CO1607 Final Report

CommitteeD2
ProficiencyTestingProgram

CrudeOil
SampleID:CO1607
July2016

Issuedby:
ASTMInternational
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Sponsored by ASTM Committee D-2 on Petroleum Products and Lubricants

Copyright 2016 ASTM International, West Conshohocken, PA. All rights reserved. This material
may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other
distribution and storage media, without the written consent of the publisher.

TABLE OF CONTENTS
Page
Report Introduction ...........................................................................................................3-7
Alphabetical Listing of Program Participants ............................................................. 8-12
Listing of ASTM Standards Used in Program ............................................................ 13
Summary of Statistics ................................................................................................. 14-15
Acid Number, D664 .........................................................................................................16-22
API Gravity
Method D287........................................................................................................ 23-28
Method D1298 (Corrected API Gravity) .............................................................. 29-33
Asphaltenes, D6560 ..........................................................................................................34-37
Carbon Residue (Micro Method), D4530.........................................................................38-44
Density
Method D1298...................................................................................................... 45-50
Method D5002...................................................................................................... 51-57
High Temperature Simulated Distillation, D7169 ...................................................... 58-111
Nitrogen
Method D4629............................................................................................................112-115
Method D5762............................................................................................................116-119
Chloride Content, D4929

Method A ....................................................................................................................120-121
Method B ....................................................................................................................122
Pour Point
Method D97................................................................................................................123-128
Method D5853 Method A ..........................................................................................129-131
Reid Vapor Pressure, D323......................................................................................... 132-135
Salts
Method D3230...................................................................................................... 136-141
Method D6470...................................................................................................... 142
Sediment
Method D473........................................................................................................ 143-149
Method D4807...................................................................................................... 150-154
Sulfur
Method D2622............................................................................................................155-158
Method D4294............................................................................................................159-167
Vanadium, Nickel, Iron
Method D5708
Method A..........................................................................................................168-175
Method B ..........................................................................................................176-183
Method D5863
Method A..........................................................................................................184-187
Method B ..........................................................................................................188-189
Total Vapor Pressure, D5191 ...................................................................................... 190-193
Vapor Pressure (Expansion Method), D6377 ............................................................. 194-197
Viscosity, Kinematic,
Method D445
25C ..........................................................................................................................198-201
40C ..........................................................................................................................202-208
Method D7042
40C .................................................................................................................... 209-211
100C .................................................................................................................... 212-213
Water
Method D4006...................................................................................................... 214-216
Method D4007...................................................................................................... 217-223
Method D4928...................................................................................................... 224-229
Method D4377(Karl Fischer) ............................................................................... 230-233
Box and Whisker Graphs ..................................................................................................234-243

Acid Number (D664)
API Gravity (D287 and D1298)
Density (D1298, D5002)
Iron (D5708-A, D5708-B, D5863-A)
Nickel (D5708-A, D5708-B, D5863-A, D5863-B)
Nitrogen (D4629, D5762)
Pour Point (D97, D5853-A)
Sulfur (D2622, D4294)
Vanadium (D5708-A, D5708-B, D5863-A, D5863-B)
Vapor Pressure (D323, D5191, D6377)
Water (D4006, D4007, D4928, D4377)
Participant Comments ................................................................................................. 244-246
Test Instructions and Lab Worksheet.......................................................................... 247-261

INTRODUCTION
3
This report constitutes the final report of results for the July 2016 Crude Oil (CO1607) Proficiency Testing
Program. This report contains tables of results for laboratory data for each test, statistical summary analyses
of data for each test, graphs charting deviations, histograms, box-and-whisker charts and statistical
statements about the test results that include a comparison of the Reproducibility from these test data against
the Reproducibility as stated in the ASTM standard. Tables and charts are labeled with the program title,
sample ID, test period, test procedure(s), and an indication of apparatus (manual / automatic) or procedure
used within a standard.
The TABLE OF RESULTS provides a listing of laboratories with corresponding test results. Each
laboratory is identified by a randomly selected code with the same laboratory code applying throughout the
entire report. Standards that report automatic and manual apparatus results are combined within the same
table and graph for statistical analysis when there is a single Reproducibility statement provided within the
respective standard. An indication of the type of apparatus used (Automatic = "A" / Manual = "M") is
provided in the table for each lab result. Separate tables and graphs are provided for automatic and manual
apparatus when the respective standard contains a separate Reproducibility statement for each type
apparatus. The same data presentation applies for standards that report multiple procedures within the same
standard.
Description of Z-Score Column: The z-score column reports each lab's deviation in units of standard
deviations. The z-score is the ratio of the deviation to the standard deviation. A z-score greater than 2 -- or
less than negative 2 -- should cause a laboratory to review their test data for any possible systematic error.
Z-scores outside this range should occur only about one time in twenty, if a laboratory has average capability
running the method. Laboratories should strive to obtain z-score values close to zero.
Description of the Robust Mean and Robust Standard Deviation
These statistics are performed on data tables containing six (6) or more test results. Means and standard
deviations are computed using a two-stage robust procedure which is designed to limit the influence of
unusually large or small results, while eliminating only the most egregious among them. The computations
and philosophy of robust statistics are explained more fully in Robust Statistics - How Not to Reject Outliers,
by the Analytical Methods Committee of the Royal Society of Chemistry, Analyst, 114 pp. 1693-97, Dec.
1989. In this report, data are subjected to these robust computations twice. At the first stage, a robust mean
estimate and a robust standard deviation estimate are computed using all results. Results which differ from
this (first stage) robust mean by more than three times the (first stage) robust standard deviation are noted as
outliers (shown in the Table of Results marked with a double asterisk) and excluded from the second-stage
robust computation. The second stage estimates are determined by applying the robust mean and standard
deviation procedure to those non-outlying results. There is no second stage exclusion. As the second-stage
robust standard deviation is generally smaller than that of the first stage, some non-excluded results may
differ from the robust mean by more than three robust standard deviations. In other words, some non-
excluded results may lead to z-scores greater than 3 or less than -3.
A description of an iterative algorithm for computing robust means and standard deviations is provided in the
next section. The process is tedious, but the estimates do have the following property which can easily be
verified. If n results are included in the computation, and if all the results which differ from the robust mean
by more than 1.5 (n 1) n times the robust standard deviation are replaced by the robust mean
1.5 (n 1) n robust standard deviations, as appropriate, then the mean of these trimmed results will
equal the robust mean, and the standard deviation of the trimmed results will be .882 times the robust
standard deviation.
Calculation of Robust Mean and Robust Standard Deviation
The robust mean and robust standard Deviation of a collection of n results may be calculated using the
following iterative process. First find initial estimates of the robust mean and robust standard deviation.
The median of all test results, and 1.5 times the median of absolute deviation from this median may be used
as the initial estimates. 4
The initial estimates or any estimates may be improved as follows: Multiply the current standard
( )
deviation estimate by 1.5 (n 1) n , and add this value to, and subtract it from, the current mean estimate
to arrive at upper and lower limits. Retain test results that fall within these limits, and replace each of the
remaining results by the limit nearest to it. (This process is called trimming.) Improved mean and
standard deviation estimates are calculated using this set of trimmed values: robust mean estimate = average
of the trimmed results; robust standard deviation estimate = standard deviation of results divided by 0.882.
Compare the improved robust standard deviation estimate to the initial or current standard deviation estimate.
If the two estimates are equal, then record the improved estimates as the robust mean and robust standard
deviation. (The two robust standard deviation estimates are considered to be equal if their decimal
expansions agree to one digit beyond the reporting resolution of the test values.) If the robust standard
deviation estimates are not equal, then the improved estimates become the current estimates and the
improvement process begins again with the calculation of a new set of upper and lower limits.
For the two-stage robust mean and standard deviation, remove all test values that are more than three robust
standard deviations from the robust mean, and repeat the entire iterative improvement process described
above until the estimates stabilize a second time.
TEST PERFORMANCE INDEX (Industry) (TPI(Industry)) - TPI(Industry) provides an index similar to

that defined in ASTM D6792 for TPI. TPI uses the ratio of "test method reproducibility / site precision"
whereas TPI(Industry) is based on the ratio of the test method reproducibility to the Robust Reproducibility
of the program data. It is suggested that the TPI interpretation guide mentioned in D 6792 section 10 can
also be applied to the interpretation of TPI (Industry). Further guidance on interpreting the results can be
found in D7372.
TPI (Industry) = RASTM / Robust R These Data
ANDERSON-DARLING STATISTIC (AD) The Anderson Darling test is used to test if a sample of data
came from a population with a specific distribution, namely: it performs a goodness of fit test to determine
if the data are from a NORMAL distribution.
PTP test data distribution is tested against normal behavior and measurement resolution adequacy using the
AD statistic. Gross violations (AD >1.0) are flagged and a comment is systematically added to the data
tables stating the data should not be interpreted using conventional normal distribution based probabilities.
For more details see ASQ publication ISBN 0-87389-015-9: How to Test Normality and Other
Distributional Assumptions Samuel S. Shapiro.
HISTOGRAMS are provided for single methods where at least 20 test results are reported. For histograms
containing 20 to 29 data points, a line indicating the median has been included however, 1 % and 99%
confidence fences are not included. For histograms containing 30 or more data points, a median line and 1%
and 99% confidence fences are superimposed over the distribution range of results. With outliers removed
from the dataset, an algorithm utilizing the minimum of round(sqrt(n))and number of possible data points per
bin is used to determine the optimal number of bins for each histogram. Each histogram bin is based on the
reporting resolution for the applicable method.
If the data are considered to be a normal distribution as determined by the Anderson Darling (AD) statistic
of a factor of NOT greater than 1.0, then the determination of the 1% and 99% confidence fences and
medians in histograms with 30 or more data points are calculated using the formula below.
Robust Mean + / - 2.33 x Robust Standard Deviation
If the AD statistic indicates a non-normal distribution of data (AD > 1.0), then the resulting histogram will
display the median and 1% and 99% confidence fences that are produced using an algorithm to determine
what intervals contain a fixed percentage of the population values. A comment will appear on the data
summary table stating the test data are non-normal. 5
GRAPHS are provided for test methods where there are six or more test results. The "Y" scale on the right
scale is in natural units, deviations are on the left scale. Laboratory codes are provided on the "X" scale.
Each laboratory's data is plotted, excluding outliers. Laboratories whose data would be plotted off the scale
are indicated with an arrow. Horizontal lines are provided at the mean and mean plus/minus two sets of three
sigma control limits. The two sets of control limits provide a means of comparing where a laboratory's data
falls in conjunction to the Reproducibility of These Test Data against the ASTM Standard Reproducibility.
The two sets of control limits are: Reproducibility of These Test Data calculated by multiplying the robust
standard deviation by 3 (or more precisely 2.77); and Reproducibility of the ASTM Standard precision
statement calculated by multiplying 1.083 times the ASTM Reproducibility.
Box and Whisker Graphs provide a cross reference of test data generated from different procedures and
methods that determine the same test parameter. The box and whiskers graph separates the test data by standard
with the box representing the middle 50% of test data centered around the median. The horizontal line within the
box represents the median of the reported data. The whisker length has been adjusted to the last data point that
falls within 1.5 times the difference between the upper and lower value of the shaded box. Data points above or
below the whisker are included, unless the data is off the "Y" axis scale. Data that would be plotted off the graph
are indicated with an arrow. Outlier data are not included in this graph. The "Y" axis scale represents the
absolute value; the "X" axis scale provides an identification of the test method and number of reporting data
points.
GENERAL COMMENTS: Notes have been added to specific tables, where appropriate, to explain any
unique situations.
For more information on the interpretation and use of ASTM Proficiency Test Program Data and Statistics,
please obtain a copy of ASTM D7372 Standard Guide for Analysis and Interpretation of Proficiency Test
Program results at www.astm.org.
USE OF CURRENT & PAST Z-SCORES TO MONITOR LAB PERFORMANCE AND

MEASUREMENT PROCESS PRECISION (JULY 2008)
Participation in any of the 26 ASTM Proficiency Test Programs where typical production samples are tested
by multiple measurement systems using specified ASTM tests, provides a cost-effective means of assessing
measurement system precision relative to average industry performance.
With each ASTM-PTPTP statistical summary report received, participants should plot their signed deviations
from the consensus values (robust mean) on control charts to ascertain if their measurement processes are
accurate and non-biased relative to these ASTM-PTPTP robust means from program trial to trial.
Per D 6299, a Z-score is defined as a standardized and dimensionless measure of the difference between an
individual result in a data set and the robust mean of the dataset, re-expressed in units of standard deviation
of the dataset (by dividing the actual difference from the robust mean by the standard deviation for the data
set).
Z-Score = X (individual lab result) - Robust Mean (These Data)

Robust Standard Deviation (These Data)
Z-Scores for the current and past six test cycles are provided for each laboratory by test parameter where the
robust statistical routine was utilized to generate statistics in the statistical summary report
The purpose of reporting the current and past Z-Scores in this format is to provide a chronological approach
to monitoring Z-Scores as a means of evaluating lab precision over time to ascertain the in-statistical-control
status of laboratory performance and the measurement system being used. By use of the Precision Indicator
for each test in each final statistical summary report, a laboratory can immediately confirm their performance
precision over the current trial and six (6) past test trials depending upon the availability of the historical Z-
Scores in the PTP database. 6
Per D7372, participants should trend analyze Z-Scores from previous rounds by plotting the Z-score values
for each test method (parameter) for successive PTP program rounds on a control chart to show precision
trends over time. The lab can use the run rules promulgated in Practice D 6299 to evaluate any observed
trends and conduct investigations to determine causes or needs for improvement as needed.
The Mean Z-Score is calculated and reported based on the current and past six valid Z-Scores. Null, 0.0,
NDS and $ do NOT count as valid Z-Scores. The sign and magnitude of this result is an indication of the
long-term relative bias. Investigations to determine the cause of any perceived bias should be conducted as
needed.
The last column contains relevant statistics performed on past Z-Scores for each lab. The Precision Indicator
(PI) is calculated by dividing the overall Pooled Standard Deviation by the Standard Deviation Z for each
lab. If the resulting calculation produces a Lab Precision Indicator value of <0.800, then a flag (X) appears in
the Significant Difference column indicating lab precision needs improvement. The Precision Indicator (PI)
formula is restricted to a minimum of four (4) valid Z-Scores before it is applied.
Note 1: The Precision Indicator is a type of test performance index (TPI) as described in the Introduction to
this report and in D6792 (10.1). The critical value of <0.8 is also described in the interpretation guide of
D6792 (10.3.1.3) and D7372 (6.1.7.1)
OTHER LEGEND SYMBOL DEFINITIONS/APPLICATIONS
** - Data for current trial is rejected
R Data was rejected and no Z-Score calculated for that past trial.
NDS Lab did not submit data for that trial
ND Not Detected = valid D4815 result
N/A Not Applicable minimum number of 4 Z-Scores not met for Precision Indicator formula to be
applied.
$ - applies to past Z-Scores possibly meaning:

All lab results submitted were the same, therefore Z-Scores non-existent
Statistics were not performed for test even if data submitted due to:
o Data too variable and/or bimodal distribution
o Insufficient data submitted for analyses (< six results)
o Robust standard deviation exceeded the robust mean for those tests that produce
positive test results
X Lab Precision May Need Improvement based on Performance Indicator value in preceding column being
< 0.800. For more guidance on this, see D6792 per Note 1 above.
* - Data was submitted, but no past Z-Scores were published because:

New program and no historical records available
New test and no historical records available
Lab Z-Scores limited to participation history
Naming convention for the test method in the ASTM database changed during the past six
cycles. Z-Scores that appear are from the time of the change forward. Six (6) Z-Scores will
populate over time.
A CHECK LIST FOR INVESTIGATING THE ROOT
CAUSE OF UNSATISFACTORY ANALYTICAL PERFORMANCE 7
To identify why a laboratorys data may have been considered a statistical outlier and/or improve the
precision, the following action items are suggested. There may be additional ways to improve the
performance.
1. Check the results for typos, calculation errors, and transcription errors.
2. Reanalyze the sample; check for repeatability.
3. Check the sample for homogeneity or contamination, and that a representative specimen has been
analyzed.
4. Review the test method and ensure that the latest version of the ASTM test method is being used.
Check the procedure step by step with the analyst.
5. Check the instrument calibration.
6. Check the statistical quality control chart to see if the problem has been developing earlier.
7. Check the quality of the reagents and standards used; and whether they are expired or
contaminated.
8. Check the equipment for proper operation against vendors operating manual.
9. Call the vendor for maintenance and/or repairs.
10. After the problem has been resolved, analyze a certified reference material if one is available,
or the laboratory quality control sample to ascertain that the analytical operation is under
control.
11. Provide training to new analysts and, if necessary, refresher training to experienced analysts.
12. Document the incident and the learnings for use in future similar problem.
Alphabetical Listing of Laboratories 8
Participating in CO1607 Crude Oil

ASTM Proficiency Testing Program
(Alphabetical list does not correspond to
randomly selected lab codes published in the report)
AGAT LABORATORIES, LAB # 2 AMSPEC SERVICES LLC CALCASIEU REFINING CO
EDMONTON, AB CANADA T6E6S4 SAINT ROSE, LA 70087 LAKE CHARLES, LA 70605
AGAT LABORATORIES AMSPEC SERVICES LLC CAMIN CARGO

CALGARY, ABAB CANADA T2E 6V6 TEXAS CITY, TX 77590 LA MARQUE, TX 77568
AIR POLLUTION TESTING INC AMSPEC SERVICES LLC CAMIN CARGO CONTROL
ARVADA, CO 80002 NEDERLAND, TX 77627 SULPHUR, LA 70663
ALBERTA INNOVATES TECHNOLOGY FUTURES AMSPEC SERVICES LLC CAMIN CARGO CONTROL INC
EDMONTON, AB CANADA T6N 1E4 CORPUS CHRISTI, TX 78409 NEDERLAND, TX 77627
ALYESKA PIPELINE SERVICE CO ANALISTAS QUIMICOS PETROLEROS S A S CAMIN CARGO CONTROL INC
MS 704 VIS 40 # 69-121 RICHMOND, CA 94804
VALDEZ, AK 99686 BARRANQUILLA, COLOMBIA 080020445
CAMIN CARGO CONTROL INC.
ALYESKA PIPELINE SERVICE CO ANALISTAS QUIMICOS PETROLEROS S.A.S. PASADENA, TX 77502
NORTH POLE METERING STATION LABORATORY CARTAGENA, COLOMBIA 130013
FAIRBANKS, AK 99701 CAMIN CARGO CONTROL SERVICES
ANDES PETROLEUM - LABORATORIO ESTACION DAYUMA
CORPUS CHRISTI, TX 78405
ALYESKA PIPELINE SERVICE CO REPUBLICA DEL SALVADOR
PUMP STATION ONE QUITO, PICHINCHA ECUADOR 170515 CAMIN CARGO CONTROL
PRUDHOE BAY, AK 99734 BUILDING NO. 0770 A/B
ARAB PETROLEUM PIPELINES - 2 LA BOCA, BALBOA, PANAMA
AMSPEC SERVICES LLC SIDI-KERIR LAB
DARTMOUTH, NS CANADA B3B 1X3 ALEXANDRIA, EGYPT CAMIN CARGO INC
UNIT #A-2
AMSPEC SERVICES, LLC ARAB PETROLEUM PIPELINES CO BELLINGHAM, WA 98229
GONZALES, LA 70737 ALEXANDRIA, EGYPT
CAMIN CARGO INC
AMSPEC LLC ARAMCO SERVICES UNIT 2
AVENEL, NJ 07001 JEDDAH REFINERY LAB 1 FIFE, WA 98424
JEDDAH, SAUDI ARABIA 21422
AMSPEC LLC CAMIN CARGO INC
CONCORD, CA 94520 ARAMCO SERVICES UNIT C
PO BOX 5000 LONG BEACH, CA 90813
AMSPEC LLC ABQAIQ, SAUDI ARABIA 31311
PLAINFIELD, IL 60585 CAMIN-CARGO CONTROL
BP EXPLORATION INC ALASKA REGION THOROFARE, NJ 08086
AMSPEC LLC 3027 RAMPART DR
SUITE 9 ANCHORAGE, AK 99501 CENOVUS FCCL LTD.
FERNDALE, WA 98248 MAINT & OPS WAREHOUSE
BP PRODUCTS NORTH AMERICA EDMONTON, AB CANADA T5V 1H8
AMSPEC LLC RECEIVING DOCK 10-2 LABORATORY
PASADENA, TX 77503 WHITING, IN 46394 CERTISPEC SERVICES USA, INC.
TEXAS CITY, TX 77590
AMSPEC SERVICES LLC BAHRAIN NATIONAL GAS CO
SIGNAL HILL, CA 90755 RIFA'A, BAHRAIN CHEMSAIN KONSULTANT SDN BHD
TAMAN PERINDUSTRAIN SURIA, JALAN KOLOMBONG
AMSPEC SERVICES LLC BAKER HUGHES KOTA KINABALU, SABAH MALAYSIA 88300
PAULSBORO, NJ 08066 MOUNT PEARL, NL CANADA A1N 4R5
CHEVRON NGC LAB
AMSPEC SERVICES LLC BINH SON REFINING COVINGTON, LA 70433
MINOT, ND 58703 QUANG NGAI CITY, VIET NAM 84553825825
CITGO LEMONT REFINERY ENBRIDGE PIPELINES INC. FORMOSA PETROCHEMICAL CORP 9
MAIN WAREHOUSE SUPERIOR, WI 54880 MAIL-LIAO VILLAGE
LEMONT, IL 60439 YUN-LIN COUNTY, TAIWAN 638
ENBRIDGE PIPELINES INC
CITGO PETROLEUM 17TH STREET FORT MACKAY LOGISTICS
CORPUS CHRISTI, TX 78407 EDMONTON, AB CANADA T6P 0A0 5744-67 AVE. NW
EDMONTON, AB CANADA T6B 3P8
COASTAL GULF ENVIRONMENT AND CLIMATE CHANGE CANADA
LULING, LA 70070 OTTAWA, ON CANADA K1A 0H3 GIBSON ENERGY
EDMONTON, AB CANADA T6B3R7
COASTAL GULF & INTERNATIONAL ESSO (THAILAND) PUBLIC COMPANY LTD
PASADENA, TX 77502 TUNGSUKHLA, SRIRACHA DISTRIC HELLENIC PETROLEUM S.A.
CHONBURI, THAILAND 20230 THESSALONIKI INDUSTRIAL COMPLEX
COASTAL GULF & INTERNATIONAL INC THESSALONIKI, VERIA GREECE 54110
NEDERLAND, TX 77627 ESSO AUSTRALIA PTY LTD
ESSO LONGFORD LABORATORY HELLENIC PETROLEUM SA
COFFEYVILLE RESOURCES REFINING LONGFORD VICTORIA, AUSTRALIA 3851 ATHENS - KORINTHOS
COFFEYVILLE, KS 67337 ASPROPYRGOS, ATTIKI GREECE 19300
ESSO AUSTRALIA PTY LTD
CORE LABORATORIES CEMETERY ROAD INA D.D.
NEDERLAND, TX 77627 HASTINGS, AUSTRALIA 3915 SISAK, CROATIA 44000
CORE LABORATORIES LP (PENCOR) ESSO NORGE AS INA-RAFINERIJA NAFTE RIJEKE

BROUSSARD, LA 70518 ESSOVEIEN 100 KOSTRENA, CROATIA 51221
TOLVSROD, NORWAY 3153
CORE LABORATORIES LTD INSPECTORATE AMERICA
CALGARY, AB CANADA T2E 7P7 EXOVA CANADA INC. BEAUMONT, TX 77705
EDMONTON, AB CANADA T6B 3J4
DIRECCION DE INVESTIGACION CRIMINAL E INTERPOL DUIN LAB DE QUIMICA INSPECTORATE AMERICA
LABORATORIO DE QUIMICA FORENSE EXOVA CANADA INC. ASTON, PA 19014
BOGOTA, CUNDINAMARCA COLOMBIA 110931 BOX 7706
DRAYTON VALLEY, AB CANADA T7A 1S8 INSPECTORATE AMERICA
DIXIE SERVICES, INC. CORPUS CHRISTI, TX 78405
GALENA PARK, TX 77547 EXXON MOBIL BEAUMONT
BEAUMONT REFINERY INSPECTORATE AMERICA
ECOPETROL - GRB BEAUMONT, TX 77701 PORTLAND, ME 04106
COORDINACION INSPECCION DE CALIDAD - CID (LABORATORIO)
BARRANCABERMEJA, SANTANDER, COLOMBIA EXXON MOBIL RES & ENG CO INSPECTORATE AMERICA CORP
PAULSBORO, NJ 08066 TORRANCE, CA 90501
ECOPETROL - GRC
KM 10 CARTAGENA EXXONMOBIL JOLIET REFINERY INSPECTORATE AMERICA CORP
SURAMERICA, COLOMBIA CHANNAHON, IL 60410 SAINT ROSE, LA 70087
ECOPETROL - ICP EXXONMOBIL PETROLEUM & CHEMICAL BVBA INSPECTORATE AMERICA CORP
KM 7 VIA A PIEDECUESTA ANTWERP, BELGIUM 2030 SUITE 7
SURAMERICA, COLOMBIA FERNDALE, WA 98248
EXXONMOBIL ASIA PACIFIC PTE LT
ELEMENT MATERIALS TECHNOLOGY SINGAPORE REFINERY LAB INSPECTORATE AMERICA CORPORATION
SCOTT, LA 70583 SINGAPORE, SINGAPORE 628498 TEXAS CITY, TX 77590
ENAP REFINERIA BIO BIO EXXONMOBIL INSPECTORATE AMERICA CORPORATION

HUALPEN TALCAHUANO REFINERY LAB STA 45 HOUSTON TECHNICAL CENTER
TALCAHUANO, CONCEPCION, CHILE BAYTOWN, TX 77520 PASADENA, TX 77506
ENAP REFINERIAS CON CON FLINT HILL RESOURCES LP INSPECTORATE AMERICA

CONCON, CHILE WICHITA, KS 67220 BUILDING F
MOBILE, AL 36619
ENBRIDGE ENERGY FLUOR FEDERAL PETROLEUM OPERATIONS, LLC (FFPO)
CUSHING, OK 74023 STRATEGIC PET RES LAB INSPECTORATE AMERICA
HACKBERRY, LA 70645 STE D
MARTINEZ, CA 94553
INSPECTORATE LTD INTERTEK INTERTEK 10
FREEPORT, BAHAMAS ESSINGTON, PA 19029 SINGAPORE TECHNICAL CENTER
SINGAPORE, SINGAPORE 628208
INSPECTORATE DE MEXICO S.A. DE C.V. INTERTEK
COL. LAS AMERICAS BELLINGHAM, WA 98225 IRVING OIL REFINING G P
COATZACOALCOS, VERACRUZ MEXICO 96480 520 GRANDVIEW AVENUE
INTERTEK (SHETLAND ISLANDS) SAINT JOHN, NB CANADA E2J 4M9
INSTITUTO MEXICANO DEL PETROLEO EXPLORATION DRIVE
COL. SAN BARTOLO ATEPEHUACAN BRIDGE OF DON, ABERDEEN UNITED KINGDOM AB23 8HZ
KUWAIT OIL COMPANY
CIUDAD DE MEXICO, MEXICO 07730 AHMADI, KUWAIT 61008
INTERTEK CALEB BRETT
INSTITUTO MEXICANO DEL PETROLEO TOKYO, JAPAN 143-0003 LABORATORIO DE REFINERIA TALARA
COL. SAN BARTOLO ATEPEHUACAN SAN ISIDRO
IMP-650823397, DISTRITO FEDERAL MEXICO 07730 INTERTEK CALEB BRETT ECUADOR S.A. LIMA, PERU
LAGO AGRIO, SUCUMBIOS, ECUADOR
INTERTEK LIMA REFINING COMPANY
CARTERET, NJ 07008 INTERTEK SUNBURY LIMA, OH 45804
UNIT A, SHEARS WAY
INTERTEK MIDDLESEX, UNITED KINGDOM TW16 7EE LION OIL CO
TEXAS CITY, TX 77590 EL DORADO, AR 71730
INTERTEK TESTING SERVICES
INTERTEK PORT MELBOURNE, AUSTRALIA 3127 LYONDELLBASELL INDUSTRIES
VALDEZ, AK 99686 12000 LAWNDALE
INTERTEK HOUSTON, TX 77017
INTERTEK 3194 AB HOOGVLIET (RT)
SAINT ROSE, LA 70087 NETHERLANDS MOL PLC DS LOGISTICS FENYESLITKE PU
FENYESLITKE, HUNGARY 4621
INTERTEK INTERTEK
BISMARCK, ND 58504 A-84 LOCAL 1 Y 2 MARATHON PETROLEUM COMPANY - GALVESTON BAY REFINERY
CARTAGENA, COLOMBIA 2401 5TH AVE SOUTH
INTERTEK TEXAS CITY, TX 77590
CUSHING, OK 74023 INTERTEK
EXPLORATION DRIVE, ABERDEEN SCIENCE AND ENERGY
MARATHON
PARK PETROLEUM COMPANY LLC
INTERTEK ABERDEEN, UNITED KINGDOM AB23 8HZ RES AND ENGRG BLDG
DEER PARK, TX 77536 CATLETTSBURG, KY 41129
INTERTEK
INTERTEK INDUSTRIAL AREA SECTOR 6 MARATHON PETROLEUM COMPANY LLC
ROMEOVILLE, IL 60446 SHARJAH, UNITED ARAB EMIRATES TEXAS CITY, TX 77592
INTERTEK INTERTEK MARATHON PETROLEUM COMPANY LLC

ELMENDORF, TX 78112 LARGS NORTH SA #2 REFINERY PRODUCT CONTROL
ADELAIDE, AUSTRALIA 5016 CATLETTSBURG, KY 41129
INTERTEK
BENICIA, CA 94510 INTERTEK MARATHON PETROLEUM COMPANY LLC
LAS VENTANAS 4663 WEST AIRLINE HIGHWAY
INTERTEK QUINTERO, CHILE GARYVILLE, LA 70051
DARTMOUTH, NS CANADA B2Y 1A1
INTERTEK MARATHON PETROLEUM COMPANY LLC
INTERTEK P O BOX 118 800 OLD OAKWOOD BLVD
EDMONTON, AB CANADA T5V1R9 COME BY CHANCE, NL CANADA A0B 1N0 DETROIT, MI 48217
INTERTEK INTERTEK MARATHON PETROLEUM COMPANY LLC

GONZALES, LA 70737 SAN MIGUEL MARATHON AVE.
LIMA, PERU 32 ROBINSON, IL 62454
INTERTEK
ALBANY, NY 12202 INTERTEK MARATHON PETROLEUM COMPANY LLC
SETTLERS BUSINESS PARK QUALITY CONTROL LAB
INTERTEK PITTSBURGH, PA 15205 CANTON, OH 44706
CORPUS CHRISTI, TX 78408
MAXXAM ANALYTICS INC
EDMONTON, AB CANADA T6B 3M9
MAXXAM ANALYTICS PETROAMAZONAS EP PT INTERTEK UTAMA SERVICES 11
6474 ROPER ROAD CAMPO LIMONCOCHA J1 RAYA BOGOR KM 28
EDMONTON, AB CANADA T6B 3P9 LIMONCOCHA, SUCUMBIOS ECUADOR JAKARTA TIMUR, INDONESIA 13710
MONROE ENERGY PETROAMAZONAS EP PUMA ENERGY PNG REFINING LIMITED

TRAINER, PA 19061 CAMPO PALO AZUL HARBOUR CITY
PALO AZUL, FEO ORELLANA ECUADOR PORT MORESBY, PAPUA NEW GUINEA 1971
MONTREAL PIPE LINE LTD
MONTREAL, QC CANADA H1B 1B3 PETROAMAZONAS EP RUDOLPH RESEARCH ANALYTICAL
ESTACION CENTRAL HACKETTSTOWN, NJ 07840
NATIONAL COOPERATIVE REFINERY SHUSHUFINDI, SUCUMBIOS ECUADOR
MCPHERSON, KS 67460 S K CORP
PETROAMAZONAS EP ULSAN, KOREA, REPUBLIC OF 680130
NATURAL RESOURCES CANADA (WRC) ESTACION SUCUMBIOS
SUITE A202 SUCUMBIOS, SUCUMBIOS ECUADOR SGS CONTROL SERVICES
DEVON, AB CANADA T9G 1A1 CARTERET, NJ 07008
PETROGAL S.A.
NORTH ATLANTIC REFINING LTD 7520-952 SINES, PORTUGAL SGS NORTH AMERICA
PO BOX 40 NEWPORT NEWS, VA 23602
COME BY CHANCE, NL CANADA A0B 1N0 PETRONAS RESEARCH SDN BHD
KAWASAN INSTITUSI BANGI SGS NORTH AMERICA INC
OIL SEARCH (PNG) LIMITED KAJANG, SELANGOR MALAYSIA 43000 SAINT ROSE, LA 70087
PORT MORESBY 121, PAPUA NEW GUINEA
PHILADELPHIA ENERGY SOLUTIONS SGS NORTH AMERICA INC
OILFIELD, ENVIRONMENTAL & COMPLIANCE, INC. 3144 PASSYUNK AVE., DROP #16 EAST ALTON, IL 62024
SUITE 300 PHILADELPHIA, PA 19145
SANTA MARIA, CA 93454 SGS NORTH AMERICA INC
PHILLIPS 66 CARSON, CA 90746
OROGENIC RESOURCES SDN BHD BARTLESVILLE, OK 74005
JALAN ASTAKA U8/84, SEKSYEN U8, BUKIT JELUTONG SGS OG & C
SHAH ALAM, MALAYSIA 40150 PHILLIPS 66, RODEO REFINERY BEAUMONT, TX 77705
RODEO, CA 94572
PSL PROANALISIS SPL, INC.
BUCARAMANGA CITY, COLOMBIA PHILLIPS 66 HOUSTON, TX 77054
MADISON AVENUE, GATE 19
PAN PACIFIC SURVEYOR, INC ROXANA, IL 62084 SABAH SHELL PETROLEUM CO LTD
WILMINGTON, CA 90744 POB 81208
PHILLIPS 66 LABUAN, MALAYSIA 87022
PETROAMAZONAS BLOQUE 12 RESEARCH WEST SHIPPING DOCK
EL EDEN, FCO ORELLANA ECUADOR PONCA CITY, OK 74602 SARAWAK SHELL BERHAD
JALAN PIASAU
PETROAMAZONAS EP PHILLIPS66 FERNDALE REFINERY MIRI, MALAYSIA 98100
CUYABENO, SUCUMBIOS ECUADOR FERNDALE, WA 98248
SAUDI ARAMCO REFINERY LAB - I
PETROAMAZONAS EP PORTLAND PIPE LINE LTD 2016 PURCHASE ORDER 4804529240
CHONTAPUNTA, NAPO ECUADOR PORTLAND, ME 04103 RAS TANURA, SAUDI ARABIA 31311
PETROAMAZONAS EP PRI ASPHALT TECHNOLOGIES, INC. SAUDI ARAMCO SERVICES CO, #2

LAGO AGRIO, SUCUMBIOS ECUADOR TAMPA, FL 33610 2016 PO4504838688
YANBU AL-SINAIYAH, SAUDI ARABIA
PETROAMAZONAS EP PROASEM S.A.
TAMBOCOCHA, FEO ORELLANA ECUADOR CALLE 120 NO. 45 A-32 SAYBOLT DE COLOMBIA LTD
BOGOTA, COLOMBIA BOGOTA, COLOMBIA 110131
PETROAMAZONAS EP
CAMPO AUCA PT INTERTEK UTAMA SERVICES SAYBOLT INC
CAMPO AUCA, FEO ORELLANA ECUADOR JAKARTA TIMUR 13710, INDONESIA SUITE A
TUKWILA, WA 98188
PETROAMAZONAS EP PT INTERTEK UTAMA SERVICES
CAMPO COCA J1 RAYA BOGOR KM 28 SAYBOLT LP
COCA, FEO ORELLANA ECUADOR JAKARTA TIMUR, INDONESIA 13710 HOUSTON, TX 77015
SAYBOLT LP TERMINALES MARIIMAS PATAGONICAS SA 12
LA PLACE, LA 70068 5TO PISO
COMODORO RIVADAVIA, ARGENTINA 9000
SAYBOLT LP
DEER PARK, TX 77536 TERMINALES MARITIMAS PATAGONICAS SA
5TO PISO
SAYBOLT LP COMODORO RIVADAVIA, ARGENTINA 9000
BLDG.10
LINDEN, NJ 07036 TESORO CORPORATION CARSON REFINERY
WAREHOUSE-GATE 7
SAYBOLT LP CARSON, CA 90745
STE 100
CONCORD, CA 94520 U S OIL & REFINING CO
TACOMA, WA 98421
SAYBOLT LP
SUITE 201 USG ENERGY
CARSON, CA 90810 STRATEGIC PET RES LAB
FREEPORT, TX 77541
SAYBOLT NEDERLAND BV
VLAARDINGEN 3133 KT, NETHERLANDS VALERO 3 RIVERS REFINERY
THREE RIVERS, TX 78071
SAYBOLT PETROLEUM SERVICES
DEER PARK, TX 77536 VALERO ENERGY CORP-HOUSTON
ATTN: LABORATORY
SGS CONTROL SERVICES HOUSTON, TX 77012
DEER PARK, TX 77536
VALERO MEMPHIS REFINERY
SGS NORTH AMERICA INC MEMPHIS, TN 38109
RESERVE, LA 70084
VALERO REFINING CO
SGS NORTH AMERICA WAREHOUSE RECEIVING
STE 7 TEXAS CITY, TX 77590
BRIDGEPORT, NJ 08014
VALERO ST. CHARLES REFINERY
SHELL CANADA NORCO, LA 70079
2840 76TH AVE NW
EDMONTON, AB CANADA T6P 0A0 VALERO WILMINGTON FUELS REFINERY
WILMINGTON, CA 90744
SHIN NIHON KENIEI KYOKAI (SK JAPAN)
SHIN YOKOHAMA 2-CHOME WESTERN REFINING CO
YOKOHAMA, KANAGAWA JAPAN 222-0033 EL PASO, TX 79905
SINCLAIR WYOMING REFINING WYNNEWOOD REFINING

SINCLAIR, WY 82334 WYNNEWOOD, OK 73098
SOUTHERN PETROLEUM LABORATORIES YPF SA

HOUSTON, TX 77054 LAB CONTROL DE CALIDAD
ENSENADA BUENOS AIRES, ARGENTINA 1925
SOUTHERN PETROLEUM LABORATORIES
8820 INTERCHANGE DRIVE YANBU ARAMCO SINOPEC REFINERY (YASREF)
HOUSTON, TX 77054 JEDDAH ROAD
YANBU, MADINA SAUDI ARABIA
SOUTHERN PETROLEUM LABS
CARENCRO, LA 70520 ZAKUM DEVELOPMENT COMPANY
ABU DHABI, UNITED ARAB EMIRATES 002
ST. PAUL PARK REFINING COMPANY
MINNESOTA REFINING DIVISION
SAINT PAUL PARK, MN 55071
SUNOCO LOGISTICS
NEDERLAND, TX 77627
13
ASTM PROFICIENCY TESTING PROGRAM

INDEX LISTING OF ASTM STANDARDS
UTILIZED IN THE JULY2016

CRUDE OIL (CO1607)
Participants are to use the most current available edition of all program tests they conduct.
To order any test used in this program, please contact:
ASTM Customer Service Department

Phone: (610) 832-9585; Fax: (610) 832-9555
service@astm.org
D97-16 Test Method for Pour Point of Petroleum Products

D287-12b Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer Method)
D323-15a Test Method for Vapor Pressure of Petroleum Products (Reid Method)
D445-15a Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic
Viscosity)
D473-07(2012) Test Method for Sediment in Crude Oils and Fuel Oils by the Extraction Method
D664-11a Test Method for Acid Number of Petroleum Products by Potentiometric Titration
D1298-12b Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum
Products by Hydrometer Method
D2622-16 Test Method for Sulfur in Petroleum Products by Wavelength-Dispersive X-Ray Fluorescence
Spectrometry
D3230-13 Test Method for Salts in Crude Oil (Electrometric Method)
D4006-16 Test Method for Water in Crude Oil by Distillation
D4007-11(2016) Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
D4294-16el Test Method for Sulfur in Petroleum Products by Energy-Dispersive X-Ray Fluorescence Spectroscopy
D4377-00(2011) Test Method for Water in Crude Oils by Potentiometric Karl Fischer Titration
D4530-15 Test Method for Determination of Carbon Residue (Micro Method)
D4629-12 Test Method for Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet Oxidative Combustion
and Chemiluminescence Detection
D4807-05(2015) Test Method for Sediment in Crude Oil by Membrane Filtration
D4928-12 Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
D4929-15a Test Methods for Determination of Organic Chloride Content in Crude Oil
D5002-16 Test Method for Density and Relative Density of Crude Oils by Digital Density Analyzer
D5191-15 Test Method for Vapor Pressure of Petroleum Products (Mini Method)
NOTEASTM D5191 and its reproducibility values are not applicable to Crude Oil. The test is included in the ILCP
program scope because of the number of industry laboratories that use it to determine this parameter.
D5708-15 Test Methods for Determination of Nickel, Vanadium, and Iron in Crude Oils and Residual Fuels by
Inductively Coupled Plasma (ICP) Atomic Emission Spectrometry
D5762-12 Test Method for Nitrogen in Petroleum and Petroleum Products by Boat/Inlet Chemiluminescence
D5853-11 Test Method for Pour Point of Crude Oils
D5863-00a(2011) Test Method for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels
by Flame Atomic Absorption Spectrometry
D6377-16 Test Method for Determination of Vapor Pressure of Crude Oil: VPCRx (Expansion Method)
D6470-99(2015) Test Method for Salt in Crude Oils (Potentiometric Method)
D6560-12 Test Method for the Determination of Asphaltenes (Heptane Insolubles) in Crude Petroleum and Petroleum
Products
D7042-16e1 Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the
Calculation of Kinematic Viscosity)
D7169-11 Test Method for Boiling Point Distribution of Samples with Residues Such as Crude Oils and Atmospheric
and Vacuum Residues by High Temperature Gas Chromatography
14
Crude Oil
July 2016
Summary of Statistics
Results Results Results Robust Robust Anderson

Method Description Total * Rejected** Valid *** Mean Std Dev ASTM R These Test R TPI Darling
D1298 Density-API Gravity 79 4 75 40.39 0.15 0.50 0.42 1.19 2.22
D1298 Density 93 6 87 0.82277 0.00056 0.00150 0.00155 0.97 1.38
D2622 Sulfur 38 0 38 0.188 0.007 0.018 0.019 0.95 0.18
D287 API Gravity 95 4 91 40.40 0.12 0.50 0.33 1.52 3.92
D323 Reid Vapor Pressure 59 1 58 1.303 0.358 N/A 0.992 0.34
D3230 Salts 102 0 102 4.985 2.008 6.903 5.562 1.24 0.34
D4006 Water Content 108 9 99 0.0082 0.0136 0.0351 0.0377 0.93 17.31
D4007 Water and Sediment by Centrifuge 144 19 125 0.034 0.024 0.28 0.066 8.49
D4294 Sulfur 177 23 154 0.189 0.007 0.025 0.019 1.32 0.36
D4377 Water Content by Karl Fischer Titration 58 5 53 0.027 0.008 0.034 0.022 1.55 3.27
D445 Viscosity, Kinematic @ 25C 65 3 62 4.20 0.29 N/A 0.80 0.52
D445 Viscosity, Kinematic @ 40C 134 13 121 2.830 0.044 N/A 0.122 2.60
D4530 Carbon Residue 132 6 126 0.35 0.06 0.16 0.17 0.94 1.43
D4629 Nitrogen 46 7 39 79.6 10.6 7.7 29.4 0.26 0.67
D473 Sediment 120 13 107 0.007 0.007 0.035 0.019 1.84 9.60
D4807 Sediment 80 7 73 0.0123 0.0074 0.0130 0.0205 0.63 2.01
D4928 Water Content 98 9 89 0.024 0.006 0.009 0.017 0.53 10.56
D4929-Method A Determination of Organic Chloride Content 10 3 7 0.18 0.15 0.45 0.42 1.07 0.36
D4929-Method B Determination of Organic Chloride Content 13 2 11 0.05 0.07 N/A 0.19 1.39
D5002 Density 149 15 134 0.82300 0.00024 0.00339 0.00066 5.14 1.82
D5191 Vapor Pressure-TVP 42 2 40 1.447 0.293 0.250 0.812 0.31 0.56
D5708 (MethodA) Metals-Iron 48 5 43 4.462 1.156 1.148 3.202 0.36 0.39
D5708 (MethodA) Metals-Nickel 46 16 30 0.08 0.10 N/A 0.28 2.25
D5708 (MethodA) Metals-Vanadium 46 15 31 0.03 0.05 N/A 0.14 4.15
D5708 (MethodB) Metals-Iron 40 1 39 12.372 3.186 N/A 8.825 0.38
D5708 (MethodB) Metals-Nickel 42 15 27 0.031 0.034 N/A 0.094 2.98
D5708 (MethodB) Metals-Vanadium 42 13 29 0.017 0.025 N/A 0.069 N/A
D5762 Nitrogen 56 8 48 74.9 13.8 19.9 38.2 0.52 0.53
D5853 MethodA Pour Point 28 0 28 9.6 4.1 18.0 11.4 1.58 0.89
D5863 (MethodA) Metals-Iron 15 0 15 11.29 3.85 N/A 10.66 0.68
D5863 (MethodA) Metals-Nickel 17 4 13 0.09 0.13 N/A 0.36 2.79
D5863 (MethodA) Metals-Vanadium 15 3 12 0.209 0.324 N/A 0.897 1.47
D5863 (MethodB) Metals-Nickel 20 4 16 0.21 0.24 N/A 0.66 3.75
D5863 (MethodB) Metals-Vanadium 20 4 16 0.06 0.11 N/A 0.30 2.63
D6377 Vapor Pressure 69 7 62 11.73 1.52 5.26 4.21 1.25 0.40
D6470 Salts 6 1 5 N/A N/A N/A N/A N/A
D6560 Asphaltenes 68 14 54 0.04 0.04 0.01 0.11 0.09 2.36
15
Crude Oil
July 2016
Summary of Statistics
Results Results Results Robust Robust Anderson

