1).
Figure 10.5 SWSI film inside, source outside (EN ISO 17636-1).
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t/De
De/f
t/De
De/f
De = external diameter of pipe, f = source to object distance,
t = nominal wall thickness
Figure 10.6 EN ISO 17636-1: Exposures required for film inside source outside
(FISO) techniques.
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This is a rather unpopular technique because a large number of exposures
(usually 8 or more) are required to cover the entire circumference of the weld.
In general it will only be used when an acceptable radiograph cannot be
achieved using either of the two single wall techniques described in 10.6.2 and
10.6.3 and can also not be achieved using the double wall techniques
described. Location markers must be placed source side. The IQI should always
be placed source side, there is no excuse for using a film side IQI when using
this technique. Identification of the films may be included as radiographic
images (although it will probably be impractical to use long identifications due
to the limited amount of area available on the film) but may also be added
later.
In the DWSI technique the source of radiation is usually placed at the minimum
possible distance from the film. The reason is that as the source to film distance
increases so does the number of exposures needed to cover the entire
circumference of the weld. In addition, any improvement in image quality due
to the reduced geometric unsharpness associated with an increase in SFD or
FFD has to be offset against a reduction in image quality due to increased
scatter.
X-ray tubes are bulky and the minimum achievable FFD will usually be about
125 mm plus the outside diameter of the pipe. A minimum of four exposures
per weld is therefore required when using an X-ray source for this technique.
Being able to place the source of radiation in close contact with the pipe gives
gamma ray another significant advantage over X-ray techniques particularly on
smaller pipe diameters. Less offset is needed with gamma ray sources in order
to ensure that the image of the source side portion of the weld is not
superimposed upon the film side part of the weld. This can increase the chance
of finding vertical defects such as lack of root fusion in the weld being
radiographed.
As the wall thickness to diameter ratio increases the DWSI technique becomes
increasingly difficult to apply, the number of exposures required increases and
the quality of the radiographs produced diminishes. For these reasons DWSI
(superimposed) techniques tend to be preferred for heavy wall small diameter
pipes.
Because there will in general be no access to the inside of the pipe when this
technique is employed the location markers and IQI are always placed film side.
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Figure 10.7 Double wall single image technique.
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De = external diameter, t = nominal thickness, SFD = source to film distance
Figure 10.8 EN ISO 17636-1: Exposures required for DWSI and SWSI source
inside film outside techniques.
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10.7.1 Double wall double image (elliptical)
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In accordance with EN ISO 17636-1 this technique is limited to girth welds in
pipe having an OD of less than 100mm. In accordance with ASME V article 2
welds in pipe of up to 3 inch nominal diameter (OD about 88.9mm), may be
radiographed using DWDI.
For pipes with a wall thickness to OD ratio in excess of about 0.12 the DWDI
(superimposed) technique is preferred.
Long source to film distances are needed because the minimum value of object
to film distance is equal to the OD of the pipe. Exposure times for this
technique, therefore, tend to be rather long especially in the case of gamma ray
techniques.
EN ISO 17636-1 requires wire type IQIs to be placed on the parent material
with their wires parallel to the weld axis, see Figure 10.9. Working in
accordance with ASME V article 2 standard wire type IQIs should be placed with
their wires across the weld at 90 to the weld axis.
In the DWSI technique the film is wrapped around the pipe to remain as close
as possible to the weld. Conversely, in the DWDI technique the film should be
kept as flat as possible, see Figure 10.9.
As the image of the source side part of the weld is superimposed on the image
of the film side part of the weld it is often not possible to accurately locate a
weld defect when using this technique. This is not usually much of a handicap
because small diameter welds tend to be cut out and re-welded rather than
being repaired locally.
A single location marker per exposure is usually sufficient when using this
technique and it may be placed either source or film side. IQIs should always be
placed source side.
The DWDI superimposed technique may be more likely than the elliptical
technique to successfully detect lack of root fusion due to the more favourable
angle of incidence of the primary beam.
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Figure 10.10 DWDI technique (superimposed).
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Section 11
Interpretation of Radiographs
11 Interpretation of Radiographs
11.1 Introduction
Interpretation of radiographs is a skill only gained through long experience. This
section gives the reader a guide to radiographic interpretation and should be
regarded as a base upon which to build.
Radiographs are easily damaged, therefore the viewing room must be clean and
dry and the radiographs must be handled with care. The viewer should be
mounted on a table or bench large enough to allow the films to be spread out
without the danger of them falling to the floor. A well shielded reading lamp will
allow reports to be read or notes to be made, without unduly increasing the
overall ambient lighting.
The viewing of radiographs is often undertaken in the dark room where the film
was processed. This is satisfactory provided that the viewing bench or table is
clean and well away from the processing tanks. Under normal circumstances
films should NEVER be viewed whilst wet. There are two reasons for this:
1 The film emulsion is swollen with water and the images are not as clear as
when the film is dry.
2 Emulsion is very delicate and any attempt to mask the film will result in
scratches or marks on the film, effectively ruining it.
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National standards generally require that the illuminance of a radiographic film
viewer be sufficient to produce a transmitted light intensity of at least 30 and
preferably 300 candela per square metre (cd/m2). This means that a viewer
suitable for viewing radiographic film with a density of 3.0 must have an
illuminance of at least 30,000 cd/m2 with as much as 300,000 cd/m2 being
desirable. BS EN 25580 requirements for radiographic film viewers are given by
Table 11.1 below. Note: These are minimum requirements.
11.3 Reporting
The initial interpretation of a radiograph should always be undertaken by the
manufacturer or designated representative. Other interested parties should be
presented with a report which includes an interpretation of each film. They
check this and agree or disagree with it. The radiographic report should contain
the following as a minimum:
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11.4 Film quality
The success of radiographic interpretation is dependent upon the quality of the
film presented. If the film does not meet the minimum applicable standards for
quality then it should be rejected and reshot. The manufacturers interpreter
may, for economic reasons, not be inclined to reject radiographs which do not
meet the minimum quality standards. Therefore any third party viewing the
radiographs should be extremely careful to correctly assess the quality of the
radiographs prior to endorsing the relevant report, otherwise they will be open
to criticism should the film become the subject of any subsequent legal inquiry.
When assessing a film for quality a number of items must be considered. These
are discussed below.
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ASME V article 2 requires that the film density within the area of interest must
not vary by more than minus 15 or plus 30% from the value measured through
the body of the IQI. If necessary additional IQIs can be used in order to satisfy
this requirement for exceptional areas.
Occasionally an upper limit is specified for film density. ASME V article 2, for
example, specifies an upper limit of 4.
1 Artefacts.
2 Surface irregularities in the component.
3 Internal discontinuities in the component.
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11.6 Artefacts
Pressure marks (crimp marks)
Produced by careless film handling - if the film is crimped or buckled either
before or after exposure crescent-shaped images in the processed radiograph
will result. Light marks indicate crimping before exposure, dark marks crimping
after exposure but before film processing.
Developer splashes
Appear as dark spots on the film and indicate poor dark room practice and are
usually visible in reflected light.
Fixer splashes
Appear as light spots on the film and again indicate poor dark room practice.
Such marks are usually visible in reflected light.
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Water splashes
Appear as either light or dark images on a radiograph. Water splashes before
exposure tend to cause light marks, after exposure tend to cause dark marks.
Such marks are usually visible in reflected light.
Water marks
Easily seen on the radiograph in both transmitted and reflected light and are
due to uneven drying. They commonly occur where a dry or partially dry film is
wetted locally either by splashing or by excess water running down from a film
clip. The appearance of water marks can be reduced or eliminated by using a
squeegee to remove excess water or a final wash that contains a small amount
of detergent (ie a wetting agent).
Air bells
Light marks caused by air bubbles adhering to the film in the early stages of
development and will not occur if the film is properly agitated.
Diffraction mottling
Can be a problem when X-rays are used to radiograph large grained material,
for example being austenitic steels. Diffraction is an apparent bending of a
beam of radiation due to interference. It occurs when radiation passes through
a grating that has spacing approximately equal to one wavelength. The spacing
of atoms in a metallic crystal is about 0.1nanometres. This corresponds to X-ray
radiation with photon energy in the region of 10keV. If low energy components
are removed from the X-ray beam by filtration the problem with diffraction
mottling will disappear. Diffraction mottling does not occur in gamma
radiography because of the absence of low energy beam components.
Diffraction can be used to advantage and it is the basis for the study of metal
crystals by X-ray crystallography.
Static marks
Penetrating radiation is by definition ionising. It always causes the build-up of
an electric charge on the film during exposure but under normal circumstances
this is not a problem because the charge quickly flows to earth. In dry climates,
however, a static charge may remain on the film until it is unloaded in the
darkroom, whereupon it flows to earth suddenly in a manner which could be
painful for the radiographer. Such a sudden dissipation of electrical energy
leads to the emission of a sudden burst of light which produces dark tree-like
marks on the finished radiograph. Static marks can be avoided by careful film
handling.
Dichroic fogging
Radiographs affected by dichroic fog will appear reddish when viewed using
transmitted light and greenish in reflected light. Dichroic means two-coloured.