Method Description Total * Rejected** Valid *** Mean Std Dev ASTM R These Test R TPI Darling
D664 Total Acid Number 136 26 110 0.035 0.020 N/A 0.055 2.44
D7042 Kinematic Viscosity @ 40C 27 1 26 2.8210 0.0462 N/A 0.1280 0.34
D7042 Kinematic Viscosity @ 100C 6 0 6 1.1718 0.0386 N/A 0.1069 0.21
D7169 High Temperature Simulated Distillation-IBP 60 3 57 46.41 17.58 N/A 48.70 1.11
D7169 High Temperature Simulated Distillation-5% 61 8 53 97.40 4.43 N/A 12.27 6.58
D7169 High Temperature Simulated Distillation-10% 61 5 56 118.93 7.16 19.50 19.83 0.98 0.50
D7169 High Temperature Simulated Distillation-FBP 54 10 44 687.33 33.25 N/A 92.10 1.48
D7169 High Temperature Simulated Distillation-Total Weight % Recovery 50 3 47 98.26 2.63 N/A 7.29 3.39
@ 720C
D7169 HTSD Additional Total Weight Recovery Data-82.2C 41 2 39 2.85 0.74 1.74 2.05 0.85 1.05
D7169 HTSD Additional Total Weight Recovery Data-720C 35 0 35 97.96 2.51 3.17 6.95 0.46 2.55
D97 Upper Pour Point 105 0 105 10.0 3.5 N/A 9.7 4.18
* Results Total = total number of results submitted including > and/or < data reported.
** Results Rejected = total number of results that were statistically rejected or excluded from statistics for reporting > and/or < data.
*** Results Valid = Results Total - Results Rejected.
N/A = Not Applicable for this data set.
Statistical analysis of data not performed when <6 valid results.
ASTM Crude Oil
Sample ID: CO1607
July 2016 16
Acid Number - D664
(mg KOH/g)
Current Data Historic Z Scores
Test Robust Z Mean Std Precision Significant
1603 1511 1507 1503 1411 1407
Lab Results Deviation Score Notes Z Dev Z Indicator(PI) Difference
001 0.020 -0.015 -0.8 NDS -0.1 NDS NDS NDS NDS -0.45 0.49 N/A N/A
003 0.049 0.014 0.7 -1.0 -0.4 $ -0.8 -0.9 0.1 -0.38 0.67 1.51
005 0.082 0.047 2.4 3 1.1 R -0.9 1.4 1.5 1.4 1.15 1.10 0.92
006 ** 0.14 R 1.8 R R 1.2 0.2 -0.5 0.68 1.02 0.99
011 0.038 0.003 0.2 NDS -1.0 -0.2 -0.7 0.6 0.8 -0.05 0.71 1.42
013 0.027 -0.008 -0.4 0.7 0.7 1.3 0.5 0.7 -0.4 0.44 0.63 1.60
014 0.038 0.003 0.2 0.0 NDS NDS NDS NDS NDS 0.10 0.14 N/A N/A
017 0.09 0.055 2.8 3 2.9 1.7 -0.1 0.2 -1.3 $ 1.03 1.70 0.59 X
020 0.04 0.005 0.2 -0.3 0.6 -0.6 1.5 1.3 -0.5 0.31 0.85 1.19
021 0.0610 0.026 1.3 -0.4 1.1 1.3 0.1 -1.1 1.4 0.53 1.00 1.01
022 0.05 0.015 0.8 NDS NDS -0.1 0.2 NDS NDS 0.30 0.46 N/A N/A
023 0.027 -0.008 -0.4 -0.3 0.0 0.1 0.5 -0.1 0.0 -0.03 0.29 3.48
025 0.01 -0.025 -1.2 NDS -0.6 NDS NDS NDS -1.5 -1.10 0.46 N/A N/A
026 0.033 -0.002 -0.1 1.7 -0.1 -0.7 -0.7 NDS NDS 0.02 0.99 1.02
027 0.00120 -0.034 -1.7 -0.3 0.5 -0.1 NDS 1.1 0.1 -0.07 0.94 1.07
028 0.041 0.006 0.3 0.4 0.2 -0.2 1.0 NDS R 0.34 0.43 2.35
029 0.03 -0.005 -0.2 -1.3 1.0 0.5 -0.3 0.0 0.1 -0.03 0.72 1.40
030 0.0223 -0.013 -0.6 -0.1 -0.3 0.2 -0.5 1.8 0.1 0.09 0.81 1.25
031 0.0890 0.054 2.7 3 NDS NDS NDS NDS NDS NDS 2.70 0.00 N/A N/A
034 0.015 -0.020 -1.0 NDS -0.7 0.8 -0.8 -0.5 2.2 0.00 1.25 0.81
041 <0.001 -0.5 NDS NDS NDS NDS NDS -0.50 0.00 N/A N/A
042 0.08 0.045 2.2 3 -1.3 $ -0.4 NDS R NDS 0.17 1.82 N/A N/A
045 <0.1 $ $ $ -0.5 -0.8 $ -0.65 0.21 N/A N/A
046 0.020 -0.015 -0.8 -0.8 -0.1 -0.1 -0.1 NDS NDS -0.38 0.38 2.66
048 0.01 -0.025 -1.2 NDS NDS $ NDS NDS NDS -1.20 0.00 N/A N/A
050 0.024 -0.011 -0.6 NDS NDS NDS NDS NDS NDS -0.60 0.00 N/A N/A
051 0.03 -0.005 -0.2 NDS -0.1 NDS 1.2 NDS NDS 0.30 0.78 N/A N/A
052 0.0267 -0.008 -0.4 0.1 NDS NDS NDS NDS NDS -0.15 0.35 N/A N/A
054 ** 0.845 R NDS $ NDS NDS NDS NDS 0.00 0.00 N/A N/A
057 <0.05 1.3 -1.2 -1.4 2.3 R -0.5 0.10 1.63 0.62 X
058 0.004 -0.031 -1.6 0.1 -0.6 -0.4 NDS -0.9 -0.7 -0.68 0.56 1.80
061 0.097 0.062 3.1 1, 3 NDS -0.5 -0.7 -0.9 -0.6 NDS 0.08 1.69 0.60 X
062 0.027 -0.008 -0.4 -0.6 0.8 R NDS 2.4 0.8 0.60 1.20 0.84
063 0.085 0.050 2.5 3 NDS -0.4 3.0 NDS NDS NDS 1.70 1.84 N/A N/A
064 0.0309 -0.004 -0.2 -0.7 NDS NDS NDS NDS 0.4 -0.17 0.55 N/A N/A
066 0.02 -0.015 -0.8 2.9 0.3 -0.7 -0.3 R 0.8 0.37 1.38 0.73 X
067 0.042 0.007 0.4 -1.2 -0.2 0.1 -1.6 -0.4 -0.9 -0.54 0.72 1.40
069 0.013 -0.022 -1.1 -1.2 0.4 R 0.2 -0.3 -0.8 -0.47 0.67 1.51
071 <0.05 $ -0.8 0.1 -0.6 -0.2 -0.5 -0.40 0.35 2.89
072 0.06 0.025 1.2 NDS 2.8 0.5 -1.1 1.3 0.6 0.88 1.27 0.80
074 0.042 0.007 0.4 0.1 2.0 0.1 NDS NDS NDS 0.65 0.91 1.11
077 0.040 0.005 0.2 0.3 -0.3 -0.2 0.2 0.2 0.1 0.07 0.23 4.39
079 0.05 0.015 0.8 1.3 0.3 $ 0.2 NDS NDS 0.65 0.51 1.98
ASTM Crude Oil
Sample ID: CO1607
July 2016 17
Acid Number - D664
(mg KOH/g)
1603 1511 1507 1503 1411 1407
082 0.0820 0.047 2.4 3 NDS 0.6 -0.1 NDS 1.5 1.0 1.08 0.94 1.07
083 0.026 -0.009 -0.4 -0.8 -1.7 1.1 -0.8 NDS -1.4 -0.67 0.98 1.03
084 <0.1 -0.4 2.3 R R 1.6 0.0 0.88 1.28 0.79 X
086 0.001 -0.034 -1.7 R 3.4 0.2 -0.5 NDS 0.7 0.42 1.89 0.53 X
087 0.03 -0.005 -0.2 -0.3 1.0 0.9 -0.1 0.2 -0.5 0.14 0.59 1.71
088 <0.10 $ 0.3 0.5 1.0 -1.8 $ 0.00 1.24 0.81
089 0.05 0.015 0.8 -0.3 -0.1 -0.8 -0.3 -0.9 -0.1 -0.24 0.56 1.80
090 0.00 -0.035 -1.8 0.1 -0.7 -0.7 0.2 -0.1 0.5 -0.36 0.78 1.29
091 0.04 0.005 0.2 -1.3 1.2 0.1 1.0 0.4 0.2 0.26 0.81 1.25
092 <0.10 $ -2.4 1.3 NDS R NDS -0.55 2.62 N/A N/A
093 0.019 -0.016 -0.8 -0.3 -0.7 -1.8 -0.4 NDS NDS -0.80 0.60 1.68
096 0.050 0.015 0.8 0.8 1.0 0.1 1.0 2.1 0.0 0.83 0.69 1.46
097 <0.010 -0.4 NDS NDS -0.1 -1.8 -0.3 -0.65 0.78 1.29
099 <0.01 0.1 -0.3 -0.7 -1.1 -1.8 -0.2 -0.67 0.69 1.46
101 ** 0.120 R 1.8 R 0.1 1.2 -0.7 0.1 0.50 0.99 1.02
103 0.02 -0.015 -0.8 -1.3 R -0.8 0.3 0.2 -1.0 -0.57 0.66 1.53
105 0.050 0.015 0.8 R -1.7 -1.1 2.1 1.6 -0.5 0.20 1.53 0.66 X
106 0.030 -0.005 -0.2 0.7 0.8 R NDS NDS NDS 0.43 0.55 N/A N/A
107 0.040 0.005 0.2 0.2 -0.4 0.9 0.8 -0.2 NDS 0.25 0.52 1.94
108 0.04 0.005 0.2 NDS NDS 0.6 1.1 -1.0 -0.6 0.06 0.86 1.17
112 0.054 0.019 1.0 0.4 0.0 -1.5 -0.3 NDS 0.6 0.03 0.88 1.15
117 0.020 -0.015 -0.8 -0.3 0.3 0.2 -1.1 -1.1 0.6 -0.31 0.70 1.44
118 0.0315 -0.003 -0.2 0.7 0.8 0.5 1.1 -0.2 NDS 0.45 0.54 1.87
123 0.0258 -0.009 -0.5 0.4 0.1 -0.7 -0.3 -0.2 -0.5 -0.24 0.38 2.66
124 0.040 0.005 0.2 2.7 0.3 0.3 0.2 0.2 -0.3 0.51 0.99 1.02
128 0.011 -0.024 -1.2 -0.5 NDS NDS NDS NDS NDS -0.85 0.49 N/A N/A
131 0.036 0.001 0.0 R -0.5 2.1 -1.6 R 0.9 0.18 1.40 0.72 X
132 0.027 -0.008 -0.4 1.7 -1.2 R 2.9 NDS 3.4 1.28 2.02 0.50 X
135 <0.03 -1.1 -0.9 0.0 -0.7 NDS NDS -0.68 0.48 2.10
137 ** 0.230 R -0.1 NDS NDS NDS -0.9 -0.7 -0.57 0.42 N/A N/A
138 0.019 -0.016 -0.8 1.8 0.1 -0.8 R 0.0 0.6 0.15 0.98 1.03
139 0.10 0.065 3.2 1, 3 3.4 -0.1 -0.1 0.5 0.7 0.6 1.17 1.49 0.68 X
141 0.029 -0.006 -0.3 -0.8 0.0 NDS -0.6 -0.4 -0.6 -0.45 0.28 3.61
145 0.041 0.006 0.3 -0.4 NDS -1.8 -0.6 0.1 -0.7 -0.52 0.74 1.36
147 0.031 -0.004 -0.2 -1.0 2.0 -0.8 -1.1 NDS NDS -0.22 1.29 0.78 X
148 0.030 -0.005 -0.2 2.4 0.8 1.7 0.1 -0.7 -0.5 0.51 1.17 0.86
150 0.02 -0.015 -0.8 0.8 -0.3 -0.7 -1.1 NDS -0.2 -0.38 0.67 1.51
152 0.00 -0.035 -1.8 -1.3 -2.4 -0.4 -1.1 -0.4 -1.5 -1.27 0.73 1.38
153 0.11 0.075 3.8 1, 3 NDS NDS NDS NDS NDS NDS 3.80 0.00 N/A N/A
158 ** 0.33 R NDS -0.6 NDS NDS NDS NDS -0.60 0.00 N/A N/A
159 0.034 -0.001 0.0 0.4 0.4 1.0 1.0 R 1.7 0.75 0.61 1.66
160 <0.05 NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 18
Acid Number - D664
(mg KOH/g)
1603 1511 1507 1503 1411 1407
161 <0.01 0.6 NDS -0.8 1.5 NDS NDS 0.43 1.16 N/A N/A
163 0.06 0.025 1.2 0.8 -0.1 -2.0 -0.3 0.4 -0.2 -0.03 1.03 0.98
164 <0.1 NDS -0.6 NDS 0.5 NDS -1.7 -0.60 1.10 N/A N/A
166 0.020 -0.015 -0.8 $ -0.6 -0.5 0.2 0.4 $ -0.26 0.53 1.91
167 0.034 -0.001 0.0 -1.1 -0.3 0.0 -1.3 NDS NDS -0.54 0.62 1.63
168 0.076 0.041 2.0 NDS 2.1 1.0 NDS R 0.8 1.48 0.67 1.51
169 0.02 -0.015 -0.8 0.3 R NDS NDS NDS NDS -0.25 0.78 N/A N/A
170 0.03 -0.005 -0.2 0.8 -0.6 -0.5 -2.4 -1.3 -0.7 -0.70 0.98 1.03
171 0.049 0.014 0.7 0.0 0.9 -1.0 0.7 R R 0.26 0.78 1.29
172 <0.1 $ NDS NDS 0.1 NDS -0.9 -0.40 0.71 N/A N/A
176 0.029 -0.006 -0.3 $ -0.2 -0.3 0.8 -0.3 -1.6 -0.32 0.76 1.33
179 0.0236 -0.011 -0.6 -0.9 3.3 1.0 0.7 -0.6 0.4 0.47 1.44 0.70 X
181 0.0510 0.016 0.8 -1.3 -1.0 NDS R 1.6 R 0.03 1.40 0.72 X
182 0.030 -0.005 -0.2 0.8 NDS 3.1 NDS 0.0 3.6 1.46 1.77 0.57 X
183 0.014 -0.021 -1.0 -0.4 -0.5 0.6 -0.8 0.5 0.3 -0.19 0.65 1.55
189 0.050 0.015 0.8 0.1 -0.8 -0.3 -1.1 NDS NDS -0.26 0.75 1.35
191 0.049 0.014 0.7 0.8 2.8 -1.3 -1.3 -0.7 -1.5 -0.07 1.58 0.64 X
192 0.021 -0.014 -0.7 -0.1 0.8 0.6 1.0 -0.2 $ 0.23 0.67 1.51
193 0.051 0.016 0.8 1.2 -0.8 -0.8 -0.1 -0.4 0.0 -0.01 0.77 1.31
196 0.027 -0.008 -0.4 NDS NDS NDS 0.1 -1.8 0.0 -0.52 0.88 1.15
201 ** 0.170 R -0.7 0.5 0.3 R 2.9 0.8 0.76 1.32 0.77 X
203 0.060 0.025 1.2 -0.8 -1.7 -0.2 -1.6 1.3 2.6 0.11 1.63 0.62 X
204 0.000 -0.035 -1.8 -1.3 0.4 NDS NDS 0.0 -1.3 -0.80 0.95 1.06
206 0.040 0.005 0.2 0.3 -0.3 NDS NDS NDS NDS 0.07 0.32 N/A N/A
209 0.022 -0.013 -0.6 3.1 -0.4 -1.1 -1.1 -1.3 3.2 0.26 2.00 0.50 X
210 <0.10 -1.3 -1.2 0.3 -0.6 0.9 3.6 0.28 1.84 0.55 X
211 0.0246 -0.010 -0.5 -0.7 -0.4 -0.3 -1.5 -0.6 0.1 -0.56 0.49 2.06
212 ** 0.136 R -0.6 0.7 NDS 0.6 NDS NDS 0.23 0.72 N/A N/A
213 0.03 -0.005 -0.2 -0.3 -0.3 0.1 -0.8 -0.7 -0.5 -0.39 0.31 3.26
214 <0.100 $ 0.3 2.0 -0.2 NDS NDS 0.70 1.15 N/A N/A
216 0.03 -0.005 -0.2 R R -0.9 -0.1 NDS NDS -0.40 0.44 N/A N/A
219 0.051 0.016 0.8 -0.2 NDS NDS NDS NDS NDS 0.30 0.71 N/A N/A
220 0.074 0.039 2.0 1.1 -1.6 1.8 0.6 R 2.4 1.05 1.45 0.70 X
224 <0.001 $ NDS NDS 0.4 R NDS 0.40 0.00 N/A N/A
226 0.0212 -0.014 -0.7 0.3 R 0.6 2.2 NDS NDS 0.60 1.20 0.84
229 0.06 0.025 1.2 R NDS -0.1 NDS NDS NDS 0.55 0.92 N/A N/A
230 0.040 0.005 0.2 2.4 0.8 1.1 -0.1 -0.2 0.1 0.61 0.92 1.10
231 0.02 -0.015 -0.8 -0.3 0.1 2.6 0.2 -0.2 2.4 0.57 1.36 0.74 X
234 0.00 -0.035 -1.8 NDS NDS 0.3 1.2 -0.8 0.1 -0.20 1.14 0.89
239 0.030 -0.005 -0.2 NDS -1.9 0.4 NDS -0.3 NDS -0.50 0.98 1.03
ASTM Crude Oil
Sample ID: CO1607
July 2016 19
Acid Number - D664
(mg KOH/g)
1603 1511 1507 1503 1411 1407
241 0.032 -0.003 -0.2 0.9 NDS NDS NDS NDS NDS 0.35 0.78 N/A N/A
Pooled Standard Deviation = 1.01

Legend:
No. Valid Results 110
1 = Test result outside 3 sigma range for these test data
Robust Mean 0.035 2 = Test result outside 3 sigma range ASTM reproducibility
3 = Z-Score outside range of -2 to 2
Robust Standard Deviation 0.020
R = Rejected
Reproducibility ASTM Standard See Comment NDS = No Data Submitted
$ = Data was submitted but no Z-score was calculated
Reproducibility These Test Data 0.055
X = Lab precision may need improvement
Anderson Darling 2.44 * = There is no available historical information for this program cycle
** = Z-Score calculation equal to or greater than +/-3. Lab data labeled
TPI
as "Rejected" and not included in statistical analysis. See report
introduction for "A Check List for Investigating the Root Cause of
Unsatisfactory Analytical Performance."
N/A = Not Applicable on < 4 Z-scores
NSP = No Statistics Performed on < 6 data points
Comments:
These data (Anderson Darling > 1.0) do not represent a NORMAL distribution/fit; hence, all statistics generated for these data should
NOT be interpreted in accordance with conventional normal distribution probabilities.
The ASTM Reproducibility in D664 is applicable in the range from 0.1 to 150 mg KOH/g, Robust Mean is outside this range, therefore
ASTM Reproducibility is not determined.
NOTE: Historic Z-scores not populated for some labs in this report that did participate in prior test cycles.NDS is displayed.
20
Page 1 of 2
Sample ID: CO1607
Acid Number - D664
(mg KOH/g)
0.08 0.115
0.06 0.095
3 Sigma Range Limit These Test Data
0.04 0.075
0.02 0.055
Deviation
0 0.035
-0.02 0.015
-0.04 -0.005

-0.06 -0.025
-0.08 -0.045
2 2 1 9 2 8 1 5 1 4 2 1 6 1 3 9 1 1 4 6 1 1 1 1 1 1 2 1 2 2 3 1 5 2 8 1 1 2 1 1 6 5 1 1 1 2 8 5 2 2 1 1 1 2 1
0 3 5 0 7 6 7 8 1 8 5 2 9 8 4 3 3 6 6 0 1 5 5 6 6 3 9 2 0 0 7 0 1 3 2 3 3 9 3 2 2 4 7 0 9 7 1 3 1 8 7 7 1 4
4 4 2 3 6 8 3 8 3 7 0 1 6 9 1 2 6 9 9 1 3 6 2 1 6 6 9 3 2 7 0 6 8
Lab Code (Presented Vertically)

21
Page 2 of 2
Sample ID: CO1607
Acid Number - D664
(mg KOH/g)
0.08 0.115
0.06 0.095
0.04 0.075
0.02 0.055
Deviation
0 0.035
-0.02 0.015
-0.04 -0.005
-0.06 -0.025
-0.08 -0.045
1 6 1 2 2 1 1 1 1 1 2 9 2 1 1 7 2 1 2 1 7 6 1 3 1 1 4 2 8 1 9 7 2 1 1 1 2 7 4 2 2 1 2 2 1 4 8 5 6 3 1 6 2 1 1
4 4 1 4 6 6 5 3 4 1 0 1 0 2 0 7 3 0 8 4 4 7 7 9 8 4 2 9 0 6 9 1 8 9 1 3 2 9 2 0 6 1 2 6 2 2 3 1 7 1 2 3 5
7 8 1 7 9 1 6 4 8 0 7 5 1 1 9 5 9 1 3 2 7 9 3 3 0 8 5 9 3

22
Sample ID: CO1607

Acid Number - D664
(mg KOH/g)
49
1% Median 99%
42
35
Number of Labs
28
21
14
0
-0.05 - -0.04 -0.03 - -0.02 -0.01 - 0 0.01 - 0.02 0.03 - 0.04 0.05 - 0.06 0.07 - 0.08 0.09 - 0.1 0.11 - 0.12 0.13 - 0.14 0.15 - 0.16
Distribution Range of Test Results
ASTM Crude Oil
Sample ID: CO1607
July 2016 23
API Gravity - D287
(API)
1603 1511 1507 1503 1411 1407
003 40.4 0.00 0.0 -0.2 -0.8 NDS NDS NDS NDS -0.33 0.42 N/A N/A
005 40.6 0.20 1.7 R -0.2 0.7 0.6 0.4 -0.5 0.45 0.77 1.34
007 ** 39.9 R 0.5 2.2 0.0 2.2 NDS NDS 1.23 1.14 0.90
008 40.3 -0.10 -0.8 -0.2 NDS 0.7 -0.2 0.4 NDS -0.02 0.58 1.78
012 40.6 0.20 1.7 1.2 0.4 -1.4 0.6 NDS NDS 0.50 1.18 0.87
013 40.5 0.10 0.8 1.9 -0.2 1.4 0.6 0.4 0.5 0.77 0.69 1.49
019 40.4 0.00 0.0 -0.9 -1.4 0.0 -0.2 NDS 1.4 -0.18 0.96 1.07
020 40.4 0.00 0.0 NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
024 40.2 -0.20 -1.7 -1.6 -0.2 0.0 -0.2 0.4 1.4 -0.27 1.09 0.94
025 40.4 0.00 0.0 NDS -0.2 NDS NDS -0.9 -0.5 -0.40 0.39 2.64
029 40.3 -0.10 -0.8 0.5 -0.2 -0.7 NDS -0.9 0.5 -0.27 0.64 1.61
033 40.2 -0.20 -1.7 NDS -0.8 0.7 NDS NDS NDS -0.60 1.21 N/A N/A
041 ** 40.9 R 0.5 NDS NDS NDS NDS NDS 0.50 0.00 N/A N/A
043 40.4 0.00 0.0 0.5 1.0 -1.4 NDS 0.4 0.5 0.17 0.83 1.24
048 40.3 -0.10 -0.8 NDS NDS -0.7 -0.2 0.4 -1.4 -0.54 0.68 1.51
049 40.3 -0.10 -0.8 0.5 1.0 0.0 1.4 NDS 2.3 0.73 1.09 0.94
054 40.6 0.20 1.7 -3.1 0.4 0.0 -0.2 1.6 -0.5 -0.01 1.61 0.64 X
058 40.4 0.00 0.0 -0.9 1.0 2.1 NDS 0.4 NDS 0.52 1.12 0.92
060 40.4 0.00 0.0 -0.2 -1.4 0.0 2.2 0.4 -2.3 -0.19 1.42 0.73 X
062 40.3 -0.10 -0.8 0.5 -1.4 0.0 NDS -0.9 1.4 -0.20 1.04 0.99
063 40.6 0.20 1.7 NDS R -0.7 NDS NDS NDS 0.50 1.70 N/A N/A
067 40.2 -0.20 -1.7 0.5 -0.8 0.0 1.4 0.4 0.5 0.04 1.01 1.02
069 40.4 0.00 0.0 0.5 0.4 0.0 -0.2 NDS 0.5 0.20 0.30 3.43
074 40.3 -0.10 -0.8 -0.9 0.4 0.0 -0.2 1.6 -0.5 -0.06 0.86 1.20
075 40.4 0.00 0.0 NDS 1.0 NDS -0.2 NDS NDS 0.27 0.64 N/A N/A
079 40.4 0.00 0.0 -0.2 -0.2 -0.7 -1.1 NDS NDS -0.44 0.45 2.29
083 40.4 0.00 0.0 0.5 1.6 1.4 0.6 NDS 0.5 0.77 0.61 1.69
084 40.4 0.00 0.0 NDS R NDS -1.1 -0.9 R -0.67 0.59 N/A N/A
085 40.4 0.00 0.0 -0.9 NDS 1.4 0.6 NDS NDS 0.27 0.97 1.06
088 40.4 0.00 0.0 1.2 1.0 1.4 -0.2 0.4 -0.5 0.47 0.74 1.39
091 40.5 0.10 0.8 0.5 NDS -0.7 -1.9 -2.1 -1.4 -0.80 1.23 0.84
092 40.4 0.00 0.0 NDS 0.4 0.7 -0.2 0.4 NDS 0.26 0.36 2.86
096 40.4 0.00 0.0 0.5 -0.2 0.7 -0.2 -0.9 0.5 0.06 0.56 1.84
101 40.4 0.00 0.0 1.2 -1.4 1.4 2.2 -0.9 -0.5 0.29 1.33 0.77 X
103 40.3 -0.10 -0.8 -0.2 0.4 -0.7 NDS 0.4 -0.5 -0.23 0.53 1.94
109 ** 39.6 R -1.6 NDS -2.1 -1.1 -2.1 -0.5 -1.48 0.69 1.49
110 40.4 0.00 0.0 -0.9 0.4 2.1 NDS NDS NDS 0.40 1.26 0.82
117 40.3 -0.10 -0.8 0.5 -1.4 0.0 -1.1 0.4 -0.5 -0.41 0.74 1.39
122 40.2 -0.20 -1.7 -0.9 -0.8 0.7 NDS NDS 2.3 -0.08 1.59 0.65 X
123 40.4 0.00 0.0 0.5 -0.2 0.0 -2.8 NDS 0.5 -0.33 1.24 0.83
ASTM Crude Oil
Sample ID: CO1607
July 2016 24
API Gravity - D287
(API)
1603 1511 1507 1503 1411 1407
125 40.5 0.10 0.8 -0.2 2.2 NDS R NDS NDS 0.93 1.21 N/A N/A
127 40.4 0.00 0.0 0.5 1.0 -0.7 -0.2 -0.9 -0.5 -0.11 0.68 1.51
129 40.5 0.10 0.8 -0.9 -0.8 0.7 -0.2 NDS NDS -0.08 0.80 1.29
132 40.4 0.00 0.0 0.5 0.4 0.7 -0.2 NDS -0.5 0.15 0.46 2.24
133 40.2 -0.20 -1.7 0.5 -0.2 NDS -0.2 R -0.5 -0.42 0.80 1.29
135 40.4 0.00 0.0 0.5 R 1.4 -0.2 NDS NDS 0.42 0.71 1.45
137 40.5 0.10 0.8 1.2 NDS NDS NDS 0.4 1.4 0.95 0.44 2.34
139 40.5 0.10 0.8 -0.2 2.2 -0.7 -0.2 -3.4 -3.2 -0.67 2.03 0.51 X
147 40.6 0.20 1.7 -0.9 0.4 0.0 -0.2 NDS NDS 0.20 0.96 1.07
152 40.4 0.00 0.0 0.5 2.2 -0.7 -0.2 0.4 -0.5 0.24 0.97 1.06
155 40.3 -0.10 -0.8 0.5 2.2 0.7 1.4 1.6 -0.5 0.73 1.10 0.94
156 40.6 0.20 1.7 1.2 -0.2 NDS 3.1 -2.1 2.3 1.00 1.88 0.55 X
157 40.3 -0.10 -0.8 0.5 1.0 0.0 -0.2 0.4 NDS 0.15 0.63 1.63
158 40.4 0.00 0.0 -1.6 0.4 R 3.1 R 1.4 0.66 1.74 0.59 X
159 40.4 0.00 0.0 1.9 0.4 -1.4 0.6 0.4 0.5 0.34 0.97 1.06
161 40.3 -0.10 -0.8 -0.2 -0.2 0.0 0.6 NDS NDS -0.12 0.50 2.06
163 40.5 0.10 0.8 1.2 1.6 0.0 1.4 2.9 1.4 1.33 0.88 1.17
166 40.4 0.00 0.0 1.2 -0.8 0.0 0.6 1.6 -0.5 0.30 0.88 1.17
167 40.6 0.20 1.7 -1.6 -0.8 0.7 -1.9 NDS NDS -0.38 1.54 0.67 X
168 ** 38.8 R NDS -2.5 -0.7 NDS -2.1 -3.2 -2.12 1.05 0.98
169 40.4 0.00 0.0 -1.6 -0.8 -1.4 NDS NDS NDS -0.95 0.72 1.43
170 40.4 0.00 0.0 0.5 0.4 0.7 -2.8 0.4 -0.5 -0.19 1.22 0.84
171 40.4 0.00 0.0 -0.2 -0.8 R NDS NDS NDS -0.33 0.42 N/A N/A
173 40.4 0.00 0.0 0.5 NDS 0.7 NDS NDS NDS 0.40 0.36 N/A N/A
180 40.3 -0.10 -0.8 NDS -0.8 -0.7 -1.1 0.4 0.5 -0.42 0.69 1.49
182 40.2 -0.20 -1.7 -0.9 NDS -0.7 NDS R -1.4 -1.17 0.46 2.24
183 40.1 -0.30 -2.5 3 NDS NDS -0.7 NDS NDS 1.4 -0.60 1.95 N/A N/A
184 40.4 0.00 0.0 -3.1 NDS 0.0 NDS NDS NDS -1.03 1.79 N/A N/A
185 40.3 -0.10 -0.8 NDS 1.0 NDS NDS NDS NDS 0.10 1.27 N/A N/A
187 40.6 0.20 1.7 NDS 0.4 NDS R NDS -0.5 0.53 1.11 N/A N/A
189 40.4 0.00 0.0 1.2 -1.4 -1.4 -0.2 NDS NDS -0.36 1.09 0.94
191 40.6 0.20 1.7 0.5 1.0 0.7 0.6 R -0.5 0.67 0.72 1.43
193 40.5 0.10 0.8 0.5 -0.2 -0.7 -0.2 -0.9 0.5 -0.03 0.65 1.58
207 40.4 0.00 0.0 NDS -1.9 -0.7 0.6 -0.9 -0.5 -0.57 0.85 1.21
208 40.3 -0.10 -0.8 -0.2 -1.4 0.7 -0.2 -0.9 -0.5 -0.47 0.67 1.54
210 40.4 0.00 0.0 0.5 1.0 -0.7 -0.2 NDS 0.5 0.18 0.60 1.72
212 40.7 0.30 2.5 3 -3.1 -0.8 2.9 0.6 NDS NDS 0.42 2.47 0.42 X
213 40.4 0.00 0.0 NDS NDS -0.7 0.6 0.4 0.5 0.16 0.53 1.94
216 40.4 0.00 0.0 1.2 -1.9 0.0 -1.1 NDS NDS -0.36 1.18 0.87
218 40.5 0.10 0.8 0.5 NDS NDS -0.2 -0.9 0.5 0.14 0.69 1.49
ASTM Crude Oil
Sample ID: CO1607
July 2016 25
API Gravity - D287
(API)
1603 1511 1507 1503 1411 1407
224 40.5 0.10 0.8 -0.2 0.4 0.0 -1.1 2.9 1.4 0.60 1.28 0.80
229 40.4 0.00 0.0 -0.2 1.0 2.1 NDS NDS NDS 0.73 1.06 0.97
231 40.4 0.00 0.0 R 2.2 0.7 2.2 0.4 R 1.10 1.03 1.00
236 40.2 -0.20 -1.7 -0.9 NDS -0.7 -1.1 NDS NDS -1.10 0.43 2.40

Legend:
R = Rejected
Reproducibility ASTM Standard 0.50 NDS = No Data Submitted
TPI 1.52
Comments:
26
Page 1 of 2
Sample ID: CO1607
API Gravity - D287
(API)
0.72 41.12
0.6 41
3 Sigma Range Limit ASTM Standard
Reproducibility
0.48 40.88
0.36 40.76
0.24 40.64
0.12 40.52
Deviation
0 40.4
-0.12 40.28
-0.24 40.16
-0.36 40.04
-0.48 3 Sigma Range Limit ASTM Standard

Reproducibility
39.92
-0.6 39.8
-0.72 39.68
1 1 1 1 3 1 2 1 6 2 1 1 1 1 2 1 1 1 8 7 6 4 4 2 8 1 3 1 2 2 4 5 6 6 7 7 8 8 8 8 9 9 1 1 1 1
8 2 8 2 3 4 4 3 7 3 5 6 8 8 0 5 2 0 1 4 2 9 8 9 1 9 0 5 3 8 0 9 5 9 3 4 5 8 2 6 0 1 1 2
3 2 2 8 3 6 7 1 0 5 8 5 4 3 7 1 0 6 3

27
Page 2 of 2
Sample ID: CO1607
API Gravity - D287
(API)
0.72 41.12
0.6 41
Reproducibility
0.48 40.88
0.36 40.76
0.24 40.64
0.12 40.52
Deviation
0 40.4
-0.12 40.28
-0.24 40.16
-0.36 40.04
-0.48 3 Sigma Range Limit ASTM Standard

Reproducibility
39.92
-0.6 39.8
-0.72 39.68
1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 2 2 2 2 2 2 2 1 1 1 9 2 1 2 1 1 1 1 1 1 1 1 1 1 6 5 5 1 5 2
2 3 3 5 5 5 6 6 7 7 7 8 8 0 0 1 1 1 2 2 3 0 9 2 2 1 2 6 1 5 3 3 3 9 8 8 6 5 4 3 4 2 9 1
7 2 5 2 8 9 6 9 0 1 3 4 9 6 7 0 3 6 5 9 1 5 3 9 5 4 3 8 3 7 9 1 7 6 7 6 7 2

28
Sample ID: CO1607

API Gravity - D287
(API)
49
42 Median
1% 99%
35
Number of Labs
28
21
14
0
40 - 40.05 40.1 - 40.15 40.2 - 40.25 40.3 - 40.35 40.4 - 40.45 40.5 - 40.55 40.6 - 40.65 40.7 - 40.75 40.8 - 40.85 40.9 - 40.95
ASTM Crude Oil
Sample ID: CO1607
July 2016 29
Density - D1298
(Corrected API Gravity)
1603 1511 1507 1503 1411 1407
007 ** 39.9 R 0.6 -1.8 0.1 NDS NDS NDS -0.37 1.27 N/A N/A
008 40.3 -0.09 -0.6 -0.1 0.1 1.0 0.0 0.5 NDS 0.15 0.55 1.76
012 40.6 0.21 1.4 1.3 NDS -1.7 0.8 NDS NDS 0.45 1.46 0.66 X
013 40.4 0.01 0.1 1.3 -0.6 1.0 0.0 -0.5 -0.2 0.16 0.73 1.33
016 40.3 -0.09 -0.6 NDS NDS NDS 0.8 0.5 R 0.23 0.74 N/A N/A
018 40.4 0.01 0.1 -0.9 NDS NDS NDS NDS NDS -0.40 0.71 N/A N/A
023 40.6 0.21 1.4 0.6 -0.6 NDS NDS 0.5 -0.2 0.34 0.77 1.26
024 40.2 -0.19 -1.3 -1.6 0.1 0.1 0.0 0.5 1.4 -0.11 1.03 0.94
025 40.4 0.01 0.1 NDS 0.1 NDS -1.5 -0.5 NDS -0.45 0.75 1.29
028 40.7 0.31 2.1 3 1.3 1.3 1.9 2.3 0.5 -1.1 1.19 1.18 0.82
029 40.3 -0.09 -0.6 0.6 0.1 -0.8 NDS -0.5 0.6 -0.10 0.62 1.56
033 40.2 -0.19 -1.3 NDS -0.6 1.0 NDS NDS NDS -0.30 1.18 N/A N/A
038 40.4 0.01 0.1 -0.1 R 0.1 -2.3 -1.4 1.4 -0.37 1.30 0.75 X
042 ** 41.2 R R 1.3 0.1 NDS -2.3 NDS -0.30 1.83 N/A N/A
047 40.4 0.01 0.1 -0.1 0.7 R -0.8 -1.4 0.6 -0.15 0.82 1.18
048 40.3 -0.09 -0.6 NDS NDS -0.8 0.0 NDS NDS -0.47 0.42 N/A N/A
067 40.2 -0.19 -1.3 NDS NDS NDS NDS 0.5 0.6 -0.07 1.07 N/A N/A
070 40.5 0.11 0.7 1.3 0.1 0.1 0.8 -0.5 -0.2 0.33 0.63 1.54
072 40.3 -0.09 -0.6 NDS 1.3 0.1 0.0 -0.5 -0.2 0.02 0.69 1.41
073 40.4 0.01 0.1 1.3 0.1 1.0 -2.3 -1.4 -0.2 -0.20 1.27 0.76 X
078 40.4 0.01 0.1 -0.1 R -0.8 0.8 0.5 0.6 0.18 0.58 1.67
079 40.4 0.01 0.1 -0.1 0.1 -0.8 R NDS NDS -0.18 0.43 2.26
085 40.3 -0.09 -0.6 -1.6 NDS 1.0 0.0 NDS NDS -0.30 1.09 0.89
086 40.7 0.31 2.1 3 0.6 0.7 -1.7 NDS -0.5 0.6 0.30 1.28 0.76 X
103 40.3 -0.09 -0.6 -0.1 0.7 -0.8 NDS 0.5 -0.2 -0.08 0.59 1.64
107 40.8 0.41 2.7 3 0.6 NDS NDS NDS NDS NDS 1.65 1.48 N/A N/A
108 40.2 -0.19 -1.3 0.6 NDS 1.9 1.5 0.5 1.4 0.77 1.15 0.84
119 40.3 -0.09 -0.6 NDS NDS -1.7 NDS NDS NDS -1.15 0.78 N/A N/A
127 40.4 0.01 0.1 0.6 1.3 -0.8 0.0 -0.5 -0.2 0.07 0.70 1.39
129 40.4 0.01 0.1 -0.9 -0.6 1.0 0.0 NDS NDS -0.08 0.73 1.33
133 40.2 -0.19 -1.3 2.7 0.7 NDS 0.0 R -0.2 0.38 1.48 0.66 X
138 40.3 -0.09 -0.6 0.6 -0.6 -0.8 0.0 NDS NDS -0.28 0.58 1.67
146 40.4 0.01 0.1 -0.9 NDS -1.7 0.8 NDS NDS -0.42 1.10 0.88
147 40.6 0.21 1.4 -0.9 0.7 0.1 0.0 NDS NDS 0.26 0.86 1.13
152 40.4 0.01 0.1 0.6 2.6 -0.8 0.0 0.5 -0.2 0.40 1.08 0.90
156 40.5 0.11 0.7 0.6 -0.6 NDS 2.3 -1.4 1.4 0.50 1.34 0.72 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 30
Density - D1298
1603 1511 1507 1503 1411 1407
160 40.7 0.31 2.1 3 NDS 0.1 1.9 NDS NDS 2.2 1.58 0.99 0.98
161 40.3 -0.09 -0.6 1.3 NDS 0.1 0.8 NDS NDS 0.40 0.83 1.17
163 40.5 0.11 0.7 1.3 1.9 0.1 1.5 2.3 1.4 1.31 0.73 1.33
167 40.6 0.21 1.4 -1.6 -0.6 1.0 -1.5 NDS NDS -0.26 1.40 0.69 X
169 40.4 0.01 0.1 -1.6 -0.6 -1.7 NDS NDS NDS -0.95 0.86 1.13
170 40.4 0.01 0.1 0.6 0.7 1.0 -2.3 0.5 -0.2 0.06 1.11 0.87
183 40.1 -0.29 -1.9 -0.9 NDS -0.8 -0.8 NDS 1.4 -0.60 1.21 0.80
185 40.3 -0.09 -0.6 -0.1 1.3 NDS -1.5 0.5 -0.2 -0.10 0.95 1.02
189 40.4 0.01 0.1 1.3 -1.2 -1.7 0.0 NDS NDS -0.30 1.18 0.82
191 40.6 0.21 1.4 0.6 1.3 R 0.8 R -0.2 0.78 0.64 1.52
193 40.5 0.11 0.7 0.6 0.7 0.1 0.0 -0.5 -0.2 0.20 0.48 2.02
196 40.6 0.21 1.4 NDS NDS -1.7 0.8 1.4 0.6 0.50 1.28 0.76 X
207 40.3 -0.09 -0.6 NDS -1.8 -0.8 0.8 -0.5 -0.2 -0.52 0.84 1.15
211 40.4 0.01 0.1 -0.1 0.1 -0.8 0.0 -0.5 -0.2 -0.20 0.34 2.85
212 40.7 0.31 2.1 3 -3.0 NDS NDS 0.8 NDS NDS -0.03 2.65 N/A N/A
221 ** 41.0 R NDS NDS NDS 0.0 NDS 2.2 1.10 1.56 N/A N/A
223 40.3 -0.09 -0.6 -0.1 NDS NDS NDS 1.4 -1.1 -0.10 1.08 0.90
224 40.5 0.11 0.7 NDS 0.7 0.1 NDS NDS NDS 0.50 0.35 N/A N/A
238 ** 39.9 R NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 31
Density - D1298
Legend:
R = Rejected
TPI 1.19
Comments:
32
Sample ID: CO1607

Density - D1298
0.6 40.99

Reproducibility
0.45 40.84
0.3 40.69
0.15 40.54
Deviation
0 40.39
-0.15 40.24
-0.3 40.09
-0.45 39.94
Reproducibility
-0.6 39.79
1 3 6 1 2 1 1 1 2 1 8 1 2 4 7 7 8 1 1 1 1 1 1 1 1 1 1 1 2 2 1 2 2 2 1 1 1 1 1 1 1 1 1 1 7 7 7 4 4 3 2 1 2 7 1 1 1 1 5 2 2 2 1 1 2 1 1 1 1 2 1 2 5 8 1
8 3 7 0 3 3 8 9 4 2 6 9 8 2 5 5 0 0 1 3 4 6 6 8 9 9 9 0 2 3 2 2 1 8 7 7 7 6 5 4 2 2 1 9 8 3 7 0 8 5 8 3 0 9 5 5 6 2 3 1 2 6 8 3 9 9 2 4 1 6 8 9 6 0
3 8 6 3 4 5 1 3 5 9 8 2 1 2 5 0 7 9 7 3 7 5 1 9 7 3 0 9 2 6 9 7 3 9 3 3 6 3 7 7 4 7 8 1 6 7 2 0 7

33
Sample ID: CO1607

Density - D1298
28
24
Median
1% 99%
20
Number of Labs
16
12
0
40.1 - 40.15 40.2 - 40.25 40.3 - 40.35 40.4 - 40.45 40.5 - 40.55 40.6 - 40.65 40.7 - 40.75 40.8 - 40.85 40.9 - 40.95
ASTM Crude Oil
Sample ID: CO1607
July 2016 34
Asphaltenes - D6560
(% mass/mass)
1603 1511 1507 1503 1411 1407
003 0.10 0.06 1.5 2 0.7 0.4 1.4 0.3 $ $ 0.86 0.56 2.05
006 0.05 0.01 0.2 -0.2 NDS NDS 3.3 0.6 0.5 0.88 1.39 0.83
008 0.02 -0.02 -0.5 2 -0.7 0.3 0.9 1.2 -0.6 NDS 0.10 0.82 1.40
011 0.12 0.08 2.0 2 NDS 0.7 2.0 0.3 -0.4 1.2 0.97 0.96 1.20
014 <0.05 $ NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
015 0.01 -0.03 -0.8 2 -0.3 0.0 -0.5 0.3 NDS NDS -0.26 0.43 2.67
017 0.01 -0.03 -0.8 2 NDS 0.3 -0.4 0.0 $ 1.3 0.08 0.80 1.44
025 0.10 0.06 1.5 2 NDS -1.7 NDS -0.5 NDS NDS -0.23 1.62 N/A N/A
026 0.05 0.01 0.2 0.5 0.3 0.9 1.4 NDS NDS 0.66 0.49 2.35
027 0.00 -0.04 -1.0 2 NDS NDS -1.0 NDS -1.0 NDS -1.00 0.00 N/A N/A
029 0.07 0.03 0.8 2 -0.8 0.4 -0.6 -1.3 0.5 4.0 0.43 1.75 0.66 X
030 0.05 0.01 0.2 -0.2 0.4 0.0 1.4 -1.0 -1.2 -0.06 0.88 1.31
043 <0.50 -0.2 0.4 NDS NDS NDS NDS 0.10 0.42 N/A N/A
054 0.02 -0.02 -0.5 2 NDS R 0.9 -3.4 2.5 R -0.12 2.50 0.46 X
057 0.15 0.11 2.8 2, 3 1.5 -0.5 2.9 2.2 1.5 0.5 1.56 1.23 0.93
060 0.00 -0.04 -1.0 2 -1.0 -1.2 -2.5 -0.1 NDS NDS -1.16 0.86 1.34
066 0.03 -0.01 -0.2 0.3 -0.1 -1.5 -3.2 -0.7 0.5 -0.70 1.29 0.89
077 0.02 -0.02 -0.5 2 -0.7 1.1 0.7 R -1.0 -1.2 -0.27 0.94 1.22
079 0.05 0.01 0.2 -1.0 0.3 -0.6 0.3 NDS NDS -0.16 0.60 1.92
088 0.05 0.01 0.2 -0.2 0.7 -0.2 0.2 1.1 $ 0.30 0.51 2.25
089 0.0 -0.04 -1.0 2 -0.2 0.6 -0.5 -1.3 -1.0 -0.3 -0.53 0.64 1.80
091 <1.0 -0.2 0.6 0.0 -0.1 $ 1.3 0.32 0.63 1.83
092 ** 0.25 R R NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
096 0.00 -0.04 -1.0 2 -0.2 0.2 0.2 -3.8 -0.5 -0.3 -0.77 1.40 0.82
101 0.00 -0.04 -1.0 2 -0.2 0.0 0.5 NDS NDS NDS -0.18 0.62 1.85
102 ** 1.34 R R -0.1 -1.0 -0.1 -0.5 0.2 -0.30 0.46 2.50
103 0.06 0.02 0.5 2 1.7 -1.2 -0.4 NDS 1.5 -0.3 0.30 1.14 1.01
105 0.05 0.01 0.2 -0.2 0.1 0.4 -0.1 -0.5 -0.5 -0.09 0.34 3.38
106 0.01 -0.03 -0.8 2 -0.8 0.7 0.9 NDS NDS NDS 0.00 0.93 1.24
108 0.12 0.08 2.0 2 NDS NDS -2.1 -0.5 R R -0.20 2.07 N/A N/A
112 0.06 0.02 0.5 2 -0.2 0.3 -0.9 0.0 NDS $ -0.06 0.54 2.13
117 0.10 0.06 1.5 2 1.5 0.4 -0.7 2.6 NDS 0.8 1.02 1.13 1.02
123 0.05 0.01 0.2 2.3 0.9 NDS 1.4 NDS NDS 1.20 0.88 1.31
126 0.05 0.01 0.2 -0.8 -2.8 -0.3 -0.5 -0.5 -0.8 -0.79 0.95 1.21
135 0.00 -0.04 -1.0 2 R -3.2 2.1 0.3 NDS NDS -0.45 2.23 0.52 X
138 0.00 -0.04 -1.0 2 -1.0 0.7 3.1 3.3 -1.0 -1.2 0.41 2.01 0.57 X
141 0.01 -0.03 -0.8 2 -0.2 0.1 0.1 -0.1 -0.7 -0.8 -0.34 0.41 2.80
144 0.1 0.06 1.5 2 NDS -2.6 NDS NDS NDS NDS -0.55 2.90 N/A N/A
147 0.00 -0.04 -1.0 2 -0.2 0.6 -0.1 -0.1 NDS NDS -0.16 0.57 2.02
ASTM Crude Oil
Sample ID: CO1607
July 2016 35
Asphaltenes - D6560
(% mass/mass)
1603 1511 1507 1503 1411 1407
161 <0.05 -0.2 NDS 0.3 -0.5 NDS NDS -0.13 0.40 N/A N/A
166 0.05 0.01 0.2 NDS 0.4 0.2 0.3 -0.5 -0.3 0.05 0.36 3.19
168 0.20 0.16 4.0 1, 2, 3 NDS -2.6 R NDS 3.0 1.3 1.42 2.91 0.40 X
170 0.00 -0.04 -1.0 2 1.5 -0.2 -0.9 0.3 2.0 0.5 0.31 1.14 1.01
173 0.06 0.02 0.5 2 -0.5 NDS -0.7 NDS NDS NDS -0.23 0.64 N/A N/A
181 0.01 -0.03 -0.8 2 0.5 NDS -0.2 0.3 R R -0.05 0.58 1.98
184 ** 0.25 R -0.7 R 0.2 -0.1 NDS NDS -0.20 0.46 N/A N/A
191 0.05 0.01 0.2 -0.2 -0.6 -0.5 -1.3 2.0 -1.0 -0.20 1.09 1.06
193 0.00 -0.04 -1.0 2 -1.0 0.4 0.0 -0.9 -0.5 -0.3 -0.47 0.54 2.13
210 0.11 0.07 1.8 2 3.2 -0.6 0.1 R 1.0 -0.8 0.78 1.54 0.75 X
211 0.00 -0.04 -1.0 2 -1.0 0.3 -1.0 -0.1 -1.0 -1.2 -0.71 0.57 2.02
212 0.01 -0.03 -0.8 2 -0.2 -3.1 R R NDS NDS -1.37 1.53 N/A N/A
213 0.0 -0.04 -1.0 2 1.5 0.7 0.5 1.0 0.5 0.5 0.53 0.77 1.49
214 <0.50 $ 0.4 -0.9 -0.1 NDS NDS -0.20 0.66 N/A N/A
216 0.07 0.03 0.8 2 -0.5 NDS 1.8 R NDS NDS 0.70 1.15 N/A N/A
219 0.2 0.16 4.0 1, 2, 3 0.2 NDS NDS NDS NDS NDS 2.10 2.69 N/A N/A
220 0.10 0.06 1.5 2 R -1.6 -0.1 -0.1 NDS $ -0.08 1.27 0.91
226 0.02 -0.02 -0.5 2 -0.2 0.1 -0.1 -0.5 NDS NDS -0.24 0.26 4.42
228 0.05 0.01 0.2 $ $ -0.3 -1.7 NDS $ -0.60 0.98 N/A N/A
231 ** 0.30 R 3.2 -0.2 -0.6 -0.1 -0.5 NDS 0.36 1.60 0.72 X
234 0.00 -0.04 -1.0 2 NDS NDS 0.6 0.3 $ $ -0.03 0.85 N/A N/A
239 0.03 -0.01 -0.2 NDS 1.3 0.5 NDS -1.0 NDS 0.15 0.98 1.17

Legend:
R = Rejected
TPI 0.09
Comments:
36
Sample ID: CO1607

Asphaltenes - D6560
(% mass/mass)
0.16 0.2
0.12 0.16
0.08 0.12
0.04 0.08
Reproducibility
Deviation
0 0.04
Reproducibility
-0.04 0
-0.08 -0.04
-0.12 -0.08
-0.16 -0.12
2 6 1 1 2 2 1 1 1 2 9 8 1 2 1 1 1 1 1 2 8 5 7 2 6 1 1 1 1 9 8 7 3 2 1 6 2 1 1 1 1 2 2 2 1 3 2 1 2 1 1 5 2 1
3 0 3 3 7 1 9 0 4 1 6 9 7 1 8 4 0 7 5 2 4 7 3 6 1 2 2 0 4 8 9 0 6 6 2 9 7 1 0 9 1 2 1 5 4 1 0 1 7 1 6
4 8 5 1 3 1 7 3 0 2 1 1 6 6 9 6 6 3 5 6 8 1 3 2 3 6 0 7 4 0 8 9 8

37
Sample ID: CO1607

Asphaltenes - D6560
(% mass/mass)
28
24 1%
Median
99%
20
Number of Labs
16
12
0
-0.05 0 0.05 0.1 0.15 0.2 0.25 0.3
ASTM Crude Oil
Sample ID: CO1607
July 2016 38
Carbon Residue (Micro Method) - D4530
(mass%)
1603 1511 1507 1503 1411 1407
003 0.43 0.08 1.3 1.1 0.5 0.4 0.0 1.3 1.2 0.83 0.52 1.87
004 0.30 -0.05 -0.8 -0.8 NDS 0.0 0.9 -1.7 -0.6 -0.50 0.88 1.10
005 0.19 -0.16 -2.7 3 -0.6 0.4 0.8 1.1 1.2 0.3 0.07 1.36 0.71 X
006 0.38 0.03 0.5 -0.7 0.2 0.8 R 1.0 -0.9 0.15 0.79 1.23
007 0.18 -0.17 -2.8 3 -1.7 -2.6 -0.5 -1.8 NDS NDS -1.88 0.91 1.07
012 0.4 0.05 0.8 NDS 0.7 NDS -1.9 NDS NDS -0.13 1.53 N/A N/A
017 0.32 -0.03 -0.5 -0.9 -0.5 -0.7 -0.5 -0.6 -0.6 -0.61 0.15 6.47
019 0.43 0.08 1.3 1.1 -1.9 -0.4 -2.6 NDS -0.2 -0.45 1.57 0.62 X
020 0.39 0.04 0.7 0.9 0.1 0.0 -0.1 0.6 0.8 0.43 0.42 2.31
021 0.41 0.06 1.0 0.7 0.7 0.8 0.4 0.4 -1.3 0.39 0.77 1.26
022 0.36 0.01 0.2 NDS NDS 0.6 -1.9 NDS NDS -0.37 1.34 N/A N/A
023 0.42 0.07 1.2 0.8 0.5 0.4 1.2 1.2 0.8 0.87 0.34 2.85
025 0.40 0.05 0.8 NDS R NDS -2.2 0.6 0.7 -0.03 1.45 0.67 X
026 0.21 -0.14 -2.3 3 0.0 0.4 -0.9 -0.2 NDS NDS -0.60 1.06 0.92
027 0.29 -0.06 -1.0 R -0.5 -2.4 NDS -0.3 R -1.05 0.95 1.02
029 0.39 0.04 0.7 -0.4 -0.5 -0.5 -1.0 0.4 0.5 -0.11 0.64 1.52
030 0.35 0.00 0.0 0.7 -1.2 -0.9 0.1 -1.1 -1.4 -0.54 0.80 1.21
034 0.43 0.08 1.3 NDS -1.1 -0.9 -1.3 -1.2 0.7 -0.42 1.12 0.87
035 0.36 0.01 0.2 1.5 -0.1 NDS 0.4 NDS NDS 0.50 0.70 1.39
042 ** 0.59 R 0.2 -1.0 R NDS 1.3 NDS 0.17 1.15 N/A N/A
043 0.35 0.00 0.0 0.7 0.6 NDS NDS NDS NDS 0.43 0.38 N/A N/A
045 0.31 -0.04 -0.7 -0.2 0.9 0.8 -0.4 -0.2 -2.7 -0.36 1.20 0.81
046 0.39 0.04 0.7 0.1 -2.0 -1.3 -0.3 NDS NDS -0.56 1.09 0.89
048 0.26 -0.09 -1.5 NDS NDS -0.9 -0.1 0.0 0.2 -0.46 0.72 1.35
049 ** 0.08 R -2.4 -1.7 0.8 -1.6 NDS -2.3 -1.44 1.30 0.75 X
054 0.17 -0.18 -3.0 2, 3 -0.5 -2.5 NDS -0.2 0.1 0.1 -1.00 1.38 0.70 X
055 ** 0.00 R 0.8 0.8 0.4 0.9 1.2 -1.6 0.42 1.02 0.95
058 0.27 -0.08 -1.3 -0.4 1.2 0.4 NDS -1.2 1.0 -0.05 1.08 0.90
060 0.32 -0.03 -0.5 0.9 -1.0 -0.5 -1.2 1.0 1.3 0.00 1.04 0.93
062 0.51 0.16 2.7 3 1.6 0.2 -0.9 NDS 0.3 -1.3 0.43 1.51 0.64 X
063 0.5 0.15 2.5 3 NDS -0.7 NDS NDS NDS NDS 0.90 2.26 N/A N/A
064 0.41 0.06 1.0 -0.7 NDS NDS NDS NDS 0.2 0.17 0.85 N/A N/A
066 0.36 0.01 0.2 -0.5 NDS NDS -0.6 -0.9 -1.8 -0.72 0.73 1.33
067 0.41 0.06 1.0 0.9 -0.1 2.9 0.5 R -1.2 0.67 1.36 0.71 X
069 0.33 -0.02 -0.3 0.8 1.2 -1.7 -0.2 NDS NDS -0.04 1.13 0.86
074 0.44 0.09 1.5 R 1.8 2.0 1.4 R R 1.67 0.28 3.46
077 0.35 0.00 0.0 -3.2 -0.1 -0.9 -1.7 -0.3 -0.6 -0.97 1.14 0.85
079 0.30 -0.05 -0.8 1.1 1.9 NDS NDS NDS NDS 0.73 1.39 N/A N/A
084 0.41 0.06 1.0 -0.4 0.7 2.5 -0.3 -0.2 -1.1 0.31 1.19 0.82
086 0.35 0.00 0.0 NDS NDS NDS -1.3 NDS NDS -0.65 0.92 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 39
(mass%)
1603 1511 1507 1503 1411 1407
087 0.35 0.00 0.0 -0.5 0.3 0.8 1.0 1.6 1.6 0.69 0.80 1.21
088 0.30 -0.05 -0.8 -0.3 0.6 1.2 0.4 -0.3 0.1 0.13 0.67 1.45
089 0.37 0.02 0.3 -0.3 -0.6 0.4 0.4 -0.5 -0.2 -0.07 0.43 2.26
090 0.42 0.07 1.2 0.5 0.7 0.4 0.2 -0.2 0.2 0.43 0.44 2.20
091 0.31 -0.04 -0.7 0.0 -0.6 0.8 -0.7 -0.2 0.6 -0.11 0.62 1.56
092 0.37 0.02 0.3 0.6 NDS -0.5 1.0 -0.3 NDS 0.22 0.62 1.56
093 0.39 0.04 0.7 1.5 0.2 -0.1 0.5 NDS NDS 0.56 0.61 1.59
096 0.33 -0.02 -0.3 0.5 0.7 0.0 0.4 0.9 1.0 0.46 0.47 2.06
099 0.29 -0.06 -1.0 0.4 -0.8 0.4 0.9 0.9 0.3 0.16 0.76 1.28
101 0.23 -0.12 -2.0 0.0 0.3 -1.3 -0.7 -3.2 -0.9 -1.11 1.20 0.81
103 0.35 0.00 0.0 -1.2 0.5 1.2 0.1 -3.0 -0.6 -0.43 1.37 0.71 X
105 0.24 -0.11 -1.8 -1.4 -0.3 -0.9 -1.6 -2.4 0.2 -1.17 0.90 1.08
106 0.43 0.08 1.3 -0.6 0.2 -0.5 NDS NDS NDS 0.10 0.88 1.10
107 0.46 0.11 1.8 0.0 NDS -1.3 1.9 0.7 NDS 0.62 1.33 0.73 X
108 0.34 -0.01 -0.2 NDS NDS 0.8 0.9 0.0 -0.3 0.24 0.57 1.70
110 0.26 -0.09 -1.5 1.5 -1.6 0.0 NDS NDS NDS -0.40 1.46 0.66 X
112 0.31 -0.04 -0.7 -1.5 0.3 0.5 -0.1 NDS 0.1 -0.23 0.74 1.31
117 0.42 0.07 1.2 0.3 -0.6 -2.1 -0.7 0.3 0.1 -0.21 1.05 0.92
118 0.18 -0.17 -2.8 3 -2.2 -0.6 R 0.0 1.2 0.3 -0.68 1.53 0.63 X
119 0.34 -0.01 -0.2 NDS NDS 1.2 NDS NDS NDS 0.50 0.99 N/A N/A
123 0.36 0.01 0.2 0.3 -0.6 -2.1 -0.6 -1.2 0.3 -0.53 0.90 1.08
124 0.36 0.01 0.2 0.2 NDS 0.4 -0.6 0.0 0.2 0.07 0.35 2.77
126 0.45 0.10 1.7 0.0 1.0 R 0.7 -2.3 -0.8 0.05 1.43 0.68 X
127 0.3 -0.05 -0.8 0.3 NDS 0.6 0.4 0.3 2.0 0.47 0.90 1.08
132 0.38 0.03 0.5 0.3 R -1.7 0.3 NDS 0.1 -0.10 0.91 1.07
133 ** 0.1 R -1.5 1.2 NDS 1.3 1.5 0.2 0.54 1.25 0.78 X
134 0.26 -0.09 -1.5 -0.5 -0.8 NDS NDS NDS NDS -0.93 0.51 N/A N/A
135 0.17 -0.18 -3.0 2, 3 0.0 0.3 -2.1 0.0 NDS NDS -0.96 1.49 0.65 X
138 0.26 -0.09 -1.5 -0.7 1.1 1.6 -0.6 -0.3 -1.6 -0.29 1.22 0.80
139 0.34 -0.01 -0.2 0.8 1.4 1.6 0.7 -1.1 2.4 0.80 1.17 0.83
140 0.34 -0.01 -0.2 -1.0 -0.5 -0.1 -0.2 -1.4 -1.1 -0.64 0.52 1.87
141 0.38 0.03 0.5 1.5 -0.6 -0.5 -0.2 0.7 1.1 0.36 0.81 1.20
144 0.38 0.03 0.5 NDS 0.1 NDS -1.6 NDS NDS -0.33 1.12 N/A N/A
145 0.41 0.06 1.0 -0.4 0.0 -0.5 0.4 0.7 -0.3 0.13 0.58 1.67
147 0.35 0.00 0.0 -0.8 -0.6 0.0 -0.9 NDS NDS -0.46 0.43 2.26
148 0.31 -0.04 -0.7 -0.5 -1.2 -0.5 0.0 -0.9 -1.8 -0.80 0.58 1.67
149 0.40 0.05 0.8 0.5 NDS R -0.5 -0.8 0.1 0.02 0.67 1.45
150 0.37 0.02 0.3 2.0 -2.0 2.0 1.8 0.4 1.1 0.80 1.43 0.68 X
151 0.33 -0.02 -0.3 -0.1 -0.1 NDS NDS 0.0 NDS -0.12 0.13 7.46
152 0.37 0.02 0.3 0.0 0.0 0.0 -0.2 0.1 0.3 0.07 0.18 5.39
155 0.38 0.03 0.5 -0.5 0.9 0.8 -0.2 -2.3 0.1 -0.10 1.10 0.88
157 0.41 0.06 1.0 0.3 -0.6 -0.5 0.6 1.9 0.8 0.50 0.87 1.11
ASTM Crude Oil
Sample ID: CO1607
July 2016 40
(mass%)
1603 1511 1507 1503 1411 1407
158 0.41 0.06 1.0 -1.5 -0.7 NDS -2.7 NDS NDS -0.98 1.55 0.63 X
159 0.40 0.05 0.8 -0.6 -0.6 R -2.6 -0.8 R -0.76 1.21 0.80
161 0.38 0.03 0.5 0.7 NDS 2.0 0.8 NDS NDS 1.00 0.68 1.43
163 0.36 0.01 0.2 -1.4 -0.3 0.0 -0.5 0.0 0.1 -0.27 0.55 1.76
164 0.38 0.03 0.5 NDS -0.9 NDS 0.1 NDS -1.1 -0.35 0.77 1.26
166 0.34 -0.01 -0.2 -0.3 0.2 0.0 0.5 R 1.0 0.20 0.49 1.98
168 0.30 -0.05 -0.8 NDS NDS 0.4 NDS 1.3 NDS 0.30 1.05 N/A N/A
170 0.31 -0.04 -0.7 -0.7 0.7 0.0 -0.3 1.8 -0.7 0.01 0.94 1.03
171 0.38 0.03 0.5 0.5 -2.3 -0.5 -1.4 0.7 1.1 -0.20 1.25 0.78 X
173 0.29 -0.06 -1.0 -1.0 NDS 1.2 NDS NDS NDS -0.27 1.27 N/A N/A
176 0.36 0.01 0.2 0.9 -1.6 0.8 0.2 1.5 1.7 0.53 1.10 0.88
181 ** 0.08 R 1.2 -1.0 0.0 1.4 1.9 1.8 0.88 1.15 0.84
182 0.19 -0.16 -2.7 3 NDS NDS -0.9 NDS R NDS -1.80 1.27 N/A N/A
183 0.38 0.03 0.5 0.9 1.9 1.6 0.8 0.4 0.1 0.89 0.65 1.49
184 0.37 0.02 0.3 1.0 -0.1 -0.5 0.9 NDS NDS 0.32 0.64 1.52
191 0.23 -0.12 -2.0 -1.2 0.3 -0.9 -1.7 -2.7 -1.1 -1.33 0.95 1.02
192 0.31 -0.04 -0.7 -0.9 -0.1 0.8 -0.2 0.3 -0.1 -0.13 0.57 1.70
193 0.32 -0.03 -0.5 R -0.8 0.0 0.1 -0.2 -0.6 -0.33 0.36 2.69
196 0.33 -0.02 -0.3 NDS NDS -0.5 0.9 NDS 0.2 0.08 0.62 1.56
201 0.32 -0.03 -0.5 -1.1 0.9 R -0.1 -0.2 0.8 -0.03 0.77 1.26
203 0.18 -0.17 -2.8 3 -0.6 -2.7 0.8 -3.1 R -1.6 -1.67 1.53 0.63 X
204 0.26 -0.09 -1.5 -1.6 0.8 0.0 3.1 0.4 0.1 0.19 1.58 0.61 X
210 0.36 0.01 0.2 R -0.5 -0.2 0.9 R -3.2 -0.56 1.57 0.62 X
211 0.34 -0.01 -0.2 0.2 0.1 0.4 0.2 0.1 1.0 0.26 0.37 2.62
213 0.37 0.02 0.3 0.6 -1.4 0.8 -0.3 0.1 0.1 0.03 0.73 1.33
214 0.37 0.02 0.3 0.1 -0.5 0.8 0.0 NDS NDS 0.14 0.47 2.06
216 0.37 0.02 0.3 -3.2 -2.6 -1.3 -1.8 NDS NDS -1.72 1.34 0.72 X
220 0.36 0.01 0.2 0.5 -0.9 -0.9 -0.2 -0.3 1.1 -0.07 0.73 1.33
224 0.36 0.01 0.2 0.4 0.8 1.2 0.9 0.6 1.3 0.77 0.40 2.42
226 0.34 -0.01 -0.2 0.0 -0.5 0.0 1.3 NDS NDS 0.12 0.69 1.41
228 0.36 0.01 0.2 0.1 1.4 1.6 0.7 NDS R 0.80 0.68 1.43
229 0.43 0.08 1.3 -0.4 0.2 -3.1 NDS NDS NDS -0.50 1.87 0.52 X
230 0.38 0.03 0.5 0.0 -0.8 -0.2 -0.9 0.0 0.2 -0.17 0.51 1.90
231 0.30 -0.05 -0.8 -2.6 R -0.5 R -0.6 0.3 -0.84 1.07 0.91
234 0.38 0.03 0.5 0.5 0.1 -0.5 0.4 0.9 0.6 0.36 0.45 2.16
240 0.29 -0.06 -1.0 NDS 0.0 0.0 NDS NDS NDS -0.33 0.58 N/A N/A
241 0.29 -0.06 -1.0 -0.8 0.6 0.4 -0.8 -1.7 -0.7 -0.57 0.81 1.20
ASTM Crude Oil
Sample ID: CO1607
July 2016 41
(mass%)
Legend:
R = Rejected
TPI 0.94
Comments:
42
Page 1 of 2
Sample ID: CO1607
(mass%)
0.24 0.59

0.18 0.53
Reproducibility
0.12 0.47
0.06 0.41
Deviation
0 0.35
-0.06 0.29
-0.12 0.23

Reproducibility
-0.18 0.17
-0.24 0.11
5 1 1 7 2 5 1 2 1 1 1 4 1 1 1 2 5 1 2 2 2 1 9 1 8 4 7 2 1 1 1 9 1 1 4 1 5 1 2 2 6 1 1 6 9 1 1 1 1 9 2 2 1 1 1 8 1 8 1 7 3 4 4
4 3 1 0 8 6 9 0 0 8 3 3 1 0 8 4 7 4 4 7 9 6 8 9 3 8 2 1 1 4 7 5 9 9 7 0 1 0 9 5 9 6 9 4 6 3 4 2 1 0 1 1 6 0 7 4 7 0 3 1
5 8 3 2 1 1 5 8 4 0 4 0 1 3 8 1 9 7 2 8 0 2 1 9 3 1 6 0 6 9 6 1 8 6 9 3 7

43
Page 2 of 2
Sample ID: CO1607
(mass%)
0.24 0.59

0.18 0.53
Reproducibility
0.12 0.47
0.06 0.41
Deviation
0 0.35
-0.06 0.29
-0.12 0.23
Reproducibility
-0.18 0.17
-0.24 0.11
2 3 6 1 1 1 1 1 1 2 2 2 2 2 1 1 2 2 1 9 8 1 1 1 1 1 2 6 2 1 1 1 2 2 9 4 5 2 1 9 1 1 6 2 6 1 8 1 1 9 1 2 1 2 3 1 3 7 1 1 2 6 6
2 5 6 2 2 6 6 7 7 1 2 2 2 1 5 5 1 1 8 2 9 6 5 6 7 8 3 3 4 3 4 9 0 3 6 6 5 2 5 4 7 1 4 4 4 5 5 0 1 3 0 2 9 4 4 2 0 2 3 2
3 4 0 3 6 7 0 0 4 8 6 2 0 3 4 4 1 5 4 1 3 0 4 4 2 1 9 9 5 7 8 7 6 9 6 7 5

44
Sample ID: CO1607

(mass%)
49
42 1% Median 99%
35
Number of Labs
28
21
14
0
0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.5 0.55 0.6 0.65
ASTM Crude Oil
Sample ID: CO1607
July 2016 45
Density - D1298
(kg/L) at 15C
1603 1511 1507 1503 1411 1407
004 0.8224 -0.00037 -0.7 2.4 NDS -1.4 0.5 0.5 NDS 0.26 1.45 0.66 X
005 0.8218 -0.00097 -1.7 -0.5 0.0 -0.2 0.5 NDS NDS -0.38 0.82 1.17
007 ** 0.8251 R -0.7 1.8 -0.1 0.5 NDS NDS 0.38 1.07 0.90
008 0.8231 0.00033 0.6 -0.5 -0.1 -1.2 0.3 -1.3 NDS -0.37 0.78 1.23
010 0.8223 -0.00047 -0.8 -1.4 0.0 -1.5 1.9 0.4 0.2 -0.17 1.19 0.81
012 0.8218 -0.00097 -1.7 -1.3 NDS 1.3 -0.7 NDS NDS -0.60 1.33 0.72 X
013 0.8224 -0.00037 -0.7 -1.9 0.3 -1.1 -0.5 -0.3 -0.3 -0.64 0.70 1.37
016 0.8232 0.00043 0.8 NDS NDS NDS -0.7 -0.6 R -0.17 0.84 N/A N/A
023 0.8222 -0.00057 -1.0 -0.2 1.0 0.1 -0.3 0.2 0.4 0.03 0.62 1.55
024 0.8237 0.00093 1.7 1.6 0.0 -0.1 -0.1 -0.6 -1.5 0.14 1.15 0.83
025 0.8230 0.00023 0.4 NDS 0.0 NDS 1.3 0.5 NDS 0.55 0.54 1.78
028 0.8213 -0.00147 -2.6 3 -1.4 -1.2 -1.5 -2.0 -0.6 1.2 -1.16 1.21 0.79 X
029 0.8232 0.00043 0.8 -0.7 0.0 0.1 NDS 0.4 -0.7 -0.02 0.60 1.60
033 0.8230 0.00023 0.4 NDS NDS -1.0 NDS NDS NDS -0.30 0.99 N/A N/A
038 0.8232 0.00043 0.8 0.7 -3.0 0.5 0.8 2.0 -0.7 0.16 1.60 0.60 X
040 0.8232 0.00043 0.8 R NDS NDS NDS NDS NDS 0.80 0.00 N/A N/A
042 ** 0.8193 R R -0.7 0.5 NDS 2.8 NDS 0.87 1.78 N/A N/A
047 0.8226 -0.00017 -0.3 0.0 -0.5 -2.7 0.6 1.0 -0.5 -0.34 1.18 0.81
048 0.8232 0.00043 0.8 NDS NDS 0.6 -0.1 -0.6 1.2 0.38 0.72 1.33
059 0.8216 -0.00117 -2.1 3 NDS NDS NDS NDS NDS NDS -2.10 0.00 N/A N/A
064 0.8230 0.00023 0.4 0.1 -0.1 -0.4 NDS -0.5 0.0 -0.08 0.33 2.91
066 0.8226 -0.00017 -0.3 0.7 NDS NDS -0.2 -0.3 -0.7 -0.16 0.52 1.85
067 0.8237 0.00093 1.7 -0.7 0.6 -0.1 -1.9 -1.3 -0.7 -0.34 1.21 0.79 X
069 0.8230 0.00023 0.4 -0.4 -0.8 0.1 0.0 NDS NDS -0.14 0.47 2.04
070 0.8227 -0.00007 -0.1 -0.7 0.5 0.5 -0.2 1.0 1.0 0.29 0.64 1.50
073 0.8228 0.00003 0.1 -1.3 0.0 -0.8 1.9 1.2 0.2 0.19 1.09 0.88
076 0.8229 0.00013 0.2 3.0 1.2 0.4 0.3 -0.3 1.8 0.94 1.14 0.84
078 0.8227 -0.00007 -0.1 0.1 0.3 0.7 -0.7 0.0 0.0 0.04 0.42 2.29
079 0.8227 -0.00007 -0.1 0.1 0.0 0.6 R NDS NDS 0.15 0.31 3.10
080 0.8232 0.00043 0.8 1.0 -0.1 -0.4 NDS -0.5 0.0 0.13 0.63 1.52
086 0.8221 -0.00067 -1.2 -0.2 -0.3 1.6 0.3 1.0 0.0 0.17 0.91 1.05
101 0.8228 0.00003 0.1 -1.3 0.8 NDS -2.0 NDS NDS -0.60 1.28 0.75 X
103 0.8230 0.00023 0.4 0.0 -0.5 NDS NDS -0.8 1.0 0.02 0.72 1.33
108 0.8239 0.00113 2.0 -0.7 NDS -1.0 -1.4 -1.0 -1.3 -0.57 1.28 0.75 X
109 ** 0.8261 R NDS NDS 2.0 0.5 1.2 1.0 1.18 0.62 1.55
119 0.8232 0.00043 0.8 NDS NDS 0.6 NDS NDS NDS 0.70 0.14 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 46
Density - D1298
(kg/L) at 15C
1603 1511 1507 1503 1411 1407
126 0.8230 0.00023 0.4 1.2 1.4 1.1 1.0 1.2 1.2 1.07 0.32 3.00
127 0.8228 0.00003 0.1 NDS -0.6 0.6 0.5 0.4 0.2 0.20 0.43 2.23
129 0.8223 -0.00047 -0.8 0.9 0.6 -0.8 -0.1 NDS NDS -0.04 0.78 1.23
133 0.8235 0.00073 1.3 -1.7 -0.8 NDS 0.5 R NDS -0.18 1.34 0.72 X
138 0.8232 0.00043 0.8 -0.7 0.8 0.5 0.0 1.4 0.4 0.46 0.67 1.43
142 ** 0.8192 R R NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
147 0.8218 -0.00097 -1.7 0.9 -0.6 -0.1 -0.1 NDS NDS -0.32 0.94 1.02
152 0.8230 0.00023 0.4 -0.5 -2.4 0.6 0.8 -0.6 0.2 -0.21 1.10 0.87
156 0.8216 -0.00117 -2.1 3 -1.0 0.0 NDS -2.4 0.8 -2.7 -1.23 1.41 0.68 X
158 0.8228 0.00003 0.1 NDS -0.6 R -2.6 NDS NDS -1.03 1.40 N/A N/A
161 0.8232 0.00043 0.8 -2.0 NDS -0.1 NDS NDS NDS -0.43 1.43 N/A N/A
163 0.8223 -0.00047 -0.8 -1.3 -1.8 -0.1 -1.4 -2.3 -1.5 -1.31 0.71 1.35
165 0.8230 0.00023 0.4 -0.4 0.0 NDS -0.5 -0.5 -0.7 -0.28 0.41 2.34
167 0.8218 -0.00097 -1.7 1.6 0.6 -0.8 1.3 NDS NDS 0.20 1.41 0.68 X
169 0.8228 0.00003 0.1 1.6 0.6 1.3 NDS NDS NDS 0.90 0.68 1.41
170 0.8227 -0.00007 -0.1 -0.7 -0.6 -0.2 2.5 -0.6 0.2 0.07 1.12 0.86
173 0.8228 0.00003 0.1 -0.7 NDS 0.3 NDS NDS NDS -0.10 0.53 N/A N/A
179 0.8229 0.00013 0.2 1.3 1.6 -0.8 -0.3 -0.2 2.3 0.59 1.15 0.83
183 0.8233 0.00053 0.9 0.9 NDS 0.6 0.5 NDS -0.7 0.44 0.66 1.45
185 0.8234 0.00063 1.1 0.7 -0.4 NDS 1.5 0.4 1.0 0.72 0.66 1.45
189 0.8228 0.00003 0.1 NDS 1.2 1.3 -0.1 NDS NDS 0.62 0.73 1.32
191 0.8218 -0.00097 -1.7 -0.7 -1.2 2.8 NDS R 0.2 -0.12 1.78 0.54 X
193 0.8223 -0.00047 -0.8 -0.7 -0.6 1.2 -0.1 -0.2 0.2 -0.14 0.69 1.39
196 0.8216 -0.00117 -2.1 3 NDS NDS 1.5 -0.6 -1.5 -0.3 -0.60 1.37 0.70 X
207 0.8232 0.00043 0.8 0.6 1.7 0.5 1.0 0.2 0.0 0.69 0.56 1.71
211 0.8229 0.00013 0.2 0.0 0.1 0.9 -0.1 0.2 0.6 0.27 0.35 2.74
212 0.8213 -0.00147 -2.6 3 3.2 0.6 NDS -0.7 NDS NDS 0.13 2.43 0.40 X
213 0.8229 0.00013 0.2 -1.0 -1.2 0.9 -0.9 -0.3 -0.9 -0.46 0.77 1.25
216 0.8230 0.00023 0.4 -0.5 1.8 -0.1 0.5 NDS NDS 0.42 0.87 1.10
221 ** 0.8203 R NDS NDS NDS 0.5 NDS -2.5 -1.00 2.12 N/A N/A
224 0.8223 -0.00047 -0.8 NDS -0.1 -0.1 0.5 NDS NDS -0.12 0.53 1.81
234 0.8225 -0.00027 -0.5 NDS NDS NDS -0.1 NDS NDS -0.30 0.28 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 47
Density - D1298
(kg/L) at 15C
1603 1511 1507 1503 1411 1407
239 0.8229 0.00013 0.2 NDS 0.7 0.3 NDS 0.7 NDS 0.48 0.26 3.69

Legend:
R = Rejected
TPI 0.97
Comments:
48
Page 1 of 2
Sample ID: CO1607
Density - D1298
(kg/L) at 15C
0.00224 0.82501

0.00168 0.82445
Reproducibility
0.00112 0.82389
0.00056 0.82333
Deviation
0 0.82277
-0.00056 0.82221
-0.00112 0.82165

Reproducibility
-0.00168 0.82109
-0.00224 0.82053
2 2 1 5 1 1 1 5 1 1 2 1 8 2 1 2 1 1 2 1 1 1 1 4 2 5 6 4 1 2 2 1 7 7 7 1 1 1 1 1 7 1 1 1
1 8 9 9 5 9 4 2 6 3 5 6 2 8 3 8 6 2 2 9 0 3 3 2 6 7 7 1 2 1 8 9 0 5 6 7 8 2 3 0 1 9
2 6 6 1 7 7 7 3 5 8 3 4 9 3 4 0 7 3 3 8 9 3 9 7 1 0 9

49
Page 2 of 2
Sample ID: CO1607
Density - D1298
(kg/L) at 15C
0.00224 0.82501
0.00168 0.82445
Reproducibility
0.00112 0.82389
0.00056 0.82333
Deviation
0 0.82277
-0.00056 0.82221
-0.00112 0.82165

Reproducibility
-0.00168 0.82109
-0.00224 0.82053
2 2 1 1 2 2 1 7 9 2 6 1 2 3 1 1 6 1 1 2 8 4 4 4 3 2 1 2 1 1 1 8 1 2 1 1 1 1 2 6 1 1 1
3 3 9 3 1 1 7 6 5 1 9 0 5 3 2 0 4 5 6 0 9 8 0 8 9 6 0 6 3 1 0 8 2 8 3 9 6 4 7 4 0 8
9 6 0 0 3 1 9 6 3 6 5 2 5 2 7 1 8 9 3 7 5 3 7 2 8 4

50
Sample ID: CO1607

Density - D1298
(kg/L) at 15C
35
30 1% Median 99%
25
Number of Labs
20
15
10
0
0.8208 - 0.8212 - 0.8216 - 0.822 - 0.8223 0.8224 - 0.8228 - 0.8232 - 0.8236 - 0.824 - 0.8243 0.8244 -
0.8211 0.8215 0.8219 0.8227 0.8231 0.8235 0.8239 0.8247