It is caused when the development process continues during the fixing process,
when the fixer solution has become insufficiently acidic to stop the development
process. The use of an acidic stop bath between the development and fixing
processes will generally prevent the occurrence of this seldom seen artefact.
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Interpretation of Radiographs 11-6 Copyright TWI Ltd
Reticulation
Appears on the radiograph as an orange peel-like mottling effect. It is caused
when the film emulsion is subjected to a temperature shock at any stage during
the film processing as the sudden change in temperature causes the film
emulsion to wrinkle. It will not generally occur as long as the sudden change in
temperature is less than 10C.
Light fogging
Exposure to light other than from darkroom safe lamps (and even prolonged
exposure to safe lamps) will cause fogging at any stage prior to fixing the film.
Such fogging may be localised or general - localised is not a problem unless it
encroaches onto the diagnostic film area but general light has the same effect
as fogging due to exposure to ionising radiation.
Solarisation
Image reversal due to extreme over exposure to X or gamma rays or caused by
exposure to light during film development.
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Listed below are some of the common surface conditions that can produce
radiographic images.
Root concavity
A shallow groove which may occur in the root of a single sided weld, it appears
in the radiograph as a series of dark areas along the centre of the weld varying
in density according to the depth of imperfection and it is often seen in welds
made with the use of a backing gas. The pressure of the backing gas can cause
the weld root to collapse during welding of the first subsequent weld run (hot-
pass). Other possible causes are no root face; travel speed too slow, amperage
too high, incorrect polarity on the hot pass; excessive pre-heat and root gap too
narrow.
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Lack of reinforcement
This is a concave area of the weld cap where the weld is locally thinner,
sometimes thinner than the parent material. In the radiograph it appears as a
dark area towards the centre of the weld which has diffuse edges and is caused
by poor welding practice.
Undercut
An irregular groove at the toe the weld in the parent material due to burning
away during welding. It appears in the radiograph as a dark/irregular/
intermittent band in a position adjacent to either the cap or root weld toe or
between adjacent capping runs. It may therefore appear inside or outside the
weld image on the radiograph. The major causes are excessive amperage and
poor welding technique. Welds in the vertical or horizontal vertical position
tend to be prone to undercutting.
Spatter
Spatter consists of globules of molten filler metal expelled during arc welding on
to the surface of the parent material or weld. It appears in the radiograph as
small light spots and the major causes of spatter are incorrect polarity and
welding current too high. Spatter particularly affects MIG, MAG, MMA and
FCAW, and is highly unlikely to be seen in association with welds made by TIG
or SAW. In pipe welding spatter is possible on both external and internal
surfaces.
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Figure 11.6 Weld spatter.
Torn surface
A surface irregularity due to breaking off of temporary attachments. The
radiographic indication produced has a shape corresponding to that of the
affected area which may be either light or dark depending on whether part of
the attachment has remained or parent material has been torn away, caused by
poor fabrication practice, often seen in association with storage tank or ship hull
welds.
Surface pitting
Surface imperfection, usually of the parent material but also the weld metal
where a component has been in service. It usually takes the form of small
depressions resulting from localised corrosion. Pitting appears in a radiograph
as small dark rounded images and it is possible to mistake this for a welding
defect, as its appearance can be identical to that of porosity.
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Internal defects:Cracks
In weld radiography four basic types of crack are sometimes detected by
radiography.
1 Centreline (shrinkage).
2 Transverse (including chevron).
3 Heat affected zone or toe.
4 Crater.
Cracks are often invisible on radiographs but if detected appear as dark, fine
often branching lines, usually diffuse or discontinuous. The ability of the
radiographic technique to detect a crack is dependent on the cracks orientation
relative to the direction of the radiation. Figure 11.8 shows how even a slight
deviation from the optimum orientation will greatly reduce the change in section
thickness which the radiation experiences due to a planar defect such as a
crack. In the case shown a variation from optimum incidence of just 1 will
reduce the change in penetrated thickness from 10 to 1mm for a planar defect
measuring 10mm by 17m.
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A shrinkage or solidification crack which usually occur at 90 to the weld axis,
often affecting the root pass of single sided welds. In nature they are very
similar to centreline cracks, but the source of restraint is different and are
relatively easy to detect by radiography.
The second type is a chevron crack, which occurs at about 45 to the weld axis,
usually after the completion of welding. Chevron cracks are a special type of
hydrogen induced crack; the stress that causes the crack being due to an
excessive amount of dissolved hydrogen in the weld metal. They are sometimes
detected by radiography, but where there is a known problem, other NDT
methods with a higher probability of detection should be used.
The first involves dissolved hydrogen. Molten iron has a very high solubility for
hydrogen while solid iron has a very low solubility. Thus as the metal freezes
hydrogen will attempt to leave solution and escape from the weld pool but this
process is slow compared with freezing, therefore most of the hydrogen
becomes trapped in the solidified metal. The trapped hydrogen then diffuses
through the metal crystals and begins to build up an internal pressure at points
of weakness, usually the grain boundaries. In some cases the internal pressure
exceeds the strength of the material and hydrogen cracking occurs. Hydrogen
induced cracking may occur up to 48 hours after welding. Where ferrous
materials operate in a hydrogen rich environment, for example in sour gas
service, hydrogen cracking can occur as an in-service defect. High strength,
high carbon equivalent steels are most prone to hydrogen cracking. The
presence of trace elements, especially sulphur and phosphorus can make
hydrogen cracking much more likely to occur. Hydrogen induced cracks are not
likely to be detected by radiography and other methods such as ultrasonic
testing should be used in any situation where there is a high probability of
occurrence.
A second type of cracking that can occur in the HAZ of a weld is sometimes
called weld decay. This can affect stainless steels and is caused by the
precipitation of brittle material (chromium carbide) at the grain boundaries. All
stainless steels contain a small proportion of carbon which is generally held in
solution within the austenitic grains, but the heat from welding can cause it to
combine with the chromium which is present forming chromium carbide which
is an extremely brittle material. Weld decay can be avoided by reducing the
carbon content of the parent material and filler wire. Cracking caused by weld
decay is unlikely to be detected by radiography.
Crater cracks
Occurs when the heat source is removed too suddenly at the end of a weld run.
The cracking mechanism is the same as that for centreline cracking. The major
dimension of a crater crack is usually less than 5mm, are often star shaped in a
radiograph and relatively easy to detect. Some standards will permit this type
of cracking provided that it does not exceed a specified maximum dimension.
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Figure 11.9 Typical radiographic appearance of a crack.
Lack of fusion
Can occur either between the weld deposit and the parent material or between
successive layers of weld material, also due to lack of fill or penetration.
Lack of fusion is where the solid material immediately adjacent to the molten
weld pool failed to become molten during the welding process leading to a lack
of union between the molten weld material and the adjacent solid material. The
ability of radiographic techniques to successfully detect lack of fusion is strongly
dependent on the orientation of the defect with respect to the incident beam of
radiation, (see Figure 11.8). Given favourable orientation lack of fusion with the
parent material will appear in the radiograph as a fine dark straight line which
may be continuous or intermittent. Unfavourably orientated lack of fusion with
the parent material may sometimes still be detected due to the presence of
associated slag inclusions or porosity. A slag inclusion with a straight edge
normally indicates lack of fusion and gas escaping from an area lack of fusion
during the deposition of a subsequent welding run may lead to a line of linear
porosity.
Lack of fusion between subsequent layers of weld material will generally not be
detected by radiography unless it is associated with another type of defect such
as slag.
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Figure 11.10 Types of lack of fusion.
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Figure 11.11 Lack of fusion in the radiograph.
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Incomplete root penetration
The failure of the weld material to extend into the root of a joint and is a fusion
defect, not to be confused with root concavity.
Where welds are deposited without a root gap, lack of penetration may appear
as a single continuous or intermittent dark line. It should be noted that root
gaps frequently close during welding so even where there should have been a
root gap lack of penetration may appear in the radiograph as a single dark line.
Non-metallic inclusions
Usually formed by slag, but occasionally other foreign matter such as
windblown sand may become entrapped within the molten weld material. Slag
inclusions are irregularly shaped and may be either rounded/isolated or
linear/elongated. Linear slag inclusions with a straight edge often indicate lack
of fusion. Sometimes linear slag will appear on the radiograph as two parallel
lines, often referred to as tram lines or wagon tracks.
Although very rarely used, some types of covered welding electrode have a high
barium content in the flux coating and produce a slag radiographically denser
than steel so slag inclusion may appear as a light image.
Metallic inclusions
Dependent upon the nature of the welding process it is possible for foreign
metallic material to become entrapped within the molten weld material.
Associated with the gas tungsten arc welding process, tungsten inclusions are
probably the most commonly encountered form of metallic inclusion. They are
caused by the break-up of the non-consumable tungsten electrode during
welding and since tungsten has a melting point well in excess of 3000C
particles of tungsten falling into the weld pool do not become molten. Tungsten
is radiographically extremely dense; therefore tungsten inclusions always
appear as bright - light images which tend to be angular. They are usually quite
small - typically around 0.5mm.
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Copper inclusions can occur particularly with submerged arc or other welding
process where the consumable electrode is fed through a copper contact. If the
copper contact gets too near to touches the weld pool molten copper (melting
point about 900C) will become included in the weld pool. Copper is
radiographically more absorbing than most other materials including steel so
copper inclusions may produce light rounded images with extremely diffuse
edges. Copper inclusions in ferritic steel welds usually cause severe transverse
cracking.
Metallic inclusions are quite common in aluminium welds, where such welds are
not properly segregated from their steel counterparts. Aluminium melts at
around 660C, steel above 1400oC so particles of steel or iron oxide falling into
the weld pool will not become molten. Contamination can easily occur if tools
such as grinding disks which have been used for steel are used on aluminium.
Steel inclusions in aluminium appear as very bright angular shapes with sharp
edges.
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Hollow bead can be caused by holding the arc at too shallow an angle with
respect to the work piece or by a strong draught of air along the inside of the
pipe during welding. On the radiograph it looks very similar to slag - the
radiographic indication usually has rounded ends and it is always situated along
the centre of the root bead.
Wormholes
These are gas pores which have become frozen in the weld pool while
attempting to migrate to the surface of the weld pool. In addition to occurring
due to an excess of dissolved gas in the weld pool, they sometimes occur due to
laminations in the parent material which extend to the weld face. Lack of fusion
contains a small amount of entrapped air and this can cause wormholes in a
similar way.
A crater pipe will appear in the radiograph with an image very similar to that of
a wormhole. It can only be distinguished from a wormhole by its position in the
weld. Crater cracks are shrinkage cracks so have a relatively greater volume
than most other cracks. They often have a star like appearance in a radiograph
and their radiographic image rarely measures more than 3 or 4mm.
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11.8 Interpretation of casting radiographs
Five groups of defect images may be seen in radiographs of metal castings:
Voids.
Cracks.
Cold shuts.
Segregation.
Inclusions.
Voids
Voids in castings are formed by gases dissolved in the molten material
precipitating from solution during the solidification process or by shrinkage
caused by inadequate feeding.
Macroshrinkage (piping)
Large cavity formed during the solidification process which occurs due to lack of
sufficient feed material. With good mould design macro-shrinkage should be
confined to the feeder heads.
Microporosity/microshrinkage
Very fine form of filamentary shrinkage due to lack of sufficient feed metal, gas
or both, in which a number of cavities occur either round the grain boundaries
or between the dendrite arms (a dendrite is a material crystal which in the
initial stages of growth is tree-like). These cavities tend to link up in a three
dimensional network throughout the material.
In the radiograph the images of these cavities are superimposed and generally
produce a mottled or cloudy effect. In non-ferrous alloys, particularly
magnesium-based alloys, microshrinkage may occur in layers and produce dark
streaks in the radiograph.
Pinhole porosity
Cavities less than 1.5mm diameter formed due to the evolution of gas from the
molten material. The defect may be evenly distributed throughout the casting
or localised in a particular area. When it is local to the surface of the casting,
due to gas evolved at the mould face, it is known as subcutaneous pinhole
porosity.
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Interpretation of Radiographs 11-19 Copyright TWI Ltd
The defect appears in the radiograph as an assemblage of small, rounded,
widely distributed dark images, distinguishable from microporosity by the size
and rounded nature of the images which do not show the same tendency to
interconnect. This defect can arise from the accidental injection of air during
pressure die casting.
Gas holes
Discrete cavity greater than about 1.5mm diameter caused by gas evolved from
the material as it freezes. It may also arise from gas evolved from the core or
mould, in which case it is called blowhole.
The radiographic image appears as a dark area of smooth outline which may be
circular or elongated and can be associated with pinhole porosity. Gas holes
occasionally become elongated as they try to rise to the surface of the molten
material during cooling, in this form they are known as wormholes. The
radiographic image of a wormhole may vary from a circular to an extremely
elongated image depending upon the angle of view.
In pressure die casting where air may be injected with the material the defect is
usually more severe in the runners and may assume an angular form. In
pressure and gravity die castings this defect may occur in clusters or as strings
of small voids, whereas, in investment casting it may appear as small rounded
voids.
Cracks
Cracks are discontinuities caused by fracture of the material at the point of
solidification or some time thereafter. They appear on the radiograph as one or
more dark lines. The width and form of the indication depends on the type of
crack and radiographic technique used.
Hot tears
Discontinuities of a decidedly ragged form resulting from stress developed near
the solidification temperature when a material has low mechanical strength.
They usually arise when the natural contraction of the casting is restrained by
the mould or core and occur mainly at or near a change of section.
The defects are not necessarily continuous, they may exist in groups and will
often terminate at the surface and are sometimes referred to as pulls.
Radiographically hot tears are wavy, ragged dark lines, often discontinuous,
with areas appearing as approximately parallel dark lines which may possibly be
overlapping. Generally, the ends of the indication taper to become fine.
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Interpretation of Radiographs 11-20 Copyright TWI Ltd
Stress cracks
Well defined and approximately straight cracks formed after the material has
become completely solid, quite large stresses being required to cause fracture.
Distinctions are sometimes drawn between types depending on the time at
which fracture occurred.
In the radiograph stress cracks are often revealed as clearly defined smooth
dark lines - thus differing from the ragged appearance of hot tears.
Cold shuts
Discontinuities caused by the failure of a stream of molten material to unite
with either a confluent stream, or solid material, such as a chaplet, internal chill
or pouring splash.
In the radiograph these defects usually appear as dark lines and may be
difficult to distinguish from hot tears except by the typical involute appearance
of the end of the defects. The shape of an unfused chaplet or chill in a
radiograph is dependent upon orientation of the beam. A cold shut resulting
from a splash may appear as a dark crescent or circle.
Inclusions
Foreign matter (sand, slag, flux, dross, etc) entrapped in the casting. As an
inclusion may be of greater or lesser opacity then the surrounding material it
may appear radiographically as a light or dark area (eg a sand inclusion will
appear dark in steel and light in aluminium). Slag usually gives a rounded
image whereas material included in the casting as a solid (eg dross and sand),
will give an irregular shape. If dross is trapped as an oxide film it will often
produce a characteristic folded appearance in the radiograph inclusions may in
many respects resemble voids in radiographic appearance but they will
generally exhibit a greater variation in density.
Segregations
Result from local concentrations of any of the constituents of an alloy and may
be classified as general, localised or banded.
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Section 12
Localisation
12 Localisation
A radiograph is a two dimensional image of a three dimensional object. When a
flaw is detected using a standard technique there is no certain way of telling
how far below the surface the flaw is. In some cases it might be desirable to
have three dimensional information about the position of a flaw. A technique
called localisation can be used to estimate the through wall position of a
volumetric flaw such as a slag inclusion. It is important to note that localisation
of planar flaws such as cracks or lack of fusion is generally not possible by
radiographic methods.
12.1 90 method
The simplest method of localisation, but rather limited in its field of application.
A typical test object, where this method might be useful would be a small to
medium sized casting that has a fairly simple cross section. Figure 11.9 shows
how this method would work on a small cylindrical object. Two radiographs are
taken with primary beam mutually at 90 to each other. In an ideal situation the
component would be placed on some kind of turntable so that it could be
moved accurately keeping the two exposures in the same plane relative to the
axis of the component. The apparent defect position in each radiograph can be
measured relative to convenient datum point, the results plotted on a sketch
and the defect position then deduced by triangulation.
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Figure 12.1 The 90 method for a small cylindrical casting.
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Localisation 12-2 Copyright TWI Ltd
Figure 12.2 Tube shift method.
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Using similar triangles:
A d x s
B m
But
so:
A d t d s
B m
Am + dm = tB - dB + sB
dB + dm = tB + sB - Am
d(B + m) = B(t + s) - Am
B t s Am
d
B m
12.3 Tube (source) shift method with lead markers
Placing lead markers on the component source and film side as shown in Figure
12.3 removes the need for accurate measurement of the source to object,
object to film distances and the distance that the source is moved between the
successive exposures.
Refer to Figure 12.3 below. The three triangles in the enlarged view will be very
similar as long as the source or focus to film distance is long in relation to with
the thickness.
a b c
x y z
CX cy
So it follows that: a and : b
Z z
CX cy
Therefore we can write: c t and : c d
Z z
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Figure 12.3 Tube shift method with lead markers.
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CX cy
We have already established that: c t and c d
Z Z
cy
From this we can see that: d C
Z
CX
And: t c
Z
y
So: d c1 (1)
Z
X
And: t c 1 (2)
Z
y
1
d Z
t X
1
Z
t, the thickness of the plate is known and x, y and z can be measured on the
radiograph. Therefore d can be calculated.
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Localisation 12-6 Copyright TWI Ltd
Section 13
Units Used in Radiography
13 Units Used in Radiography
13.1 Ionisation (exposure)
The quantity of ionising radiation can be measured in terms of its ionising effect
or exposure on air at standard temperature and pressure (STP).
The SI unit of exposure is the coulomb per kilogram in air, the quantity of
ionising radiation that produces a total electric charge of 1 coulomb per
kilogram (Ckg-1) of air at STP.
or
1 Ckg-1 = 3876 R
Note: Unit of exposure is defined for air, hence cannot be used directly to
describe the dose to tissue.