ASTM Crude Oil
Sample ID: CO1607
July 2016 51
Density - D5002 (kg/L)
(kg/L@15C)
1603 1511 1507 1503 1411 1407
003 0.8229 -0.00010 -0.4 0.9 1.0 -1.9 NDS -0.1 0.3 -0.03 1.07 0.99
006 0.8226 -0.00040 -1.7 -0.2 -0.9 0.1 1.1 1.1 0.6 0.01 1.04 1.02
009 0.8231 0.00010 0.4 0.5 0.2 -0.6 0.2 -0.8 0.3 0.03 0.51 2.08
011 0.8232 0.00020 0.8 NDS -0.7 -1.5 1.3 -1.6 R -0.34 1.33 0.80
013 0.8230 0.00000 0.0 -0.6 1.7 -0.3 -0.3 0.3 -0.3 0.07 0.77 1.38
015 0.8232 0.00020 0.8 -0.6 -1.9 0.8 1.1 NDS NDS 0.04 1.27 0.83
017 0.8231 0.00010 0.4 0.9 1.9 2.6 1.5 R 3.9 1.87 1.26 0.84
020 ** 0.8159 R R R R NDS NDS NDS 0.00 0.00 N/A N/A
021 ** 0.8239 R 2.7 0.2 0.4 R 0.3 1.5 1.02 1.08 0.98
022 0.8228 -0.00020 -0.8 NDS NDS 0.1 -1.9 NDS NDS -0.87 1.00 N/A N/A
023 0.8232 0.00020 0.8 0.9 1.4 -0.6 -0.5 -0.5 0.0 0.21 0.81 1.31
025 0.8230 0.00000 0.0 NDS 0.1 NDS NDS 1.1 0.0 0.30 0.54 1.96
026 0.8227 -0.00030 -1.2 1.1 -1.9 -0.3 -0.1 NDS NDS -0.48 1.14 0.93
029 0.8232 0.00020 0.8 0.5 -0.6 -0.1 0.4 -0.1 0.3 0.17 0.47 2.26
030 0.8229 -0.00010 -0.4 -0.2 -0.1 -0.6 -1.0 -0.1 -0.9 -0.47 0.37 2.86
031 0.8232 0.00020 0.8 -1.5 -0.2 0.2 0.4 1.1 R 0.13 0.92 1.15
032 0.8226 -0.00040 -1.7 NDS -0.4 -1.0 -0.8 0.3 NDS -0.72 0.74 1.43
033 0.8230 0.00000 0.0 NDS 0.7 NDS NDS -0.5 R 0.07 0.60 N/A N/A
034 0.8230 0.00000 0.0 NDS 0.1 -0.1 -0.1 -0.1 -1.1 -0.22 0.44 2.41
035 0.8232 0.00020 0.8 R -0.1 NDS R 0.3 -1.1 -0.03 0.81 1.31
037 0.8227 -0.00030 -1.2 NDS -0.2 -0.8 -0.8 0.3 NDS -0.54 0.59 1.80
046 0.8231 0.00010 0.4 0.9 -0.7 -0.1 0.8 NDS NDS 0.26 0.67 1.58
048 0.8232 0.00020 0.8 NDS NDS -0.3 -0.1 0.7 1.8 0.58 0.83 1.28
051 0.8228 -0.00020 -0.8 NDS 0.6 NDS NDS NDS NDS -0.10 0.99 N/A N/A
052 0.8238 0.00080 3.3 1, 3 0.2 NDS NDS NDS NDS NDS 1.75 2.19 N/A N/A
053 0.8230 0.00000 0.0 -0.4 -0.2 -0.1 -0.8 0.3 -0.9 -0.30 0.43 2.47
054 0.8227 -0.00030 -1.2 R -1.9 1.9 -0.1 0.3 NDS -0.20 1.46 0.73 X
055 ** 0.8243 R 0.5 NDS 0.1 -0.1 -0.1 1.5 0.38 0.67 1.58
057 0.8230 0.00000 0.0 1.1 -1.7 0.2 -1.4 1.1 1.2 0.07 1.21 0.88
060 0.8228 -0.00020 -0.8 0.2 NDS NDS NDS -1.2 3.3 0.37 2.04 0.52 X
061 ** 0.8188 R -0.6 -2.5 -0.3 -0.3 1.8 -0.9 -0.47 1.38 0.77 X
062 0.8232 0.00020 0.8 -0.6 2.0 NDS NDS NDS NDS 0.73 1.30 N/A N/A
066 0.8229 -0.00010 -0.4 0.9 0.7 1.0 -0.5 -0.5 -1.1 0.01 0.83 1.28
067 0.8232 0.00020 0.8 -0.4 0.4 0.2 -0.1 0.7 0.6 0.31 0.44 2.41
068 0.8231 0.00010 0.4 0.2 -0.4 0.2 1.1 -0.5 0.9 0.27 0.60 1.77
071 0.8230 0.00000 0.0 -0.9 0.2 1.7 0.8 0.7 -1.1 0.20 0.98 1.08
ASTM Crude Oil
Sample ID: CO1607
July 2016 52
(kg/L@15C)
1603 1511 1507 1503 1411 1407
072 0.8230 0.00000 0.0 NDS -1.9 -0.3 -0.8 -0.8 -0.6 -0.73 0.65 1.63
074 0.8231 0.00010 0.4 0.9 -0.1 1.3 3.6 -0.8 0.3 0.80 1.41 0.75 X
077 0.8230 0.00000 0.0 -0.4 0.4 -0.1 -0.5 -0.8 -0.6 -0.29 0.41 2.59
078 ** 0.8221 R 0.5 0.4 -0.8 -0.8 -0.8 -0.3 -0.30 0.61 1.74
081 0.8231 0.00010 0.4 1.4 NDS -0.1 NDS NDS NDS 0.57 0.76 N/A N/A
082 0.8228 -0.00020 -0.8 NDS NDS R NDS -0.1 1.8 0.30 1.35 N/A N/A
087 0.8230 0.00000 0.0 -0.2 -0.4 0.4 -0.1 -0.5 1.2 0.06 0.58 1.83
088 0.8232 0.00020 0.8 -0.6 -0.4 NDS -0.1 NDS NDS -0.07 0.62 1.71
089 0.8230 0.00000 0.0 -0.4 -0.1 -0.6 -0.5 -1.6 -0.6 -0.54 0.52 2.04
090 0.8229 -0.00010 -0.4 -0.6 -0.2 0.2 -0.3 -0.1 -0.6 -0.29 0.29 3.66
091 0.8225 -0.00050 -2.1 3 0.0 0.1 0.4 1.1 3.0 3.6 0.87 1.93 0.55 X
092 0.8229 -0.00010 -0.4 -0.4 NDS -0.8 -0.5 1.8 NDS -0.06 1.05 1.01
096 0.8226 -0.00040 -1.7 -2.0 0.4 -0.3 -0.1 0.3 0.0 -0.49 0.97 1.09
098 0.8227 -0.00030 -1.2 0.2 NDS NDS 0.8 NDS 0.0 -0.05 0.84 1.26
099 0.8237 0.00070 2.9 3 -0.6 R 0.8 -0.1 1.1 -1.4 0.45 1.51 0.70 X
102 0.8230 0.00000 0.0 1.4 -0.4 -0.1 1.8 2.6 R 0.88 1.22 0.87
103 0.8230 0.00000 0.0 0.2 -0.7 0.2 NDS -1.6 1.8 -0.02 1.13 0.94
104 0.8231 0.00010 0.4 -0.4 0.7 0.8 -0.1 -0.5 0.3 0.17 0.52 2.04
105 0.8230 0.00000 0.0 -0.4 -0.9 0.8 0.4 0.3 -0.6 -0.06 0.61 1.74
106 0.8231 0.00010 0.4 -1.8 -3.0 -0.1 NDS NDS NDS -1.12 1.56 0.68 X
107 0.8231 0.00010 0.4 -1.3 2.8 2.0 0.6 -0.8 NDS 0.62 1.58 0.67 X
109 ** 0.8261 R 1.1 2.3 0.4 -0.5 1.5 0.3 0.85 0.99 1.07
111 0.8229 -0.00010 -0.4 -0.4 1.0 -0.6 -0.3 1.5 NDS 0.13 0.88 1.20
112 0.8232 0.00020 0.8 -0.6 0.1 -0.3 -0.1 NDS R -0.02 0.53 2.00
114 0.8227 -0.00030 -1.2 1.4 1.4 -0.8 -1.7 NDS NDS -0.18 1.48 0.72 X
115 ** 0.8170 R -0.2 0.7 NDS R NDS NDS 0.25 0.64 N/A N/A
117 0.8231 0.00010 0.4 2.0 1.4 -1.0 0.6 -2.8 0.9 0.21 1.62 0.65 X
118 0.8234 0.00040 1.7 -0.6 -0.2 -0.1 -0.3 0.7 NDS 0.20 0.85 1.25
120 0.8234 0.00040 1.7 -2.0 0.2 2.2 1.3 NDS NDS 0.68 1.67 0.63 X
122 0.8232 0.00020 0.8 -0.2 1.0 1.0 NDS NDS -1.4 0.24 1.04 1.02
123 0.8229 -0.00010 -0.4 -1.1 0.2 -0.1 R 1.8 -0.3 0.02 0.97 1.09
124 0.8230 0.00000 0.0 -0.4 0.9 3.1 R -0.1 0.6 0.68 1.28 0.83
131 ** 0.8239 R -0.6 -0.2 2.6 2.9 -1.2 -1.1 0.40 1.86 0.57 X
132 0.8228 -0.00020 -0.8 -0.6 -0.9 -1.5 -0.1 NDS 0.3 -0.60 0.63 1.68
135 0.8225 -0.00050 -2.1 3 -1.1 R -1.5 0.6 NDS NDS -1.03 1.16 0.91
136 0.8230 0.00000 0.0 -0.9 -1.2 NDS 2.9 -0.1 -0.6 0.02 1.49 0.71 X
138 0.8229 -0.00010 -0.4 -0.2 1.4 0.1 -1.2 -1.2 -1.1 -0.37 0.94 1.13
140 0.8226 -0.00040 -1.7 NDS -1.9 -0.3 NDS 0.3 -0.9 -0.90 0.93 1.14
141 0.8228 -0.00020 -0.8 0.2 2.0 1.5 -0.1 -0.1 0.3 0.43 0.98 1.08
ASTM Crude Oil
Sample ID: CO1607
July 2016 53
(kg/L@15C)
1603 1511 1507 1503 1411 1407
144 0.8231 0.00010 0.4 NDS 1.0 NDS R NDS NDS 0.70 0.42 N/A N/A
145 0.8229 -0.00010 -0.4 -1.1 1.2 0.6 0.4 -0.1 0.0 0.09 0.74 1.43
146 0.8230 0.00000 0.0 2.9 NDS -1.9 -0.8 NDS NDS 0.05 2.05 0.52 X
147 0.8228 -0.00020 -0.8 0.5 -0.9 -0.3 -0.1 NDS NDS -0.32 0.57 1.86
148 0.8232 0.00020 0.8 1.1 0.6 -1.9 1.5 -0.8 -0.6 0.10 1.22 0.87
149 0.8228 -0.00020 -0.8 -1.8 NDS 0.2 1.1 NDS NDS -0.32 1.25 0.85
150 0.8231 0.00010 0.4 1.1 -0.9 -0.1 R 0.3 2.7 0.58 1.23 0.86
151 0.8237 0.00070 2.9 3 0.2 -0.7 NDS NDS 1.1 NDS 0.88 1.54 0.69 X
152 0.8230 0.00000 0.0 -0.4 -1.4 1.3 1.5 0.7 0.6 0.33 1.01 1.05
154 0.8232 0.00020 0.8 0.5 NDS -0.3 2.4 3.0 -0.9 0.92 1.52 0.70 X
155 0.8226 -0.00040 -1.7 NDS NDS -0.1 2.0 -0.1 0.0 0.02 1.31 0.81
161 0.8232 0.00020 0.8 0.2 NDS -0.3 1.5 NDS NDS 0.55 0.78 1.36
166 0.8232 0.00020 0.8 0.2 1.0 -1.5 -1.2 0.7 0.0 0.00 0.99 1.07
170 0.8228 -0.00020 -0.8 -0.2 -0.9 0.6 -1.4 0.7 0.9 -0.16 0.91 1.16
172 0.8237 0.00070 2.9 3 -0.4 NDS -0.3 -1.4 -1.6 -0.9 -0.28 1.64 0.65 X
173 0.8228 -0.00020 -0.8 R NDS 0.8 NDS NDS NDS 0.00 1.13 N/A N/A
174 ** 0.8213 R R -0.6 NDS 1.3 0.7 -0.3 0.27 0.88 1.20
175 0.8231 0.00010 0.4 -2.0 -0.4 -0.6 -1.0 0.3 -0.3 -0.51 0.82 1.29
176 0.8223 -0.00070 -2.9 3 -0.6 -0.1 NDS -0.1 0.7 NDS -0.60 1.37 0.77 X
178 0.8231 0.00010 0.4 0.7 0.2 -0.8 -0.8 -0.5 -0.6 -0.20 0.62 1.71
181 0.8233 0.00030 1.2 R -0.9 0.8 R 0.3 NDS 0.35 0.91 1.16
184 0.8224 -0.00060 -2.5 3 R 0.7 -0.3 0.6 NDS NDS -0.38 1.49 0.71 X
187 ** 0.8259 R -1.3 NDS -0.6 0.4 -0.5 NDS -0.50 0.70 1.51
191 0.8232 0.00020 0.8 -0.2 -1.2 0.6 -0.8 0.7 0.6 0.07 0.81 1.31
192 0.8228 -0.00020 -0.8 -0.6 -1.9 0.8 -0.1 1.1 -0.9 -0.34 1.04 1.02
193 0.8230 0.00000 0.0 0.5 -0.6 0.8 2.7 1.1 0.0 0.64 1.07 0.99
194 0.8230 0.00000 0.0 -0.4 0.2 0.2 1.1 -0.1 0.0 0.14 0.47 2.26
198 0.8229 -0.00010 -0.4 0.9 0.4 1.3 0.2 -0.1 R 0.38 0.63 1.68
203 0.8227 -0.00030 -1.2 -0.6 0.1 1.5 0.6 1.5 NDS 0.32 1.10 0.96
204 0.8227 -0.00030 -1.2 -0.6 0.1 0.8 -1.2 -1.2 -0.9 -0.60 0.78 1.36
206 0.8231 0.00010 0.4 -0.6 -0.7 NDS -0.5 NDS NDS -0.35 0.51 2.08
207 0.8228 -0.00020 -0.8 0.9 2.5 1.1 -0.8 0.3 0.0 0.46 1.17 0.91
208 0.8229 -0.00010 -0.4 0.0 1.9 -2.1 -1.0 -0.5 -0.9 -0.43 1.22 0.87
209 0.8237 0.00070 2.9 3 0.9 0.1 -1.0 -0.1 NDS 0.6 0.57 1.32 0.80
210 0.8227 -0.00030 -1.2 -0.6 -1.5 0.4 -0.3 1.5 -1.1 -0.40 1.05 1.01
211 0.8230 0.00000 0.0 -0.4 0.4 1.9 -0.3 0.3 0.0 0.27 0.77 1.38
213 0.8229 -0.00010 -0.4 -1.1 -1.7 1.3 -1.9 -1.6 -1.1 -0.93 1.10 0.96
214 0.8233 0.00030 1.2 -0.9 -0.4 0.2 -0.5 NDS NDS -0.08 0.82 1.29
215 0.8235 0.00050 2.1 3 -1.3 -0.9 1.9 -0.8 -0.1 -1.4 -0.07 1.48 0.72 X
220 ** 0.8253 R NDS NDS NDS R 1.8 R 1.80 0.00 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 54
(kg/L@15C)
1603 1511 1507 1503 1411 1407
222 0.8232 0.00020 0.8 1.1 0.6 -0.6 0.4 -0.1 2.1 0.61 0.87 1.22
226 0.8229 -0.00010 -0.4 -1.1 -0.6 0.1 R NDS NDS -0.50 0.50 2.12
229 0.8223 -0.00070 -2.9 3 0.5 -1.0 NDS NDS NDS NDS -1.13 1.70 N/A N/A
232 0.8232 0.00020 0.8 0.9 -0.4 -0.6 NDS -0.8 0.3 0.03 0.73 1.45
233 0.8231 0.00010 0.4 0.2 0.2 0.6 0.2 -0.5 -0.3 0.11 0.38 2.79
234 0.8229 -0.00010 -0.4 -0.2 0.7 -0.8 0.2 -0.5 -0.9 -0.27 0.56 1.89
235 0.8232 0.00020 0.8 0.9 0.4 -0.3 NDS -0.8 1.2 0.37 0.77 1.38
239 0.8233 0.00030 1.2 NDS 0.7 0.1 NDS 2.6 NDS 1.15 1.07 0.99
240 0.8224 -0.00060 -2.5 3 NDS 1.9 -0.1 NDS NDS NDS -0.23 2.20 N/A N/A
241 0.8233 0.00030 1.2 -0.6 -0.6 -0.1 -0.3 -2.4 0.3 -0.36 1.10 0.96

Legend:
R = Rejected
TPI 5.14
Comments:
55
Page 1 of 2
Sample ID: CO1607
(kg/L@15C)
0.00384
0.0036 3 Sigma Range Limit ASTM Standard 0.82252
Reproducibility
0.00336
0.00312 0.82228
0.00288
0.00264
0.82204
0.0024
0.00216
0.00192 0.8218
0.00168
0.00144 0.82156
0.0012
0.00096 0.82132
0.00072
0.00048 3 Sigma Range Limit These Test Data
0.82108
Deviation
0.00024
0
-0.00024 0.82084
-0.00048 3 Sigma Range Limit These Test Data
-0.00072 0.8206
-0.00096
-0.0012 0.82036
-0.00144
-0.00168 0.82012
-0.00192
-0.00216 0.81988
-0.0024
-0.00264
-0.00288 0.81964
-0.00312
-0.00336 3 Sigma Range Limit ASTM Standard 0.8194
Reproducibility
-0.0036
-0.00384 0.81916
2 1 1 2 1 9 3 1 9 6 1 2 6 5 2 2 4 3 2 1 9 2 1 8 6 5 2 1 2 1 1 1 1 1 1 1 3 1 9 6 3 1 2 5 4 2 9 3 2 1 2 1 1 2 1 2 3 3 5 5 7 7 7 8 8 1 1
2 7 8 4 3 1 2 4 6 5 6 4 4 0 0 3 7 1 1 8 1 3 2 0 1 2 3 0 9 7 7 5 4 4 4 0 2 0 6 9 0 0 4 1 2 6 0 4 3 1 3 2 3 5 3 4 3 7 1 2 7 7 9 0 0
9 6 4 0 5 0 5 3 4 0 4 9 0 2 7 2 3 0 6 9 7 1 3 8 0 3 8 5 4 1 8 6 2 3

56
Page 2 of 2
Sample ID: CO1607
(kg/L@15C)
0.00384 0.82684
Reproducibility
0.00336 0.82636
0.00312 0.82612
0.00288 0.82588
0.00264 0.82564
0.0024 0.8254
0.00216 0.82516
0.00192 0.82492
0.00168 0.82468
0.00144 0.82444
0.0012 0.8242
0.00096 0.82396
0.00072 0.82372
0.00048 0.82348
Deviation
0.00024 0.82324
0 0.823
-0.00024 0.82276
-0.00048 3 Sigma Range Limit These Test Data 0.82252
-0.00072 0.82228
-0.00096 0.82204
-0.0012 0.8218
-0.00144 0.82156
-0.00168 0.82132
-0.00192 0.82108
-0.00216 0.82084
-0.0024 0.8206
-0.00264 0.82036
-0.00288 0.82012
-0.00312 0.81988
Reproducibility
-0.0036 0.8194
-0.00384 0.81916
1 1 1 1 1 1 1 1 2 9 2 3 4 6 7 8 1 1 1 1 1 1 1 1 1 2 2 1 2 1 1 2 2 2 3 3 4 6 6 8 9 1 1 1 1 1 1 1 2 2 2 2 2 1 2 2 2 1 1 1 2 2 1 1 1 9 5
0 1 2 3 4 5 9 9 1 3 9 6 8 4 1 0 0 0 1 3 4 5 7 7 0 0 7 1 5 3 7 9 1 5 8 2 7 8 3 1 2 4 5 6 6 9 2 3 3 3 2 2 4 3 1 8 2 1 1 0 7 5 5 9 2
5 3 4 6 6 2 3 4 1 3 4 6 7 7 4 4 0 5 8 2 6 2 2 8 4 1 6 1 2 0 2 5 5 1 1 9 4 1 0 8 5 9 2 9 1

57
Sample ID: CO1607

(kg/L@15C)
49
1% Median 99%
42
35
Number of Labs
28
21
14
0
0.8219 - 0.8221 - 0.8223 - 0.8225 - 0.8227 - 0.8229 - 0.8231 - 0.8233 - 0.8235 - 0.8237 - 0.8239 - 0.8241 -
0.822 0.8222 0.8224 0.8226 0.8228 0.823 0.8232 0.8234 0.8236 0.8238 0.824 0.8242

58
ASTM Crude Oil
Sample ID: CO1607
July 2016
High Temperature Simulated Distillation - D7169 Total Weight % Recovery
82.2C 193.3C 248.9C 343.3C 426.7C 565.6C 596.1C 720C
Lab Code (180F) (380F) (480F) (650F) (800F) (1050F) (1105F) (1328F)
003 3.4 28.4 42.8 65.2 80.2 93.9 95.3 97.6
013 3.4 28.3 42.7 65.3 81.1 95.4 97.0 99.5
015 ** 7.8 ** 34.0 ** 48.6 ** 71.0 81.9 95.7 97.2 99.8
017 1.4 26.9 41.7 64.5 80.2 94.5 96.1 99.1
020 3.1 29.7 43.2 63.9 77.7 90.6 92.0 94.3
022 2.6 29.6 44.1 66.4 81.5 95.6 96.8 100.0
023 3.4 28.5 43.0 65.6 81.0 94.9 96.5 99.8
027 4.4 29.6 43.4 63.0 76.5 87.6 88.8 91.4
029 0.9 24.9 38.7 59.9 74.2 87.3 88.7 91.2
034 1.4 27.0 41.3 64.3 79.5 93.7 95.4 99.1
041 2.5 28.5 42.7 65.6 81.2 95.1 96.7 100.0
046 3.0 30.0 45.0 67.5 82.5 96.5 97.5 100.0
055 3.5 ** 35.4 -- 69.1 -- 96.1 97.4 100.0
065 2.8 29.5 43.2 65.4 81.0 95.2 96.8 99.7
067 1.9 25.4 38.6 59.8 73.5 ** 86.0 ** 87.3 98.4
071 2.4 26.8 40.8 62.7 77.3 90.6 92.0 94.5
077 3.5 28.1 42.1 64.8 80.0 94.2 95.8 98.7
084 1.3 27.4 41.1 62.7 77.9 91.9 93.8 97.1
086 2.8 27.8 42.2 64.6 79.9 93.6 95.1 97.9
088 4.6 29.3 42.5 64.6 79.5 93.7 95.4 98.9
089 3.1 27.8 42.6 66.2 81.7 96.0 97.5 100.0
096 2.3 29.0 42.6 64.5 80.2 94.7 96.3 100.0
**Z-Score calculation equal to or greater than +/-3. Lab data labeled as "Rejected" and not included in statistical analysis. See report introduction for " A Check List for Investigating the Root Cause of
Unsatisfactory Analytical Performance.
59
ASTM Crude Oil
Sample ID: CO1607
July 2016
82.2C 193.3C 248.9C 343.3C 426.7C 565.6C 596.1C 720C
107 3.5 29.7 44.0 64.4 78.8 96.3 97.8 100.0
122 -- 28.5 42.6 64.6 80.0 94.0 95.6 98.1
128 3.1 26.1 40.4 63.5 79.8 95.3 96.9 --
135 4.7 26.7 42.2 66.2 82.0 95.9 97.1 99.0
139 3.1 29.4 43.6 66.2 81.2 94.7 96.2 99.3
144 2.5 29.5 44.0 66.5 81.5 95.4 97.0 --
156 0.9 26.3 40.6 62.0 76.8 90.4 91.6 92.5
164 3.3 27.8 42.4 65.8 81.5 95.9 97.4 100.0
176 2.4 28.8 43.7 67.2 83.1 97.7 -- --
189 2.9 27.1 40.5 61.9 76.5 89.8 91.3 93.8
191 2.5 29.0 43.4 65.3 79.3 92.2 93.4 --
192 2.4 29.2 43.3 65.7 80.9 95.1 96.7 99.3
193 2.4 27.7 41.6 63.9 78.7 92.1 93.5 95.5
201 3.2 25.5 39.2 61.6 77.1 91.6 93.1 95.7
206 4.4 28.5 42.2 63.5 77.9 91.0 92.4 95.1
210 2.6 28.3 43.2 66.2 81.8 96.0 97.6 --
213 2.9 28.7 43.1 66.0 81.7 95.8 97.3 --
220 3.0 30.0 45.0 68.0 84.0 98.0 99.0 --
239 3.1 27.0 41.8 65.3 81.2 95.5 97.1 100.0
241 ** 25.5 ** 71.0 ** 86.6 -- -- -- -- 95.2
60
ASTM Crude Oil
Sample ID: CO1607
July 2016
82.2C 193.3C 248.9C 343.3C 426.7C 565.6C 596.1C 720C
No. Valid Results 39 39 39 40 40 40 39 35
Robust Mean 2.85 28.18 42.43 64.82 79.94 94.16 95.58 97.96
Robust Standard Deviation 0.74 1.38 1.37 1.82 2.19 2.41 2.30 2.51
Reproducibility ASTM Standard 1.74 1.92 2.05 2.28 2.58 3.03 3.12 3.17
Reproducibility These Test Data 2.05 3.82 3.79 5.04 6.07 6.68 6.37 6.95
ASTM Crude Oil
Sample ID: CO1607
July 2016 61
Recovery wt% @ 82.2C (180F)
1603 1511 1507 1503 1411 1407
013 3.4 0.55 0.7 -0.1 -0.7 R 0.0 0.0 -0.1 -0.03 0.45 2.13
015 ** 7.8 R 0.8 0.3 1.6 2.1 NDS NDS 1.20 0.80 1.20
017 1.4 -1.45 -2.0 -0.1 -0.4 -0.7 -1.1 0.8 -0.7 -0.60 0.86 1.12
020 3.1 0.25 0.3 0.3 1.1 0.4 0.5 0.6 0.8 0.57 0.29 3.31
027 4.4 1.55 2.1 3 -3.2 -2.0 NDS NDS NDS NDS -1.03 2.78 N/A N/A
029 0.9 -1.95 -2.6 2, 3 NDS NDS NDS R NDS NDS -2.60 0.00 N/A N/A
034 1.4 -1.45 -2.0 NDS -0.7 2.2 -1.1 -1.4 0.3 -0.45 1.51 0.64 X
046 3.0 0.15 0.2 R 1.4 0.6 -0.3 NDS NDS 0.47 0.72 1.33
055 3.5 0.65 0.9 0.3 NDS -0.3 -0.5 NDS 0.9 0.26 0.65 1.48
065 2.8 -0.05 -0.1 0.6 -0.4 0.6 0.4 NDS NDS 0.22 0.45 2.13
067 1.9 -0.95 -1.3 0.8 -2.6 0.1 NDS 1.6 NDS -0.28 1.68 0.57 X
071 2.4 -0.45 -0.6 -1.0 0.6 -2.3 -1.0 -0.7 0.0 -0.71 0.91 1.05
084 1.3 -1.55 -2.1 3 NDS -1.2 NDS 0.7 NDS NDS -0.87 1.43 N/A N/A
086 2.8 -0.05 -0.1 0.4 1.1 0.6 1.3 0.3 1.0 0.66 0.50 1.92
088 4.6 1.75 2.4 3 0.3 0.6 NDS 0.5 NDS 0.1 0.78 0.93 1.03
089 3.1 0.25 0.3 0.1 0.3 0.1 -1.5 0.0 0.1 -0.09 0.63 1.52
096 2.3 -0.55 -0.7 NDS NDS NDS NDS -2.2 R -1.45 1.06 N/A N/A
135 4.7 1.85 2.5 3 1.7 -2.6 -1.0 R NDS NDS 0.15 2.37 0.41 X
139 3.1 0.25 0.3 0.9 0.3 R NDS NDS -0.4 0.28 0.53 1.81
156 0.9 -1.95 -2.6 2, 3 R -2.6 NDS -3.2 R -2.2 -2.65 0.41 2.34
164 3.3 0.45 0.6 NDS NDS NDS -0.7 NDS -1.5 -0.53 1.06 N/A N/A
176 2.4 -0.45 -0.6 0.0 0.6 0.6 0.5 NDS -0.5 0.10 0.55 1.75
189 2.9 0.05 0.1 0.6 -0.2 -1.1 NDS NDS NDS -0.15 0.71 1.35
191 2.5 -0.35 -0.5 -0.5 0.6 0.9 NDS R -0.5 0.00 0.69 1.39
192 2.4 -0.45 -0.6 -1.4 -1.5 0.3 0.2 -1.2 -0.1 -0.61 0.76 1.26
193 2.4 -0.45 -0.6 -0.5 -0.7 -0.2 0.3 1.0 -0.8 -0.21 0.65 1.48
201 3.2 0.35 0.5 0.6 1.1 0.4 0.4 -0.4 1.6 0.60 0.62 1.55
210 2.6 -0.25 -0.3 -1.8 -0.4 -1.1 -2.1 2.0 -0.7 -0.63 1.34 0.72 X
213 2.9 0.05 0.1 -1.2 1.1 -1.5 0.5 0.0 0.3 -0.10 0.93 1.03
239 3.1 0.25 0.3 NDS 1.1 0.6 NDS -0.2 NDS 0.45 0.54 1.78
ASTM Crude Oil
Sample ID: CO1607
July 2016 62
Legend:
R = Rejected
TPI 0.85
Comments:
63
Sample ID: CO1607

2.96 5.81
2.22 5.07

Reproducibility
1.48 4.33
0.74 3.59
Deviation
0 2.85
-0.74 2.11
-1.48 1.37
Reproducibility

-2.22 0.63
-2.96 -0.11
2 1 8 3 1 6 9 1 1 1 7 1 4 1 2 2 8 6 1 2 4 2 1 1 2 2 8 2 1 2 3 1 1 7 5 2 2 8 1
9 5 4 4 7 7 6 9 7 9 1 4 1 9 1 2 6 5 8 1 6 2 3 2 3 0 9 0 6 3 3 0 7 5 0 7 8 3
6 3 6 2 4 1 0 9 3 0 9 8 9 1 4 7 6 5

64
Sample ID: CO1607

18
Median
1% 99%
15
12
Number of Labs
0
0.4 - 1.05 1.1 - 1.75 1.8 - 2.45 2.5 - 3.15 3.2 - 3.85 3.9 - 4.55 4.6 - 5.25
ASTM Crude Oil
Sample ID: CO1607
July 2016 65
Recovery wt%@193.3C (380F)
1603 1511 1507 1503 1411 1407
013 28.3 0.12 0.1 -0.1 -0.1 R 0.1 -0.2 0.2 0.00 0.15 5.80
015 ** 34.0 R 0.9 1.6 0.9 1.5 NDS NDS 1.23 0.38 2.29
017 26.9 -1.28 -0.9 -0.1 -1.0 -0.6 -0.3 -0.2 -0.2 -0.47 0.36 2.42
020 29.7 1.52 1.1 1.1 -0.5 0.2 0.4 -0.6 0.7 0.34 0.69 1.26
027 29.6 1.42 1.0 R -1.2 NDS NDS NDS NDS -0.10 1.56 N/A N/A
029 24.9 -3.28 -2.4 2, 3 NDS NDS NDS 0.3 NDS NDS -1.05 1.91 N/A N/A
034 27.0 -1.18 -0.9 NDS -1.5 0.4 -0.8 -0.2 0.3 -0.45 0.74 1.18
046 30.0 1.82 1.3 1.1 1.3 2.0 0.5 NDS NDS 1.24 0.54 1.61
055 ** 35.4 R 0.4 R -1.2 -0.6 NDS 0.2 -0.30 0.74 1.18
065 29.5 1.32 1.0 1.0 -1.1 0.3 -0.2 -1.9 1.0 0.01 1.15 0.76 X
067 25.4 -2.78 -2.0 2 0.3 -1.1 -0.2 NDS 0.1 NDS -0.58 0.96 0.91
071 26.8 -1.38 -1.0 -0.7 0.5 -1.5 -0.2 -0.4 -0.3 -0.51 0.64 1.36
077 28.1 -0.08 -0.1 -1.3 0.7 NDS NDS NDS NDS -0.23 1.01 N/A N/A
084 27.4 -0.78 -0.6 NDS -0.5 NDS 0.1 2.8 NDS 0.45 1.60 0.54 X
086 27.8 -0.38 -0.3 0.1 0.3 -0.2 0.6 0.0 1.0 0.21 0.46 1.89
088 29.3 1.12 0.8 -0.2 -0.1 NDS 0.4 NDS 0.4 0.26 0.41 2.12
089 27.8 -0.38 -0.3 R 0.2 -0.5 -1.6 -0.8 -0.4 -0.57 0.60 1.45
096 29.0 0.82 0.6 NDS -0.5 NDS NDS 0.1 -2.6 -0.60 1.41 0.62 X
107 29.7 1.52 1.1 NDS NDS 1.1 2.0 NDS NDS 1.40 0.52 N/A N/A
122 28.5 0.32 0.2 0.8 -0.7 0.5 NDS NDS NDS 0.20 0.65 1.34
128 26.1 -2.08 -1.5 2 0.2 NDS NDS NDS NDS NDS -0.65 1.20 N/A N/A
135 26.7 -1.48 -1.1 -2.7 1.0 1.4 -2.2 NDS NDS -0.72 1.85 0.47 X
139 29.4 1.22 0.9 1.3 1.9 R NDS NDS -0.5 0.90 1.02 0.85
156 26.3 -1.88 -1.4 -1.5 -2.2 NDS -1.6 0.5 1.4 -0.80 1.41 0.62 X
164 27.8 -0.38 -0.3 NDS NDS NDS -0.6 NDS -1.3 -0.73 0.51 N/A N/A
176 28.8 0.62 0.4 0.3 2.1 1.6 0.9 NDS -0.4 0.82 0.92 0.95
189 27.1 -1.08 -0.8 -0.1 -0.5 -0.5 NDS NDS NDS -0.48 0.29 3.00
191 29.0 0.82 0.6 0.3 0.5 0.9 NDS 2.6 -0.8 0.68 1.11 0.78 X
192 29.2 1.02 0.7 -0.1 -0.5 0.5 0.5 0.5 0.9 0.36 0.49 1.78
193 27.7 -0.48 -0.3 -0.2 0.0 0.4 0.8 0.5 0.0 0.17 0.40 2.17
201 25.5 -2.68 -1.9 2 -2.9 -1.7 -2.0 -2.5 -2.2 -2.4 -2.23 0.41 2.12
210 28.3 0.12 0.1 -0.5 -1.0 R -2.7 0.9 0.1 -0.52 1.25 0.70 X
213 28.7 0.52 0.4 -0.2 0.7 -0.3 0.7 -0.9 1.5 0.27 0.80 1.09
239 27.0 -1.18 -0.9 NDS -0.4 -1.0 NDS 0.3 NDS -0.50 0.59 1.47
ASTM Crude Oil
Sample ID: CO1607
July 2016 66
Legend:
R = Rejected
TPI 0.50
Comments:
67
Sample ID: CO1607

5.52 33.7
4.14 32.32
2.76 30.94

Reproducibility
1.38 29.56
Deviation
0 28.18
-1.38 26.8
Reproducibility
-2.76 25.42
-4.14 24.04
-5.52 22.66
2 6 2 1 1 1 7 1 3 2 1 8 1 1 8 8 7 1 2 3 1 2 4 2 2 1 9 1 1 8 1 6 1 2 2 2 1 2 4
9 7 0 2 5 3 1 7 4 3 8 4 9 6 9 6 7 3 1 2 3 1 0 1 7 6 9 9 8 3 5 4 2 7 0 0 2 6
1 8 6 5 9 9 3 4 0 2 6 3 6 1 2 9 4 7 0

68
Sample ID: CO1607

14
12
Median
1%
10
Number of Labs
0
24.15 - 25.05 25.1 - 26 26.05 - 26.95 27 - 27.9 27.95 - 28.85 28.9 - 29.8 29.85 - 30.75
ASTM Crude Oil
Sample ID: CO1607
July 2016 69
1603 1511 1507 1503 1411 1407
013 42.7 0.27 0.2 0.1 0.0 R 0.1 -0.4 0.4 0.07 0.27 3.15
015 ** 48.6 R 1.1 1.5 0.6 1.4 NDS NDS 1.15 0.40 2.12
017 41.7 -0.73 -0.5 -0.1 -1.0 -0.6 -0.2 -0.7 -0.1 -0.46 0.34 2.50
020 43.2 0.77 0.6 0.5 -0.5 0.1 0.2 -0.2 0.7 0.20 0.44 1.93
027 43.4 0.97 0.7 R -1.2 NDS NDS NDS NDS -0.25 1.34 N/A N/A
029 38.7 -3.73 -2.7 2, 3 NDS NDS NDS 0.1 NDS NDS -1.30 1.98 N/A N/A
034 41.3 -1.13 -0.8 NDS -1.1 0.3 -0.9 -1.1 -0.2 -0.63 0.56 1.52
046 45.0 2.57 1.9 2 1.3 1.1 2.3 0.5 NDS NDS 1.42 0.70 1.21
065 43.2 0.77 0.6 1.0 -0.9 0.3 -1.2 NDS NDS -0.04 0.96 0.89
067 38.6 -3.83 -2.8 2, 3 -0.1 -1.1 -0.7 NDS 0.1 NDS -0.92 1.15 0.74 X
071 40.8 -1.63 -1.2 -0.8 0.2 -1.4 -0.3 -0.9 -0.5 -0.70 0.55 1.55
084 41.1 -1.33 -1.0 NDS -0.4 NDS -0.2 1.8 NDS 0.05 1.22 0.70 X
086 42.2 -0.23 -0.2 0.1 -0.1 -0.3 0.4 -0.2 1.0 0.10 0.46 1.85
088 42.5 0.07 0.1 -0.3 0.0 NDS 0.4 NDS 0.4 0.12 0.29 2.93
089 42.6 0.17 0.1 R 0.7 -0.3 -1.4 -1.4 -0.2 -0.42 0.84 1.01
096 42.6 0.17 0.1 NDS -0.4 NDS NDS -0.7 -2.2 -0.80 0.99 0.86
122 42.6 0.17 0.1 0.4 -2.0 0.3 NDS NDS NDS -0.30 1.14 0.75 X
135 42.2 -0.23 -0.2 -2.8 1.3 1.9 -2.7 NDS NDS -0.50 2.19 0.39 X
139 43.6 1.17 0.9 1.4 1.2 R NDS NDS -0.8 0.68 1.00 0.85
156 40.6 -1.83 -1.3 -1.0 R NDS -1.8 -0.4 1.4 -0.62 1.24 0.69 X
164 42.4 -0.03 0.0 NDS NDS NDS -0.9 NDS -1.2 -0.70 0.62 N/A N/A
176 43.7 1.27 0.9 0.3 2.9 1.9 1.2 NDS -0.2 1.17 1.12 0.76 X
189 40.5 -1.93 -1.4 -0.2 -0.9 -0.5 NDS NDS NDS -0.75 0.52 1.63
191 43.4 0.97 0.7 0.6 0.5 0.9 NDS 0.7 -0.3 0.52 0.42 2.02
192 43.3 0.87 0.6 0.0 -0.7 0.6 0.5 0.2 0.8 0.29 0.51 1.67
193 41.6 -0.83 -0.6 -0.3 0.0 0.4 0.7 2.0 -0.1 0.30 0.86 0.99
201 39.2 -3.23 -2.4 2, 3 -3.3 -1.4 R R R R -2.37 0.95 N/A N/A
210 43.2 0.77 0.6 -0.2 -1.2 R R 1.1 0.7 0.20 0.91 0.93
213 43.1 0.67 0.5 -0.1 0.4 -0.2 0.6 R 0.8 0.33 0.40 2.12
239 41.8 -0.63 -0.5 NDS -0.8 -1.3 NDS -1.3 NDS -0.98 0.39 2.18
ASTM Crude Oil
Sample ID: CO1607
July 2016 70
Legend:
R = Rejected
TPI 0.54
Comments:
71
Sample ID: CO1607

5.48 47.91
4.11 46.54
2.74 45.17

Reproducibility
1.37 43.8
Deviation
0 42.43
-1.37 41.06
Reproducibility
-2.74 39.69
-4.11 38.32
-5.48 36.95
6 2 2 1 1 1 7 8 3 1 1 2 7 2 8 1 1 8 8 9 1 4 1 3 2 2 6 2 2 1 2 1 1 1 1 1 2 2 4
7 9 0 2 8 5 1 4 4 9 7 3 7 0 6 3 6 8 9 6 2 1 3 3 1 5 1 0 9 7 9 3 7 4 0 2 2 6
1 8 9 6 3 9 6 5 4 2 3 0 2 1 9 6 4 7 0

72
Sample ID: CO1607

18
Median
1% 99%
15
12
Number of Labs
0
37.65 - 38.8 38.85 - 40 40.05 - 41.2 41.25 - 42.4 42.45 - 43.6 43.65 - 44.8 44.85 - 46
ASTM Crude Oil
Sample ID: CO1607
July 2016 73
1603 1511 1507 1503 1411 1407
013 65.3 0.48 0.3 0.1 0.2 R 0.2 -0.2 0.5 0.18 0.23 4.30
015 ** 71.0 R NDS 0.7 0.3 1.2 NDS NDS 0.73 0.45 N/A N/A
017 64.5 -0.32 -0.2 -0.1 -0.8 -0.4 0.2 -0.8 0.0 -0.30 0.39 2.54
020 63.9 -0.92 -0.5 0.2 -0.5 -0.1 0.1 -0.4 0.7 -0.07 0.44 2.25
027 63.0 -1.82 -1.0 R -1.6 NDS NDS NDS NDS -1.30 0.42 N/A N/A
029 59.9 -4.92 -2.7 2, 3 NDS NDS NDS -0.5 NDS NDS -1.60 1.56 N/A N/A
034 64.3 -0.52 -0.3 NDS -0.4 0.1 -0.5 -0.8 -0.1 -0.33 0.31 3.19
046 67.5 2.68 1.5 2 1.5 1.3 2.1 0.6 NDS NDS 1.40 0.54 1.83
055 69.1 4.28 2.4 2, 3 0.4 -1.1 -1.4 -1.3 NDS -0.5 -0.25 1.46 0.68 X
065 65.4 0.58 0.3 0.8 -0.8 0.1 -2.4 0.9 0.9 -0.03 1.21 0.82
067 59.8 -5.02 -2.8 2, 3 -0.3 -0.5 -0.4 NDS 0.9 NDS -0.62 1.34 0.74 X
071 62.7 -2.12 -1.2 -1.3 -0.1 -1.2 -0.5 -0.5 -0.9 -0.81 0.46 2.15
077 64.8 -0.02 0.0 -2.0 1.2 NDS NDS NDS NDS -0.27 1.62 N/A N/A
084 62.7 -2.12 -1.2 NDS -0.3 NDS 1.0 R NDS -0.17 1.11 N/A N/A
086 64.6 -0.22 -0.1 0.0 -0.6 -0.4 0.1 0.0 0.8 -0.03 0.44 2.25
088 64.6 -0.22 -0.1 -0.5 0.2 NDS 0.4 NDS 0.5 0.10 0.41 2.41
089 66.2 1.38 0.8 3.2 1.5 -0.1 -0.5 -1.0 -0.1 0.54 1.43 0.69 X
096 64.5 -0.32 -0.2 NDS -0.3 NDS NDS -0.7 -1.9 -0.77 0.78 1.27
107 64.4 -0.42 -0.2 NDS NDS 2.4 1.9 NDS NDS 1.37 1.38 N/A N/A
122 64.6 -0.22 -0.1 -0.3 -3.1 -0.1 NDS NDS NDS -0.90 1.47 0.67 X
135 66.2 1.38 0.8 -3.4 1.9 1.6 -2.6 NDS NDS -0.34 2.48 0.40 X
139 66.2 1.38 0.8 1.4 0.8 2.4 NDS NDS -1.1 0.86 1.28 0.77 X
156 62.0 -2.82 -1.5 2 -0.8 R NDS -1.5 -0.7 1.4 -0.62 1.19 0.83
176 67.2 2.38 1.3 0.3 R 1.7 1.4 NDS -0.1 0.92 0.78 1.27
189 61.9 -2.92 -1.6 2 -0.6 -1.0 -0.4 NDS NDS NDS -0.90 0.53 1.87
191 65.3 0.48 0.3 1.2 1.1 0.6 NDS 0.8 -1.0 0.50 0.80 1.24
192 65.7 0.88 0.5 0.0 -0.4 0.6 0.5 0.0 0.8 0.29 0.43 2.30
193 63.9 -0.92 -0.5 -0.3 0.1 0.2 0.6 2.9 -0.3 0.39 1.17 0.85
201 61.6 -3.22 -1.8 2 R -1.1 R R R R -1.45 0.49 N/A N/A
210 66.2 1.38 0.8 0.1 -1.3 R R 1.0 0.9 0.30 0.96 1.03
213 66.0 1.18 0.6 0.1 0.6 0.0 0.6 -2.6 0.4 -0.04 1.15 0.86
239 65.3 0.48 0.3 NDS -0.7 -1.3 NDS -1.5 NDS -0.80 0.81 1.22
ASTM Crude Oil
Sample ID: CO1607
July 2016 74
Legend:
R = Rejected
TPI 0.45
Comments:
75
Sample ID: CO1607

7.28 72.1
5.46 70.28
3.64 68.46

Reproducibility
1.82 66.64
Deviation
0 64.82
-1.82 3 Sigma Range Limit ASTM Standard 63

Reproducibility
-3.64 61.18
-5.46 59.36
-7.28 57.54
6 2 2 1 1 7 8 2 1 2 1 2 3 1 1 9 8 8 1 7 3 1 2 1 6 4 2 1 1 2 1 1 8 2 2 1 1 4 2 5
7 9 0 8 5 1 4 7 2 0 9 0 4 0 7 6 6 8 2 7 9 3 3 5 1 3 9 6 1 3 3 9 1 2 4 7 6 2 5
1 9 6 8 6 3 7 2 1 9 2 4 3 9 5 0 4 6 0

76
Sample ID: CO1607

16
Median
14 1% 99%
12
10
Number of Labs
0
58.4 - 60.1 60.15 - 61.85 61.9 - 63.6 63.65 - 65.35 65.4 - 67.1 67.15 - 68.85 68.9 - 70.6
ASTM Crude Oil
Sample ID: CO1607
July 2016 77
Recovery wt%@426.7C(800F)
1603 1511 1507 1503 1411 1407
013 81.1 1.16 0.5 0.3 0.3 R 0.4 0.2 0.6 0.38 0.15 6.27
015 81.9 1.96 0.9 0.9 0.6 0.2 1.2 NDS NDS 0.76 0.38 2.47
017 80.2 0.26 0.1 -0.1 -0.5 -0.5 0.5 -0.8 0.3 -0.14 0.48 1.96
020 77.7 -2.24 -1.0 0.1 -0.6 -0.2 0.0 -0.6 0.6 -0.24 0.53 1.77
027 76.5 -3.44 -1.6 2 R -2.0 NDS NDS NDS NDS -1.80 0.28 N/A N/A
034 79.5 -0.44 -0.2 NDS -0.2 -0.1 -0.2 -0.4 -0.2 -0.22 0.10 9.40
046 82.5 2.56 1.2 1.3 1.1 2.0 0.7 NDS NDS 1.26 0.47 2.00
065 81.0 1.06 0.5 0.6 -0.7 0.0 -2.9 NDS NDS -0.50 1.44 0.65 X
067 73.5 -6.44 -2.9 2, 3 -0.6 -0.3 -0.5 NDS 0.8 NDS -0.70 1.35 0.70 X
071 77.3 -2.64 -1.2 -1.5 -0.3 -1.2 -0.5 -0.5 -1.2 -0.91 0.47 2.00
077 80.0 0.06 0.0 -2.2 1.4 NDS NDS NDS NDS -0.27 1.81 N/A N/A
084 77.9 -2.04 -0.9 NDS 0.1 NDS -0.8 0.1 NDS -0.38 0.55 1.71
086 79.9 -0.04 0.0 0.0 -0.7 -0.5 -0.1 0.3 0.7 -0.04 0.47 2.00
088 79.5 -0.44 -0.2 -0.5 0.3 NDS 0.6 NDS 0.4 0.12 0.45 2.09
089 81.7 1.76 0.8 2.2 1.7 0.0 0.0 -0.6 -0.1 0.57 1.04 0.90
096 80.2 0.26 0.1 NDS -0.1 NDS NDS -0.4 -1.8 -0.55 0.86 1.09
107 78.8 -1.14 -0.5 NDS NDS 2.5 1.6 NDS NDS 1.20 1.54 N/A N/A
122 80.0 0.06 0.0 -0.6 R -0.2 NDS NDS NDS -0.27 0.31 N/A N/A
135 82.0 2.06 0.9 -3.2 2.4 1.6 -2.4 NDS NDS -0.14 2.50 0.38 X
139 81.2 1.26 0.6 1.1 0.6 1.7 NDS NDS -1.1 0.58 1.04 0.90
156 76.8 -3.14 -1.4 2 -0.4 -3.4 NDS -1.2 -1.2 1.1 -1.08 1.46 0.64 X
176 83.1 3.16 1.4 2 0.4 R 1.8 1.7 NDS -0.1 1.04 0.84 1.12
189 76.5 -3.44 -1.6 2 -0.7 -1.2 -0.5 NDS NDS NDS -1.00 0.50 1.88
191 79.3 -0.64 -0.3 1.3 1.4 0.4 NDS 1.0 -0.9 0.48 0.93 1.01
192 80.9 0.96 0.4 0.7 -0.4 0.6 0.8 0.0 0.8 0.41 0.46 2.04
193 78.7 -1.24 -0.6 -0.4 0.2 0.2 0.7 2.9 -0.4 0.37 1.20 0.78 X
201 77.1 -2.84 -1.3 2 R -1.9 R R R R -1.60 0.42 N/A N/A
210 81.8 1.86 0.8 0.4 -1.5 R R 1.0 0.9 0.32 1.04 0.90
213 81.7 1.76 0.8 0.4 1.0 0.1 1.0 -1.5 0.8 0.37 0.89 1.06
239 81.2 1.26 0.6 NDS -0.6 -1.4 NDS -1.2 NDS -0.65 0.90 1.04
ASTM Crude Oil
Sample ID: CO1607
July 2016 78
Legend:
R = Rejected
TPI 0.43
Comments:
79
Sample ID: CO1607

8.76 88.7
6.57 86.51
4.38 84.32

Reproducibility
2.19 82.13
Deviation
0 79.94

Reproducibility
-4.38 75.56
-6.57 73.37
-8.76 71.18
6 2 1 2 1 2 7 2 8 2 1 1 1 3 8 1 8 7 1 9 3 1 1 2 6 1 2 1 4 2 1 1 8 2 2 1 1 4 1 2
7 9 8 7 5 0 1 0 4 0 9 0 9 4 8 2 6 7 2 6 7 9 3 5 3 3 3 1 2 6 4 9 1 1 5 3 6 7 2
9 6 1 6 3 7 1 8 2 2 9 9 4 4 3 0 5 6 0