The CGS unit of absorbed dose is the roentgen absorbed dose (rad). One rad
represents absorption of 100 ergs of energy per gram of irradiated material.
1 Gy = 100 rad
The units of radiation absorbed dose can be approximately related to the units
of ionising effect. One Roentgen corresponds to 1.61 x 1015 ion per one kg of air
which has than absorbed 8.8 mJ.
1R = 0.88 rad
The conversions above are approximate since the relationship between the
roentgen and the rad or the coulomb per kilogram and the gray varies to some
extent with radiation energy.
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13.3 Man mammal equivalent or radiobiological equivalent
The effect which ionising radiation has on our bodies varies with the type of
radiation and also, to some extent, with radiation energy. Also the chemical and
biological effectiveness of a particular radiation depends on the distribution of
the absorbed energy within the medium. In order to compensate for this a
quality factor (QF) is introduced. Quality factors for several types of ionising
radiation are listed in Table 12.1 below.
In order to compare the biological effectiveness and also for radiation protection
measure the quantity dose equivalent is used. The SI unit of dose equivalent
is Sievert (Sv) and is given by:
In the CGS system multiplying the dose in rad by the appropriate quality factor
gives the dose in roentgen equivalent man (Rem) where 1Rem is the amount of
ionising radiation which has the same biological effect as 1rad of X-rays.
In the SI system multiplying the dose in gray by the appropriate quality factor
gives the dose in sievert (Sv) where 1Sv is the amount of ionising radiation
which has the same biological effect as 1Gy of X-rays.
Thus:
1Sv = 100Rem
or
1Rem = 0.01Sv
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13.4 Dose rate
Dose rate in the SI system is generally measured in microsieverts per hour
(Sv/h), but may also be measured in millisieverts (mSv) or sieverts (Sv) per
hour. Alternatively dose rate can be expressed in micrograys (mGy), milligrays
(mGy) or grays per hour.
In the cgs system dose rate is generally measured in millirem per hour
(mRem/h) but may be measured in Rem per hour (Rem/h).
1 mRem/h = 10 Sv/h
or
The cgs unit of source strength or activity is the curie (Ci). One curie is equal to
3.7 x 1010 disintegrations per second.
1Ci = 37GBq
or
1GBq = 0.027Ci
13.7 Output
The output of a source of ionising radiation is the dose rate per hour at some
fixed distance, usually 1m from the source. For radioactive isotopes it is useful
to state output in grays, sieverts, rads or Rems per hour per curie at 1m. Table
12.2 gives some examples.
Output,
Isotope name mSv per hour per Ci
Thulium 170 0.026
Ytterbium 169 1.25
Selenium 75 1.8
Iridium 192 4.8
Cobalt 60 13.0
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The output of radiation from a typical 200kV industrial constant potential X-ray
machine is as much as 1,000mSv per milliampere of tube current at a distance
of 1m from the focal spot.
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Section 14
Radiation Monitoring Devices
14 Radiation Monitoring Devices
Ionising radiation cannot be detected by humans and is extremely harmful to
health therefore it is imperative we have reliable equipment that can measure
the radiation dose. Two basic types of radiation monitoring device exist: (1)
Those which give a read out of the current dose rate and (2) devices which
measure the accumulated dose over a given period of time.
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Figure 14.2 Simplified layout of an ionisation chamber.
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14.1.4 Solid state radiation detectors
Solid state radiation detectors have been available since the 1950s. Various
types of semiconductor are available which begin to conduct electricity under
the influence of ionising radiation. Instruments based on this type of
semiconductor are able to differentiate between different photon energies. Thus
in addition to measuring dose rate they can provide information as to the
spectrum of radiation that is present.
Phosphors have been used as radiation detectors since the very early days of
the discovery of ionising radiation; both Roentgen and Becquerel used them.
The amount of light produced can be quite small so phosphors are always used
in conjunction with a light amplification system such as the photomultiplier
tube. Modern instruments use charge coupled devices (CCDs) in conjunction
with a radiation sensitive phosphor. A CCD is at the heart of any modern digital
camera. Those used for radiation detection measure the intensity of light
emitted from the phosphorescent layer under the influence of ionising radiation.
Whichever system is used, scintillation counters relate the intensity of light
produced by the phosphor to the intensity of the ionising radiation received.
Generally they give a reading in counts per second but occasionally they will be
calibrated to read directly in microsieverts or millisieverts per hour.
Scintillation counters are extremely sensitive, and can detect very low levels of
ionising radiation. They are direction sensitive and very useful when searching
for radioactive contamination. They are used in industrial radiography to check
for leakage of fissile material from a sealed source.
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14.2.1 Film badges
Monitoring film
Plastic filter
Copper filters
Open window
Aluminium filters
Plastic filter
The principle of a film badge is that when exposed to ionising radiation followed
by developing under tightly controlled conditions the film density produced can
be related to the radiation dose received. Film badges, as shown in Figure 14.3,
can be used to detect x-, gamma and beta radiation. Coupled with the right
type of intensification screen radiographic film can be used to detect and
measure other types of ionising radiation.
The film badge of the type shown in Figure 14.3 contains a section of carefully
manufactured radiographic film having two emulsions, one fast and one slow.
The use of two emulsions extends the measurement range of the badge. The
badge holder is equipped with various filters which extend the range of
measurement and additionally enable the badge to give some information as to
the type and photon energy of the ionising radiation received.
The film badge has, in large part, been replaced by the thermoluminescent
dosimeter (TLD) (see below). Table 14.2 gives a comparison of typical film
badge and TLD specifications.
Film badges
Radiation type Gamma X-ray Beta
Measuring range 10keV to 7MeV 10keV to 7MeV 700keV to 3.5MeV
(photon energy)
Measuring range 0.1mSv to 10Sv 0.1mSv to 400mSv 0.1mSv to 10Sv
(dose)
Typical period of 2 to 4 weeks
use
Thermoluminescent dosimeters
Radiation type Gamma X-ray Beta
Measuring range 10keV to 10MeV 10keV to 10MeV 700keV to 3.5MeV
(photon energy)
Measuring range 0.05mSv to 10Sv 0.05mSv to 10Sv 0.05mSv to 10Sv
(dose)
Typical period of 4 weeks
use
NDT20-71015
Radiation Monitoring Devices 14-4 Copyright TWI Ltd
14.2.2 Thermoluminescent dosimeters (TLD)
Thermoluminescent dosimeters offer several significant advantages over the
film badge:
TLD badges are worn in specially designed plastic holders similar to those used
for film badges. The addition of plastic or aluminium filters extends the
measurement range and facilitates the obtaining of information concerning the
photon energy and type of radiation.
The quartz fibre electrometer (QFE) is a gaseous detector like the ionisation
chamber, proportional counter and Geiger counter described above. When
raised to the light a scale like on the right of Figure 14.4 can be seen through
the lens of the instrument. The vertical line is the quartz fibre. When a static
electrical charge is applied to the instrument the quartz fibre moves to the zero
point of the scale. As the gas inside the QFE becomes ionised the static charge
is gradually dissipated and the fibre begins to move to the right. The
corresponding total dose received can be read on the upper scale.
NDT20-71015
Radiation Monitoring Devices 14-5 Copyright TWI Ltd
The QFE has quite a narrow measuring range, typically 0-50mSv or less. The
example shown above has a measurement range of 0-200mRem, equivalent to
0-2mSv. The QFE is sensitive to x- and gamma radiation in the photon energy
range 45keV to 3.5MeV and is a very convenient means for checking how
radiation doses are accumulating during a working day but it suffers from
fragility and is very easily damaged.
NDT20-71015
Radiation Monitoring Devices 14-6 Copyright TWI Ltd
Section 15
Radiation Safety
15 Radiation Safety
All personnel working with ionising radiation should be aware that it is injurious
to the human body, or any other biological tissue. Anyone working where
radiography is carried out should make themselves fully aware of the safety
procedures and regulations in force and take care to observe all warning
barriers. Ionising radiation cannot be detected by the five human senses and
has cumulative effects upon the human metabolism and causes genetic damage
to the human body, the full effects of which may not be apparent until 15-35
years after the initial exposure. Regardless of any nominal safe limits it is
always prudent to avoid exposure to radiation whenever possible.
15.1 Precautions
15.1.1 Exposure booths
At locations where a large volume of industrial radiography is carried out
exposure booths of various shapes and sizes will generally be available, which
usually consist of enclosures having lead lined walls. Some exposure booths
have walls filled with spent casting sand or other radiation absorbing material.
Safety switches are usually fitted to doors of exposure booths to prevent the
operation of x-ray sets or gamma ray equipment whilst the door is open. Where
overhead cranes might have to pass over an open topped exposure booth
similar safety switches are normally installed o trip out the x-ray set, or wind
back the gamma ray source, should the crane encroach upon the irradiated
area during exposure.
Exposure booths should be equipped with switches inside the x-ray compound
which can be operated to prevent the operation of the x- or gamma ray
equipment should any personnel be accidentally trapped inside.
Areas which will be irradiated at greater than the legal limit must be cleared of
all non-classified personnel prior to any exposure. Audible and visible warnings
must be given before any exposure takes place.