80
Sample ID: CO1607

21
18
Median
1% 99%
15
Number of Labs
12
0
71.95 - 73.85 73.9 - 75.8 75.85 - 77.75 77.8 - 79.7 79.75 - 81.65 81.7 - 83.6 83.65 - 85.55
ASTM Crude Oil
Sample ID: CO1607
July 2016 81
1603 1511 1507 1503 1411 1407
003 93.9 -0.26 -0.1 0.5 -0.1 NDS NDS NDS NDS 0.10 0.35 N/A N/A
013 95.4 1.24 0.5 0.5 0.7 R 0.6 0.1 0.7 0.52 0.22 4.05
015 95.7 1.54 0.6 1.0 0.3 0.4 1.1 NDS NDS 0.68 0.36 2.47
017 94.5 0.34 0.1 0.1 -0.7 -0.5 0.7 -0.9 0.2 -0.14 0.57 1.56
020 90.6 -3.56 -1.5 2 -0.1 -0.6 -0.3 -0.1 -0.8 0.7 -0.39 0.68 1.31
027 87.6 -6.56 -2.7 2, 3 R -2.5 NDS NDS NDS NDS -2.60 0.14 N/A N/A
034 93.7 -0.46 -0.2 NDS 0.0 -0.1 0.4 0.0 -0.1 0.00 0.21 4.24
046 96.5 2.34 1.0 1.2 0.8 2.1 0.6 NDS NDS 1.14 0.58 1.53
055 96.1 1.94 0.8 0.7 NDS -1.6 -1.3 NDS -1.0 -0.48 1.14 0.78 X
065 95.2 1.04 0.4 0.6 -0.7 -0.1 -1.8 1.4 0.7 0.07 1.05 0.85
067 ** 86.0 R -0.9 -0.1 -0.4 NDS 1.0 NDS -0.10 0.80 1.11
071 90.6 -3.56 -1.5 2 -1.7 -0.5 -1.2 -0.5 R -1.4 -1.13 0.52 1.71
084 91.9 -2.26 -0.9 NDS 0.0 NDS -1.0 -0.5 NDS -0.60 0.45 1.98
086 93.6 -0.56 -0.2 0.2 -0.9 -0.5 0.0 0.0 0.6 -0.11 0.48 1.85
088 93.7 -0.46 -0.2 -0.6 0.2 NDS 0.6 NDS 0.4 0.08 0.48 1.85
089 96.0 1.84 0.8 1.4 2.1 0.6 0.7 -0.8 -0.1 0.67 0.94 0.95
096 94.7 0.54 0.2 NDS -0.2 NDS NDS -0.9 -1.8 -0.68 0.88 1.01
122 94.0 -0.16 -0.1 -0.8 R 0.1 NDS NDS NDS -0.27 0.47 N/A N/A
135 95.9 1.74 0.7 -3.4 3.0 2.3 -1.6 NDS NDS 0.20 2.68 0.33 X
139 94.7 0.54 0.2 0.7 0.1 1.0 NDS NDS -1.1 0.18 0.80 1.11
156 90.4 -3.76 -1.6 2 0.0 R NDS -1.2 -2.8 0.9 -0.94 1.43 0.62 X
176 97.7 3.54 1.5 2 0.5 R 1.8 1.6 NDS 0.2 1.12 0.72 1.24
189 89.8 -4.36 -1.8 2 -0.9 -1.3 -0.5 NDS NDS NDS -1.12 0.56 1.59
191 92.2 -1.96 -0.8 1.3 1.4 0.2 NDS 1.0 -1.0 0.35 1.06 0.84
192 95.1 0.94 0.4 0.2 -0.3 0.6 0.6 0.0 0.9 0.34 0.41 2.17
193 92.1 -2.06 -0.9 -0.4 0.3 0.2 0.3 2.5 0.1 0.30 1.07 0.83
201 91.6 -2.56 -1.1 R -1.3 R R R R -1.20 0.14 N/A N/A
210 96.0 1.84 0.8 0.7 -1.6 R R 0.7 0.8 0.28 1.05 0.85
213 95.8 1.64 0.7 0.7 0.9 0.4 1.1 0.9 1.0 0.81 0.23 3.87
239 95.5 1.34 0.6 NDS -0.5 -1.2 NDS -0.9 NDS -0.50 0.79 1.13
ASTM Crude Oil
Sample ID: CO1607
July 2016 82
Legend:
R = Rejected
TPI 0.45
Comments:
83
Sample ID: CO1607

9.64 103.8
7.23 101.39
4.82 98.98

Reproducibility
2.41 96.57
Deviation
0 94.16

Reproducibility
-4.82 89.34
-7.23 86.93
-9.64 84.52
2 2 1 1 2 7 2 2 8 1 1 8 3 8 3 1 7 1 1 9 2 4 1 6 1 1 1 2 2 1 2 1 1 8 2 5 1 4 1 2
9 7 8 5 0 1 0 0 4 9 9 6 4 8 2 7 7 3 6 3 1 9 5 2 4 3 3 2 5 1 3 6 9 1 5 0 6 7 2
9 6 6 1 3 1 2 9 2 8 4 9 3 5 4 0 7 6 0

84
Sample ID: CO1607

21
18
Median
1% 99%
15
Number of Labs
12
0
85.7 - 87.65 87.7 - 89.65 89.7 - 91.65 91.7 - 93.65 93.7 - 95.65 95.7 - 97.65 97.7 - 99.65
ASTM Crude Oil
Sample ID: CO1607
July 2016 85
Recovery wt% @596.1C (1105F)
1603 1511 1507 1503 1411 1407
013 97.0 1.42 0.6 0.5 0.8 3.0 0.7 0.2 0.7 0.93 0.93 0.98
015 97.2 1.62 0.7 1.1 0.3 0.4 1.1 NDS NDS 0.72 0.38 2.39
017 96.1 0.52 0.2 0.2 -0.6 -0.5 0.7 -1.0 0.2 -0.11 0.60 1.52
020 92.0 -3.58 -1.6 2 -0.1 -0.6 -0.3 -0.1 -0.9 0.7 -0.41 0.72 1.26
034 95.4 -0.18 -0.1 NDS 0.0 -0.2 0.4 0.2 0.0 0.05 0.22 4.14
046 97.5 1.92 0.8 1.2 0.7 1.7 0.6 NDS NDS 1.00 0.45 2.02
055 97.4 1.82 0.8 0.7 NDS -1.6 NDS NDS -0.9 -0.25 1.19 0.76 X
065 96.8 1.22 0.5 0.6 -0.6 -0.2 -1.5 NDS NDS -0.24 0.86 1.06
067 ** 87.3 R -1.1 0.0 -0.5 NDS 1.0 NDS -0.15 0.89 1.02
071 92.0 -3.58 -1.6 2 -1.7 -0.5 -1.2 -0.5 R -1.4 -1.15 0.53 1.72
084 93.8 -1.78 -0.8 NDS 0.0 NDS -1.0 -0.4 NDS -0.55 0.44 2.07
086 95.1 -0.48 -0.2 0.1 -0.9 -0.5 0.0 0.0 0.6 -0.13 0.48 1.90
088 95.4 -0.18 -0.1 -0.7 0.1 NDS 0.6 NDS 0.4 0.06 0.50 1.82
089 97.5 1.92 0.8 1.3 2.1 0.6 0.9 -0.7 0.0 0.71 0.90 1.01
096 96.3 0.72 0.3 NDS -0.1 NDS NDS -0.2 -1.8 -0.45 0.93 0.98
122 95.6 0.02 0.0 -0.8 R 0.1 NDS NDS NDS -0.23 0.49 N/A N/A
135 97.1 1.52 0.7 -3.5 2.8 2.0 -1.6 NDS NDS 0.08 2.60 0.35 X
139 96.2 0.62 0.3 0.5 0.1 0.7 NDS NDS -1.0 0.12 0.66 1.38
156 91.6 -3.98 -1.7 2 0.0 -2.8 NDS -1.1 -3.1 0.8 -1.32 1.54 0.59 X
189 91.3 -4.28 -1.9 2 -0.9 -1.2 -0.6 NDS NDS NDS -1.15 0.56 1.62
191 93.4 -2.18 -0.9 1.3 1.4 0.1 NDS 1.0 -1.0 0.32 1.08 0.84
192 96.7 1.12 0.5 0.2 -0.3 0.4 0.6 -0.1 0.5 0.26 0.34 2.68
193 93.5 -2.08 -0.9 -0.5 0.3 0.1 0.2 2.7 0.2 0.30 1.15 0.79 X
201 93.1 -2.48 -1.1 R -1.1 R R R R -1.10 0.00 N/A N/A
210 97.6 2.02 0.9 0.7 -1.5 R R 0.8 0.9 0.36 1.04 0.88
213 97.3 1.72 0.7 0.7 0.9 0.2 1.1 1.2 1.2 0.86 0.36 2.53
239 97.1 1.52 0.7 NDS -0.4 -1.0 NDS -0.8 NDS -0.38 0.76 1.20
ASTM Crude Oil
Sample ID: CO1607
July 2016 86
Legend:
R = Rejected
TPI 0.49
Comments:
87
Sample ID: CO1607

9.2 104.78
6.9 102.48
4.6 100.18

Reproducibility
2.3 97.88
Deviation
0 95.58
-2.3 93.28
Reproducibility
-4.6 90.98
-6.9 88.68
-9.2 86.38
2 2 1 1 7 2 2 2 1 1 8 8 3 8 3 1 7 1 1 9 2 1 4 2 6 1 1 1 2 1 1 2 1 5 4 8 2 1 2
9 7 8 5 1 0 0 0 9 9 4 6 8 4 2 7 7 3 6 3 9 1 2 5 2 4 3 3 3 5 1 6 5 6 9 1 0 2
9 6 6 1 1 3 2 9 2 8 4 9 5 3 4 0 7 0

88
Sample ID: CO1607

18
16
Median
14
12
Number of Labs
10
0
87.3 - 89.15 89.2 - 91.05 91.1 - 92.95 93 - 94.85 94.9 - 96.75 96.8 - 98.65 98.7 - 100.55
ASTM Crude Oil
Sample ID: CO1607
July 2016 89
Recovery wt%@720C(1328F)
1603 1511 1507 1503 1411 1407
003 97.6 -0.36 -0.1 0.4 -0.1 NDS NDS NDS NDS 0.07 0.29 N/A N/A
013 99.5 1.54 0.6 0.5 0.7 1.3 0.7 0.5 0.8 0.73 0.28 3.11
015 99.8 1.84 0.7 NDS 0.2 0.2 1.2 NDS NDS 0.57 0.48 1.81
017 99.1 1.14 0.5 0.3 -0.8 -0.9 0.7 -0.9 0.3 -0.11 0.72 1.21
020 94.3 -3.66 -1.5 2 0.0 -0.6 -0.6 -0.4 -0.7 0.7 -0.44 0.68 1.28
029 91.2 -6.76 -2.7 2, 3 NDS NDS NDS NDS NDS NDS -2.70 0.00 N/A N/A
034 99.1 1.14 0.5 NDS -0.9 -1.1 0.2 -0.2 0.1 -0.23 0.64 1.36
046 100.0 2.04 0.8 0.9 0.0 1.1 0.2 NDS NDS 0.60 0.47 1.85
055 100.0 2.04 0.8 NDS NDS NDS NDS NDS -1.3 -0.25 1.48 N/A N/A
065 99.7 1.74 0.7 0.9 -0.5 -0.2 0.2 1.8 1.4 0.61 0.84 1.04
067 98.4 0.44 0.2 -1.5 0.0 -0.5 NDS 0.9 NDS -0.18 0.89 0.98
071 94.5 -3.46 -1.4 2 -1.3 -0.4 -1.0 -0.5 -0.7 -1.3 -0.94 0.41 2.12
084 97.1 -0.86 -0.3 NDS -0.1 NDS -1.6 NDS NDS -0.67 0.81 N/A N/A
086 97.9 -0.06 0.0 0.2 -1.0 -0.8 -0.3 -0.1 0.6 -0.20 0.56 1.55
088 98.9 0.94 0.4 -0.6 -0.1 NDS 0.7 NDS 0.4 0.16 0.51 1.71
089 100.0 2.04 0.8 0.9 1.9 0.5 1.3 -0.6 0.0 0.69 0.82 1.06
096 100.0 2.04 0.8 NDS -0.1 NDS NDS -1.1 -1.5 -0.48 1.03 0.84
122 98.1 0.14 0.1 -0.6 R -0.1 NDS NDS NDS -0.20 0.36 N/A N/A
135 99.0 1.04 0.4 -3.9 2.2 1.6 -2.3 NDS NDS -0.40 2.61 0.33 X
139 99.3 1.34 0.5 0.2 0.1 0.6 NDS NDS -0.8 0.12 0.55 1.58
156 92.5 -5.46 -2.2 2, 3 -0.2 -1.8 NDS -1.7 R 0.9 -1.00 1.31 0.66 X
189 93.8 -4.16 -1.7 2 -0.6 -1.0 -0.6 NDS NDS NDS -0.98 0.52 1.67
192 99.3 1.34 0.5 R -0.3 0.1 0.6 -0.1 0.5 0.22 0.37 2.35
193 95.5 -2.46 -1.0 -0.3 0.4 0.2 -0.1 0.9 0.5 0.09 0.62 1.40
201 95.7 -2.26 -0.9 R -0.9 R R NDS R -0.90 0.00 N/A N/A
239 100.0 2.04 0.8 NDS -0.5 NDS NDS -0.6 NDS -0.10 0.78 N/A N/A
241 95.2 -2.76 -1.1 $ NDS NDS NDS NDS NDS -1.10 0.00 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 90
Legend:
R = Rejected
TPI 0.46
Comments:
91
Sample ID: CO1607

10.04 108
7.53 105.49
5.02 102.98

Reproducibility
2.51 100.47
Deviation
0 97.96

Reproducibility
-5.02 92.94
-7.53 90.43
-10.04 87.92
2 2 1 1 2 7 2 2 1 2 8 3 8 1 6 7 8 1 3 1 1 1 1 6 2 1 1 1 4 2 2 5 8 9 4
9 7 5 8 0 1 0 4 9 0 4 6 2 7 7 8 3 4 7 9 3 3 5 3 5 6 0 1 2 3 5 9 6 6
6 9 6 1 3 1 2 5 2 9 4 7 9

92
Sample ID: CO1607

14
Median 99%
12 1%
10
Number of Labs
0
89.7 - 91.65 91.7 - 93.65 93.7 - 95.65 95.7 - 97.65 97.7 - 99.65 99.7 - 101.65
ASTM Crude Oil 93
Sample ID: CO1607

July 2016
High Temperature Simulated Distillation - D7169
Lab Code IBP 5% 10% 20% 30% 40% 50% 60% 70% 80% 90% 95% FBP Total Weight % Recovery
@ 720C
003 <36.0 98.5 115.5 158.0 196.0 235.5 274.0 317.0 368.5 425.0 507.5 589.0 >720.0 97.6
007 15.2 ** 48.6 ** 84.2 145.9 190.1 230.2 270.2 315.6 368.8 424.4 494.8 545.7 632.9 --
013 44.0 98.3 118.6 158.9 197.3 236.7 273.1 317.0 367.4 420.8 493.6 558.4 733.0 99.5
015 26.8 ** 70.5 93.3 ** 133.7 ** 173.6 215.9 253.8 299.0 335.3 415.9 488.4 552.9 >720.0 99.8
017 48.2 ** 123.8 138.8 169.6 201.2 241.0 278.0 320.6 370.6 425.8 503.6 574.8 -- 99.1
020 36.1 98.3 118.3 157.8 194.4 235.0 275.0 322.2 378.3 440.6 553.9 -- 683.9 94.3
022 65.2 98.5 119.5 157.3 195.0 234.4 269.7 312.6 360.6 415.7 487.2 551.9 672.8 102.0
023 61.0 93.5 115.5 159.5 197.0 235.5 271.5 315.5 367.0 421.0 498.0 567.5 703.0 99.8
026 52.7 ** 70.6 ** 84.0 ** 132.2 189.3 232.5 270.3 313.4 363.2 419.6 494.8 560.8 717.7 99.8
027 54.9 84.7 104.0 149.9 196.3 234.4 279.6 326.4 383.9 456.2 ** 632.8 >720.0 >720.0 91.4
029 58.6 ** 126.2 140.8 174.3 ** 213.8 253.9 295.7 343.8 402.0 470.1 ** 628.7 -- -- 91.21
034 74.5 100.6 124.3 163.3 203.5 243.9 280.8 322.8 372.9 429.5 512.2 587.4 720.0 99.16
041 -- 97.1 117.9 159.1 196.1 235.8 272.4 315.9 366.2 420.0 494.8 563.6 707.2 100
042 31.1 77.8 ** 90.6 ** 112.5 ** 135.1 ** 160.3 ** 189.4 ** 221.5 ** 273.8 -- -- -- -- --
046 37.2 98.9 114.0 151.8 193.5 230.4 267.1 307.3 356.0 411.4 481.2 542.7 643.0 100
054 59.5 99.2 121.0 158.6 196.1 235.4 271.7 315.9 365.7 420.2 493.5 560.6 690.3 --
055 62.6 98.4 107.9 ** 128.7 ** 167.1 ** 212.2 254.0 296.9 345.6 405.8 479.6 544.9 680.4 100
065 36.1 98.4 119.3 157.2 195.9 236.4 272.6 315.1 367.4 420.7 493.2 559.4 -- 99.7
067 71.8 101.7 127.7 167.8 ** 213.7 254.1 296.7 344.9 404.4 ** 479.3 444.5 -- ** 1328.0 89.4
071 38.7 99.9 125.7 163.1 202.5 246.2 285.9 329.8 383.7 445.7 554.6 -- -- 94.5
077 37.2 96.6 117.1 160.0 196.7 238.9 276.7 319.6 370.4 426.9 505.8 580.3 720.0 98.72
083 78.9 96.7 110.0 150.5 190.0 230.0 266.7 308.3 355.6 410.6 482.8 546.1 653.9 --
084 40.3 102.4 127.4 163.6 202.4 246.9 285.6 329.6 381.3 440.5 540.2 651.9 ** 96.0 96.0
086 37.4 105.2 127.1 161.7 197.2 238.4 276.6 319.6 370.8 427.5 511.2 593.2 720.0 97.9
087 55.8 104.4 125.6 164.4 200.8 243.3 278.8 318.7 369.2 421.9 493.1 559.8 711.2 99.6
088 40.0 85.0 111.5 156.0 194.0 237.0 277.0 320.5 372.5 430.0 515.0 588.0 >720.0 98.9
089 32.0 97.3 119.2 160.7 197.6 237.4 273.4 315.1 364.6 417.4 487.8 549.4 659.6 100.0
090 25.2 89.8 110.2 154.6 191.6 232.2 269.1 310.1 360.1 413.4 486.1 549.2 677.9 --
092 43.9 ** 120.3 137.1 172.6 ** 213.9 254.3 ** 301.9 ** 355.9 ** 416.9 ** 501.9 -- -- 745.6 ** 87.97
096 67.0 99.6 123.3 157.3 194.2 236.3 277.2 320.9 371.6 425.3 501.7 570.2 714.3 100.00
102 74.5 101.8 122.9 162.1 205.6 251.4 299.9 ** 362.1 ** 438.8 ** 552.1 -- -- 710.7 ** 88.08
107 68.0 96.5 114.0 155.0 193.5 232.5 269.0 312.0 381.5 431.5 485.0 544.5 689.5 100
122 -- -- -- 155.8 196.7 236.3 272.9 317.0 368.4 422.7 500.2 570.3 -- 98.5
ASTM Crude Oil 94
Sample ID: CO1607

July 2016
@ 720C
128 36.1 98.4 125.7 167.5 207.5 248.1 285.5 327.3 376.3 428.9 500.9 564.5 698.8 100
135 12.2 85.3 129.4 163.1 199.8 237.4 272.3 313.6 359.8 410.8 478.6 534.4 664.3 ** 74.5
137 ** 167.8 ** 172.2 ** 182.8 ** 218.3 ** 251.7 ** 281.1 ** 312.8 ** 347.2 385.6 427.8 485.6 ** 827.2 577.2 100
139 33.5 96.2 113.2 155.5 193.7 233.0 268.7 312.3 360.8 416.4 492.2 561.8 595.1 103.7
144 64.3 95.7 119.9 160.2 195.2 232.9 270.0 312.6 363.2 417.5 493.6 560.2 683.3 99.0
150 37.7 89.4 112.8 152.7 193.2 232.8 268.6 313.6 365.2 421.4 501.7 577.0 577.0 --
156 80.7 108.2 129.0 165.5 208.3 248.5 287.4 331.5 387.5 448.2 562.1 626.7 720.0 92.5
159 44.9 88.1 104.8 152.2 194.7 234.2 271.1 315.5 366.9 421.7 499.5 564.4 676.1 100.0
161 34.8 97.5 113.7 151.6 190.8 230.7 268.5 309.5 358.3 414.0 485.6 547.0 711.3 100
164 36.0 98.8 117.0 159.4 198.0 237.6 273.4 316.2 364.8 418.2 489.0 549.6 674.4 100
166 <36.1 98.8 116.3 158.8 196.3 236.1 273.5 317.1 368.6 425.6 506.3 584.6 >720.0 98.27
168 45.5 77.0 110.9 157.4 196.2 246.9 289.1 328.8 380.8 454.4 541.5 647.8 >720.0 --
176 70.4 100.0 124.8 161.1 198.8 241.2 279.6 322.7 374.5 430.7 517.1 602.6 717.9 97.7
189 39.7 99.8 122.6 161.7 201.2 246.8 287.0 331.2 388.5 450.8 568.7 -- -- 93.84
191 69.0 98.8 116.9 156.5 194.3 233.4 272.2 315.6 370.4 431.2 531.2 638.3 715.9 --
192 51.4 100.2 116.6 155.6 195.6 234.8 271.4 315.2 365.5 421.6 496.8 563.9 685.0 99.3
193 37.8 100.5 123.4 160.5 196.9 241.1 279.9 324.2 377.0 434.6 528.8 649.8 >720.0 95.5
201 36.1 98.4 123.4 168.5 210.7 252.8 289.8 333.9 386.7 444.9 540.7 655.4 -- 95.8
206 52.4 88.4 112.9 156.6 198.1 237.6 278.7 324.2 379.7 440.4 547.4 ** 711.8 722.0 95.1
210 67.4 98.8 124.5 158.8 195.8 234.9 271.1 314.9 362.9 416.8 486.6 547.8 655.0 --
212 39.5 74.3 111.5 149.9 188.4 228.9 265.8 305.8 355.2 409.8 478.5 537.4 650.3 --
213 56.1 98.9 117.2 157.8 196.1 235.6 270.6 315.6 364.4 417.2 487.8 551.7 680.6 --
214 20.3 99.0 115.5 157.1 196.0 235.0 271.4 314.9 363.2 418.0 490.5 556.5 669.1 100
219 36.8 86.0 114.9 157.8 195.9 240.2 280.0 325.4 378.2 450.3 535.7 649.4 688.8 --
220 43.0 99.5 117.0 156.0 195.5 233.5 268.5 307.0 354.0 404.5 466.5 516.5 596.0 99
230 37.8 100.0 116.1 157.2 196.1 235.6 271.1 315.0 363.3 418.3 491.7 556.1 681.7 100
239 36.0 101.0 123.5 162.5 200.0 240.5 276.5 317.0 367.5 420.0 493.0 557.0 693.0 100.0
240 36.1 98.8 124.1 165.9 212.4 253.1 294.8 342.8 399.1 466.9 ** 591.0 ** 676.1 720.0 94.5
241 20.8 ** 38.4 ** 52.8 ** 72.2 ** 92.0 ** 115.4 ** 136.8 ** 161.2 ** 190.3 ** 221.8 ** 271.6 ** 324.0 ** 1328.0 95.17
ASTM Crude Oil 95
Sample ID: CO1607

July 2016
@ 720C
No. Valid Results 57 53 56 56 54 58 58 57 58 57 55 49 44 47
Robust Mean 46.41 97.40 118.93 158.97 196.73 238.00 275.21 318.18 369.95 425.42 500.87 566.85 687.33 98.26
Robust Standard Deviation 17.58 4.43 7.16 5.18 3.94 6.61 7.51 8.04 10.93 12.51 20.39 23.99 33.25 2.63
Reproducibility ASTM Standard *(1) *(1) 19.50 *(1) *(1) *(1) *(1) *(1) *(1) *(1) *(1) *(1) *(1) *(1)
Reproducibility These Test Data 48.70 12.27 19.83 14.35 10.91 18.31 20.80 22.27 30.28 34.65 56.48 66.45 92.10 7.29
*(1) ASTM Reproducibility not defined for this Robust Mean value.
ASTM Crude Oil
Sample ID: CO1607
July 2016 96
Temperature C at 10% Weight Recovery
1603 1511 1507 1503 1411 1407
003 115.5 -3.43 -0.5 -0.8 0.2 0.3 -0.9 0.2 -0.6 -0.30 0.52 1.94
013 118.6 -0.33 0.0 0.4 -0.3 R 0.0 0.0 -0.5 -0.07 0.31 3.26
015 93.3 -25.63 -3.6 1, 2, 3 -1.0 -2.1 -1.6 -1.9 NDS NDS -2.04 0.97 1.04
017 138.8 19.87 2.8 3 0.2 0.9 0.7 0.8 -0.1 0.3 0.80 0.95 1.06
020 118.3 -0.63 -0.1 -0.6 0.3 -0.3 -0.6 0.0 -0.7 -0.29 0.37 2.73
022 119.5 0.57 0.1 NDS NDS -0.4 -0.5 NDS NDS -0.27 0.32 N/A N/A
026 ** 84.0 R -3.4 NDS -1.0 NDS NDS NDS -2.20 1.70 N/A N/A
027 104.0 -14.93 -2.1 3 R 1.1 NDS NDS NDS NDS -0.50 2.26 N/A N/A
029 140.8 21.87 3.1 1, 2, 3 NDS NDS NDS NDS NDS NDS 3.10 0.00 N/A N/A
034 124.3 5.37 0.8 NDS 1.1 -1.0 0.1 0.2 -0.5 0.12 0.78 1.29
042 ** 90.6 R -0.6 NDS NDS NDS NDS NDS -0.60 0.00 N/A N/A
046 114.0 -4.93 -0.7 -0.2 -1.4 -2.1 -0.4 NDS NDS -0.96 0.78 1.29
054 121.0 2.07 0.3 0.5 -0.5 R NDS -0.5 R -0.05 0.53 1.91
055 107.9 -11.03 -1.5 0.4 3.6 1.5 0.7 0.8 -0.6 0.70 1.62 0.62 X
065 119.3 0.37 0.1 -0.6 1.0 -0.5 -0.6 1.9 -0.6 0.10 0.99 1.02
067 127.7 8.77 1.2 -1.1 0.9 0.4 0.3 -0.3 NDS 0.23 0.83 1.22
071 125.7 6.77 0.9 0.9 -0.6 1.5 0.7 0.3 -0.3 0.49 0.74 1.36
077 117.1 -1.83 -0.3 0.4 -1.0 1.3 R -0.2 0.3 0.08 0.78 1.29
083 110.0 -8.93 -1.2 0.0 -0.8 -2.8 -0.9 NDS -0.7 -1.07 0.94 1.07
084 127.4 8.47 1.2 NDS 0.4 0.6 -0.5 R -0.2 0.30 0.67 1.51
086 127.1 8.17 1.1 -0.2 -0.4 0.2 -0.8 -0.2 -0.6 -0.13 0.63 1.60
087 125.6 6.67 0.9 0.4 0.6 0.6 0.7 3.1 0.9 1.03 0.93 1.09
088 111.5 -7.43 -1.0 -0.2 -0.2 -0.3 -0.4 -0.2 -0.4 -0.39 0.29 3.48
089 119.2 0.27 0.0 0.1 -0.7 0.4 2.9 0.5 -0.5 0.39 1.19 0.85
090 110.2 -8.73 -1.2 -1.3 -0.6 -0.3 -0.8 -1.0 -0.7 -0.84 0.35 2.89
092 137.1 18.17 2.5 3 NDS R NDS NDS -1.5 NDS 0.50 2.83 N/A N/A
096 123.3 4.37 0.6 NDS 0.3 NDS NDS -0.4 1.8 0.57 0.92 1.10
102 122.9 3.97 0.6 -0.1 0.5 1.3 1.4 1.3 0.5 0.79 0.56 1.80
107 114.0 -4.93 -0.7 -2.1 NDS -0.6 -1.6 NDS NDS -1.25 0.72 1.40
135 129.4 10.47 1.5 -2.0 -0.8 -1.2 R NDS NDS -0.62 1.50 0.67 X
137 ** 182.8 R NDS NDS NDS NDS -3.1 R -3.10 0.00 N/A N/A
139 113.2 -5.73 -0.8 -1.3 -2.7 R NDS NDS -0.6 -1.35 0.95 1.06
144 119.9 0.97 0.1 NDS R -2.1 0.7 NDS NDS -0.43 1.47 N/A N/A
150 112.8 -6.13 -0.9 -0.7 R -0.3 -0.4 1.2 -0.5 -0.27 0.75 1.35
156 129.0 10.07 1.4 2.7 3.1 NDS 2.7 -0.7 -0.7 1.42 1.74 0.58 X
159 104.8 -14.13 -2.0 2.4 0.3 -0.2 -0.6 -0.5 -0.8 -0.20 1.35 0.75 X
161 113.7 -5.23 -0.7 -2.3 NDS -0.4 0.6 NDS NDS -0.70 1.20 0.84
164 117.0 -1.93 -0.3 NDS 0.4 NDS 0.7 NDS 1.3 0.52 0.67 1.51
166 116.3 -2.63 -0.4 0.3 0.1 -2.7 0.8 -3.4 0.9 -0.63 1.72 0.59 X
168 110.9 -8.03 -1.1 NDS 0.4 -0.6 NDS R -2.3 -0.90 1.12 0.90
176 124.8 5.87 0.8 0.4 -0.9 -0.5 -0.4 NDS 0.3 -0.05 0.65 1.55
ASTM Crude Oil
Sample ID: CO1607
July 2016 97
1603 1511 1507 1503 1411 1407
189 122.6 3.67 0.5 -0.7 0.6 0.5 NDS NDS NDS 0.22 0.62 1.63
191 116.9 -2.03 -0.3 -0.3 -0.7 -1.1 -0.4 -2.8 0.5 -0.73 1.03 0.98
192 116.6 -2.33 -0.3 0.6 0.4 -0.9 -0.2 -1.0 -0.3 -0.24 0.60 1.68
193 123.4 4.47 0.6 0.4 -0.2 -0.4 -0.4 -0.7 0.2 -0.07 0.48 2.10
201 123.4 4.47 0.6 -0.6 1.7 1.1 -0.6 1.1 -0.9 0.34 1.03 0.98
210 124.5 5.57 0.8 1.0 1.1 R 3.0 -1.5 0.2 0.77 1.46 0.69 X
212 111.5 -7.43 -1.0 -1.0 1.7 R 1.4 NDS NDS 0.27 1.48 0.68 X
213 117.2 -1.73 -0.2 0.7 -0.7 0.5 -0.5 0.0 -0.6 -0.11 0.55 1.84
214 115.5 -3.43 -0.5 0.4 0.8 0.0 0.5 NDS NDS 0.24 0.50 2.02
220 117.0 -1.93 -0.3 0.7 NDS -0.1 -0.2 R NDS 0.02 0.46 2.20
230 116.1 -2.83 -0.4 -0.7 -0.6 -0.1 -0.5 -0.2 -0.6 -0.44 0.22 4.59
239 123.5 4.57 0.6 NDS 0.4 1.2 NDS -0.2 NDS 0.50 0.58 1.74
241 ** 52.8 R -2.7 3.7 -0.2 NDS 0.5 1.1 0.48 2.31 0.44 X

Legend:
R = Rejected
TPI 0.98
Comments:
The following labs have been converted for statistical analysis.

Labs: 042, 054, 137
98
Sample ID: CO1607

28.64 147.57
21.48 140.41
Reproducibility
14.32 133.25
7.16 126.09
Deviation
0 118.93
-7.16 111.77
-14.32 104.61

Reproducibility
-21.48 97.45
-28.64 90.29
1 2 1 5 8 9 1 8 2 1 2 1 1 1 4 2 2 2 3 2 1 1 1 2 1 7 2 4 2 1 8 6 2 1 5 1 1 9 2 1 2 2 3 2 1 8 1 7 8 8 6 1 1 9 1 2
5 7 5 5 3 0 6 8 1 5 0 3 6 0 6 1 1 3 3 6 9 9 2 6 7 1 1 0 3 9 5 2 4 4 8 0 6 0 9 3 4 4 1 7 7 2 1 6 4 7 5 3 2 7 9
9 8 2 0 6 9 1 7 9 4 0 6 2 1 0 4 3 4 9 2 1 3 9 0 0 6 8 6 5

99
Sample ID: CO1607

24
Median
20
16
Number of Labs
12
0
87.3 - 94.7 94.75 - 102.15 102.2 - 109.6 109.65 - 117.05 117.1 - 124.5 124.55 - 131.95 132 - 139.4 139.45 - 146.85
ASTM Crude Oil
Sample ID: CO1607
July 2016 100
1603 1511 1507 1503 1411 1407
003 274.0 -1.21 -0.2 -0.7 0.5 0.5 0.0 1.0 -0.2 0.13 0.57 1.60
013 273.1 -2.11 -0.3 -0.2 -0.1 R -0.1 -0.1 -0.4 -0.20 0.13 7.00
015 253.8 -21.41 -2.9 3 -1.1 -0.4 -0.2 -1.3 NDS NDS -1.18 1.07 0.85
017 278.0 2.79 0.4 0.0 0.8 0.5 -0.1 0.3 -0.1 0.26 0.34 2.68
020 275.0 -0.21 0.0 -0.6 0.8 0.2 0.0 0.0 -0.7 -0.04 0.50 1.82
022 269.7 -5.51 -0.7 NDS NDS -0.4 -0.7 NDS NDS -0.60 0.17 N/A N/A
026 270.3 -4.91 -0.7 R NDS -1.1 NDS NDS NDS -0.90 0.28 N/A N/A
027 279.6 4.39 0.6 $ 2.6 NDS NDS NDS NDS 1.60 1.41 N/A N/A
034 280.8 5.59 0.7 NDS 0.3 0.1 0.7 0.4 -0.1 0.35 0.32 2.84
046 267.1 -8.11 -1.1 -1.2 -0.8 -1.7 -0.6 NDS NDS -1.08 0.42 2.17
054 271.7 -3.51 -0.5 0.4 -3.1 R NDS -1.0 R -1.05 1.48 0.61 X
055 254.0 -21.21 -2.8 3 -0.5 0.3 2.0 1.8 3.2 0.4 0.63 1.96 0.46 X
065 272.6 -2.61 -0.3 -1.2 0.8 0.0 R -0.8 -1.0 -0.42 0.74 1.23
067 296.7 21.49 2.9 3 -0.2 0.3 0.4 -1.0 -1.0 NDS 0.23 1.44 0.63 X
071 285.9 10.69 1.4 0.8 0.5 1.3 0.8 0.2 0.7 0.81 0.42 2.17
077 276.7 1.49 0.2 1.5 -1.1 0.6 R 0.0 -0.2 0.17 0.86 1.06
083 266.7 -8.51 -1.1 -0.8 -1.4 -2.6 -1.8 NDS -1.3 -1.50 0.63 1.44
084 285.6 10.39 1.4 NDS 0.2 0.3 0.7 -1.1 0.1 0.27 0.82 1.11
086 276.6 1.39 0.2 -0.2 0.9 0.5 0.0 -0.3 -0.9 0.03 0.58 1.57
087 278.8 3.59 0.5 0.1 0.8 0.4 0.0 0.7 0.9 0.49 0.34 2.68
088 277.0 1.79 0.2 0.2 -0.1 0.3 -0.3 0.2 -0.4 0.01 0.28 3.25
089 273.4 -1.81 -0.2 R -1.3 0.0 0.8 0.6 0.1 0.00 0.74 1.23
090 269.1 -6.11 -0.8 -0.9 0.1 0.1 -0.3 -0.6 0.0 -0.34 0.43 2.12
092 ** 301.9 R NDS R NDS NDS -0.8 NDS -0.80 0.00 N/A N/A
096 277.2 1.99 0.3 NDS 0.3 NDS NDS 0.3 1.9 0.70 0.80 1.14
102 299.9 24.69 3.3 1, 3 0.6 0.3 2.5 0.2 3.5 -0.3 1.44 1.60 0.57 X
107 269.0 -6.21 -0.8 -2.2 NDS -2.0 -2.1 NDS NDS -1.78 0.66 1.38
122 272.9 -2.31 -0.3 -0.4 R 0.2 NDS NDS R -0.17 0.32 N/A N/A
135 272.3 -2.91 -0.4 1.0 -1.3 -1.1 1.0 NDS NDS -0.16 1.11 0.82
137 ** 312.8 R NDS NDS NDS NDS 0.7 1.7 1.20 0.71 N/A N/A
139 268.7 -6.51 -0.9 -1.8 -0.6 -1.8 NDS NDS 0.8 -0.86 1.07 0.85
144 270.0 -5.21 -0.7 NDS R -1.5 -0.5 NDS NDS -0.90 0.53 N/A N/A
150 268.6 -6.61 -0.9 0.5 R 0.3 0.3 0.5 -0.1 0.10 0.54 1.69
156 287.4 12.19 1.6 0.8 R NDS 2.1 0.3 -1.3 0.70 1.32 0.69 X
159 271.1 -4.11 -0.5 0.7 0.8 0.7 0.2 -0.4 1.1 0.37 0.62 1.47
161 268.5 -6.71 -0.9 -1.6 NDS 0.4 0.0 NDS NDS -0.52 0.90 1.01
164 273.4 -1.81 -0.2 NDS 0.8 NDS 1.3 NDS 1.0 0.73 0.65 1.40
166 273.5 -1.71 -0.2 -0.3 0.2 -0.6 1.3 -0.9 0.4 -0.01 0.73 1.25
168 289.1 13.89 1.8 NDS 0.7 0.6 NDS -2.7 -1.5 -0.22 1.83 0.50 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 101
1603 1511 1507 1503 1411 1407
176 279.6 4.39 0.6 -0.4 -1.4 -0.4 -0.9 NDS 0.1 -0.40 0.71 1.28
189 287.0 11.79 1.6 0.1 1.4 0.5 NDS NDS NDS 0.90 0.72 1.26
191 272.2 -3.01 -0.4 -0.8 -1.0 -0.4 -1.2 -0.8 1.1 -0.50 0.76 1.20
192 271.4 -3.81 -0.5 -0.2 0.5 -0.6 -0.6 -0.6 -0.9 -0.41 0.45 2.02
193 279.9 4.69 0.6 0.2 0.0 -0.2 -0.7 -2.5 0.1 -0.36 1.02 0.89
201 289.8 14.59 1.9 R 2.2 0.8 0.9 0.3 -1.6 0.75 1.35 0.67 X
210 271.1 -4.11 -0.5 0.1 1.8 R R -1.3 -0.7 -0.12 1.18 0.77 X
212 265.8 -9.41 -1.3 -0.9 -0.3 -1.9 -0.5 NDS NDS -0.98 0.64 1.42
213 270.6 -4.61 -0.6 -0.1 -0.7 -0.2 -0.7 2.6 -0.7 -0.06 1.20 0.76 X
214 271.4 -3.81 -0.5 -0.3 1.7 0.4 0.4 NDS NDS 0.34 0.86 1.06
220 268.5 -6.71 -0.9 3.0 NDS -0.7 -0.2 R NDS 0.30 1.82 0.50 X
230 271.1 -4.11 -0.5 -0.5 0.3 0.5 0.2 0.3 -0.7 -0.06 0.49 1.86
239 276.5 1.29 0.2 NDS 0.8 1.7 NDS 0.9 NDS 0.90 0.62 1.47
241 ** 136.8 R -1.4 R -1.1 NDS 0.7 1.1 -0.18 1.26 0.72 X

Legend:
R = Rejected
TPI
Comments:
The ASTM Reproducibility in D7169 for 50% is applicable in the range from 285 to 325. The Robust Mean is outside this range, therefore
ASTM Reproducibility not determined.
Labs: 042, 054, 137
102
Sample ID: CO1607

30.04 305.25
22.53 297.74
15.02 290.23
7.51 282.72
Deviation
0 275.21
-7.51 267.7
-15.02 260.19
-22.53 252.68
-30.04 245.17
1 5 2 8 4 1 2 1 1 1 9 2 1 7 2 2 1 2 2 1 2 2 5 1 1 4 6 1 1 8 1 1 3 2 2 8 7 8 9 1 2 8 1 2 1 2 3 1 8 7 1 1 1 2 2 2 6 1
5 5 1 3 6 6 2 5 3 0 0 2 4 6 1 5 1 3 9 1 3 4 9 3 1 5 2 3 9 6 6 0 3 6 7 8 6 7 0 7 7 7 9 1 4 2 4 1 8 5 6 0 4 9 7 0
2 1 0 0 9 7 4 3 9 0 0 2 4 1 5 2 4 6 9 6 6 3 9 8 9 6 8 1 0 2

103
Sample ID: CO1607

28
Median
24
20
Number of Labs
16
12
0
247.95 - 255.15 255.2 - 262.4 262.45 - 269.65 269.7 - 276.9 276.95 - 284.15 284.2 - 291.4 291.45 - 298.65 298.7 - 305.9
ASTM Crude Oil
Sample ID: CO1607
July 2016 104
1603 1511 1507 1503 1411 1407
003 507.5 6.63 0.3 -0.5 0.8 $ 0.3 1.3 0.1 0.38 0.61 1.49
013 493.6 -7.27 -0.4 -0.4 -0.3 -2.1 -0.5 -0.3 -0.5 -0.64 0.65 1.40
015 488.4 -12.47 -0.6 -0.8 0.4 NDS -1.0 NDS NDS -0.50 0.62 1.47
017 503.6 2.73 0.1 0.0 NDS NDS -0.6 0.7 0.0 0.04 0.46 1.98
020 553.9 53.03 2.6 3 0.0 NDS NDS 0.7 0.6 -0.5 0.68 1.18 0.77 X
022 487.2 -13.67 -0.7 NDS NDS NDS 0.0 NDS NDS -0.35 0.49 N/A N/A
026 494.8 -6.07 -0.3 -2.9 NDS -0.2 NDS NDS NDS -1.13 1.53 N/A N/A
027 ** 632.8 R $ $ NDS NDS NDS NDS 0.00 0.00 N/A N/A
034 512.2 11.33 0.6 NDS NDS NDS -0.2 -0.1 0.3 0.15 0.37 2.46
046 481.2 -19.67 -1.0 -0.8 0.3 -0.3 -0.4 NDS NDS -0.44 0.50 1.82
054 493.5 -7.37 -0.4 0.0 -2.9 R NDS -0.9 R -1.05 1.29 0.71 X
055 479.6 -21.27 -1.0 -0.5 0.0 NDS NDS R 1.8 0.08 1.22 0.75 X
065 493.2 -7.67 -0.4 -0.5 NDS 1.0 1.0 -1.5 -0.5 -0.15 0.98 0.93
067 444.5 -56.37 -2.8 3 0.8 0.5 NDS -1.1 -1.0 NDS -0.72 1.44 0.63 X
071 554.6 53.73 2.6 3 1.6 1.1 NDS 0.9 0.5 2.5 1.53 0.86 1.06
077 505.8 4.93 0.2 2.7 -0.8 NDS 1.3 -0.1 -0.4 0.48 1.30 0.70 X
083 482.8 -18.07 -0.9 -0.7 -1.4 -2.3 -1.6 NDS -1.1 -1.33 0.58 1.57
084 540.2 39.33 1.9 NDS 0.7 NDS NDS 0.8 1.4 1.20 0.56 1.62
086 511.2 10.33 0.5 -0.1 NDS NDS 0.5 -0.2 -0.4 0.06 0.42 2.17
087 493.1 -7.77 -0.4 -0.6 NDS NDS 0.1 -0.2 -0.2 -0.26 0.26 3.50
088 515.0 14.13 0.7 0.6 0.6 $ -0.4 -0.3 -0.2 0.17 0.52 1.75
089 487.8 -13.07 -0.6 -1.4 -1.4 1.0 -0.8 0.7 0.3 -0.31 0.98 0.93
090 486.1 -14.77 -0.7 -0.7 0.6 NDS 0.0 -0.7 0.5 -0.17 0.62 1.47
096 501.7 0.83 0.0 NDS 0.7 NDS NDS 0.8 3.3 1.20 1.44 0.63 X
107 485.0 -15.87 -0.8 -1.4 NDS -1.1 -1.5 NDS NDS -1.20 0.32 2.84
122 500.2 -0.67 0.0 0.7 NDS NDS NDS NDS 3.3 1.33 1.74 N/A N/A
135 478.6 -22.27 -1.1 -0.3 -1.4 -0.4 -0.7 NDS NDS -0.78 0.47 1.94
137 485.6 -15.27 -0.7 NDS NDS NDS NDS -0.7 -0.5 -0.63 0.12 N/A N/A
139 492.2 -8.67 -0.4 -1.1 0.3 0.7 NDS NDS 1.4 0.18 0.97 0.94
144 493.6 -7.27 -0.4 NDS R -0.6 -1.0 NDS NDS -0.67 0.31 N/A N/A
150 501.7 0.83 0.0 2.2 R NDS 0.4 -0.2 0.5 0.58 0.95 0.96
156 562.1 61.23 3.0 1, 3 0.1 0.8 NDS 1.8 2.8 -0.7 1.30 1.49 0.61 X
159 499.5 -1.37 -0.1 -0.4 0.6 1.6 0.3 -0.5 R 0.25 0.78 1.17
161 485.6 -15.27 -0.7 -0.5 NDS NDS -0.2 NDS NDS -0.47 0.25 N/A N/A
164 489.0 -11.87 -0.6 NDS 0.7 NDS 0.9 NDS 1.3 0.57 0.82 1.11
166 506.3 5.43 0.3 -0.3 NDS 0.9 1.7 -0.7 0.4 0.38 0.85 1.07
168 541.5 40.63 2.0 NDS 0.0 $ NDS -0.9 -1.0 0.03 1.39 0.65 X
176 517.1 16.23 0.8 -0.5 0.2 NDS -0.9 NDS 0.0 -0.08 0.65 1.40
189 568.7 67.83 3.3 1, 3 0.8 3.1 NDS NDS NDS NDS 2.40 1.39 N/A N/A
191 531.2 30.33 1.5 -1.1 -0.9 NDS -0.7 -1.1 1.7 -0.10 1.33 0.68 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 105
1603 1511 1507 1503 1411 1407
192 496.8 -4.07 -0.2 -0.1 0.9 NDS -0.4 0.1 -0.4 -0.02 0.49 1.86
193 528.8 27.93 1.4 0.4 0.0 NDS 0.3 -2.7 0.1 -0.08 1.38 0.66 X
201 540.7 39.83 2.0 R NDS NDS 1.2 -0.3 -1.3 0.40 1.48 0.61 X
210 486.6 -14.27 -0.7 -0.5 1.1 1.0 $ -0.9 -0.7 -0.12 0.91 1.00
212 478.5 -22.37 -1.1 -1.0 -0.7 0.0 -0.8 NDS NDS -0.72 0.43 2.12
213 487.8 -13.07 -0.6 -0.6 -0.3 NDS -1.1 -0.6 -0.8 -0.67 0.27 3.37
214 490.5 -10.37 -0.5 -0.4 NDS NDS 0.5 NDS NDS -0.13 0.55 N/A N/A
230 491.7 -9.17 -0.4 0.0 0.6 NDS 0.6 0.8 -0.1 0.25 0.48 1.90
239 493.0 -7.87 -0.4 NDS NDS NDS NDS 0.8 NDS 0.20 0.85 N/A N/A
241 ** 271.6 R 0.5 R 0.1 NDS 2.4 2.8 1.45 1.35 0.67 X