The barrier should be monitored with an efficient radiation detector and should
be guarded by classified personnel during exposure.
NDT20-71015
Radiation Safety 15-1 Copyright TWI Ltd
15.1.3 Scatter
Personnel should be aware that radiation can be scattered by structures,
apparently safe locations may be subject to stray scattered radiation.
15.2.1 Dosimeters
For work in radioactive environments (ie nuclear reactors) personnel must be
equipped with direct reading dosimeters which will display immediately the
accumulated dose received. Personnel working in these locations must take
particular care to avoid ingesting radioactive particles. Tightly fitting breathing
masks are required and protective clothing should be worn.
Supervised area
Defined as an area where the annual dose is expected to equal or exceed
1mSv. Such areas should be clearly signed; unclassified persons are permitted
to pass through such areas but must not remain in them for extended periods.
Verbal warnings should be given by the radiographer where possible.
NDT20-71015
Radiation Safety 15-2 Copyright TWI Ltd
For any source of ionising radiation:
Dose rate =
If the source of ionising radiation is x-ray then it will not be possible to calculate
the dose rate at 1m although the dose rate will be proportional to the tube
current. Halving the tube current at a given tube voltage will halve the radiation
dose rate. If the source is gamma ray then the dose rate at 1m can be
calculated if the source strength (curies or gigabecquerels) and output of the
source are known. Output for any given isotope is the dose rate per curie or
gigabecquerel at 1m from the source.
Thus:
If we take 7.5Sv/hr to be the safe dose rate then we can calculate the safe
distance using the formula below:
C is a constant for each isotope, for thulium 170 C = 1.86, ytterbium 169 C =
12.91, selenium 75 C = 15.49, iridium 192 C = 25.30 and for cobalt 60 C =
41.63.
15.4.1 Shielding
If shielding is introduced then the reduction in the minimum safe working
distance can be calculated if the magnitude of the half or tenth value layer of
the shielding material is known. The half value layer for any material is the
thickness of material that will reduce the radiation dose rate, for a given
radiation energy, by a factor of two. The tenth value layer is similarly the
thickness of material that will reduce the dose rate by a factor of ten. For
example the half value layer of lead for cobalt 60 is about 12.5mm while for
iridium 192 it is about 4.8mm. The tenth value layer of lead for cobalt 60 is
about 41.5mm while for iridium 192 it is about 16mm. If the shielding thickness
is an exact multiple of the half or tenth value layer then the dose rate after
shielding can be found simply by dividing the unshielded rate by two for each
half value layer or by ten for each tenth value layer. Where this is not the case
the formulae given below can be used.
NDT20-71015
Radiation Safety 15-3 Copyright TWI Ltd
RU RU
RS t / hvl or RS
2 10 t / tvl
Where:
Ru = Unshielded dose rate.
Rs = Shielded dose rate.
t = Thickness of shielding material.
hvl = Half value layer.
tvl =Tenth value layer.
NDT20-71015
Radiation Safety 15-4 Copyright TWI Ltd
Glossary
Glossary
The following is a compilation of the more common terms used in connection with
radiographic testing. Other lists can be found in BS EN 1330-3 and ASME V, Appendix A.
Absorbed dose (of ionising radiation) Energy per unit mass imparted
to the irradiated material. Absorbed dose is
measured in Grays (Gy) (1 Gy = J kg-1).
Atomic mass number Total number of protons plus neutrons in the nucleus
of an atom, standard abbreviation A.
Atomic mass unit (AMU) Measure of atomic weight, roughly speaking the
proton has a weight of 1amu while that of the
neutron is marginally greater than 1amu. The
weight of the electron is roughly 0.00054amu.
NDT20-71015
Glossary 1 Copyright TWI Ltd
Background radiation Ionising radiation present at any given site due to
natural causes: sunlight contains a proportion of
ionising radiation; some natural rocks such as
granite are weakly radioactive.
Bunsen-Roscoe law Reciprocity law which basically states that the film
density produced by a dose of ionising radiation is
independent of the radiation dose rate (ie a low
dose rate for a long exposure time will produce the
same film density as a high dose rate for a short
exposure time so long as (dose rate) x (time)
remains constant).
NDT20-71015
Glossary 2 Copyright TWI Ltd
Cassette Lightproof container for holding x-ray film during
exposure may be rigid or flexible. They must be
designed to maintain good contact between the x-
ray film and intensifying screens.
Characteristic curve The curve for a given photographic (or x-ray) film
which relates the logarithm to the base of 10 of the
relative amount of radiation exposure (ie radiation
intensity x exposure time) to the achieved
photographic density under specified processing
conditions. Also known as Hunter & Driffield curve
(H&D curve) or sensiometric curve. The process by
which a characteristic curve is produced is called
sensiometry.
NDT20-71015
Glossary 3 Copyright TWI Ltd
Density Degree of darkness of a radiograph expressed as
the logarithm to the base 10 of the ratio of the
intensity of incident light to intensity of the light
transmitted through the film.
NDT20-71015
Glossary 4 Copyright TWI Ltd
Exposure chart Chart which relates the required radiographic
exposure for a given radiographic film and film
density to the penetrated thickness of a specified
material.
NDT20-71015
Glossary 5 Copyright TWI Ltd
Fluorometallic screen Intensifying screen used in radiography which
combines the scatter reducing properties of a lead
screen with the image intensification properties of a
salt screen.
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Glossary 6 Copyright TWI Ltd
Image quality Indicator Any device which gives an indication of radiographic
quality. The commonest are wire, step hole and
plaque IQIs. The quality (or sensitivity) of the image
is defined as the smallest discernible wire diameter
or step thickness expressed as a percentage of the
total thickness.
Investment casting Also called the lost wax process. A wax model of the
required item is made and a mould is formed around
this using some type of refractory material. After
firing to harden the mould and burn out the wax,
molten metal is poured in to produce the desired
component. Investment casting is an expensive
method but it produces the best surface finish and
material properties of all of the casting processes.
NDT20-71015
Glossary 7 Copyright TWI Ltd
MAG Metal active gas welding, often referred to as CO2
welding, mainly applicable to carbon steel. MAG is
an automatic or semi-automatic arc welding process
involving a reel fed consumable electrode; the arc is
shielded by an active gas, usually CO2. Porosity and
lack of sidewall fusion are common defects.
NDT20-71015
Glossary 8 Copyright TWI Ltd
Pressure mark Variation in photographic density caused by the
application of local pressure to the emulsion; the
mark may be light or dark according to
circumstances.
Quality factor To account for the fact that, for instance 1Gy or
100R of alpha radiation is biologically much more
damaging than 1Gy or 100R of x- or gamma
radiation a quality factor is used. The dose in
Sieverts or Rem is then equal to the dose in Grays
or Rads multiplied by the quality factor, 1 Sievert or
100 Rem of any type of ionising radiation has the
same biological effect.
Reciprocity law Law which states that, all other conditions remaining
constant, the time of exposure required to produce
a given density is inversely proportional to the
intensity of the radiation (see Bunsen-Roscoe Law).
NDT20-71015
Glossary 9 Copyright TWI Ltd
Rem Roentgen equivalent mammal, old unit of man
mammal equivalent absorbed radiation dose. 1
Roentgen of alpha radiation has a much greater
biological affect than 1 Roentgen of x- or gamma
rays whereas 1Rem has the same biological affect
whatever the type of ionising radiation. Despite the
name the Rem is arrived at by multiplying the dose
in rad (radiation absorbed dose) by a quality factor.
SI equivalent is the Sievert.
Screen-type film X-ray film designed for use with salt screens. It is
sensitive to the fluorescent light emitted by such
screens under the action of x-rays.
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Glossary 10 Copyright TWI Ltd
Source-to-film distance Distance from a source of radiation to a film set up
for a radiographic exposure, abbreviation: SFD.
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Glossary 11 Copyright TWI Ltd
Appendix
Appendix: Ionising radiation regulations
NDT20-71015
Appendix: Ionising radiation regulations 1 Copyright TWI Ltd
Trainees
The annual dose of a trainee under the age of The annual ionising radiation whole
18 must not exceed the stated limit of 6mSv, body dose for a trainee under the
but it is likely to be higher than that of a age of 18 shall not exceed 6mSv.
general member of the public. Typically a A person under the age of 18 cannot
trainee would be spending a higher than be classified
average amount of time within a supervised
area.
General public
In setting the dose limit for members of the The annual ionising radiation whole
public (and other mammals) it is taken into body dose for a member of the
consideration that such members of the public general public shall not exceed
(or other mammals) could be pregnant. A 1mSv.
developing foetus is particularly sensitive to
ionising radiation.
Annual dose limitations summary (SI 1999 n0. 3232 schedule 4)
Description Classified worker Trainee General public
Whole body 20mSv (1.) (2.) (3.) 6mSv 1mSv(4.)
Lens of the eye 150mSv 50mSv 15mSv
Skin 500mSv 150mSv 50mSv
Hands, forearms, 500mSv 150mSv 50mSv
feet, ankles
Notes
Where special circumstances apply an employer is able to show that the
annual limit of 20mSv is impractical, up to 50mSv can be received in a single
calendar year but not more than 100mSv over any five year period. Any
employee exceeding these limits is likely to be suspended from work pending
an investigation by the HSE.