Legend:
R = Rejected
TPI
Comments:
THERE IS NO ASTM PUBLISHED REPRODUCIBILITY FOR THIS TEST

Labs: 042, 054, 137
106
Sample ID: CO1607

81.56
61.17 562.04
40.78 541.65
20.39 521.26
Deviation
0 500.87
-20.39 480.48
-40.78 460.09

-61.17 439.7
-81.56 419.31
6 2 2 1 5 4 8 1 1 1 9 2 2 2 8 1 1 2 2 1 2 8 6 5 1 1 2 4 7 1 2 1 1 1 9 1 1 7 1 3 8 3 8 1 1 1 2 8 2 1 2 2 7 1 1
7 2 1 3 5 6 3 0 6 3 0 1 2 1 9 5 6 1 3 3 3 7 5 4 4 3 6 1 9 3 5 2 2 6 5 7 7 6 6 4 8 7 9 9 1 4 0 6 0 0 1 5 8
0 2 5 7 1 7 0 3 4 4 0 9 9 4 2 9 2 8 0 6 6 3 1 9 1 8 6 6 9

107
Sample ID: CO1607

32
28
Median
1% 99%
24
20
Number of Labs
16
12
0
428.85 - 448.25 448.3 - 467.7 467.75 - 487.15 487.2 - 506.6 506.65 - 526.05 526.1 - 545.5 545.55 - 564.95 565 - 584.4
ASTM Crude Oil
Sample ID: CO1607
July 2016 108
Total Weight % Recovery @ 720C
1603 1511 1507 1503 1411 1407
003 97.6 -0.66 -0.3 0.5 -0.2 -0.1 -0.4 -0.9 0.2 -0.17 0.45 2.09
013 99.5 1.24 0.5 0.6 0.5 1.7 0.6 0.5 0.7 0.73 0.43 2.19
015 99.8 1.54 0.6 NDS 0.1 0.3 1.2 NDS NDS 0.55 0.48 1.96
017 99.1 0.84 0.3 0.4 -0.9 -1.0 0.6 -0.6 0.3 -0.13 0.68 1.38
020 94.3 -3.96 -1.5 0.2 -0.7 -0.6 -0.5 -0.4 0.6 -0.41 0.67 1.40
026 99.8 1.54 0.6 NDS NDS R NDS NDS NDS 0.60 0.00 N/A N/A
027 91.4 -6.86 -2.6 3 R -2.3 NDS NDS NDS NDS -2.45 0.21 N/A N/A
034 99.16 0.90 0.3 NDS NDS -1.2 0.1 -0.1 0.0 -0.18 0.59 1.59
041 100 1.74 0.7 0.9 NDS NDS NDS NDS NDS 0.80 0.14 N/A N/A
046 100 1.74 0.7 0.9 -0.1 1.4 0.9 NDS NDS 0.76 0.55 1.71
055 100 1.74 0.7 NDS NDS NDS NDS NDS -1.4 -0.35 1.48 N/A N/A
065 99.7 1.44 0.5 0.9 -0.6 -0.1 0.1 1.6 1.4 0.54 0.81 1.16
067 89.4 -8.86 -3.4 1, 3 -0.5 0.9 -0.5 1.1 0.9 NDS -0.25 1.70 0.55 X
071 94.5 -3.76 -1.4 -0.7 -0.5 -1.0 -0.6 -0.4 -1.5 -0.87 0.44 2.14
077 98.72 0.46 0.2 -2.0 1.2 -0.5 -0.6 0.1 0.6 -0.14 1.03 0.91
084 96.0 -2.26 -0.9 NDS 0.0 -0.5 -1.9 -1.2 NDS -0.90 0.72 1.31
086 97.9 -0.36 -0.1 0.4 -0.8 -0.9 -0.4 0.0 0.5 -0.19 0.55 1.71
087 99.6 1.34 0.5 0.7 -0.8 -0.6 0.0 0.4 0.5 0.10 0.59 1.59
088 98.9 0.64 0.2 -0.2 -0.2 0.0 0.6 0.3 0.3 0.14 0.29 3.24
089 100.0 1.74 0.7 0.9 1.6 0.6 1.3 -0.3 -0.1 0.67 0.69 1.36
092 ** 87.97 R NDS NDS NDS NDS -0.4 NDS -0.40 0.00 N/A N/A
096 100.00 1.74 0.7 NDS -0.2 NDS NDS -0.8 -1.7 -0.50 1.01 0.93
102 ** 88.08 R -3.2 -1.0 -2.2 -0.4 R 0.5 -1.26 1.46 0.64 X
107 100 1.74 0.7 NDS NDS 2.0 1.3 NDS NDS 1.33 0.65 N/A N/A
122 98.5 0.24 0.1 -0.3 R 0.0 NDS NDS -0.8 -0.25 0.40 2.35
135 ** 74.5 R -2.6 1.9 2.0 -2.6 NDS NDS -0.33 2.63 0.36 X
137 100 1.74 0.7 NDS NDS NDS NDS 1.1 NDS 0.90 0.28 N/A N/A
139 103.7 5.44 2.1 3 0.4 0.1 0.9 NDS NDS -0.7 0.56 1.04 0.90
144 99.0 0.74 0.3 NDS 1.4 NDS NDS NDS NDS 0.85 0.78 N/A N/A
156 92.5 -5.76 -2.2 3 0.0 -1.8 NDS -1.9 -2.5 0.9 -1.25 1.37 0.69 X
159 100.0 1.74 0.7 0.9 -0.1 -0.4 -0.2 1.1 -2.5 -0.07 1.22 0.77 X
161 100 1.74 0.7 0.9 NDS 0.0 0.6 NDS NDS 0.55 0.39 2.41
164 100 1.74 0.7 NDS -0.3 NDS -0.8 NDS -1.1 -0.38 0.79 1.19
166 98.27 0.01 0.0 NDS -0.6 0.7 -1.6 0.5 0.2 -0.13 0.85 1.11
176 97.7 -0.56 -0.2 0.9 0.1 0.3 0.9 NDS 0.3 0.38 0.44 2.14
189 93.84 -4.42 -1.7 -0.2 -1.1 -0.6 NDS NDS NDS -0.90 0.65 1.45
192 99.3 1.04 0.4 R 0.3 0.2 0.5 0.0 0.4 0.30 0.18 5.22
193 95.5 -2.76 -1.0 0.0 0.2 0.3 -0.2 0.7 0.5 0.07 0.56 1.68
201 95.8 -2.46 -0.9 -3.6 -0.9 -0.2 -1.0 0.4 0.8 -0.77 1.43 0.66 X
214 100 1.74 0.7 0.9 -0.3 NDS NDS NDS NDS 0.43 0.64 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 109
1603 1511 1507 1503 1411 1407
220 99 0.74 0.3 R NDS NDS NDS -3.1 NDS -1.40 2.40 N/A N/A
230 100 1.74 0.7 0.2 0.3 0.1 0.0 -0.4 0.6 0.21 0.37 2.54
239 100.0 1.74 0.7 NDS -0.6 -1.2 NDS -0.3 NDS -0.35 0.79 1.19
241 95.17 -3.09 -1.2 -1.4 3.0 1.1 NDS -2.3 -1.6 -0.40 2.02 0.47 X

Legend:
R = Rejected
TPI
Comments:

Labs: 042, 054, 137
110
Sample ID: CO1607

10.52 108.78
7.89 106.15
5.26 103.52
2.63 100.89
Deviation
0 98.26
-2.63 95.63
-5.26 93
-7.89 90.37
-10.52 87.74
6 2 2 1 1 2 2 7 2 2 1 2 8 3 1 8 1 1 7 8 2 1 1 3 1 1 8 6 1 2 2 2 2 2 8 9 1 1 1 1 1 1 5 4 4 2 1
7 9 7 5 8 0 4 1 0 4 9 0 4 7 6 6 2 7 8 2 4 7 4 9 3 7 5 5 3 6 3 3 1 9 6 6 6 5 0 2 3 5 1 6 2 3
6 9 0 6 1 3 1 6 6 2 0 4 2 9 0 4 4 1 9 7 8 7 9

111
Sample ID: CO1607

35
30 Median
1% 99%
25
Number of Labs
20
15
10
0
87.3 - 89.9 89.95 - 92.55 92.6 - 95.2 95.25 - 97.85 97.9 - 100.5 100.55 - 103.15 103.2 - 105.8
ASTM Crude Oil
Sample ID: CO1607
July 2016 112
Nitrogen - D4629
(mg/kg)
1603 1511 1507 1503 1411 1407
001 60.4 -19.2 -1.8 2 NDS -0.6 NDS NDS NDS NDS -1.20 0.85 N/A N/A
003 82 2.4 0.2 NDS NDS NDS NDS NDS NDS 0.20 0.00 N/A N/A
004 87 7.4 0.7 -0.9 NDS NDS NDS 0.4 0.8 0.25 0.79 1.01
007 ** 173 R 0.7 NDS -0.5 -1.0 NDS NDS -0.27 0.87 N/A N/A
010 69 -10.6 -1.0 2 NDS NDS NDS NDS NDS NDS -1.00 0.00 N/A N/A
012 86 6.4 0.6 -1.0 -1.1 NDS NDS NDS NDS -0.50 0.95 N/A N/A
013 113 33.4 3.2 1, 2, 3 1.5 0.5 -0.3 -0.1 NDS NDS 0.96 1.43 0.56 X
014 ** 9 R R NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
019 64 -15.6 -1.5 2 0.5 NDS NDS NDS NDS NDS -0.50 1.41 N/A N/A
030 81 1.4 0.1 -0.2 0.5 -0.4 0.3 0.0 0.2 0.07 0.30 2.67
058 ** 140.9 R -0.3 -0.9 -0.9 NDS -2.7 -2.4 -1.44 1.05 0.76 X
060 110 30.4 2.9 2, 3 -0.4 -0.9 0.8 -1.1 NDS NDS 0.26 1.65 0.48 X
062 56 -23.6 -2.2 2, 3 -0.2 NDS NDS NDS NDS NDS -1.20 1.41 N/A N/A
071 80 0.4 0.0 0.7 1.0 1.0 0.9 0.7 1.0 0.76 0.36 2.22
077 72 -7.6 -0.7 1.3 0.4 0.4 0.3 0.3 1.2 0.46 0.67 1.19
079 80 0.4 0.0 NDS NDS 0.6 NDS NDS NDS 0.30 0.42 N/A N/A
089 75 -4.6 -0.4 0.8 0.9 0.7 0.9 0.4 0.6 0.56 0.46 1.74
091 93 13.4 1.3 2 0.2 0.4 -1.3 NDS NDS -0.8 -0.04 1.03 0.78 X
093 75.00 -4.6 -0.4 0.6 -0.2 0.0 -0.3 NDS NDS -0.06 0.40 2.00
106 74.0 -5.6 -0.5 -1.7 -0.8 -0.9 NDS NDS NDS -0.98 0.51 1.57
118 ** 205 R -1.8 NDS -1.0 NDS -0.5 NDS -1.10 0.66 N/A N/A
124 59 -20.6 -1.9 2 -1.8 -0.7 -1.2 -2.4 -1.2 NDS -1.53 0.61 1.31
135 ** 0 R NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
139 93 13.4 1.3 2 1.3 1.0 1.7 1.5 1.2 1.7 1.39 0.26 3.08
141 76 -3.6 -0.3 -0.2 -0.5 0.0 0.0 -0.1 NDS -0.18 0.19 4.21
144 76 -3.6 -0.3 NDS NDS NDS NDS NDS NDS -0.30 0.00 N/A N/A
147 79 -0.6 -0.1 2.2 -0.5 -0.5 NDS NDS NDS 0.28 1.30 0.62 X
149 50.8 -28.8 -2.7 2, 3 NDS NDS NDS -0.5 -1.0 NDS -1.40 1.15 N/A N/A
152 95 15.4 1.5 2 NDS 0.8 0.3 0.6 0.9 0.8 0.82 0.40 2.00
159 99.7 20.1 1.9 2 1.2 1.6 1.3 2.2 0.0 0.6 1.26 0.76 1.05
160 70 -9.6 -0.9 2 NDS NDS NDS NDS NDS NDS -0.90 0.00 N/A N/A
163 83 3.4 0.3 0.1 -1.8 0.4 -0.8 1.5 3.2 0.41 1.60 0.50 X
168 ** 393 R NDS 0.2 -0.3 NDS -1.2 -1.0 -0.57 0.64 1.25
173 86.0 6.4 0.6 R NDS 0.0 NDS NDS NDS 0.30 0.42 N/A N/A
181 73 -6.6 -0.6 -0.3 -0.8 NDS NDS NDS NDS -0.57 0.25 N/A N/A
211 84 4.4 0.4 0.4 0.5 0.8 0.6 0.1 0.9 0.53 0.27 2.96
214 79 -0.6 -0.1 $ $ 0.9 NDS NDS NDS 0.40 0.71 N/A N/A
216 ** 164.0 R 0.4 NDS -0.5 -1.0 NDS NDS -0.37 0.71 N/A N/A
226 73 -6.6 -0.6 -1.3 0.4 -1.6 -0.9 NDS NDS -0.80 0.77 1.04
ASTM Crude Oil
Sample ID: CO1607
July 2016 113
Nitrogen - D4629
(mg/kg)
1603 1511 1507 1503 1411 1407
231 74.8 -4.8 -0.5 -0.2 0.5 0.2 0.3 0.0 0.2 0.07 0.34 2.35

Legend:
R = Rejected
TPI 0.26
Comments:
114
Sample ID: CO1607

Nitrogen - D4629
(mg/kg)
42.4 122
31.8 111.4
21.2 100.8
10.6 90.2
Reproducibility
Deviation
0 79.6
Reproducibility
-10.6 69
-21.2 58.4
-31.8 47.8
-42.4 37.2
1 6 1 1 1 1 1 7 2 1 1 2 9 8 1 1 1 2 7 7 3 1 3 1 1 1 2 2 6 1 1 1 4 9 1 1 1 6 1
4 2 2 9 0 6 7 2 8 0 3 3 9 4 4 4 1 1 9 0 2 6 5 7 1 1 6 7 2 1 3 5 5 0 3
9 4 0 6 1 6 1 4 1 7 4 3 3 7 1 0 6 3 9 2 9

115
Sample ID: CO1607

Nitrogen - D4629
(mg/kg)
21
18
Median
1% 99%
15
Number of Labs
12
0
41 - 52 53 - 64 65 - 76 77 - 88 89 - 100 101 - 112 113 - 124
ASTM Crude Oil
Sample ID: CO1607
July 2016 116
Nitrogen - D5762
(g/g)
1603 1511 1507 1503 1411 1407
003 84 9.1 0.7 -0.1 -0.2 -0.6 0.2 0.2 0.5 0.10 0.44 2.20
005 52 -22.9 -1.7 2 -0.6 0.6 NDS 0.5 -0.1 1.9 0.10 1.22 0.80
006 82 7.1 0.5 0.8 0.2 0.1 0.0 -1.2 -0.9 -0.07 0.73 1.33
015 77 2.1 0.2 -0.6 -1.3 -0.9 -1.6 NDS NDS -0.84 0.69 1.41
017 87.4 12.5 0.9 -0.6 0.9 0.4 0.8 1.3 0.8 0.64 0.61 1.59
020 51.0 -23.9 -1.7 2 0.1 0.7 1.3 1.1 -0.1 0.0 0.20 1.00 0.97
023 80 5.1 0.4 0.3 -1.1 -1.1 -0.7 0.3 0.3 -0.23 0.70 1.39
025 72 -2.9 -0.2 NDS 0.2 NDS -1.0 NDS NDS -0.33 0.61 N/A N/A
026 ** 163 R -0.3 -0.6 -0.4 1.1 NDS NDS -0.05 0.78 1.24
027 59 -15.9 -1.2 R 0.2 2.0 NDS -2.0 -2.1 -0.62 1.73 0.56 X
029 78.0 3.1 0.2 0.3 1.1 -0.7 NDS -0.2 0.3 0.17 0.60 1.62
045 81 6.1 0.4 0.0 -0.2 0.0 NDS NDS NDS 0.05 0.25 3.88
049 130.5 55.6 4.0 1, 2, 3 -1.6 0.7 1.0 0.7 NDS NDS 0.96 2.00 0.48 X
055 ** 350 R NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
067 70.2 -4.7 -0.3 -0.4 0.2 0.4 1.8 2.0 0.5 0.60 0.95 1.02
079 82 7.1 0.5 -0.6 0.8 -0.4 -0.3 NDS NDS 0.00 0.61 1.59
084 ** 190 R -2.1 -1.4 R -2.3 R R -1.93 0.47 N/A N/A
088 78 3.1 0.2 -0.5 -0.6 0.3 0.4 2.2 0.1 0.30 0.92 1.05
089 80 5.1 0.4 1.6 0.8 0.3 0.6 0.7 0.5 0.70 0.43 2.26
091 96 21.1 1.5 0.1 -0.2 -3.0 -0.7 -1.0 -1.0 -0.61 1.36 0.71 X
092 53 -21.9 -1.6 2 0.6 NDS NDS NDS NDS NDS -0.50 1.56 N/A N/A
096 85 10.1 0.7 0.3 -0.5 -1.5 0.2 -0.5 0.3 -0.14 0.74 1.31
101 30 -44.9 -3.3 1, 2, 3 0.6 0.6 0.1 NDS -0.8 -1.2 -0.67 1.49 0.65 X
105 ** 200 R 0.1 1.1 -0.2 0.3 0.4 0.4 0.35 0.43 2.26
110 83 8.1 0.6 NDS 1.1 NDS NDS NDS NDS 0.85 0.35 N/A N/A
112 70 -4.9 -0.4 -1.3 0.2 -0.6 -0.3 NDS 0.0 -0.40 0.53 1.83
117 59 -15.9 -1.2 -0.9 -0.5 -0.8 -1.2 -0.9 0.4 -0.73 0.55 1.76
126 75.3 0.4 0.0 NDS -0.8 NDS -2.4 NDS NDS -1.07 1.22 N/A N/A
133 84 9.1 0.7 2.0 -3.0 NDS NDS NDS NDS -0.10 2.59 N/A N/A
147 100 25.1 1.8 2 2.8 1.1 -1.8 -1.1 NDS NDS 0.56 1.95 0.50 X
148 66 -8.9 -0.6 -0.1 0.5 1.1 0.6 -0.8 -1.7 -0.14 0.96 1.01
150 74.4 -0.5 0.0 1.1 0.8 0.2 0.1 0.9 -0.1 0.43 0.49 1.98
151 74 -0.9 -0.1 0.1 NDS NDS NDS -0.9 NDS -0.30 0.53 N/A N/A
157 89 14.1 1.0 1.1 -0.2 0.6 0.2 NDS -1.4 0.22 0.93 1.04
161 91 16.1 1.2 NDS NDS -1.1 0.4 NDS NDS 0.17 1.17 N/A N/A
166 75 0.1 0.0 -0.6 NDS -0.1 0.2 R 1.3 0.16 0.70 1.39
171 ** 138.6 R 0.6 -2.2 R -2.6 NDS NDS -1.40 1.74 N/A N/A
172 86 11.1 0.8 0.1 0.6 0.0 -0.5 0.1 NDS 0.18 0.46 2.11
176 66.3 -8.6 -0.6 1.1 2.4 1.4 1.0 2.0 0.1 1.06 1.04 0.93
ASTM Crude Oil
Sample ID: CO1607
July 2016 117
Nitrogen - D5762
(g/g)
1603 1511 1507 1503 1411 1407
191 74 -0.9 -0.1 -0.1 -0.2 -0.5 -1.0 -0.4 -0.2 -0.36 0.32 3.03
192 90 15.1 1.1 -2.3 1.4 0.4 1.0 -2.0 -1.4 -0.26 1.59 0.61 X
193 53.0 -21.9 -1.6 2 -1.6 -1.1 -0.8 -0.3 -0.8 -1.0 -1.03 0.46 2.11
201 ** 210 R -0.9 1.0 1.3 R -1.0 -0.5 -0.02 1.09 0.89
204 ** 161 R NDS 0.6 0.1 0.1 0.1 -0.2 0.14 0.29 3.34
213 74 -0.9 -0.1 -0.4 NDS -2.7 -1.5 -2.6 -0.6 -1.32 1.13 0.86
214 76 1.1 0.1 -0.9 -0.5 1.1 -0.7 NDS NDS -0.18 0.81 1.20
220 61.1 -13.8 -1.0 NDS NDS 0.0 0.9 -0.4 -0.7 -0.24 0.74 1.31
224 60 -14.9 -1.1 -1.4 R NDS 0.8 -0.1 0.2 -0.32 0.91 1.07
228 81 6.1 0.4 0.2 -0.2 -0.4 -1.8 NDS 0.9 -0.15 0.93 1.04
230 65.1 -9.8 -0.7 -1.1 0.2 0.4 -0.5 -0.8 -0.6 -0.44 0.54 1.80

Legend:
R = Rejected
TPI 0.52
Comments:
118
Sample ID: CO1607

Nitrogen - D5762
(g/g)
55.2 130.1
41.4 116.3
27.6 102.5

Reproducibility
13.8 88.7
Deviation
0 74.9
-13.8 61.1
Reproducibility
-27.6 47.3
-41.4 33.5
-55.2 19.7
1 2 5 1 9 1 1 2 2 2 2 1 1 1 1 6 2 2 1 1 1 9 1 1 2 5 1 2 8 2 8 4 2 7 6 1 3 1 9 1 1 1 1 1 1 9 1 4
0 0 9 2 8 1 7 2 2 3 4 7 0 1 7 5 1 5 9 5 4 6 2 1 6 5 9 8 3 9 5 2 9 1 3 6 7 7 5 9 6 4 1 4 9
1 3 1 7 4 0 0 8 6 2 3 1 1 0 6 6 4 8 0 3 2 7 2 1 7

119
Sample ID: CO1607

Nitrogen - D5762
(g/g)
32
28
Median
1% 99%
24
20
Number of Labs
16
12
0
15 - 33 34 - 52 53 - 71 72 - 90 91 - 109 110 - 128 129 - 147
ASTM Crude Oil
Sample ID: CO1607
July 2016 120
D4929-Method A
Chloride Content
1603 1511 * 1507 1503 1411 * 1407 *
001 0.2 0.02 0.1 NDS NDS NDS 0.10 0.00 N/A N/A
006 0.0 -0.18 -1.2 -0.6 NDS NDS -0.90 0.42 N/A N/A
046 0.5 0.32 2.1 3 -0.6 NSP NSP 0.75 1.91 0.51 X
062 <1.0 $ NDS NDS 0.00 0.00 N/A N/A
093 0.3 0.12 0.8 R NDS NDS 0.80 0.00 N/A N/A
103 0.2 0.02 0.1 -0.6 NSP NDS -0.25 0.49 N/A N/A
161 <1.0 1.3 NSP NDS 1.30 0.00 N/A N/A
166 0.1 -0.08 -0.5 $ NSP NSP -0.50 0.00 N/A N/A
168 ** 104.0 R NDS NSP NDS 0.00 0.00 N/A N/A
191 0.1 -0.08 -0.5 1.3 NDS NDS 0.40 1.27 N/A N/A

Legend:
No. Valid Results 7
R = Rejected
TPI 1.07
Comments:
121
Sample ID: CO1607

D4929-Method A
Chloride Content
0.6 0.78
Reproducibility
0.45 0.63
0.3 0.48
0.15 0.33
Deviation
0 0.18
-0.15 0.03
-0.3 -0.12
-0.45 -0.27
Reproducibility
-0.6 -0.42
6 1 1 1 1 9 4
6 9 0 3 6
6 1 3

ASTM Crude Oil
Sample ID: CO1607
July 2016 122
4929-Method B
Chloride Content
1603 1511 1507 1503 1411 * 1407 *
013 0.0 -0.05 -0.7 -0.8 -0.9 -1.2 NDS -0.90 0.22 3.91
025 0.0 -0.05 -0.7 NDS -0.3 NDS NDS -0.50 0.28 N/A N/A
066 0.1 0.05 0.7 0.5 -0.6 2.4 NDS 0.75 1.24 0.69 X
089 0.0 -0.05 -0.7 1.8 -0.3 0.0 2.0 0.56 1.25 0.69 X
090 0.2 0.15 2.1 3 -0.8 -0.9 NDS NDS 0.13 1.70 N/A N/A
103 0.0 -0.05 -0.7 -0.8 NDS 0.0 -0.4 -0.48 0.36 2.39
118 0.0 -0.05 -0.7 0.5 NDS 0.0 NDS -0.07 0.60 N/A N/A
134 0.0 -0.05 -0.7 -0.8 NDS NDS NDS -0.75 0.07 N/A N/A
166 0.1 0.05 0.7 $ NDS -0.6 0.5 0.20 0.70 N/A N/A
191 0.1 0.05 0.7 -0.8 $ R NDS -0.05 1.06 N/A N/A
193 0.1 0.05 0.7 0.5 1.0 0.6 0.8 0.72 0.19 4.53
211 <0.1 $ -0.6 -0.6 NDS -0.60 0.00 N/A N/A
214 <1.0 $ $ $ NDS 0.00 0.00 N/A N/A

Legend:
R = Rejected
TPI
Comments:
The Robust mean is outside this range therefore ASTM Reproducibility not determined.
The Robust Standard Deviation exceeds the Robust Mean of these test data. Interpret these statistics with caution. Graphs are not provided.
ASTM Crude Oil
Sample ID: CO1607
July 2016 123
Pour Point - D97
(C)
1603 1511 1507 1503 1411 1407
003 12 2.0 0.6 $ -0.8 0.8 0.1 $ -1.0 -0.06 0.81 1.23
004 12 2.0 0.6 NDS NDS -1.0 NDS NDS 0.8 0.13 0.99 N/A N/A
005 6 -4.0 -1.1 $ $ 0.2 -0.4 NDS 0.2 -0.28 0.62 1.61
006 15 5.0 1.4 $ NDS 0.8 0.1 -0.6 0.8 0.50 0.77 1.30
007 3 -7.0 -2.0 $ $ -1.0 -1.4 NDS NDS -1.47 0.50 N/A N/A
008 15 5.0 1.4 $ -1.1 -1.5 $ $ NDS -0.40 1.57 N/A N/A
013 15 5.0 1.4 -0.5 0.8 1.3 1.1 -0.6 0.2 0.53 0.84 1.19
015 18 8.0 2.3 3 $ -1.1 -0.4 -1.9 NDS NDS -0.28 1.82 0.55 X
017 12 2.0 0.6 $ 0.0 0.2 -1.9 NDS 1.4 0.06 1.22 0.82
021 9 -1.0 -0.3 -0.5 1.5 1.3 1.1 $ 0.8 0.65 0.85 1.18
023 12 2.0 0.6 NDS NDS -1.0 NDS NDS NDS -0.20 1.13 N/A N/A
026 9 -1.0 -0.3 $ $ 0.8 NDS NDS NDS 0.25 0.78 N/A N/A
029 12 2.0 0.6 NDS 0.0 -1.0 0.1 -0.9 -1.0 -0.37 0.69 1.45
030 15 5.0 1.4 -1.2 -0.4 -0.4 -0.4 $ -1.0 -0.33 0.92 1.09
032 15 5.0 1.4 NDS -0.8 0.8 -3.4 -1.0 NDS -0.60 1.87 0.53 X
037 12 2.0 0.6 NDS -0.8 0.8 -2.9 -1.0 NDS -0.66 1.49 0.67 X
045 9 -1.0 -0.3 $ $ -0.4 0.1 $ -1.6 -0.55 0.73 1.37
046 12 2.0 0.6 NDS 0.8 0.8 -0.4 NDS NDS 0.45 0.57 1.75
049 3 -7.0 -2.0 $ 1.1 0.2 0.6 NDS NDS -0.02 1.37 0.73 X
052 12 2.0 0.6 $ NDS NDS NDS NDS NDS 0.60 0.00 N/A N/A
054 12 2.0 0.6 NDS $ 0.2 1.1 NDS 0.8 0.68 0.38 2.63
057 12 2.0 0.6 $ 1.1 0.2 $ $ NDS 0.63 0.45 N/A N/A
058 15 5.0 1.4 $ $ 0.8 NDS $ $ 1.10 0.42 N/A N/A
060 18 8.0 2.3 3 $ 0.4 -1.0 $ 0.8 -1.0 0.30 1.38 0.72 X
062 0 -10.0 -2.9 3 $ 2.3 0.8 NDS $ $ 0.07 2.68 N/A N/A
064 9 -1.0 -0.3 $ $ 1.3 NDS NDS NDS 0.50 1.13 N/A N/A
066 12 2.0 0.6 NDS 0.0 -2.1 -0.4 0.9 0.2 -0.13 1.07 0.93
067 6 -4.0 -1.1 1.1 1.1 NDS 0.1 $ NDS 0.30 1.05 0.95
074 9 -1.0 -0.3 NDS 0.0 0.2 0.6 -0.9 -1.0 -0.23 0.63 1.59
078 12 2.0 0.6 0.6 0.0 1.3 -0.4 0.6 -0.4 0.33 0.62 1.61
079 12 2.0 0.6 NDS NDS NDS $ NDS NDS 0.60 0.00 N/A N/A
080 3 -7.0 -2.0 $ $ 1.3 NDS NDS NDS -0.35 2.33 N/A N/A
083 6 -4.0 -1.1 NDS -0.8 -1.5 -0.4 NDS 0.2 -0.72 0.65 1.54
086 3 -7.0 -2.0 NDS NDS NDS NDS $ $ -2.00 0.00 N/A N/A
087 6 -4.0 -1.1 NDS -0.4 -1.5 0.6 $ -1.6 -0.80 0.91 1.10
088 9 -1.0 -0.3 $ 0.0 0.8 0.6 NDS -1.6 -0.10 0.95 1.05
089 9 -1.0 -0.3 $ -0.8 -0.4 0.6 -0.3 0.2 -0.17 0.49 2.04
090 12 2.0 0.6 NDS NDS -0.4 NDS 1.3 -0.4 0.28 0.83 1.20
091 12 2.0 0.6 $ $ -1.0 -2.9 $ 1.4 -0.48 1.90 0.53 X
092 12 2.0 0.6 $ NDS NDS NDS NDS NDS 0.60 0.00 N/A N/A
093 3 -7.0 -2.0 2.7 -0.4 2.5 $ NDS NDS 0.70 2.29 0.44 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 124
Pour Point - D97
(C)
1603 1511 1507 1503 1411 1407
094 3 -7.0 -2.0 $ NDS NDS NDS NDS NDS -2.00 0.00 N/A N/A
101 9 -1.0 -0.3 $ NDS NDS NDS NDS NDS -0.30 0.00 N/A N/A
102 6 -4.0 -1.1 0.3 -0.8 -0.4 0.6 $ NDS -0.28 0.72 1.39
103 12 2.0 0.6 NDS NDS -0.4 0.6 NDS 0.2 0.25 0.47 2.13
105 9 -1.0 -0.3 $ -0.8 0.2 1.1 $ -1.0 -0.16 0.84 1.19
107 12 2.0 0.6 0.6 -0.8 NDS 0.1 NDS NDS 0.12 0.66 1.52
110 12 2.0 0.6 NDS $ 0.8 NDS NDS NDS 0.70 0.14 N/A N/A
112 6 -4.0 -1.1 $ $ -1.0 0.6 NDS 0.2 -0.32 0.85 1.18
117 9 -1.0 -0.3 NDS NDS 0.2 NDS NDS NDS -0.05 0.35 N/A N/A
118 9 -1.0 -0.3 $ 1.5 0.2 $ NDS R 0.47 0.93 N/A N/A
122 9 -1.0 -0.3 $ $ 0.8 NDS NDS 0.2 0.23 0.55 N/A N/A
123 15 5.0 1.4 $ -1.9 -0.4 0.1 NDS 0.2 -0.12 1.19 0.84
124 9 -1.0 -0.3 $ $ 0.8 1.1 $ -0.4 0.30 0.76 1.32
127 12 2.0 0.6 NDS NDS -1.0 0.6 NDS NDS 0.07 0.92 N/A N/A
128 12 2.0 0.6 -0.4 NDS NDS NDS NDS NDS 0.10 0.71 N/A N/A
132 12 2.0 0.6 $ $ 0.8 $ NDS 0.8 0.73 0.12 N/A N/A
133 6 -4.0 -1.1 NDS 0.8 NDS NDS NDS -2.2 -0.83 1.52 N/A N/A
135 12 2.0 0.6 -1.2 1.9 1.3 -0.9 NDS NDS 0.34 1.35 0.74 X
141 9 -1.0 -0.3 -1.2 -1.1 -1.0 -0.4 $ 0.2 -0.63 0.55 1.82
147 9 -1.0 -0.3 $ $ -0.4 $ NDS NDS -0.35 0.07 N/A N/A
148 6 -4.0 -1.1 NDS -0.4 -0.4 -1.4 NDS R -0.82 0.51 1.96
151 9 -1.0 -0.3 NDS 0.4 NDS NDS $ NDS 0.05 0.49 N/A N/A
152 6 -4.0 -1.1 -0.5 0.4 0.2 -0.9 NDS -1.0 -0.48 0.64 1.56
154 12 2.0 0.6 $ NDS 0.8 3.1 $ -2.8 0.43 2.43 0.41 X
155 12 2.0 0.6 NDS 1.1 NDS NDS NDS NDS 0.85 0.35 N/A N/A
161 6 -4.0 -1.1 $ NDS -1.0 $ NDS NDS -1.05 0.07 N/A N/A
163 9 -1.0 -0.3 $ $ 0.8 $ $ $ 0.25 0.78 N/A N/A
166 12 2.0 0.6 $ 0.4 -1.0 1.1 -0.6 0.8 0.22 0.83 1.20
168 12 2.0 0.6 NDS -1.1 R NDS 1.3 1.4 0.55 1.16 0.86
169 15 5.0 1.4 $ NDS -0.4 NDS NDS NDS 0.50 1.27 N/A N/A
170 12 2.0 0.6 NDS $ -0.4 -0.4 NDS 0.2 0.00 0.49 2.04
171 12 2.0 0.6 1.1 1.1 0.8 -2.4 NDS 0.2 0.23 1.33 0.75 X
172 9 -1.0 -0.3 $ NDS -0.4 $ NDS NDS -0.35 0.07 N/A N/A
173 6 -4.0 -1.1 $ NDS 0.2 NDS NDS NDS -0.45 0.92 N/A N/A
176 9 -1.0 -0.3 NDS $ 0.8 -0.9 NDS 0.2 -0.05 0.72 1.39
184 15 5.0 1.4 $ $ 0.2 1.1 NDS NDS 0.90 0.62 N/A N/A
191 6 -4.0 -1.1 -1.2 -0.4 1.3 $ -1.0 0.8 -0.27 1.07 0.93
192 12 2.0 0.6 $ $ 1.3 $ $ 0.2 0.70 0.56 N/A N/A
193 9 -1.0 -0.3 NDS 0.8 0.8 0.6 0.9 -0.4 0.40 0.59 1.69
194 12 2.0 0.6 NDS 0.4 0.2 1.1 1.1 0.2 0.60 0.41 2.44
210 9 -1.0 -0.3 -1.2 -0.4 -0.4 0.6 $ -2.2 -0.65 0.95 1.05
211 12 2.0 0.6 $ -0.8 -1.5 0.6 NDS 0.2 -0.18 0.93 1.08
ASTM Crude Oil
Sample ID: CO1607
July 2016 125
Pour Point - D97
(C)
1603 1511 1507 1503 1411 1407
212 9 -1.0 -0.3 NDS NDS -1.5 2.1 NDS NDS 0.10 1.83 N/A N/A
213 9 -1.0 -0.3 $ 0.0 0.2 0.1 $ -0.4 -0.08 0.26 3.85
214 12 2.0 0.6 $ 0.4 0.8 1.1 NDS NDS 0.73 0.30 3.33
216 9 -1.0 -0.3 $ $ 0.2 -1.4 NDS NDS -0.50 0.82 N/A N/A
218 9 -1.0 -0.3 $ NDS NDS 0.1 NDS NDS -0.10 0.28 N/A N/A
220 9 -1.0 -0.3 $ 0.0 0.8 NDS $ -1.0 -0.12 0.75 1.33
224 15 5.0 1.4 $ NDS 0.2 NDS NDS NDS 0.80 0.85 N/A N/A
226 9 -1.0 -0.3 $ -0.4 -1.0 -0.4 NDS NDS -0.52 0.32 3.12
228 12 2.0 0.6 0.0 $ -2.7 $ NDS $ -0.70 1.76 N/A N/A
229 12 2.0 0.6 $ $ -0.4 NDS NDS NDS 0.10 0.71 N/A N/A
234 12 2.0 0.6 NDS 1.5 0.2 -0.4 $ -0.4 0.30 0.79 1.27
241 9 -1.0 -0.3 0.9 1.1 0.8 0.6 0.9 -0.4 0.51 0.61 1.64

Legend:
R = Rejected
TPI
Comments:
126
Page 1 of 2
Sample ID: CO1607
Pour Point - D97
(C)
14 24
10.5 20.5
7 17
3.5 13.5
Deviation
0 10
-3.5 6.5
-7 3

-10.5 -0.5
-14 -4
6 3 2 7 9 9 8 8 5 4 8 1 8 1 1 1 4 1 6 5 1 5 1 1 2 2 4 6 7 8 8 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 2 2 2 2 2 2
2 5 2 4 3 6 0 9 9 3 6 7 7 9 0 3 5 7 4 0 3 1 1 6 5 4 4 8 9 0 0 1 1 2 2 4 4 5 6 7 7 9 1 1 1 1 2 2 3 4
5 1 3 1 2 2 8 3 2 1 5 7 8 2 4 1 7 1 3 2 6 3 0 2 3 8 0 6 7 1

127
Page 2 of 2
Sample ID: CO1607
Pour Point - D97
(C)
14 24
10.5 20.5
7 17
3.5 13.5
Deviation
0 10
-3.5 6.5
-7 3
-10.5 -0.5
-14 -4
2 3 2 4 2 2 2 2 2 1 1 1 1 1 1 1 2 2 3 4 5 5 5 6 7 7 9 9 9 1 1 1 1 1 1 1 1 1 1 1 1 2 1 5 8 3 3 6 1 1 1 1 6
1 3 2 2 1 1 1 9 9 9 7 7 6 7 3 9 7 6 2 4 7 6 8 9 0 1 2 0 0 1 1 2 2 3 3 5 5 5 6 2 8 8 2 0 6 2 3 5 0
6 4 9 8 9 4 1 6 4 2 1 0 8 3 7 0 6 7 8 2 5 4 5 8 6 4 4 9 3

128
Sample ID: CO1607

Pour Point - D97
(C)
49
42
1% Median 99%
35
Number of Labs
28
21
14
0
-6 -3 0 3 6 9 12 15 18 21 24
ASTM Crude Oil
Sample ID: CO1607
July 2016 129
Pour Point - D5853
Method A (C)
1603 1511 1507 1503 1411 1407
003 12 2.4 0.6 NSP $ 0.1 0.0 NSP -0.5 0.05 0.45 2.00
014 12 2.4 0.6 NSP NDS NDS NDS NDS NDS 0.60 0.00 N/A N/A
017 12 2.4 0.6 NSP -0.8 -0.4 -2.0 NDS 1.4 -0.24 1.31 0.69 X
028 6 -3.6 -0.9 NDS NDS 2.1 NDS NDS NDS 0.60 2.12 N/A N/A
034 9 -0.6 -0.1 NDS $ 0.1 1.0 NSP NDS 0.33 0.59 1.53
052 12 2.4 0.6 NSP NDS NDS NDS NDS NDS 0.60 0.00 N/A N/A
087 6 -3.6 -0.9 NDS -0.1 -1.3 0.5 NSP -1.7 -0.70 0.89 1.01
089 12 2.4 0.6 NSP -0.8 -0.4 0.5 NSP 0.1 0.00 0.60 1.50
096 9 -0.6 -0.1 NSP -0.1 -1.3 0.0 NDS -3.0 -0.90 1.29 0.70 X
099 12 2.4 0.6 NSP 0.6 -0.9 $ NDS NDS 0.10 0.87 1.03
102 6 -3.6 -0.9 NSP -1.1 -0.4 1.0 NSP 0.1 -0.26 0.84 1.07
138 9 -0.6 -0.1 NSP $ 1.1 $ NSP 0.1 0.37 0.64 1.41
144 15 5.4 1.3 NDS NDS NDS 0.0 NDS NDS 0.65 0.92 N/A N/A
155 12 2.4 0.6 NDS 0.9 2.1 0.0 NSP 0.8 0.88 0.77 1.17
176 9 -0.6 -0.1 NSP $ 0.6 -0.5 NDS 0.1 0.02 0.46 1.96
179 6 -3.6 -0.9 NSP $ 0.6 1.0 NSP -2.4 -0.42 1.55 0.58 X
214 9 -0.6 -0.1 NSP NDS NDS NDS NDS NDS -0.10 0.00 N/A N/A
234 12 2.4 0.6 NDS 1.2 0.1 -1.0 NSP NDS 0.22 0.93 0.97

Legend:
R = Rejected
TPI 1.58
Comments:
130
Sample ID: CO1607

Pour Point - D5853
Method A (C)
24.6 34.2
20.5 30.1
Reproducibility
16.4 26
12.3 21.9
8.2 17.8
4.1 13.7
Deviation
0 9.6
-4.1 5.5
-8.2 1.4
-12.3 -2.7
-16.4 -6.8
Reproducibility
-20.5 -10.9
-24.6 -15
1 1 5 1 1 5 1 2 8 1 2 9 3 3 1 1 9 8 5 1 3 1 2 2 3 2 1 1
9 0 9 5 7 0 0 8 7 7 1 6 4 7 3 5 9 9 2 7 4 3 0 2 4 4 8
5 8 9 9 2 6 4 8 5 4 4 0 4 9

131
Sample ID: CO1607

Pour Point - D5853
Method A (C)
10
Median
6
Number of Labs
0
3 6 9 12 15 18

ASTM Crude Oil
Sample ID: CO1607
July 2016 132
Reid Vapor Pressure - D323
(p.s.i)
1603 1511 1507 1503 1411 1407
003 0.95 -0.353 -1.0 -1.3 -0.5 0.1 -0.1 0.2 -1.3 -0.56 0.65 1.38
006 0.20 -1.103 -3.1 1, 3 -0.5 NDS 1.2 1.0 1.9 R 0.10 1.99 0.45 X
013 1.35 0.047 0.1 0.3 -1.5 -0.9 -0.3 -0.5 -0.2 -0.43 0.61 1.48
015 0.55 -0.753 -2.1 3 0.8 1.5 NDS -1.1 NDS NDS -0.23 1.66 0.54 X
016 1.30 -0.003 0.0 NDS NDS NDS -0.4 0.2 0.0 -0.05 0.25 3.60
017 1.20 -0.103 -0.3 0.2 -0.5 -0.2 NDS NDS NDS -0.20 0.29 3.10
021 1.35 0.047 0.1 -1.3 -0.9 -0.8 -1.3 -1.4 -1.3 -0.99 0.53 1.70
022 1.25 -0.053 -0.1 NDS NDS 0.8 NDS NDS NDS 0.35 0.64 N/A N/A
023 1.60 0.297 0.8 -0.9 0.4 -0.6 R 1.2 1.3 0.37 0.93 0.97
026 2.20 0.897 2.5 3 NDS -0.2 NDS NDS NDS NDS 1.15 1.91 N/A N/A
032 0.75 -0.553 -1.5 NDS -0.5 R -1.3 1.3 NDS -0.50 1.28 0.70 X
037 1.35 0.047 0.1 NDS 1.1 1.1 1.3 R NDS 0.90 0.54 1.67
046 1.55 0.247 0.7 -0.6 -0.5 -0.6 -0.9 NDS NDS -0.38 0.62 1.45
057 1.00 -0.303 -0.8 -0.6 0.0 0.6 1.1 -0.5 -0.1 -0.04 0.69 1.30
067 1.40 0.097 0.3 0.4 0.1 1.4 1.2 -0.2 1.6 0.69 0.70 1.29
072 ** 0.00 R NDS 0.9 0.5 0.5 0.6 0.5 0.60 0.17 5.29
074 1.25 -0.053 -0.1 -0.4 -0.2 R -0.2 -1.0 -0.5 -0.40 0.33 2.73
083 1.50 0.197 0.6 0.7 2.0 0.1 -0.2 NDS 1.0 0.70 0.77 1.17
087 0.85 -0.453 -1.3 -0.9 0.3 1.7 -0.3 1.0 -0.8 -0.04 1.10 0.82
091 1.95 0.647 1.8 0.8 0.9 0.6 -0.3 -0.7 -0.4 0.39 0.89 1.01
102 2.10 0.797 2.2 3 0.4 0.1 -0.2 1.3 -0.7 2.8 0.84 1.30 0.69 X
123 1.40 0.097 0.3 0.2 -0.5 -0.6 -2.0 -1.0 -0.5 -0.59 0.77 1.17
126 1.60 0.297 0.8 R 0.3 1.3 NDS 0.7 1.0 0.82 0.37 2.43
129 1.25 -0.053 -0.1 0.0 -0.1 0.3 1.4 NDS NDS 0.30 0.64 1.41
138 1.00 -0.303 -0.8 -0.6 -1.1 0.1 NDS NDS NDS -0.60 0.51 1.76
147 0.60 -0.703 -2.0 -0.6 0.3 -0.3 1.4 NDS NDS -0.24 1.25 0.72 X
149 1.45 0.147 0.4 -0.4 NDS 0.9 1.3 0.8 1.6 0.77 0.71 1.27
154 0.70 -0.603 -1.7 0.2 NDS -1.1 -0.6 -0.8 -0.8 -0.80 0.62 1.45
155 1.20 -0.103 -0.3 0.7 -0.2 0.1 -0.2 NDS NDS 0.02 0.41 2.20
156 1.30 -0.003 0.0 -0.5 NDS NDS -1.0 -0.6 0.1 -0.40 0.45 2.00
161 1.10 -0.203 -0.6 -0.1 NDS 0.3 -2.7 NDS NDS -0.78 1.34 0.67 X
166 1.30 -0.003 0.0 1.8 NDS 2.4 1.3 -2.2 R 0.66 1.83 0.49 X
170 1.25 -0.053 -0.1 2.6 2.4 2.6 0.3 1.2 1.4 1.49 1.11 0.81
174 1.15 -0.153 -0.4 0.4 -1.0 -0.2 0.1 -1.2 -1.2 -0.50 0.65 1.38
183 1.00 -0.303 -0.8 -1.8 -1.1 0.1 0.3 -0.6 0.0 -0.56 0.75 1.20
ASTM Crude Oil
Sample ID: CO1607
July 2016 133
(p.s.i)
1603 1511 1507 1503 1411 1407
187 1.55 0.247 0.7 0.3 -0.5 -1.1 -0.7 -0.6 -0.4 -0.33 0.62 1.45
191 1.30 -0.003 0.0 0.7 -0.9 0.5 0.1 0.2 -0.3 0.04 0.53 1.70
192 1.20 -0.103 -0.3 2.7 -0.7 -3.2 -1.9 -0.8 -1.7 -0.84 1.84 0.49 X
194 1.60 0.297 0.8 0.2 0.0 -0.3 0.7 0.1 0.4 0.27 0.39 2.31
196 1.20 -0.103 -0.3 NDS NDS -1.1 0.7 -0.3 0.1 -0.18 0.66 1.36
211 1.50 0.197 0.6 0.3 1.0 0.4 0.7 -0.2 0.3 0.44 0.38 2.37
214 1.00 -0.303 -0.8 NDS 0.0 -1.4 1.7 NDS NDS -0.13 1.35 0.67 X
220 1.20 -0.103 -0.3 -3.0 -2.7 -2.7 R -2.4 -2.1 -2.20 0.98 0.92
221 1.05 -0.253 -0.7 NDS -0.1 -0.3 -0.2 R -0.2 -0.30 0.23 3.91
234 1.50 0.197 0.6 -0.4 2.4 3.1 R -0.2 0.8 1.05 1.41 0.64 X
235 0.70 -0.603 -1.7 -1.6 -1.4 0.1 NDS -0.8 0.3 -0.85 0.87 1.03

Legend:
R = Rejected
TPI
Comments:

Labs: 059, 067.
134
Sample ID: CO1607

(p.s.i)
1.432 2.735
1.074 2.377
0.716 2.019
0.358 1.661
Deviation
0 1.303
-0.358 0.945
-0.716 0.587

-1.074 0.229
-1.432 -0.129
6 1 1 2 1 3 8 3 1 1 5 2 1 5 2 1 1 2 4 2 1 1 1 1 7 1 1 2 1 1 1 1 3 2 1 1 6 2 1 6 2 2 8 1 4 1 2 4 1 1 2 1 1 1 9 5 1 2
5 4 3 5 2 7 3 1 7 1 8 9 2 6 7 2 5 2 9 5 7 9 4 7 2 2 9 6 5 6 7 1 3 2 7 4 4 4 3 1 3 8 6 4 3 2 9 2 2 3 5 1 0 0 6
7 5 4 8 6 4 3 1 1 4 8 0 6 5 2 0 9 1 6 6 3 0 9 4 1 7 6 4 5 4 4 3 2

135
Sample ID: CO1607

(p.s.i)
21
Median
1% 99%
18
15
Number of Labs
12
0
-0.07 - 0.24 0.25 - 0.56 0.57 - 0.88 0.89 - 1.2 1.21 - 1.52 1.53 - 1.84 1.85 - 2.16 2.17 - 2.48
ASTM Crude Oil
Sample ID: CO1607
July 2016 136
Salts - D3230 (lb/1000bbl)
(lb/1000bbl)
1603 1511 1507 1503 1411 1407
003 6.30 1.315 0.7 -0.3 0.2 0.7 0.0 -0.5 -0.2 0.09 0.47 1.85
005 1.00 -3.985 -2.0 NDS NDS -2.3 -1.4 -0.5 -1.1 -1.46 0.72 1.21
006 3.20 -1.785 -0.9 -1.2 -0.2 NDS -1.3 NDS NDS -0.90 0.50 1.74
007 2.23 -2.755 -1.4 0.1 NDS -1.5 NDS NDS NDS -0.93 0.90 N/A N/A
008 3.50 -1.485 -0.7 -1.2 0.4 -2.0 -0.1 -1.4 NDS -0.83 0.88 0.99
013 6.50 1.515 0.8 1.6 -0.5 -0.8 0.8 0.5 1.3 0.53 0.89 0.98
017 4.40 -0.585 -0.3 -1.0 -0.2 0.4 -0.2 0.6 0.9 0.03 0.64 1.36
019 7.20 2.215 1.1 NDS NDS 0.0 0.1 NDS 1.0 0.55 0.58 1.50
020 3.90 -1.085 -0.5 -1.2 1.3 0.7 0.1 -0.2 0.7 0.13 0.85 1.02
021 1.34 -3.645 -1.8 0.7 -1.3 -1.4 -2.4 -0.5 -0.3 -1.00 1.04 0.84
022 6.40 1.415 0.7 NDS NDS 1.6 -0.2 NDS NDS 0.70 0.90 N/A N/A
023 5.40 0.415 0.2 -0.1 NDS 0.6 0.5 -1.3 -0.6 -0.12 0.73 1.19
026 3.95 -1.035 -0.5 $ -0.6 0.1 NDS NDS NDS -0.33 0.38 N/A N/A
028 2.24 -2.745 -1.4 0.9 $ 0.8 0.2 R 0.8 0.26 0.97 0.90
035 5.30 0.315 0.2 0.5 NDS NDS 0.3 1.0 1.6 0.72 0.58 1.50
046 4.70 -0.285 -0.1 -1.2 1.3 -0.4 NDS NDS NDS -0.10 1.04 0.84
048 6.48 1.495 0.7 NDS NDS 0.3 0.5 0.1 NDS 0.40 0.26 3.35
051 5.78 0.795 0.4 NDS 0.8 NDS 1.0 NDS NDS 0.73 0.31 N/A N/A
052 4.90 -0.085 0.0 -1.2 NDS NDS NDS NDS NDS -0.60 0.85 N/A N/A
054 5.00 0.015 0.0 NDS -1.1 NDS $ NDS NDS -0.55 0.78 N/A N/A
058 4.00 -0.985 -0.5 0.9 -0.7 0.2 NDS R -0.5 -0.12 0.66 1.32
062 3.90 -1.085 -0.5 -1.2 NDS -1.3 NDS R NDS -1.00 0.44 N/A N/A
066 7.10 2.115 1.1 -0.4 -0.8 0.6 0.5 1.2 0.8 0.43 0.75 1.16
067 7.50 2.515 1.3 0.9 -1.2 -1.0 -0.9 -1.7 -1.5 -0.59 1.19 0.73 X
072 3.80 -1.185 -0.6 NDS -0.6 0.1 -0.3 0.4 0.4 -0.10 0.46 1.89
074 5.15 0.165 0.1 -0.8 0.1 1.4 0.7 R 3.2 0.78 1.39 0.63 X
086 4.73 -0.255 -0.1 -0.4 0.8 0.3 -0.6 0.3 0.7 0.14 0.53 1.64
088 5.00 0.015 0.0 2.2 -0.7 -0.1 0.1 1.1 0.6 0.46 0.95 0.92
089 4.49 -0.495 -0.2 0.2 0.4 0.0 0.0 2.7 0.6 0.53 0.99 0.88
092 6.00 1.015 0.5 NDS NDS NDS -0.7 -0.5 NDS -0.23 0.64 N/A N/A
096 4.90 -0.085 0.0 -1.2 0.2 0.7 -0.4 0.0 -0.1 -0.11 0.58 1.50
097 2.80 -2.185 -1.1 -1.0 -0.9 NDS R -1.6 -1.7 -1.26 0.36 2.42
102 6.40 1.415 0.7 0.5 -1.1 0.1 0.2 1.8 0.2 0.34 0.86 1.01
103 4.70 -0.285 -0.1 -0.4 -0.7 -0.2 NDS 0.3 1.3 0.03 0.70 1.24
105 0.80 -4.185 -2.1 3 -0.1 0.2 -0.4 -0.9 -0.9 0.6 -0.51 0.89 0.98
107 5.50 0.515 0.3 -0.5 1.0 -0.8 1.2 -0.8 NDS 0.07 0.90 0.97
ASTM Crude Oil
Sample ID: CO1607
July 2016 137
(lb/1000bbl)
1603 1511 1507 1503 1411 1407
108 7.18 2.195 1.1 NDS NDS 1.8 1.6 1.5 -1.0 1.00 1.15 0.76 X
109 4.60 -0.385 -0.2 -1.2 0.3 0.2 -1.0 0.0 0.9 -0.14 0.74 1.18
111 5.70 0.715 0.4 $ $ 0.2 0.4 -0.4 NDS 0.15 0.38 2.29
114 3.80 -1.185 -0.6 -0.7 NDS 2.0 1.5 NDS NDS 0.55 1.40 0.62 X
117 8.50 3.515 1.8 0.9 1.1 1.4 0.5 -0.5 0.0 0.74 0.80 1.09
118 2.70 -2.285 -1.1 1.8 -1.3 0.7 -2.8 -1.1 -1.7 -0.79 1.54 0.56 X
119 2.71 -2.275 -1.1 NDS NDS 0.2 NDS NDS NDS -0.45 0.92 N/A N/A
122 10.40 5.415 2.7 3 0.7 NDS -0.3 NDS NDS -1.6 0.38 1.81 0.48 X
123 5.11 0.125 0.1 0.9 -0.5 -0.7 0.7 0.8 1.1 0.34 0.72 1.21
129 6.46 1.475 0.7 -0.6 0.6 0.7 0.4 NDS NDS 0.36 0.55 1.58
131 3.76 -1.225 -0.6 0.0 1.2 R NDS NDS -0.6 0.00 0.85 1.02
132 5.20 0.215 0.1 -0.6 0.2 0.4 NDS NDS NDS 0.03 0.43 2.02
133 2.90 -2.085 -1.0 -0.6 0.7 NDS 0.2 0.5 0.0 -0.03 0.65 1.34
135 6.57 1.585 0.8 -0.4 0.5 0.0 -2.5 NDS NDS -0.32 1.30 0.67 X
138 3.00 -1.985 -1.0 $ 0.0 -0.9 0.0 0.7 -0.5 -0.28 0.64 1.36
146 7.00 2.015 1.0 0.9 NDS -0.1 -0.5 NDS NDS 0.32 0.74 1.18
152 6.50 1.515 0.8 0.1 0.7 1.0 NDS NDS NDS 0.65 0.39 2.23
154 10.40 5.415 2.7 3 -0.2 NDS 0.6 NDS 0.6 NDS 0.92 1.24 0.70 X
159 4.70 -0.285 -0.1 0.1 -1.0 -0.1 -1.0 -0.2 -1.4 -0.53 0.59 1.47
163 8.00 3.015 1.5 $ 1.2 0.6 0.1 0.7 0.6 0.78 0.50 1.74
165 5.41 0.425 0.2 0.2 -0.9 NDS -1.2 0.7 -0.7 -0.28 0.75 1.16
166 2.61 -2.375 -1.2 $ 1.3 1.4 0.9 -0.6 0.9 0.45 1.08 0.81
167 4.62 -0.365 -0.2 1.6 0.7 -0.1 0.7 NDS NDS 0.54 0.73 1.19
168 0.70 -4.285 -2.1 3 NDS 0.2 -2.1 NDS -1.6 -1.1 -1.34 0.96 0.91
171 4.10 -0.885 -0.4 0.3 -0.3 -0.8 0.3 0.7 0.6 0.06 0.56 1.55
172 5.70 0.715 0.4 $ R 0.6 0.6 0.7 -0.2 0.42 0.36 2.42
176 6.60 1.615 0.8 1.8 -1.2 0.1 0.6 -0.4 -0.1 0.23 0.96 0.91
180 5.70 0.715 0.4 -0.6 1.0 -0.3 -0.2 NDS -0.1 0.03 0.58 1.50
182 2.40 -2.585 -1.3 -0.8 NDS -0.5 NDS -1.0 NDS -0.90 0.34 2.56
189 4.00 -0.985 -0.5 $ 0.7 -1.0 0.1 NDS NDS -0.18 0.74 1.18
191 5.00 0.015 0.0 3.1 -0.2 0.0 NDS 1.3 0.3 0.75 1.27 0.69 X
192 7.50 2.515 1.3 NDS -0.5 1.1 1.7 -0.5 0.5 0.60 0.94 0.93
193 5.40 0.415 0.2 -0.1 1.0 0.6 -0.3 -1.6 -0.3 -0.07 0.83 1.05
202 4.29 -0.695 -0.3 -0.1 1.2 NDS NDS NDS NDS 0.27 0.81 N/A N/A
208 4.00 -0.985 -0.5 0.9 1.1 1.0 0.9 0.6 -0.2 0.54 0.63 1.38
ASTM Crude Oil
Sample ID: CO1607
July 2016 138
(lb/1000bbl)
1603 1511 1507 1503 1411 1407
210 6.90 1.915 1.0 -0.6 -1.3 -1.5 0.9 1.4 -1.6 -0.24 1.30 0.67 X
212 6.29 1.305 0.6 0.5 NDS NDS -2.1 NDS NDS -0.33 1.53 N/A N/A
213 9.50 4.515 2.2 3 1.4 -0.3 -1.0 0.9 2.2 R 0.90 1.32 0.66 X
214 5.80 0.815 0.4 0.5 $ 0.5 1.4 NDS NDS 0.70 0.47 1.85
231 2.77 -2.215 -1.1 0.0 -1.7 -1.7 -2.6 -1.4 1.9 -0.94 1.48 0.59 X
234 4.30 -0.685 -0.3 0.4 2.0 -0.1 0.4 -1.1 0.0 0.19 0.95 0.92
235 6.00 1.015 0.5 0.9 2.0 0.9 NDS 0.7 0.1 0.85 0.64 1.36
236 5.50 0.515 0.3 0.1 NDS -1.1 1.0 NDS NDS 0.07 0.87 1.00

Legend:
R = Rejected
TPI 1.24
Comments:
139
Page 1 of 2
Sample ID: CO1607
(lb/1000bbl)
8.032 13.017
Reproducibility
6.024 11.009
4.016 9.001
2.008 6.993
Deviation
0 4.985
-2.008 2.977
-4.016 0.969
-6.024 -1.039
Reproducibility
-8.032 -3.047
2 1 1 1 5 5 1 2 7 2 1 1 1 1 1 1 2 9 1 1 6 8 1 1 7 1 1 6 2 2 1 2 5 1 2 2 2 1 8 2 1 1 1 1 1 4 8 9 5 1 5
2 5 6 0 0 3 1 8 8 5 4 6 1 1 3 7 3 3 3 5 2 8 1 2 0 6 8 0 8 7 4 0 3 7 9 3 3 0 6 0 5 6 6 6 2 9 4
5 3 8 5 4 2 6 8 9 1 3 8 1 1 1 4 9 8 1 2 4 7 0 9 7 3 9 1

140
Page 2 of 2
Sample ID: CO1607
(lb/1000bbl)
8.032 13.017
Reproducibility
6.024 11.009
4.016 9.001
2.008 6.993
Deviation
0 4.985
-2.008 2.977
-4.016 0.969
-6.024 -1.039
Reproducibility
-8.032 -3.047
8 1 1 7 1 3 2 1 1 9 1 2 1 1 1 5 2 2 9 2 2 1 2 3 1 2 1 4 1 1 1 1 2 1 5 2 6 1 1 1 2 1 1 6 1 4 1 7 2 1 1
8 2 2 4 3 5 3 9 6 8 0 3 7 1 8 1 1 3 2 0 4 6 1 0 2 2 8 3 5 3 7 1 4 9 5 6 3 0 9 1 9 9 7 6 4 1 8 1 5 2
8 3 2 3 5 7 6 2 1 0 4 5 0 1 0 2 2 9 2 5 6 0 6 7 8 9 5 2 3 7 3 4 2

141
Sample ID: CO1607

(lb/1000bbl)
24
Median
1% 99%
20
16
Number of Labs
12
0
-0.43 - 0.63 0.64 - 1.7 1.71 - 2.77 2.78 - 3.84 3.85 - 4.91 4.92 - 5.98 5.99 - 7.05 7.06 - 8.12 8.13 - 9.19 9.2 - 10.26 10.27 -
11.33

ASTM Crude Oil
Sample ID: CO1607
July 2016 142
Salts - D6470
(mass %)
1603 1511 1507 1503 1411 1407
003 0.0020 $ -0.7 NSP NSP NSP NSP -0.70 0.00 0.00 X
017 0.0024 $ 0.3 NSP NSP NSP NSP 0.30 0.00 0.00 X
045 <0.0005 -0.4 -0.7 NSP NSP NDS NDS -0.55 0.21 3.62
095 0.0039 NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
130 0.0023 -0.3 1.1 NDS NDS NDS NDS 0.40 0.99 N/A N/A
202 0.0022 -0.3 1.3 NDS NDS NDS NDS 0.50 1.13 N/A N/A
Pooled Standard Deviation =

Legend:
No. Valid Results 5
Robust Mean 2 = Test result outside 3 sigma range ASTM reproducibility
Robust Standard Deviation
R = Rejected
Reproducibility ASTM Standard NDS = No Data Submitted
Reproducibility These Test Data
Anderson Darling * = There is no available historical information for this program cycle
TPI
Comments:
Statistical analyses of data not performed due to insufficient data points.
ASTM Crude Oil
Sample ID: CO1607
July 2016 143
Sediment - D473
(mass%)
1603 1511 1507 1503 1411 1407
003 0.00 -0.007 -1.0 -0.7 0.0 0.3 -1.0 -1.2 -1.5 -0.73 0.65 1.42
004 0.01 0.003 0.4 1.0 NDS -0.8 0.3 2.7 -0.4 0.53 1.24 0.74 X
005 0.01 0.003 0.4 1.0 0.4 0.3 0.3 1.4 -1.5 0.33 0.91 1.01
006 0.01 0.003 0.4 -0.7 R 0.3 0.3 0.1 0.7 0.18 0.48 1.92
007 ** 0.06 R -0.7 -1.5 -0.8 0.3 NDS NDS -0.68 0.74 1.24
008 0.02 0.013 1.9 1.0 -1.5 0.3 0.3 1.4 NDS 0.57 1.19 0.77 X
010 0.01 0.003 0.4 1.0 0.4 0.3 0.3 0.1 0.7 0.46 0.30 3.07
012 0.01 0.003 0.4 -0.7 0.0 0.3 0.3 NDS NDS 0.06 0.45 2.04
013 0.01 0.003 0.4 1.0 1.4 -1.9 0.3 0.1 0.7 0.29 1.06 0.87
015 0.00 -0.007 -1.0 2.7 0.9 NDS 0.3 NDS NDS 0.72 1.54 0.60 X
017 0.00 -0.007 -1.0 -0.7 0.4 -0.8 -1.0 -1.2 1.8 -0.36 1.09 0.84
019 ** 0.58 R NDS NDS 0.3 0.3 NDS 0.7 0.43 0.23 N/A N/A
024 0.01 0.003 0.4 1.0 -1.0 -0.8 0.3 0.1 -0.4 -0.06 0.71 1.30
025 0.02 0.013 1.9 NDS NDS NDS 0.3 1.4 0.7 1.08 0.71 1.30
026 0.01 0.003 0.4 -0.7 -1.0 0.3 0.3 NDS NDS -0.14 0.66 1.39
028 0.01 0.003 0.4 NDS -1.0 -0.8 0.3 NDS 0.7 -0.08 0.77 1.19
029 0.00 -0.007 -1.0 1.0 0.0 0.3 0.3 -1.2 0.7 0.01 0.83 1.11
030 0.01 0.003 0.4 -0.7 0.9 2.6 1.7 0.1 -1.5 0.50 1.39 0.66 X
043 0.00 -0.007 -1.0 -0.7 0.4 0.3 NDS 0.1 0.7 -0.03 0.67 1.37
046 0.00 -0.007 -1.0 -0.7 0.4 -0.8 0.3 NDS NDS -0.36 0.66 1.39
048 0.01 0.003 0.4 NDS NDS -0.8 0.3 0.1 -0.4 -0.08 0.51 1.80
049 ** 0.12 R NDS -0.5 0.3 NDS NDS -0.4 -0.20 0.44 N/A N/A
053 0.01 0.003 0.4 1.0 1.4 0.3 0.3 0.1 1.8 0.76 0.65 1.42
054 0.00 -0.007 -1.0 -0.7 -1.0 -0.8 $ 1.4 -0.4 -0.42 0.92 1.00
058 0.00 -0.007 -1.0 1.0 -1.0 -0.8 NDS 0.1 -0.4 -0.35 0.78 1.18
060 0.00 -0.007 -1.0 -0.7 -2.0 -1.9 -1.0 0.1 -1.5 -1.14 0.73 1.26
062 0.01 0.003 0.4 1.0 -1.5 -0.8 NDS 0.1 -1.5 -0.38 1.04 0.88
067 0.02 0.013 1.9 1.0 0.0 -0.8 0.3 -1.2 2.9 0.59 1.46 0.63 X
068 0.00 -0.007 -1.0 -0.7 0.0 0.3 0.3 0.1 0.7 -0.04 0.60 1.53
070 0.01 0.003 0.4 -0.7 -1.5 -1.9 NDS -1.2 -1.5 -1.07 0.82 1.12
073 0.02 0.013 1.9 -0.7 0.0 2.6 3.1 0.1 -0.4 0.94 1.55 0.59 X
079 ** 0.04 R R 0.0 -0.8 -1.0 NDS NDS -0.60 0.53 N/A N/A
085 0.01 0.003 0.4 -0.7 NDS -0.8 -1.0 NDS NDS -0.52 0.63 1.46
087 0.01 0.003 0.4 -0.7 -1.5 -1.9 -1.0 -1.2 -1.5 -1.06 0.75 1.23
088 0.01 0.003 0.4 -0.7 0.4 -0.8 $ -1.2 -0.4 -0.38 0.66 1.39
089 0.00 -0.007 -1.0 2.7 -1.0 0.3 1.7 0.1 0.7 0.50 1.36 0.68 X
091 0.00 -0.007 -1.0 -0.7 0.9 0.3 -1.0 2.7 -0.4 0.11 1.34 0.69 X
092 0.01 0.003 0.4 -0.7 -0.5 R -1.0 -1.2 NDS -0.60 0.62 1.48
096 0.00 -0.007 -1.0 -0.7 2.8 1.4 -1.0 0.1 0.7 0.33 1.42 0.65 X
098 0.01 0.003 0.4 -0.7 NDS -0.8 -1.0 NDS 0.7 -0.28 0.77 1.19
099 <0.01 $ -1.0 R 0.3 0.1 -0.4 -0.25 0.58 1.59
102 ** 0.08 R -0.7 R 0.3 0.3 2.7 0.7 0.66 1.25 0.74 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 144
Sediment - D473
(mass%)
1603 1511 1507 1503 1411 1407
103 0.00 -0.007 -1.0 -0.7 -1.5 -0.8 NDS 0.1 1.8 -0.35 1.17 0.79 X
105 0.01 0.003 0.4 1.0 -0.5 0.3 -1.0 0.1 R 0.05 0.71 1.30
107 0.00 -0.007 -1.0 R 0.0 -1.9 R R NDS -0.97 0.95 N/A N/A
110 0.00 -0.007 -1.0 -0.7 -0.5 $ NDS NDS NDS -0.73 0.25 N/A N/A
112 0.00 -0.007 -1.0 1.0 -0.5 1.4 $ NDS -0.4 0.10 1.04 0.88
117 0.02 0.013 1.9 2.7 -2.0 0.3 0.3 0.1 -0.4 0.41 1.53 0.60 X
118 0.00 -0.007 -1.0 -0.7 -0.5 0.3 0.3 R NDS -0.32 0.59 1.56
120 0.01 0.003 0.4 1.0 -1.0 0.3 0.3 NDS NDS 0.20 0.73 1.26
122 0.00 -0.007 -1.0 R 1.4 1.4 NDS NDS -1.5 0.07 1.54 0.60 X
123 0.01 0.003 0.4 1.0 -1.0 1.4 1.7 0.1 0.7 0.61 0.90 1.02
124 0.01 0.003 0.4 -0.7 0.4 -0.8 -1.0 -1.2 -0.4 -0.47 0.64 1.44
126 0.01 0.003 0.4 R -1.0 -0.8 0.3 -1.2 -0.4 -0.45 0.67 1.37
127 0.01 0.003 0.4 1.0 -1.5 -0.8 0.3 1.4 -0.4 0.06 1.02 0.90
129 0.01 0.003 0.4 1.0 -0.5 -0.8 NDS NDS NDS 0.02 0.83 1.11
132 0.00 -0.007 -1.0 -0.7 0.4 -0.8 1.7 NDS NDS -0.08 1.13 0.81
133 0.00 -0.007 -1.0 -0.7 -0.5 NDS 0.3 -1.2 0.7 -0.40 0.75 1.23
138 0.01 0.003 0.4 -0.7 -0.5 NDS 0.3 -1.2 -0.4 -0.35 0.61 1.51
141 0.00 -0.007 -1.0 1.0 0.0 -0.8 -1.0 0.1 -0.4 -0.30 0.73 1.26
144 0.02 0.013 1.9 NDS 0.9 NDS 0.3 NDS NDS 1.03 0.81 N/A N/A
147 0.00 -0.007 -1.0 -0.7 0.4 0.3 -1.0 NDS NDS -0.40 0.70 1.31
151 0.00 -0.007 -1.0 1.0 -0.5 NDS NDS 0.1 NDS -0.10 0.86 1.07
152 0.00 -0.007 -1.0 -0.7 -0.5 1.4 0.3 2.7 -0.4 0.26 1.34 0.69 X
154 0.03 0.023 3.3 1, 3 R NDS R 1.7 R R 2.50 1.13 N/A N/A
155 0.00 -0.007 -1.0 NDS 0.0 -0.8 0.3 -1.2 -1.5 -0.70 0.70 1.31
161 0.01 0.003 0.4 -0.7 NDS 2.6 0.3 NDS NDS 0.65 1.39 0.66 X
163 0.01 0.003 0.4 -0.7 0.9 0.3 -1.0 0.1 -0.4 -0.06 0.67 1.37
166 0.00 -0.007 -1.0 -0.7 1.4 0.3 0.3 -1.2 -0.4 -0.19 0.91 1.01
167 0.01 0.003 0.4 1.0 0.4 0.3 1.7 NDS NDS 0.76 0.59 1.56
169 0.01 0.003 0.4 -0.7 0.9 -0.8 NDS NDS NDS -0.05 0.83 1.11
170 0.01 0.003 0.4 1.0 0.0 -0.8 -1.0 0.1 -0.4 -0.10 0.70 1.31
176 0.02 0.013 1.9 R 0.0 -0.8 1.7 -1.2 -0.4 0.20 1.30 0.71 X
179 0.00 -0.007 -1.0 -0.7 1.4 0.3 -1.0 0.1 0.7 -0.03 0.92 1.00
181 0.00 -0.007 -1.0 -0.7 -0.5 -1.9 -1.0 0.1 -0.4 -0.77 0.63 1.46
182 ** 0.05 R -0.7 NDS R NDS NDS R -0.70 0.00 N/A N/A
183 ** 0.10 R -0.7 R 0.3 NDS 0.1 R -0.10 0.53 N/A N/A
184 0.02 0.013 1.9 2.7 0.4 0.3 -1.0 NDS NDS 0.86 1.45 0.63 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 145
Sediment - D473
(mass%)
1603 1511 1507 1503 1411 1407
191 0.00 -0.007 -1.0 -0.7 -1.0 -0.8 0.3 0.1 -1.5 -0.66 0.64 1.44
192 ** 0.08 R -0.7 0.0 R 1.7 $ -0.4 0.15 1.07 0.86
193 0.00 -0.007 -1.0 1.0 0.4 -0.8 1.7 1.4 R 0.45 1.13 0.81
196 0.00 -0.007 -1.0 NDS NDS -0.8 0.3 2.7 -0.4 0.16 1.50 0.61 X
204 0.01 0.003 0.4 -0.7 -0.5 -0.8 R 1.4 0.7 0.08 0.89 1.03
207 0.00 -0.007 -1.0 R -1.0 -0.8 0.3 0.1 -1.5 -0.65 0.70 1.31
210 ** 0.04 R 1.0 0.0 1.4 3.1 0.1 NDS 1.12 1.26 0.73 X
211 0.01 0.003 0.4 -0.7 0.4 0.3 -1.0 -1.2 -0.4 -0.31 0.68 1.35
213 0.01 0.003 0.4 -0.7 -0.5 R -1.0 R -1.5 -0.66 0.70 1.31
216 0.01 0.003 0.4 1.0 0.0 1.4 0.3 NDS NDS 0.62 0.57 1.61
218 0.00 -0.007 -1.0 1.0 NDS NDS 1.7 1.4 0.7 0.76 1.05 0.88
220 0.01 0.003 0.4 -0.7 0.9 -0.8 0.3 0.1 0.7 0.13 0.66 1.39
222 0.01 0.003 0.4 -0.7 -0.5 -0.8 0.3 -1.2 -0.4 -0.41 0.58 1.59
223 0.01 0.003 0.4 -0.7 NDS NDS NDS 0.1 0.7 0.12 0.60 1.53
224 0.02 0.013 1.9 1.0 0.4 0.3 0.3 1.4 0.7 0.86 0.61 1.51
226 0.02 0.013 1.9 -0.7 0.9 1.4 -1.0 NDS NDS 0.50 1.29 0.71 X
228 0.00 -0.007 -1.0 $ -1.5 -0.8 $ NDS -1.5 -1.20 0.36 2.56
229 0.01 0.003 0.4 -0.7 0.0 R NDS NDS NDS -0.10 0.56 N/A N/A
232 0.01 0.003 0.4 -0.7 0.0 -0.8 NDS 0.1 0.7 -0.05 0.60 1.53
233 0.00 -0.007 -1.0 NDS NDS 0.3 NDS 0.1 0.7 0.02 0.73 1.26
234 0.01 0.003 0.4 NDS 0.9 -1.9 -1.0 0.1 NDS -0.30 1.13 0.81
241 0.02 0.013 1.9 1.0 1.4 2.6 0.3 -1.2 0.7 0.96 1.22 0.75 X

Legend:
R = Rejected
TPI 1.84
ASTM Crude Oil
Sample ID: CO1607
July 2016 146
Sediment - D473
Comments : (mass%)
147
Page 1 of 2
Sample ID: CO1607
Sediment - D473
(mass%)
0.042 0.049

0.035 Reproducibility 0.042
0.028 0.035
0.021 0.028
0.014 0.021
0.007 0.014
Deviation
0 0.007
-0.007 0
-0.014 -0.007
-0.021 -0.014
-0.028 -0.021

-0.035 Reproducibility -0.028
-0.042 -0.035
3 2 1 2 4 4 4 5 5 5 6 6 8 9 9 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 2 1 4 5 6 1 1 1 1 2 2 2 3 4 5
3 7 9 0 3 6 4 8 9 0 8 9 1 6 0 0 1 1 1 2 3 3 4 4 5 5 5 6 7 7 8 9 9 9 9 9 0 1 2 5 0 2 3 8 4 6 8 0 8 3
3 3 7 0 2 8 2 2 3 1 7 1 2 5 6 3 9 1 1 3 6 7 9 7 8 8

148
Page 2 of 2
Sample ID: CO1607
Sediment - D473
(mass%)
0.042 0.049

0.035 Reproducibility
0.042
0.028 0.035
0.021 0.028
0.014 0.021
0.007 0.014
Deviation
0 0.007
-0.007 0
-0.014 -0.007
-0.021 -0.014
-0.028 -0.021

-0.035 Reproducibility -0.028
-0.042 -0.035
6 7 8 8 8 9 9 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 2 2 2 2 2 2 2 2 2 2 2 8 2 6 7 1 1 2 1 1 1 1 2 2 1
2 0 5 7 8 2 8 0 2 2 2 2 2 2 3 3 4 5 6 6 6 6 6 7 8 9 0 1 1 1 1 2 2 2 2 2 3 3 3 5 7 3 1 1 4 4 1 7 8 2 2 5
5 0 3 4 6 7 9 4 8 2 8 1 2 3 7 9 0 8 0 4 1 3 6 7 0 2 3 7 9 2 4 7 6 7 1 4 9 6 4 4 6 4

149
Sample ID: CO1607

Sediment - D473
(mass%)
63
54
1% Median 99%
45
Number of Labs
36
27
18
0
-0.03 -0.01 0.01 0.03 0.05 0.07

ASTM Crude Oil
Sample ID: CO1607
July 2016 150
Sediment - D4807
(mass%)
1603 1511 1507 1503 1411 1407
003 0.013 0.0007 0.1 0.4 0.2 0.3 -0.1 0.0 R 0.15 0.19 5.26
005 0.022 0.0097 1.3 0.9 -1.0 0.7 -0.2 0.7 NDS 0.40 0.84 1.19
006 0.021 0.0087 1.2 -0.5 NDS 0.4 2.2 0.2 -0.4 0.52 1.03 0.97
009 0.009 -0.0033 -0.4 -0.8 -0.1 -1.2 -1.2 -1.2 0.4 -0.64 0.63 1.59
012 0.010 -0.0023 -0.3 -1.0 -0.8 -0.3 -0.4 NDS NDS -0.56 0.32 3.12
013 0.014 0.0017 0.2 -0.5 -1.1 2.9 -0.2 -1.1 R 0.03 1.49 0.67 X
015 0.007 -0.0053 -0.7 0.4 0.8 NDS 2.2 NDS NDS 0.68 1.20 0.83
016 0.010 -0.0023 -0.3 NDS NDS NDS -0.8 0.1 -0.7 -0.42 0.41 2.44
017 0.011 -0.0013 -0.2 -0.6 -0.1 -1.1 -1.2 -1.1 1.0 -0.47 0.79 1.27
021 0.006 -0.0063 -0.9 -0.8 -1.7 -0.9 -1.1 -1.1 -0.6 -1.01 0.35 2.86
023 0.028 0.0157 2.1 2, 3 4.9 -0.6 R 0.4 -0.1 -0.4 1.05 2.12 0.47 X
025 0.022 0.0097 1.3 NDS NDS NDS -1.4 2.3 NDS 0.73 1.91 N/A N/A
026 0.014 0.0017 0.2 0.5 NDS 0.7 0.9 NDS NDS 0.57 0.30 3.33
030 0.016 0.0037 0.5 -0.9 0.3 1.9 2.6 -1.3 -1.5 0.23 1.59 0.63 X
032 0.010 -0.0023 -0.3 NDS 0.7 -0.6 -0.1 -0.9 NDS -0.24 0.61 1.64
037 0.010 -0.0023 -0.3 NDS 0.8 -0.5 -0.6 -0.1 NDS -0.14 0.56 1.79
045 0.007 -0.0053 -0.7 -0.4 -1.4 -0.5 -0.6 -0.5 0.4 -0.53 0.53 1.89
047 0.012 -0.0003 0.0 -0.4 0.6 -1.1 -0.4 -0.6 -0.1 -0.29 0.53 1.89
048 0.006 -0.0063 -0.9 NDS NDS -1.6 -1.2 -0.8 -1.1 -1.12 0.31 3.23
051 0.008 -0.0043 -0.6 NDS -0.2 NDS 1.7 NDS NDS 0.30 1.23 N/A N/A
054 0.016 0.0037 0.5 2.9 -0.2 NDS NDS -0.6 NDS 0.65 1.57 0.64 X
055 0.000 -0.0123 -1.7 NDS NDS NDS -1.4 R NDS -1.55 0.21 N/A N/A
060 0.035 0.0227 3.1 1, 2, 3 -1.0 -2.0 -1.3 NDS 0.5 NDS -0.14 2.03 0.49 X
066 0.016 0.0037 0.5 R 3.3 -1.0 0.5 0.7 R 0.80 1.56 0.64 X
067 ** 0.045 R R -0.1 0.9 R -0.9 NDS -0.03 0.90 N/A N/A
074 0.019 0.0067 0.9 3.3 -0.2 -0.2 -0.5 R R 0.66 1.57 0.64 X
078 0.011 -0.0013 -0.2 -0.1 -1.9 -0.2 -0.9 -0.9 -0.1 -0.61 0.67 1.49
082 ** 0.126 R NDS -0.2 -1.3 NDS 1.3 0.4 0.05 1.09 0.92
089 0.024 0.0117 1.6 -0.8 -1.3 0.1 -0.8 -0.9 0.3 -0.26 1.00 1.00
091 0.001 -0.0113 -1.5 -1.0 0.3 -0.4 0.4 NDS -0.3 -0.42 0.74 1.35
092 0.010 -0.0023 -0.3 3.2 -0.4 -0.4 NDS -0.3 NDS 0.36 1.59 0.63 X
096 0.010 -0.0023 -0.3 0.6 1.7 -0.1 0.0 -0.6 1.1 0.34 0.83 1.20
100 0.013 0.0007 0.1 -0.4 -2.2 NDS -1.2 -1.0 -0.5 -0.87 0.80 1.25
101 0.036 0.0237 3.2 1, 2, 3 -0.9 -0.4 NDS 0.7 2.5 -1.4 0.62 1.88 0.53 X
102 ** 0.236 R -0.6 -1.6 R NDS NDS NDS -1.10 0.71 N/A N/A
103 0.008 -0.0043 -0.6 -1.0 0.3 -1.0 0.9 0.1 NDS -0.22 0.77 1.30
106 0.022 0.0097 1.3 2.8 R R NDS NDS NDS 2.05 1.06 N/A N/A
108 0.010 -0.0023 -0.3 NDS NDS NDS -0.9 1.2 0.6 0.15 0.93 1.08
112 0.004 -0.0083 -1.1 $ -0.4 -1.0 -1.2 NDS -0.8 -0.90 0.32 3.12
ASTM Crude Oil
Sample ID: CO1607
July 2016 151
Sediment - D4807
(mass%)
1603 1511 1507 1503 1411 1407
118 0.009 -0.0033 -0.4 -0.3 NDS 2.4 -0.4 NDS NDS 0.32 1.38 0.72 X
123 0.001 -0.0113 -1.5 0.5 -0.8 1.2 0.9 0.9 -0.5 0.10 1.03 0.97
124 0.006 -0.0063 -0.9 -0.5 -0.2 -1.3 -1.0 -1.0 -0.7 -0.80 0.37 2.70
127 0.010 -0.0023 -0.3 0.3 -2.0 -1.2 -0.5 1.6 -0.6 -0.39 1.14 0.88
131 0.012 -0.0003 0.0 R 3.5 1.2 0.1 1.2 -1.2 0.80 1.60 0.62 X
132 0.009 -0.0033 -0.4 -0.8 1.8 -1.0 0.8 NDS NDS 0.08 1.19 0.84
138 0.029 0.0167 2.3 2, 3 1.9 -0.2 NDS 1.3 1.1 1.5 1.32 0.86 1.16
147 0.011 -0.0013 -0.2 -0.6 0.3 -0.3 -0.8 NDS NDS -0.32 0.42 2.38
148 0.020 0.0077 1.0 -1.0 0.0 R 2.9 1.4 1.4 0.95 1.34 0.75 X
152 0.014 0.0017 0.2 -0.1 R 0.5 -0.4 -0.5 -1.1 -0.23 0.56 1.79
154 ** 0.050 R NDS NDS 2.2 2.2 NDS 2.3 2.23 0.06 N/A N/A
155 0.008 -0.0043 -0.6 1.4 -1.3 1.5 -0.5 -0.6 -1.1 -0.17 1.15 0.87
161 0.025 0.0127 1.7 R NDS 0.1 R NDS NDS 0.90 1.13 N/A N/A
164 0.011 -0.0013 -0.2 NDS 0.9 NDS 0.6 NDS -0.5 0.20 0.66 1.52
165 0.009 -0.0033 -0.4 NDS NDS NDS NDS -0.7 0.1 -0.33 0.40 N/A N/A
166 0.016 0.0037 0.5 -0.1 0.0 0.4 -0.6 -1.1 0.5 -0.06 0.61 1.64
181 0.010 -0.0023 -0.3 0.1 0.2 0.4 NDS -0.3 1.2 0.22 0.56 1.79
185 0.014 0.0017 0.2 -0.5 1.8 NDS R -0.9 -0.9 -0.06 1.13 0.88
189 0.030 0.0177 2.4 2, 3 2.8 0.3 1.5 0.4 NDS NDS 1.48 1.13 0.88
191 0.011 -0.0013 -0.2 -0.6 1.3 -0.5 0.6 NDS NDS 0.12 0.81 1.23
194 ** 0.044 R 1.4 2.4 0.4 1.1 1.0 0.5 1.13 0.73 1.37
202 0.012 -0.0003 0.0 -0.5 0.8 NDS NDS NDS NDS 0.10 0.66 N/A N/A
210 0.016 0.0037 0.5 0.3 1.6 -0.3 R 0.1 0.2 0.40 0.64 1.56
211 0.007 -0.0053 -0.7 -0.9 -0.4 -0.6 -1.0 -1.2 -0.7 -0.79 0.27 3.70
214 ** 0.050 R 2.8 0.3 -0.6 -0.1 NDS NDS 0.60 1.51 0.66 X
215 0.010 -0.0023 -0.3 -0.5 -0.1 -0.8 -0.3 -0.6 0.5 -0.30 0.42 2.38
216 ** 0.045 R NDS NDS -0.8 1.7 NDS NDS 0.45 1.77 N/A N/A
220 0.010 -0.0023 -0.3 -0.4 NDS -0.8 -1.1 NDS NDS -0.65 0.37 2.70
224 0.029 0.0167 2.3 2, 3 NDS 0.2 1.0 NDS 1.0 NDS 1.12 0.87 1.15
ASTM Crude Oil
Sample ID: CO1607
July 2016 152
Sediment - D4807
(mass%)
Legend:
R = Rejected
TPI 0.63
Comments:
153
Sample ID: CO1607