Where the person in question note 1 above, is a pregnant female the dose
shall not exceed 13mSv in any period of 3 months.
Where the recorded dose exceeds 20mSv in one year the employer is required
to make a formal investigation to determine whether the dose limitations of
note 1 are likely to be complied with. The employer must report the matter to
the HSE and must put in place a programme to ensure that the dose
limitations of note 1 are not exceeded.
For persons who act as carers to others who receiving exposure to ionising
radiation for medical purposes the dose limit is 5mSv in any five year period.
Annual dose limitations general.
The dose limitations, items 1 to 6 above are additional to exposure to radiation for
medical purposes.
Radiation monitors
Radiation monitors must be checked before use Radiation monitoring equipment
to ensure correct functioning; typically this shall be properly maintained.
would involve a battery check and a check to Radiation monitoring equipment
see that a reading is produced when the shall be fit for the designated
instrument is exposed to a source of ionising purpose.
radiation. Radiation monitoring equipment
Radiation monitors must have a scale shall be calibrated at appropriate
appropriate to the magnitude of the doses intervals.
being measured. General good practice is to
have portable monitors calibrated on an annual
basis.
Appropriate calibration periods can vary
dependent on the type and usage of the
radiation monitor in question.
NDT20-71015
Appendix: Ionising radiation regulations 2 Copyright TWI Ltd
Radiation protection adviser
Usually a person, but may be an organisation, All organisations working with
meeting the HSEs criteria of competence. In ionising radiation shall appoint a
general the RPA must be fully aware of the radiation protection adviser.
companys activities involving ionising
radiation.
The local rules should be approved by, if not
written by the RPA. The RPA is often called
upon to undertake training of the radiation
protection supervisors.
Radiation protection supervisor
A person appointed by the employer and named All companies working with ionising
in the local rules to act as such. The RPS has in radiation must appoint at least one
depth knowledge of the local rules. RPS.
The RPS would generally take control where an The names and contact details of
emergency situation occurs and carry out initial all RPS shall be listed in the local
investigation of any recorded or suspected rules
overdose.
General good practice requires the presence of
at least one RPS where radiography is
performed at an on-site location.
Appointed doctor
A registered medical practitioner appointed in Once a year all classified personnel
writing by the HSE. shall be certified fit by an
appointed doctor.
Approved dosimetry service
An organisation, approved in writing by the All companies employing classified
HSE, which monitors and records the ionising personnel must contract out their
radiation doses of classified personnel. dose monitoring to an approved
dosimetry service company.
Minimum notification period
Under most circumstances all work involving The minimum notification period is
the use of ionising radiation must be notified to 28 days prior to the planned
the HSE. commencement of work.
Local rules
The local rules are employer specific and A copy of the local rules must be
describe in detail how the employer will control present at all work sites.
ionising radiation work such that the ionising The local rules must be regularly
radiation regulations are fully complied with. updated to reflect regulatory
changes, changes in working
conditions and changes in
personnel.
NDT20-71015
Appendix: Ionising radiation regulations 3 Copyright TWI Ltd
Course Tips
1
Course Objectives
History of Radiography
W C Roentgen
1895
1
History of Radiography History of Radiography
William Coolidge
1920s
First radiograph 22 December 1895.
Sent to Physicist Franz Exner in
Invented the X-ray tube Vienna. (Mrs. Roentgen's hand.)
as we know it today
which revolutionised
industrial radiography.
2
What is radiation?
Electromagnetic Spectrum
Radiation
Radio waves, light, X-rays, g-rays and other
forms of radiation take the form of waves of
energy associated with electrical and magnetic
fields which are at right angles to each other
and the direction of propagation.
Electromagnetic radiation
Electromagnetic radiation has no mass and is
not affected by magnetic or electrical fields
nor to any great extent by gravity.
V
f
V 2 . 997 x 10 8
m / sec
E = hf
Where h is planks constant
(= 6.626196 x 10-34Js)
Properties of Electromagnetic
Inverse Square Law
Radiation
Travels at the speed of light.
Travels through a vacuum.
Travels in a straight line.
No electrical charge or mass.
D1
Intensity proportional to 1/D where D is the
distance from the source.
D2
3
Properties of Electromagnetic
Atomic Structure
Radiation
X and gamma rays Atoms are thought to consist of a positively
Absorbed and scattered by matter. charged nucleus surrounded by one or more
Not refracted by matter. negatively charged electrons that orbit the
nucleus.
Cause ionisation referred to as ionising
radiation. The nucleus consists of positively charged
particles called protons and electrically neutral
Will darken photographic film emulsion and particles called neutrons.
will cause some materials to fluoresce in the
visible or ultraviolet spectrum. A neutron can be thought of as a proton
closely combined with an electron.
Cannot be detected by human senses.
Extremely hazardous to health.
Protons have positive charge and by definition The nucleus of the atom is made up of protons and
an atomic mass of 1. neutrons. The electrons orbits the nucleus.
Neutrons have no electrical charge, atomic
mass very slightly greater than 1. Proton: Positive charge.
2 PROTONS
1 PROTON
2 ELECTRON
1 ELECTRON
2 NEUTRONS
No charge Positive charge: Ionisation has occurred
4
Atomic Structure Atomic Structure
LITHIUM
BERYLIUM
3 PROTONS
4 PROTONS
3 ELECTRONS
4 NEUTRONS
4 ELECTRONS
5 NEUTRONS
5
Atomic Structure Isotopes
Isotopes of Hydrogen
Deuterium
DEUTERIUM
1 PROTON
1 NEUTRON
1 ELECTRON
Isotopes of Hydrogen
Tritium
TRITIUM
1 PROTON
Isotopes of Hydrogen
2 NEUTRONS
1 ELECTRON
6
Radioactive Isotopes Radioactive Emissions
Alpha particles: +
Emitted by large nuclei such as uranium or
Some isotopes are stable, others are not. plutonium.
Unstable isotopes transform into another Composed of two protons and two neutrons
element and in so doing emit radiation. with a helium nucleus.
Three forms of radiation:
1. Alpha .
2. Beta .
3. Gamma .
Neutrons may also be emitted.
226
88 Ra 222
86 Rn 2 He
4
14
6 C 147 N e
7
Rate of Decay
Rate of Decay
Industrial Radiography
Gamma Rays
X - Rays
Generated by the
Electrically
decay of unstable
generated.
isotopes.
8
Radiographic Testing (RT) Welds Part 2: Equipment
NDT20 Covering pages 16-40 of your notes
1
X-Ray Production X-Ray Production
Current Current
Free electrons
-ve
-ve +ve -ve +ve
Tungsten
Focusing cup concentrates electrons into a beam
target
2
X-Ray Production X-Ray Production
3. Means of halting electrons: High density material Kinetic energy converted to heat and x-rays
X-rays / Bremsstrahlung
In any x-ray tube around 95 % of the energy A rotating anode may be used in order to help
generated is in the form of heat. dissipate heat. This type of arrangement is
For typical 200 kV portable equipment around generally limited to X-ray units intended for
1 kW of heat has to be dissipated. medical use.
For a 300 kV constant potential laboratory unit Modern X-ray units have so-called metal-ceramic
heat generation is typically 7.5 kW. envelopes. The use of such envelopes makes it
X-ray tubes of all types therefore require a cooling practical to have a much higher potential
system in order to prevent overheating and difference between the electrodes and the
increase duty cycle. envelope than was the case with glass.
Older type sets having glass envelope tubes are This in turn permits the use of grounded anodes.
generally oil or gas cooled. Such anodes are at zero volts and can therefore
be cooled directly by water.
3
X-Ray Production: Anodes X-Ray Production: Anodes
Rod-anode Rotating-anode
Beryllium window
Aluminium tube
X-ray
or intensity of or penetrating ability tube
radiation. of the radiation. AC
Power
HT transformer Rheostat
Autotransformer
mA
AC
Power
kV
4
X-Ray Production X-Ray Production
Current can flow across an X-ray tube only Output of C-rays can be more than doubled if
when the cathode (i.e. the filament) is the AC supply is rectified.
negative and the anode (i.e. the target) is X-ray equipment fitted with a rectifying circuit
positive. is referred to as constant potential.
Therefore if an X-ray tube is energised using a Most CP units use a Greinacher circuit to
simple AC supply X-rays will be produced only rectify the AC supply.
when the supply polarity is such that the CP units produce harder radiation than SR
cathode is negative and the anode is positive. even when operating at the same tube
Simple AC X-ray machines are therefore voltage.
referred to as self-rectified.
Radiation intensity
X-Ray Production
X-Ray Production
X-Ray Production
Decreasing energy
Radiation intensity
Increasing wavelength
5
X-Ray Production High Energy X-Ray Sources
Gamma rays
Isotope container
Projection
tube
Wind-out
6
Isotopes Used in Industrial Isotopes Used in Industrial
Radiography Radiography
Radiation energy/MeV
7
Advantages Disadvantages
Gamma rays compared with X- rays Gamma rays compared with X- rays
No water or electrical supplies needed. Reduced radiographic contrast.
Equipment smaller and lighter therefore more Exposure times generally longer.
portable. Sources need replacing potentially greater in-
Easier to perform radiography in confined or service costs.
difficult to access areas. Radiation cannot be switched off.
Equipment simpler and more robust. Generally inferior geometric unsharpness, SFD
Less scatter no low energy radiation. is usually minimised to obtain economic
Less initial cost. exposure time.
Greater penetrating power. Remote handling necessary.
Penetrating power cannot be adjusted.
8
Radiographic testing (RT) Welds Part 3: Image processing
NDT20 Covering pages 40-48 of your notes
Subbing
Base Base
Subbing
Supercoat
Emulsion mainly AgBr in gelatine base Emulsion mainly AgBr in gelatine base
Subbing Subbing
Base Base
Subbing Subbing
Emulsion mainly AgBr in gelatine base Emulsion mainly AgBr in gelatine base
Supercoat
1
Radiographic Film Latent Image Formation
Silver bromide crystals are not perfect they The interstitial silver atoms nucleate silver
contain interstitial silver ions. crystals.
When an interstitial silver ion accepts a free A single interstitial silver atom is sufficient to
electron it becomes a silver atom. cause an entire silver bromide crystal to
The silver atom is larger than the ion and convert to metallic silver.
exerts a stress on the crystal lattice. The typical size of a silver bromide crystal in a
In the presence of developer this stress causes typical photographic film emulsion is about
instability and the crystal breaks down 1 m.
resulting in the whole of the crystal changing Sensitisation of a silver bromide crystal can be
to black metallic silver. caused by just a single photon of X-ray
energy.
2
Intensifying Screens Intensifying Screens: Metallic
Metallic: Usually lead but other metals such as For radiation energy of 120 keV or greater front and
copper may be used. back lead intensifying screens are commonly used.
The optimum thickness of such screens varies with
Salt: Usually calcium tungstate. radiation energy but 0.03 - 0.15 mm is typical.
Fluorometallic: These are salt screens with a The front screen reduces the effect of radiation
metal foil backing. They combine the scattered by objects situated in front of the film
advantages of metallic and salt screens, including the object which is being radiographed and
helps to shorten exposure time.
however, they are extremely expensive and
The back screen reduces the effect of radiation
they are easily damaged.
scattered by objects situated behind the film and to a
lesser extent when compared with the front screen
helps to shorten exposure time.
Front screen
Primary radiation
Front emulsion
Secondary electrons No screens Pb screens: Poor contact
Metal usually Pb: Intensification factor about Developer: Reducing agent: Alkaline.
2x for radiation energies in excess of 120 keV. Stop bath: Acetic acid.
Salt: Intensification factor may be as high as Fixer: Dissolves silver halide: Acidic.
500x. Washing.
Fluorometallic: Intensification factor about Drying.
50x.
3
Film Processing Developer
A soaking time in the stop bath of just a few seconds is Fixing time is generally taken to be twice the clearing time.
sufficient to arrest development and neutralise alkalinity. Leaving film in fixer for an extended period may cause the film
emulsion to peel away from the base.
Fixer Fixer
4
Film Processing
Advanced Imaging Techniques
Washing Computed
20-30 minutes in clean running water. radiography Optical
Photo-multiplier
scanner
Usually followed by dipping in a clean water bath containing a tube
wetting agent which helps to promote even drying.
Laser
Note: Over washing must be avoided. beam
A/D
Over washing will cause swelling and excessive softening of converter
the film emulsion a major cause of drying marks.
Image type
The image formed is a positive image since
brighter areas on the image indicates where
higher levels of transmitted radiation reached
the screen.
5
Computed Tomography CT Images
6
Radiographic testing (RT) Welds Part 4: Image quality
NDT20 Covering pages 48-65 of your notes
Sensitivity Sensitivity
Film Film Quality of Subject Film Film Film Quality of Subject Film
density type radiation contrast processing density type radiation contrast processing
1
Factors Influencing Sensitivity Factors Influencing Sensitivity
Sensitivity Sensitivity
Type of Intensifying Radiation Relative Geometry Film Type Intensifying Radiation Relative Geometry Film
film screens quality movement processing of screens quality movement processing
film
Radiographic Quality
Geometric Unsharpness
Definition
The sharpness of the dividing line between
different density fields.
2
Geometric Unsharpness Geometric Unsharpness
=
Low Ug
Geometric Unsharpness
Geometric Unsharpness
High Ug Low Ug
Geometric Unsharpness
Geometric Unsharpness
High Ug Low Ug
3
Geometric Unsharpness
Reducing Geometric Unsharpness
High Ug
The drilled holes in step: Hole and plaque type EN ISO 19232-5 defined duplex wire IQI
IQIs are intended as an indicator of geometric containing 13 pairs of circular cross-section
unsharpness. wires made of platinum and tungsten.
Standard wire type IQIs (EN ISO 19232-1) are
poor indicators of geometric unsharpness.
A special type of IQI called a duplex wire IQI
is designed with a view to measuring
geometric unsharpness (EN ISO 19232-5).
Note: EN 462-5 was former standard which is technically identical with EN ISO
19232-5
Achieved
Wire Achieved basic
Duplex geometrical
diameter spatial resolution
identification unsharpness [mm]
[mm] [mm]
4
Inherent Unsharpness Inherent Unsharpness
Three major causes of scatter are: In the photoelectric effect an electron absorbs
Photoelectric effect. all of the energy of the incident X-ray photon.
Compton scattering (incoherent scatter). If the photon energy is sufficient the electron
Pair production. will be completely ejected from the atom and
ionisation will occur.
Other scattering mechanisms exist for Where the incident photon has exactly the
example: Rayleigh scattering (coherent right amount of energy the electron may
scattering). simply jump from one energy level to another.
As the affected atom returns to its base state
low energy X-rays are emitted in all directions.
5
Photoelectric Effect Compton Scattering
6
Coherent (Rayleigh) Scattering Coherent (Rayleigh) Scattering
Scatter Scatter
Internal scatter originating within the Side scatter from walls and nearby objects in
specimen the path of the primary beam
7
Scatter Checking For Back Scatter
Back scatter materials located behind the film British, European and American codes and
standards describe a method of checking for
back scatter.
A lead letter B is attached to the back of the
film cassette during exposure.
If a light image of the letter B appears in the
radiographic image then excessive back
scatter is present and the radiograph must be
retaken.
A dark image of B does not indicate
backscatter!!!
Angle
Dark image
of
of B:
scatter
Accept
Primary radiation
8
Control of Scatter Inherent Unsharpness
Collimation.
Typical inherent unsharpness for
Lead screens. Pb screens/fine grain film
Protection from back scatter. Radiation source Inherent unsharpness
Beam filtration (X-ray only). (mm)
Blocking. 100 kV X-rays 0.05
9
Radiographic testing (RT) Part 5: Exposure calculation
welds Covering pages 65-83 of your notes
NDT20
National codes and standards for radiography of Radiographic films provide good contrast at
welds and castings invariably define a minimum film densities exceeding about 1.5.
level of film density: Radiographs with a density exceeding 3.5 or
ASME V requires a minimum film density of perhaps 4.0 cannot be properly viewed and
1.8 for X-radiography of welds and a minimum assessed on standard radiographic film
of 2.0 for gamma techniques. illuminators.
EN ISO 17636-1 requires a minimum film Film density is easily measured using a
density of 2.0 for class A (basic techniques of densitometer or by comparison with a
X- or gamma radiography of welds) and a calibrated density strip.
minimum of 2.3 for class B (improved
techniques).
1
Radiographic Film Density
Radiographic Film Density
Exhausted Excessive
developer. development.
Developer too weak. Too strong a
solution.
Exposure/ mAmin
45
45
Specimen Radiographic
Steel Thickness / mm
40 35
Steel Thickness / mm
40
30
30
FFD or SFD.
25 20
20 25
Screens.
Filters.
15
15
Development.
10
10
Density required.
5
5
Intensity of radiation.
Exposure / mAmin
Aluminium 0.08 0.12 0.18 - 0.35 For example: Convert 10mm of steel to an
Al alloy 4.5% Cu 0.13 0.16 0.22 - 0.35 equivalent thickness of copper using 100 kV
X-rays:
Titanium 0.5 0.45 0.35 - -
Te = 10 x 1.6 = 16 mm
2
Film Factors Exposure Calculation
D7 D5 D4
EN ISO
11699-1
ASTM E
1815
AGFA CF KODAK CF FUJI CF FOMA CF Agfa
9.0 6.5 9.0
C1 Special D2 DR 50 7.2 IX 25 R2
CX AA 400 MX12
Kodak
4.2 3.3 4.2
C2 D3 M 100 4.2 IX 50 R3
5
2.6 2.6
C3 Class 1 D4 MX 125 2.8 --- R4
1.6 1.6 1.6
C4 D5 T 200 1.7 IX 80 R5 IX IX IX 80
C5 Class 2 D7
1.0
AA 400 1 IX 100
1.0
R7
1.0 Fuji 150 100
0.7 0.6 0.7
2 2.5 3 3.5 4 5 6 7 8
C6 Class 3 D8 CX 0.7 IX 150 R8
10 12 14
Relative exposure
Copyright TWI Ltd Copyright TWI Ltd
Change of FFD
Change of film: From CX to MX125.
Original exposure: 4 minutes.
Original exposure: 4 minutes. Original FFD: 1000 mm.
Film factor for CX: 0.7 New FFD: 750 mm.
Film factor for MX: 2.8
2.8 750
New Exposure = 4 16 minutes New time = 4 2.25 minutes
0.7 1000
Characteristic Curves
Characteristic Curves
3
Characteristic Curves Characteristic Curves
1.63 - 1.31 = 0.32 Antilog 0.32 = 2.1 2.07 - 1.63 = 0.44 Antilog 0.44 = 2.75 Using D7 film a
Original exposure = 10 mAmin Original exposure = 10 mAmin
New exposure = 2.1 X 10 = 21 mAmin New exposure = 2.75 X 10 = 27.5 density of 2.5
Using D7 film a
mAmin was achieved
density of 1.5 was
achieved using an using an
exposure of exposure of
10 mAmin. 10 mAmin.
What exposure is
required to achieve What exposure is
a density of 2.5? required to
achieve a
density of 2.5
using MX film?
4
Image Quality Indicators Image Quality Indicators
EN ISO 19232-2 Step-hole type IQIs ASTM E 1025 Plaque type IQIs
Sensitivity is
measured in terms
2-2T where 2 equals
a plaque thickness of
2T 2T
2 % of the test
specimen thickness
1T
4T 1T and 2T is the hole
XX: IQI thickness thousandths of that is visible on the
an Plaque
T: inch. radiographic image.
thickness.
5
Image Quality Indicators
6
Radiographic testing (RT)
Part 6: Techniques
Welds Covering pages 84-96 of your notes
NDT20
Radiographic Techniques
Radiographic Techniques
Required number of
exposures: 1
Location marker
placement: External
1
Radiographic Techniques Radiographic Techniques
Radiographic Techniques
Radiographic Techniques
Technique: DWDI
(superimposed)
Radiographic Techniques
Radiographic Techniques
Identification Identification
Unique identification. Unique identification.
Pitch markers: Location markers.
2
Radiographic Techniques Localisation
Localisation
Using similar
triangles:
Therefore:
=t-
3
Radiographic Testing (RT) Welds Part 7: Interpretation
NDT20 Covering pages 97-125 of your notes
Butt joints
In order to correctly interpret radiographs it is Square Edged
essential that the interpreter has a good Closed Open
knowledge of the product under examination and
the possible defects that may arise due to various
processes carried out on the test piece. Single Sided Butt
Vee Bevel
1
Welds Welding
2
Manual Metal Arc Welding Manual Metal Arc (MMA)
Weld metal
Flux Consumable
retrieval electrode Reel feed
Slag
Flux feed
3
Welding Defects Welding Defects
Cracks
Cracks
Classified by shape Classified by position Four crack types:
Longitudinal HAZ Solidification cracks.
Transverse Centreline
Crater Hydrogen induced cracks.
Branched
Fusion zone Lamellar tearing.
Chevron
Parent metal Reheat cracks.
Solidification cracking
Cracks
Solidification
Occurs during weld solidification process.
Steels with high sulphur content (low ductility
at elevated temperature).
Requires high tensile stress.
Occur longitudinally down centre of weld,
eg crater cracking.
4
Welding Defects Welding Defects
Cracks
Incomplete root
Re-heat cracking penetration
Occurs mainly in HAZ of low alloy steels Causes
during post weld heat treatment or service at Too large or small a root
elevated temperatures. gap.
Occurs in areas of high stress and existing Arc too long.
defects. Wrong polarity.
Prevented by toe grinding, elimination of poor Electrode too large for joint
profile material selection and controlled post preparation.
weld heat treatment. Incorrect electrode angle.
Too fast a speed of travel
for current.
Copyright TWI Ltd Copyright TWI Ltd
Root concavity
Incomplete root fusion
Causes Causes
Too small a root gap.
Arc too long.
Root gap too large.
Wrong polarity.
Electrode too large for joint Insufficient arc
preparation. energy.
Incorrect electrode angle. Excessive back purge
Too fast a speed of travel for TIG.
current.
5
Welding Defects Welding Defects
Cap undercut
Lack of fusion
Causes
Excessive welding current.
Welding speed too high. Causes
Incorrect electrode angle.
Excessive weave. Contaminated weld
Electrode too large. preparation.
Amperage too low.
Amperage too high (welder
increases speed of travel).
6
Welding Defects Welding Defects
Burn through
Inclusions: Tungsten
Causes
Causes Excessive amperage during welding of root.
Contamination of weld caused by tungsten Excessive root grinding.
touching weld metal or parent metal during Improper welding technique.
welding using the TIG welding process.
Arc strikes
Spatter
Causes
Causes Electrode straying onto parent metal.
Excessive arc energy. Electrode holder with poor insulation.
Excessive arc length. Poor contact of earth clamp.
Damp electrodes.
Arc blow.
7
Welding Defects Interpretation of Radiographs
Radiographic Details
Source of
Radiation
150 kV X-Ray Film Type Agfa D7
Screens Pb 0.125 mm front & back FFD/SFD 450
Radiographic Interpreter
Welding Details
Diameter N/A
Crimp marks.
Dirty intensifying screens.
During radiography and film processing Scratched intensifying screens.
images can be formed which are not due to a Static marks.
defect or a change in component thickness. Reticulation.
Such images are referred to as artefacts. Solarisation.
Chemical or water splashes.
Diffraction mottling.
Drying marks.
Streakiness.
8
Film Artefacts Film Artefacts
Scratched
intensifying
Dirty
screens
intensifying
screens May appear as either light
or dark images often
difficult to identify.
Static Reticulation
marks
Solarisation
Solarisation is image reversal due to extreme
over exposure or exposure to light during
development.
Water/developer
splashes
(Before development)
9
Film Artefacts Film Artefacts
Diffraction
Fixer/stop-bath
mottling
splashes
(Before development) Mottled effect
sometimes seen in x-
radiography of large
grained materials.
Drying marks
Dark marks caused by uneven drying.
Streakiness
caused by
poor agitation
during development
10
Interpretation of Radiographs Interpretation of Radiographs
Radiographic Interpreter
Welding Details
Diameter 324 mm
Radiographic Details
The film density is less than 2.0. The sensitivity is greater than
2%. No identification or location markers present. The IQI is
cannot be properly identified. A reshoot is required.
11
Interpretation of Radiographs Interpretation of Radiographs
12
Radiographic testing (RT) Welds Part 8: Safety
NDT20 Covering pages 126-138 of your notes
Principles
Justification
Due to the hazardous nature of ionising radiation Optimisation ALARA
it is important to understand the basic principles
Limitation
of radiation safety and have an understanding of
the current legislation regarding radiation
protection.
Units of dose
Units of dose
Quality factor
Gray
The degree of biological damage caused by a
The amount of radiation that will deposit one joule quantity of radiation.
of energy/kg of absorber.
1
Radiation Safety Radiation Safety
Quality factors
X or gamma rays: QF = 1.
Beta particles: QF > 1.
Units of dose Alpha particles: QF = 20.
Safe working
Safe working
Controlled area: Any area in which the dose will Supervised area: Any area in which the
exceed 3/10th annual dose for employees aged dose rate will exceed 1/3rd that of
18 or over. controlled area.
t
I I x2
0 HVL
The intensity of radiation is reduced by absorption
as is passes through matter.
t
I I x 10
Half value layer 0 TVL
The thickness of any material that will reduce the
radiation intensity to one half its initial value.
2
Radiation Safety Radiation Safety
D1 2 R1 D2 2 R2 D 1 2 R 1 D 2 R 2
2
D1 2 R1
D1: Original distance.
D2: Required distance.
R1: Original dose rate. D2
R2: Required dose rate. R2
D 1 2
R1
D2
R2 D2
1 13mGy / hr / Ci 20Ci 10001
7.5 Sv/hr
Dose rate at 1m also called output.
Co 60 13 mGy/hr/Ci. Safe distance = 186.2m
Ir 192 4.8 mGy/hr/Ci.
Yb 169 1.25 mGy/hr/Ci.
Safe distances
Personnel
Controlled area: Any area in which the dose
Radiation protection advisor (RPA). is likely to exceed 6mSv/yr or 3/10th annual
Radiation protection supervisor (RPS). dose for employees 18+.
Classified persons.
Trainee. 7.5mSvh-1: Maximum dose rate at the
Others. barrier.
3
Radiation Safety Controlled Area
4
Local Rules Radiation Safety
Survey meters produce a reading of the current For the detection of X or gamma radiation geiger
dose rate, usually in mSv/h or mSv/h. counters are usually used.
Geiger counters are effectively high voltage
Three types are used in industrial radiography: ionisation chambers.
They are designed to produce pulses of current
1. Geiger counters. when exposed to radiation.
2. Ionisation chambers. The number of pulses produced can be related to
3. Scintillation counters. the radiation dose rate.
Geiger counters are more compact and more
durable than standard ionisation chambers and
have a wider measurement range.
5
Radiation Dose Monitoring