Sediment - D4807
(mass%)
0.0296 0.0419
0.0222 0.0345
0.0148 0.0271
Reproducibility
0.0074 0.0197
Deviation
0 0.0123
-0.0074 0.0049

Reproducibility
-0.0148 -0.0025
-0.0222 -0.0099
-0.0296 -0.0173
1 5 9 1 1 4 1 1 2 4 2 1 2 4 1 5 5 1 1 1 1 9 1 1 1 1 9 9 3 3 1 2 1 2 1 1 1 1 7 1 1 2 4 1 1 3 1 1 1 2 1 5 2 5 3 6 1 7 1 6 2 5 1 4 8 1 2 7 1 2 1 6 1
7 5 1 2 1 1 3 1 0 8 1 2 1 5 5 1 0 2 5 0 1 3 6 2 0 6 2 7 2 6 2 2 1 8 7 7 9 8 6 4 0 7 3 0 5 3 3 6 8 8 1 4 0 6 6 4 4 5 0 4 9 6 3 9 3 2 8 0 0
3 3 0 4 2 0 4 1 1 5 3 8 2 5 7 8 0 5 1 7 1 4 7 2 1 0 2 0 5 0 6 8 6 1 8 4 9 1

154
Sample ID: CO1607

Sediment - D4807
(mass%)
32
28
Median
1% 99%
24
20
Number of Labs
16
12
0
-0.004 - 0 0.001 - 0.005 0.006 - 0.01 0.011 - 0.015 0.016 - 0.02 0.021 - 0.025 0.026 - 0.03 0.031 - 0.035 0.036 - 0.04
ASTM Crude Oil
Sample ID: CO1607
July 2016 155
Sulfur - D2622
(mass%)
1603 1511 1507 1503 1411 1407
011 0.19 0.002 0.3 NDS -0.4 -0.3 -0.7 NDS NDS -0.28 0.42 2.26
015 0.192 0.004 0.6 0.1 0.8 NDS 0.1 NDS NDS 0.40 0.36 2.64
020 0.1873 -0.001 -0.1 -0.4 -0.9 -0.5 -0.1 0.5 0.1 -0.20 0.45 2.11
025 0.187 -0.001 -0.1 NDS R NDS R 3.4 NDS 1.65 2.47 N/A N/A
026 0.193 0.005 0.7 2.3 NDS NDS 1.6 NDS NDS 1.53 0.80 N/A N/A
029 0.186 -0.002 -0.3 2.1 0.8 NDS -0.4 NDS NDS 0.55 1.17 0.81
030 0.195 0.007 1.0 -0.2 -1.4 -2.7 0.0 0.2 2.7 -0.06 1.71 0.56 X
042 0.1737 -0.014 -2.0 -0.9 -0.3 0.3 NDS -1.4 NDS -0.86 0.90 1.06
054 0.184925 -0.003 -0.4 -0.3 NDS NDS NDS -1.2 NDS -0.63 0.49 N/A N/A
069 0.2 0.012 1.7 -0.3 0.0 2.2 1.3 0.8 0.0 0.81 0.96 0.99
071 0.19 0.002 0.3 0.0 0.4 -1.3 0.7 -0.2 0.0 -0.01 0.64 1.48
086 0.182 -0.006 -0.9 -1.0 1.0 -0.9 -0.5 -2.8 -1.4 -0.93 1.13 0.84
089 0.188 0.000 0.0 -0.1 -0.1 -0.3 -0.7 0.0 0.1 -0.16 0.27 3.52
093 0.195 0.007 1.0 1.3 -0.4 R -3.0 NDS NDS -0.28 1.96 0.48 X
131 0.1752 -0.013 -1.8 -0.4 -1.6 0.7 R -1.4 -0.6 -0.85 0.94 1.01
137 0.1907 0.003 0.4 -1.5 NDS NDS NDS -0.2 -0.1 -0.35 0.81 1.17
139 0.201 0.013 1.9 -3.7 -2.3 -2.9 -2.1 -2.2 -0.8 -1.73 1.82 0.52 X
141 0.194 0.006 0.9 -0.6 0.6 0.0 -0.5 0.6 0.6 0.23 0.60 1.58
147 0.1943 0.006 0.9 2.2 1.0 1.1 0.7 NDS NDS 1.18 0.59 1.61
150 0.1845 -0.003 -0.5 0.0 0.2 -0.4 0.5 0.9 1.5 0.31 0.72 1.32
152 0.186 -0.002 -0.3 -0.1 0.4 0.5 0.8 0.6 1.0 0.41 0.47 2.02
157 0.18 -0.008 -1.1 -1.7 0.6 -0.6 0.2 0.8 -1.2 -0.43 0.97 0.98
166 0.183 -0.005 -0.7 0.7 0.4 -0.3 -0.8 0.8 NDS 0.02 0.71 1.34
175 0.185 -0.003 -0.4 0.3 -0.1 -0.2 0.3 2.0 1.0 0.41 0.84 1.13
182 0.204 0.016 2.3 3 1.3 NDS NDS NDS NDS R 1.80 0.71 N/A N/A
201 0.188 0.000 0.0 R NDS R R R -0.7 -0.35 0.49 N/A N/A
203 0.18 -0.008 -1.1 0.0 -0.6 -2.2 0.1 -1.4 -1.1 -0.90 0.81 1.17
224 0.1963 0.008 1.2 2.0 1.1 NDS 1.8 0.4 NDS 1.30 0.63 1.51
233 0.189 0.001 0.1 0.1 0.2 0.3 -1.9 -0.2 NDS -0.23 0.83 1.14
ASTM Crude Oil
Sample ID: CO1607
July 2016 156
Sulfur - D2622
(mass%)
Legend:
R = Rejected
TPI 0.95
Comments:

Labs: 071, 157, 203.
157
Sample ID: CO1607

Sulfur - D2622
(mass%)
0.028 0.216
0.021 0.209
Reproducibility
0.014 0.202
0.007 0.195
Deviation
0 0.188
-0.007 0.181
-0.014 0.174
Reproducibility
-0.021 0.167
-0.028 0.16
1 4 1 1 1 2 8 2 1 1 7 5 1 1 2 1 2 2 2 8 9 2 9 7 1 1 1 1 1 2 1 1 9 3 2 6 1 1
8 2 3 5 7 0 6 1 6 6 9 4 7 5 9 5 0 5 0 9 4 3 0 1 1 8 3 6 5 6 4 4 3 0 2 9 3 8
4 1 7 0 3 6 6 0 5 0 2 1 3 9 7 9 1 7 4 9 2

158
Sample ID: CO1607

Sulfur - D2622
(mass%)
21
Median
1% 99%
18
15
Number of Labs
12
0
0.16 0.17 0.18 0.19 0.2 0.21 0.22
ASTM Crude Oil
Sample ID: CO1607
July 2016 159
Sulfur - D4294
(mass%)
1603 1511 1507 1503 1411 1407
003 0.184 -0.006 -0.9 -0.2 -1.0 -1.3 -0.9 -0.9 -0.4 -0.80 0.37 2.70
005 0.182 -0.008 -1.1 0.0 -1.0 -0.6 0.1 0.4 -0.8 -0.43 0.59 1.69
006 0.191 0.001 0.1 -0.5 1.2 1.2 0.5 0.4 0.9 0.54 0.62 1.61
007 0.19 0.000 0.0 0.0 0.4 -0.8 0.9 NDS NDS 0.10 0.62 1.61
008 0.18 -0.010 -1.4 1.8 1.0 R 1.3 R NDS 0.68 1.42 0.70 X
010 0.193 0.003 0.4 2.0 0.6 0.8 0.5 0.1 0.7 0.73 0.60 1.67
012 0.1917 0.002 0.2 1.6 -0.3 0.6 -0.2 NDS NDS 0.38 0.77 1.30
013 0.193 0.003 0.4 0.0 -0.2 1.3 R 0.1 0.1 0.28 0.53 1.89
015 0.196 0.006 0.9 0.0 0.6 NDS -0.2 NDS NDS 0.32 0.51 1.96
016 0.198 0.008 1.1 NDS NDS NDS 0.8 0.3 R 0.73 0.40 N/A N/A
017 0.191 0.001 0.1 R 0.0 -0.2 -1.8 -0.9 -0.9 -0.62 0.73 1.37
019 0.186 -0.004 -0.6 2.2 0.2 R -1.5 NDS -2.2 -0.38 1.70 0.59 X
021 0.175 -0.015 -2.1 3 1.8 -0.9 -2.3 -1.3 R 0.9 -0.65 1.66 0.60 X
023 0.188 -0.002 -0.3 -0.2 -2.0 0.4 -0.9 0.6 0.3 -0.30 0.91 1.10
024 0.192 0.002 0.3 R 2.1 0.8 -3.0 -2.4 NDS -0.44 2.18 0.46 X
025 0.2 0.010 1.4 NDS -0.2 NDS NDS 0.9 0.5 0.65 0.68 1.47
026 0.181 -0.009 -1.3 3.8 1.0 0.5 0.5 NDS NDS 0.90 1.84 0.54 X
027 0.19 0.000 0.0 -0.2 -1.0 0.1 NDS -0.3 -0.8 -0.37 0.44 2.27
028 ** 0.162 R -2.8 2.5 -0.4 -0.6 NDS 1.4 0.02 2.04 0.49 X
029 0.198 0.008 1.1 0.4 R 1.2 0.0 0.1 -0.9 0.32 0.78 1.28
030 0.193 0.003 0.4 -0.4 -2.6 -1.1 -1.0 0.0 0.2 -0.64 1.04 0.96
031 0.184 -0.006 -0.9 0.8 -0.4 0.3 0.2 R 2.0 0.33 1.01 0.99
032 0.19 0.000 0.0 NDS 1.6 0.5 0.4 -0.6 NDS 0.38 0.81 1.23
033 0.19247 0.003 0.4 NDS -1.9 0.8 NDS -1.0 R -0.42 1.25 0.80
035 0.187 -0.003 -0.4 0.2 0.0 NDS NDS NDS NDS -0.07 0.31 N/A N/A
037 0.188 -0.002 -0.3 NDS 1.0 0.4 R -0.7 NDS 0.10 0.75 1.33
043 ** 0.16 R 1.5 0.8 -0.9 NDS -1.3 -0.5 -0.08 1.18 0.85
044 0.189 -0.001 -0.1 R NDS NDS NDS NDS NDS -0.10 0.00 N/A N/A
045 0.189 -0.001 -0.1 -0.2 0.4 0.0 0.5 0.3 0.6 0.21 0.31 3.23
046 0.187 -0.003 -0.4 0.5 0.4 0.2 0.2 NDS NDS 0.18 0.35 2.86
048 0.192 0.002 0.3 NDS NDS NDS 0.9 1.9 1.2 1.08 0.67 1.49
049 0.198 0.008 1.1 0.2 1.0 -0.7 0.4 NDS 0.5 0.42 0.65 1.54
051 0.21 0.020 2.9 3 NDS 1.0 NDS -0.4 NDS NDS 1.17 1.66 N/A N/A
053 0.186 -0.004 -0.6 -1.2 -0.7 0.6 -0.4 -0.6 -0.3 -0.46 0.55 1.82
054 0.18941 0.000 -0.1 -0.5 -1.4 -2.7 0.4 1.0 R -0.55 1.33 0.75 X
055 0.1861 -0.003 -0.6 2.0 -1.3 R R 0.4 -1.3 -0.16 1.39 0.72 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 160
Sulfur - D4294
(mass%)
1603 1511 1507 1503 1411 1407
057 0.185 -0.005 -0.7 -0.5 2.8 1.5 R R 0.8 0.78 1.45 0.69 X
058 0.185 -0.005 -0.7 -0.5 -1.8 1.5 NDS -0.6 -2.3 -0.73 1.32 0.76 X
060 0.196 0.006 0.9 -0.1 0.4 0.1 0.9 -0.4 0.6 0.34 0.50 2.00
061 0.188 -0.002 -0.3 NDS 0.4 0.1 2.2 0.1 0.1 0.43 0.89 1.12
063 0.185 -0.005 -0.7 NDS -0.1 R NDS NDS NDS -0.40 0.42 N/A N/A
064 0.19 0.000 0.0 1.4 -0.6 0.6 NDS -1.7 0.6 0.05 1.09 0.92
066 ** 0.23 R 1.9 3.1 0.5 0.5 R 3.6 1.92 1.44 0.69 X
067 0.194 0.004 0.6 0.8 1.2 0.9 0.5 0.9 -0.7 0.60 0.62 1.61
068 0.189 -0.001 -0.1 -0.2 0.4 -1.3 -0.8 -0.1 -0.7 -0.40 0.57 1.75
069 0.186 -0.004 -0.6 -0.4 0.4 0.3 -0.2 NDS -1.3 -0.30 0.63 1.59
072 ** 0.3 R NDS 0.4 -0.8 -1.2 2.6 3.3 0.86 2.01 0.50 X
073 0.19 0.000 0.0 1.8 1.0 -1.4 R 1.1 -1.5 0.17 1.38 0.72 X
074 0.194 0.004 0.6 R -2.2 -2.2 -2.2 0.1 -1.8 -1.28 1.28 0.78 X
077 0.189 -0.001 -0.1 -0.4 -2.2 -0.4 0.4 -0.6 0.6 -0.39 0.91 1.10
078 0.189 -0.001 -0.1 0.2 -0.2 0.0 -0.8 0.0 0.1 -0.11 0.33 3.03
079 0.202 0.012 1.7 3.0 -0.4 0.6 1.3 NDS NDS 1.24 1.27 0.79 X
080 0.18 -0.010 -1.4 -0.8 -0.6 0.6 NDS -1.7 -2.2 -1.02 0.98 1.02
081 0.192 0.002 0.3 -0.2 NDS 0.3 0.5 NDS NDS 0.22 0.30 3.33
083 0.1896 0.000 -0.1 0.2 1.5 -0.2 1.5 NDS 0.3 0.53 0.77 1.30
084 ** 0.224 R -0.2 0.0 -1.3 1.6 1.3 -0.9 0.08 1.16 0.86
085 ** 0.16 R R NDS -1.2 -1.1 NDS NDS -1.15 0.07 N/A N/A
087 0.18 -0.010 -1.4 -0.8 -3.0 -0.4 -0.8 -1.7 -0.7 -1.26 0.89 1.12
088 0.189 -0.001 -0.1 0.5 R -0.2 1.0 -0.5 0.1 0.13 0.54 1.85
089 0.177 -0.013 -1.9 -0.4 -1.0 -0.9 -1.5 -1.0 0.9 -0.83 0.90 1.11
091 0.19 0.000 0.0 0.2 -0.4 -0.1 0.4 0.3 0.5 0.13 0.31 3.23
092 0.188 -0.002 -0.3 0.2 NDS -0.3 0.5 -0.4 NDS -0.06 0.39 2.56
095 ** 0.219 R -3.4 NDS NDS NDS NDS NDS -3.40 0.00 N/A N/A
096 0.195 0.005 0.7 1.0 0.6 0.2 0.3 1.7 0.5 0.71 0.51 1.96
097 0.202 0.012 1.7 R R NDS R 1.7 -1.1 0.77 1.62 N/A N/A
099 0.2 0.010 1.4 -0.2 -0.3 -1.3 0.2 1.3 2.3 0.49 1.23 0.81
100 0.191 0.001 0.1 0.4 0.7 NDS 0.2 0.1 0.3 0.30 0.23 4.35
102 0.185 -0.005 -0.7 -1.0 0.0 -0.3 -2.5 -0.3 -0.3 -0.73 0.85 1.18
103 0.194 0.004 0.6 0.1 0.6 1.6 0.2 0.9 1.3 0.76 0.55 1.82
105 0.19 0.000 0.0 0.0 0.5 0.1 1.8 0.6 0.5 0.50 0.63 1.59
106 0.2071 0.018 2.4 3 0.4 0.3 R NDS NDS NDS 1.03 1.18 N/A N/A
108 0.19 0.000 0.0 -0.8 NDS -1.0 -1.2 -0.3 -0.7 -0.67 0.45 2.22
110 0.188 -0.002 -0.3 -1.1 -1.6 1.4 NDS NDS NDS -0.40 1.31 0.76 X
112 0.189 -0.001 -0.1 0.5 0.8 0.1 0.9 NDS 0.5 0.45 0.39 2.56
114 0.205 0.015 2.1 3 -2.2 -2.2 1.1 -2.7 NDS NDS -0.78 2.21 0.45 X
117 0.192 0.002 0.3 1.2 0.6 0.6 0.5 0.6 -0.2 0.51 0.42 2.38
118 0.1836 -0.006 -0.9 -0.1 -1.8 0.6 0.2 0.5 0.1 -0.20 0.86 1.16
119 0.2 0.010 1.4 NDS NDS -1.1 NDS NDS NDS 0.15 1.77 N/A N/A
120 0.19 0.000 0.0 0.2 NDS 1.4 0.1 NDS NDS 0.42 0.66 1.52
ASTM Crude Oil
Sample ID: CO1607
July 2016 161
Sulfur - D4294
(mass%)
1603 1511 1507 1503 1411 1407
122 0.171 -0.019 -2.7 3 -3.8 -1.1 1.5 NDS NDS 0.3 -1.16 2.15 0.47 X
123 0.185 -0.005 -0.7 -0.5 0.0 0.7 -0.2 -1.1 -0.7 -0.36 0.59 1.69
124 0.194 0.004 0.6 -0.2 -0.1 0.2 -0.2 2.6 0.5 0.49 0.99 1.01
125 0.1974 0.008 1.1 2.0 0.1 NDS -2.7 NDS NDS 0.12 2.04 0.49 X
126 0.184 -0.006 -0.9 1.5 -0.2 R -0.9 -0.9 -3.3 -0.78 1.54 0.65 X
127 0.195 0.005 0.7 -0.2 0.0 0.0 -0.2 -0.7 -0.3 -0.10 0.42 2.38
129 ** 0.158 R 0.7 0.6 0.7 0.9 NDS NDS 0.72 0.13 7.69
132 0.197 0.007 1.0 0.1 0.9 -0.8 2.6 NDS -2.5 0.22 1.74 0.57 X
133 0.194 0.004 0.6 1.4 0.0 NDS 1.9 1.1 2.0 1.17 0.77 1.30
134 ** 0.237 R R -1.5 NDS NDS NDS NDS -1.50 0.00 N/A N/A
135 ** 0.284 R -1.0 -2.5 R R NDS NDS -1.75 1.06 N/A N/A
136 0.184 -0.006 -0.9 -0.8 1.0 0.5 0.0 -0.3 0.9 0.06 0.77 1.30
137 0.1933 0.004 0.5 1.4 NDS NDS NDS R -3.5 -0.53 2.61 N/A N/A
138 0.185 -0.005 -0.7 -0.2 -2.6 -1.2 -0.9 -1.4 -0.2 -1.03 0.83 1.20
140 0.1841 -0.005 -0.8 -0.3 0.3 0.1 0.0 -0.1 0.2 -0.09 0.37 2.70
143 0.188 -0.002 -0.3 -1.2 -0.1 1.7 -0.5 -0.9 -2.3 -0.51 1.22 0.82
144 0.196 0.006 0.9 NDS -0.6 NDS 0.5 NDS NDS 0.27 0.78 N/A N/A
145 0.185 -0.005 -0.7 -0.1 -0.6 0.4 -0.2 -1.3 -0.7 -0.46 0.54 1.85
147 0.183 -0.007 -1.0 0.0 1.0 0.3 0.0 NDS NDS 0.06 0.72 1.39
148 0.187 -0.003 -0.4 -0.5 0.0 0.4 0.6 0.0 0.7 0.11 0.47 2.13
149 0.189 -0.001 -0.1 -0.2 NDS 0.0 0.0 0.1 1.4 0.20 0.60 1.67
151 0.192 0.002 0.3 0.0 0.6 NDS NDS 0.4 NDS 0.32 0.25 4.00
152 0.191 0.001 0.1 -0.2 1.4 0.4 2.2 0.3 -2.4 0.26 1.44 0.69 X
154 0.194 0.004 0.6 0.2 NDS 0.0 0.5 0.9 0.0 0.37 0.36 2.78
155 0.185 -0.005 -0.7 NDS 0.0 -0.1 -0.2 -0.3 -0.5 -0.30 0.26 3.85
158 0.199 0.009 1.3 NDS NDS -0.7 NDS 2.4 1.7 1.18 1.33 0.75 X
159 0.181 -0.009 -1.3 -2.1 1.0 -1.4 0.9 0.0 2.0 -0.13 1.51 0.66 X
161 0.193 0.003 0.4 2.2 NDS 0.2 0.1 NDS NDS 0.73 0.99 1.01
163 0.186 -0.004 -0.6 0.2 0.2 0.8 0.5 0.0 1.1 0.31 0.56 1.79
164 0.193 0.003 0.4 NDS -0.6 NDS 0.0 NDS 0.7 0.12 0.56 1.79
166 0.189 -0.001 -0.1 -0.1 0.0 -0.3 0.5 -0.4 -0.9 -0.19 0.43 2.33
167 0.184 -0.006 -0.9 -2.2 0.2 0.8 -1.0 NDS NDS -0.62 1.16 0.86
168 ** 0.165 R NDS 0.2 2.1 NDS -2.0 R 0.10 2.05 N/A N/A
170 0.187 -0.003 -0.4 0.0 NDS 0.9 -1.4 0.9 0.2 0.03 0.87 1.15
171 0.1852 -0.004 -0.7 0.7 0.1 1.4 0.8 -1.7 R 0.10 1.13 0.88
172 0.198 0.008 1.1 -0.1 1.4 -1.1 -0.2 0.3 1.1 0.36 0.90 1.11
174 0.199 0.009 1.3 NDS NDS R -1.9 0.9 NDS 0.10 1.74 N/A N/A
176 0.195 0.005 0.7 0.0 -0.1 0.6 0.0 -0.4 0.2 0.14 0.39 2.56
181 0.191 0.001 0.1 R -0.3 R -1.6 R 0.2 -0.40 0.83 1.20
ASTM Crude Oil
Sample ID: CO1607
July 2016 162
Sulfur - D4294
(mass%)
1603 1511 1507 1503 1411 1407
183 0.189 -0.001 -0.1 -1.0 R 0.7 0.3 0.1 -0.7 -0.12 0.63 1.59
184 0.197 0.007 1.0 0.8 0.4 1.4 0.0 NDS NDS 0.72 0.54 1.85
191 0.189 -0.001 -0.1 0.5 -1.0 0.0 0.0 0.0 0.3 -0.04 0.47 2.13
192 0.184 -0.006 -0.9 -0.6 -0.1 -0.2 0.5 -0.4 0.4 -0.19 0.51 1.96
193 0.192 0.002 0.3 0.1 0.8 -0.3 1.8 0.9 0.9 0.64 0.68 1.47
194 0.194 0.004 0.6 1.8 0.4 1.2 0.5 0.3 0.8 0.80 0.53 1.89
196 ** 0.248 R NDS NDS -0.7 2.6 2.6 3.3 1.95 1.80 0.56 X
198 0.18 -0.010 -1.4 -0.8 -0.2 0.0 -1.8 -0.9 -0.5 -0.80 0.64 1.56
204 0.193 0.003 0.4 0.2 0.2 0.6 0.5 -1.0 -0.7 0.03 0.62 1.61
206 0.193 0.003 0.4 0.7 1.6 NDS 3.0 NDS NDS 1.42 1.17 0.85
209 0.176 -0.014 -2.0 -1.9 -1.2 NDS -1.5 NDS -2.3 -1.78 0.43 2.33
210 0.198 0.008 1.1 -0.5 1.4 0.7 -0.3 1.6 1.5 0.79 0.86 1.16
211 0.188 -0.002 -0.3 -0.4 -1.6 -1.8 -1.2 -0.7 -1.6 -1.09 0.62 1.61
212 0.198 0.008 1.1 2.6 0.9 -1.1 -0.5 NDS NDS 0.60 1.45 0.69 X
213 0.197 0.007 1.0 -0.1 1.1 -0.3 0.2 0.1 R 0.33 0.58 1.72
214 0.191 0.001 0.1 -0.2 -0.2 0.0 0.9 NDS NDS 0.12 0.45 2.22
215 0.196 0.006 0.9 0.6 0.2 NDS 2.6 1.1 1.0 1.07 0.82 1.22
216 0.173 -0.017 -2.4 3 -1.2 0.4 -0.6 0.1 NDS NDS -0.74 1.12 0.89
218 0.182 -0.008 -1.1 3.8 NDS NDS 0.5 -0.9 0.3 0.52 1.97 0.51 X
220 0.191 0.001 0.1 R 0.2 0.4 1.3 1.6 -0.1 0.58 0.70 1.43
223 0.1885 -0.001 -0.2 -0.6 NDS NDS NDS -1.0 0.1 -0.42 0.48 2.08
224 0.1893 0.000 -0.1 -0.2 0.5 0.4 0.1 0.1 R 0.13 0.27 3.70
226 0.197 0.007 1.0 1.5 0.0 1.3 0.1 NDS NDS 0.78 0.69 1.45
228 0.191 0.001 0.1 0.5 0.8 0.9 0.5 NDS 0.7 0.58 0.29 3.45
229 0.1935 0.004 0.5 -0.4 1.8 -0.7 NDS NDS NDS 0.30 1.12 0.89
230 0.178 -0.012 -1.7 0.0 NDS -1.2 1.5 -0.9 1.6 -0.12 1.40 0.71 X
231 0.204 0.014 2.0 R 0.0 -2.1 -2.3 0.5 -0.3 -0.37 1.63 0.61 X
234 0.193 0.003 0.4 -1.1 -2.6 -1.2 0.5 -0.3 NDS -0.72 1.17 0.85
235 0.2 0.010 1.4 -0.8 2.0 R NDS 1.1 2.7 1.28 1.31 0.76 X
236 0.206 0.016 2.3 3 -1.1 NDS -0.2 0.8 NDS NDS 0.45 1.46 0.68 X
240 0.1819 -0.008 -1.2 NDS 0.0 -1.4 NDS NDS NDS -0.87 0.76 N/A N/A
241 0.1951 0.006 0.7 0.8 0.4 -0.8 -1.1 0.0 R 0.00 0.79 1.27
ASTM Crude Oil
Sample ID: CO1607
July 2016 163
Sulfur - D4294
(mass%)
Legend:
R = Rejected
TPI 1.32
Comments:
164
Page 1 of 3
Sample ID: CO1607
Sulfur - D4294
(mass%)
0.028 0.218
Reproducibility
0.021 0.211
0.014 0.204
0.007 0.197
Deviation
0 0.19
-0.007 0.183
-0.014 0.176
-0.021 0.169
Reproducibility
-0.028 0.162
1 2 2 5 2 8 2 8 1 4 1 8 8 1 2 2 1 2 1 5 4 2 2 1 3 1 1 3 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 5 5 6 6 1 5 1 1 6 1 1
2 1 1 0 0 9 3 9 1 5 0 7 9 6 1 5 1 8 4 3 4 1 2 1 7 6 6 3 9 8 0 1 2 3 4 4 5 1 2 7 8 3 9 9 3 9 7 2 6 7
2 6 9 0 7 3 8 9 9 8 0 7 7 6 8 7 7 2 6 2 8 2 6 3 8 0 5 5 7 7 9 1 3 0

165
Page 2 of 3
Sample ID: CO1607
Sulfur - D4294
(mass%)
0.028 0.218
Reproducibility
0.021 0.211
0.014 0.204
0.007 0.197
Deviation
0 0.19
-0.007 0.183
-0.014 0.176
-0.021 0.169

Reproducibility
-0.028 0.162
4 5 1 1 3 1 2 2 1 1 3 6 9 8 7 7 6 4 4 4 2 2 1 1 1 1 1 1 1 2 7 2 3 5 6 7 8 9 1 1 2 1 1 6 2 2 2 1 1 1 1 8 4 1 1
6 5 4 9 5 4 1 3 1 4 7 1 2 8 8 7 8 5 4 0 2 9 8 6 4 1 2 2 2 7 2 4 4 3 3 1 0 0 1 0 7 2 2 0 8 5 2 5 1 8 1 9
2 0 8 1 0 3 3 1 3 6 9 2 0 8 4 5 8 4 0 8 0 0 1 2 1 7 3

166
Page 3 of 3
Sample ID: CO1607
Sulfur - D4294
(mass%)
0.028 0.218
Reproducibility
0.021 0.211
0.014 0.204
0.007 0.197
Deviation
0 0.19
-0.007 0.183
-0.014 0.176
-0.021 0.169
Reproducibility
-0.028 0.162
2 2 2 1 3 3 1 1 1 2 6 1 1 1 2 1 1 1 7 9 1 1 1 2 6 1 2 1 2 2 1 1 1 1 4 2 1 2 2 1 1 1 2 2 9 2 2 7 9 2 1 2 1 5
4 0 0 3 0 3 6 0 6 3 7 0 9 5 2 3 3 2 4 6 7 2 5 1 0 4 4 3 1 2 7 8 2 7 9 9 6 1 1 5 7 1 2 5 9 3 2 9 7 3 1 3 0 1
6 4 1 4 4 3 4 4 9 3 7 4 6 7 5 4 1 2 3 6 3 4 5 2 0 2 8 4 9 5 5 1 4 6 6

167
Sample ID: CO1607

Sulfur - D4294
(mass%)
98
Median
1% 99%
84
70
Number of Labs
56
42
28
14
0
0.13 0.14 0.15 0.16 0.17 0.18 0.19 0.2 0.21 0.22 0.23 0.24 0.25
ASTM Crude Oil
Sample ID: CO1607
July 2016 168
ICP with an Organic Solvent Specimen Solution - D5708 Method A
Iron (mg/kg)
1603 1511 1507 1503 1411 1407
015 2.86 -1.602 -1.4 2 -0.5 2.4 NDS -0.3 NDS NDS 0.05 1.64 0.59 X
017 4.6 0.138 0.1 NDS 0.3 $ $ R 1.2 0.53 0.59 N/A N/A
027 4.96 0.498 0.4 $ 0.5 0.2 NDS -0.6 -0.6 -0.02 0.54 1.80
029 ** 0.00 R 1.1 1.1 NDS 1.2 -0.9 0.8 0.66 0.88 1.10
030 4.24 -0.222 -0.2 0.0 0.1 -0.5 -0.1 0.5 0.1 -0.01 0.31 3.13
034 6.02 1.558 1.3 2 NDS 0.5 0.5 1.7 2.6 1.8 1.40 0.81 1.20
046 6.56 2.098 1.8 2 3.2 1.8 NDS NDS NDS NDS 2.27 0.81 N/A N/A
055 4.86 0.398 0.3 -0.1 0.9 1.0 0.6 -1.1 -0.9 0.10 0.84 1.15
056 2.48 -1.982 -1.7 2 -0.2 NDS NDS NDS NDS NDS -0.95 1.06 N/A N/A
058 3.73 -0.732 -0.6 NDS 0.0 1.1 NDS -0.2 -0.7 -0.08 0.72 1.35
061 5.14 0.678 0.6 -0.4 1.4 -0.3 -1.0 0.7 -0.2 0.11 0.82 1.18
071 4.05 -0.412 -0.4 -0.1 -0.6 -0.3 -0.2 -0.2 -0.9 -0.39 0.28 3.46
079 4.34 -0.122 -0.1 R 2.0 NDS 0.9 NDS NDS 0.93 1.05 N/A N/A
084 2.57 -1.892 -1.6 2 0.6 -0.3 NDS 3.7 0.8 0.5 0.62 1.75 0.55 X
088 7.0 2.538 2.2 2, 3 $ 0.4 NDS -0.3 NDS -0.7 0.40 1.28 0.76 X
089 4.66 0.198 0.2 -0.9 -0.3 0.8 -0.4 0.2 -0.5 -0.13 0.56 1.73
091 <1 -2.9 -0.8 R NDS NDS NDS -1.85 1.48 N/A N/A
092 5.25 0.788 0.7 R 1.5 -1.5 -0.1 0.8 NDS 0.28 1.15 0.84
093 4.39 -0.072 -0.1 0.0 0.0 -1.3 -0.3 NDS NDS -0.34 0.55 1.76
096 5.65 1.188 1.0 -0.2 0.7 0.8 0.7 0.8 0.1 0.56 0.44 2.20
106 1.30 -3.162 -2.7 2, 3 0.4 -0.4 -1.3 NDS NDS NDS -1.00 1.33 0.73 X
107 4.42 -0.042 0.0 NDS 0.1 NDS R -1.0 NDS -0.30 0.61 N/A N/A
123 5.95 1.488 1.3 2 0.2 0.6 0.3 R 1.4 1.9 0.95 0.68 1.43
126 4.67 0.208 0.2 -0.5 -0.7 -0.1 0.0 -1.0 -0.6 -0.39 0.43 2.26
129 3.05 -1.412 -1.2 2 NDS -0.5 NDS 1.0 NDS NDS -0.23 1.12 N/A N/A
135 4.44 -0.022 0.0 1.7 1.4 -2.5 R NDS NDS 0.15 1.92 0.51 X
141 4.38 -0.082 -0.1 0.3 1.8 0.2 0.7 0.9 -0.3 0.50 0.71 1.37
144 4.9 0.438 0.4 NDS NDS NDS -2.8 NDS NDS -1.20 2.26 N/A N/A
152 3.76 -0.702 -0.6 -0.8 -0.6 0.0 -0.3 1.5 1.5 0.10 0.99 0.98
159 3.20 -1.262 -1.1 2 -1.1 -0.5 -0.3 -0.9 -0.6 -1.1 -0.80 0.33 2.94
164 3.27 -1.192 -1.0 NDS NDS NDS NDS NDS -0.4 -0.70 0.42 N/A N/A
166 5.60 1.138 1.0 $ -0.7 0.5 -1.5 -1.0 -0.4 -0.35 0.94 1.03
168 3.30 -1.162 -1.0 NDS 0.2 0.4 NDS R -0.7 -0.28 0.68 1.43
171 4.4 -0.062 -0.1 R -0.4 1.1 NDS 1.5 1.2 0.66 0.85 1.14
191 6.54 2.078 1.8 2 -0.5 -0.8 0.5 -1.0 -1.9 1.5 -0.06 1.37 0.71 X
192 4.76 0.298 0.3 0.9 -0.6 -0.1 -0.3 -0.5 0.7 0.06 0.59 1.64
198 <2 $ -1.4 $ R 0.5 -0.8 -0.57 0.97 N/A N/A
212 4.99 0.528 0.5 0.4 -0.9 0.5 0.3 NDS NDS 0.16 0.60 1.62
216 ** 9.01 R 4.8 NDS R R NDS NDS 4.80 0.00 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 169
Iron (mg/kg)
1603 1511 1507 1503 1411 1407
220 5.037 0.575 0.5 2.8 $ $ 3.1 NDS -0.7 1.42 1.83 0.53 X
230 3.50 -0.962 -0.8 -0.7 -0.5 0.2 -0.3 -0.2 -0.4 -0.39 0.33 2.94
231 4.38 -0.082 -0.1 -0.3 0.6 4.5 -0.6 NDS 0.8 0.82 1.88 0.52 X

Legend:
R = Rejected
TPI 0.36
Comments:
170
Sample ID: CO1607

Iron (mg/kg)
4.624 9.086
3.468 7.93
2.312 6.774

Reproducibility
Deviation
0 4.462

Reproducibility
-1.156 3.306
-2.312 2.15
-3.468 0.994
-4.624 -0.162
1 5 8 1 1 1 1 1 2 2 1 5 1 7 3 7 2 1 9 1 1 1 1 1 8 1 3 1 5 1 2 2 2 6 9 1 9 1 3 1 4 1 8
0 6 4 5 2 5 6 6 2 3 3 8 5 1 0 9 3 4 3 7 0 3 3 7 9 2 2 9 5 4 7 1 2 1 2 6 6 2 4 9 6 4 8
6 9 9 4 8 0 2 1 1 1 7 5 4 6 2 4 2 0 6 3 1 7

171
Sample ID: CO1607

Iron (mg/kg)
18
16
Median
1% 99%
14
12
Number of Labs
10
0
0.48 - 1.52 1.53 - 2.57 2.58 - 3.62 3.63 - 4.67 4.68 - 5.72 5.73 - 6.77 6.78 - 7.82
ASTM Crude Oil
Sample ID: CO1607
July 2016 172
Nickel (mg/kg)
1603 1511 1507 1503 1411 1407
015 0.00 -0.08 -0.8 -0.4 1.5 NDS -0.2 NDS NDS 0.02 1.01 1.02
017 <0.5 NDS -0.3 -1.0 -0.7 0.6 $ -0.35 0.70 1.47
027 <1.0 $ -0.6 -0.2 NDS -0.5 NDS -0.43 0.21 N/A N/A
029 0.00 -0.08 -0.8 -0.2 0.3 NDS -0.9 1.4 -0.7 -0.15 0.88 1.17
030 0.00 -0.08 -0.8 -1.9 -0.7 -2.3 -0.8 -0.5 -0.8 -1.11 0.69 1.49
034 0 -0.08 -0.8 NDS -0.3 0.2 1.0 1.3 4.5 0.98 1.89 0.54 X
055 0.00 -0.08 -0.8 -1.3 -0.2 -0.7 -0.1 0.4 2.5 -0.03 1.24 0.83
056 0 -0.08 -0.8 -0.6 NDS NDS NDS NDS NDS -0.70 0.14 N/A N/A
058 0.150 0.07 0.7 NDS -0.4 -0.9 NDS 0.0 0.3 -0.06 0.62 1.66
071 <0.752 $ 0.1 1.1 0.0 -0.3 $ 0.23 0.61 1.69
079 0.302 0.23 2.2 3 R 2.0 NDS -1.0 NDS NDS 1.07 1.79 N/A N/A
084 <0.5 0.6 1.0 0.4 R 1.1 NDS 0.78 0.33 3.12
088 0.000 -0.08 -0.8 $ 0.7 NDS 1.0 1.9 $ 0.70 1.12 0.92
089 0.00 -0.08 -0.8 -0.4 R 1.2 -0.9 -0.3 -0.8 -0.33 0.79 1.30
091 <1 -1.9 -2.8 0.8 NDS NDS NDS -1.30 1.87 N/A N/A
092 ** 1.57 R R -3.4 -3.7 1.4 0.8 NDS -1.22 2.70 0.38 X
093 <0.1 0.0 1.0 1.0 1.5 NDS NDS 0.88 0.63 1.63
096 0.000 -0.08 -0.8 -1.4 0.5 0.1 R 0.7 -0.2 -0.18 0.80 1.29
106 0.02 -0.06 -0.6 0.6 0.3 0.3 NDS NDS NDS 0.15 0.52 1.98
107 0.043 -0.03 -0.4 NDS 0.0 NDS -1.2 -1.3 NDS -0.73 0.63 1.63
123 0.106 0.03 0.3 0.4 0.7 -0.4 R 0.7 1.0 0.45 0.48 2.15
126 0.2 0.12 1.2 0.2 -0.6 -2.2 -0.1 0.5 -0.8 -0.26 1.09 0.94
129 0.231 0.16 1.5 NDS -2.4 NDS 0.3 NDS NDS -0.20 2.00 N/A N/A
135 0.29 0.21 2.1 3 1.5 1.8 -0.6 R NDS NDS 1.20 1.22 0.84
141 0.18 0.10 1.0 0.0 -0.1 0.0 0.0 -0.4 $ 0.08 0.48 2.15
144 ** 1.4 R NDS NDS NDS -0.2 NDS NDS -0.20 0.00 N/A N/A
152 ** 0.748 R -0.5 -0.8 -0.3 0.8 -1.8 $ -0.52 0.94 1.10
159 <0.10 1.0 0.2 0.3 0.1 -0.2 $ 0.28 0.44 2.34
166 0.00 -0.08 -0.8 $ -0.6 1.2 -0.7 -1.2 $ -0.42 0.93 1.11
168 <0.100 NDS -0.1 -0.1 NDS $ $ -0.10 0.00 N/A N/A
171 0.1 0.02 0.2 R -0.6 0.2 NDS -0.2 -0.3 -0.14 0.34 3.03
191 0.085 0.01 0.0 -0.7 -2.2 -1.2 -1.3 -3.2 -0.8 -1.34 1.06 0.97
192 0.000 -0.08 -0.8 -0.4 -0.8 0.0 1.2 -0.4 $ -0.20 0.75 1.37
198 <0.85 0.8 0.7 -2.6 0.6 1.8 -0.8 0.08 1.55 0.66 X
212 0.10 0.02 0.2 -0.1 0.4 1.6 1.1 NDS NDS 0.64 0.69 1.49
216 0.204 0.13 1.2 -0.5 NDS -0.3 0.7 NDS NDS 0.27 0.81 1.27
220 <0.001 $ $ 2.1 0.2 NDS $ 1.15 1.34 N/A N/A
230 <2.00 $ -0.5 -0.6 -0.4 $ NDS -0.50 0.10 N/A N/A
ASTM Crude Oil
Sample ID: CO1607
July 2016 173
Nickel (mg/kg)
1603 1511 1507 1503 1411 1407
231 0.249 0.17 1.7 0.4 2.0 R R NDS 0.7 1.20 0.77 1.34

Legend:
R = Rejected
TPI
Comments:
The Reproducibility in D5708 addresses Nickel in the concentration range of 10 to 100 mg/kg. The Robust Mean is outside this range,
therefore ASTM Reproducibility not determined.
The Robust Standard Deviation exceeds the Robust Mean of these test data.Interpret these statistics
with caution. Graphs aren't provided.
ASTM Crude Oil
Sample ID: CO1607
July 2016 174
Vanadium (mg/kg)
1603 1511 1507 1503 1411 1407
015 0.00 -0.03 -0.6 -0.4 2.0 NDS -0.3 NDS NDS 0.18 1.22 0.92
017 <0.5 NDS 0.2 -0.6 -0.3 $ $ -0.23 0.40 N/A N/A
027 <0.5 $ -0.7 -0.6 NDS NDS NDS -0.65 0.07 N/A N/A
029 0.056 0.02 0.5 0.2 0.3 NDS -0.9 2.5 -0.5 0.35 1.18 0.95
030 0.00 -0.03 -0.6 -1.7 0.6 0.1 0.7 -0.3 -1.0 -0.31 0.87 1.29
034 0 -0.03 -0.6 NDS -0.6 -0.5 3.4 1.2 4.0 1.15 2.10 0.53 X
055 ** 0.29 R 0.2 0.2 -0.5 0.6 -1.8 -0.2 -0.25 0.85 1.32
056 0 -0.03 -0.6 -0.7 NDS NDS NDS NDS NDS -0.65 0.07 N/A N/A
058 <0.1 NDS -0.6 -1.3 NDS NDS $ -0.95 0.49 N/A N/A
071 <1.068 $ 0.5 0.5 -0.5 $ $ 0.17 0.58 N/A N/A
079 0.00 -0.03 -0.6 R 3.0 NDS -1.5 NDS NDS 0.30 2.38 N/A N/A
084 <0.5 0.6 1.8 0.6 R 0.1 NDS 0.78 0.72 1.56
088 0.000 -0.03 -0.6 $ 0.5 NDS -0.4 $ $ -0.17 0.59 N/A N/A
089 0.00 -0.03 -0.6 -0.8 -1.7 1.5 -0.4 0.1 -0.6 -0.36 0.98 1.14
091 <1 -1.7 -0.7 0.7 NDS NDS NDS -0.57 1.21 N/A N/A
092 <0.05 R -0.8 -2.5 0.9 -0.9 NDS -0.82 1.39 0.81
093 <0.1 -0.4 0.9 0.4 1.9 NDS NDS 0.70 0.96 1.17
096 0.058 0.02 0.6 -0.2 1.1 0.3 1.2 0.5 0.1 0.51 0.51 2.20
106 0.04 0.01 0.2 0.3 0.4 -0.6 NDS NDS NDS 0.08 0.46 2.43
107 0.026 -0.01 -0.1 NDS 0.3 NDS -0.6 -0.5 NDS -0.22 0.41 2.73
123 0.127 0.09 1.9 0.4 0.9 -0.8 R 1.9 1.2 0.92 1.02 1.10
126 0.2 0.17 3.4 1, 3 -0.1 -0.5 -1.6 -0.5 -1.0 -1.0 -0.19 1.65 0.68 X
129 0.048 0.01 0.4 NDS -1.7 NDS 0.9 NDS NDS -0.13 1.38 N/A N/A
134 0.198 0.16 3.4 1, 3 1.2 -1.4 NDS NDS NDS NDS 1.07 2.40 N/A N/A
135 0.23 0.20 4.0 1, 3 R 1.4 2.8 -1.3 NDS NDS 1.72 2.28 0.49 X
141 0.01 -0.02 -0.4 -0.7 -0.5 0.6 0.6 0.3 3.8 0.53 1.54 0.73 X
144 0 -0.03 -0.6 NDS NDS NDS 0.1 NDS NDS -0.25 0.49 N/A N/A
152 0.0 -0.03 -0.6 -0.2 -1.0 NDS 0.7 0.7 0.1 -0.05 0.69 1.62
159 <0.10 -0.5 0.7 -0.1 -0.5 -0.4 0.2 -0.10 0.48 2.33
166 0.00 -0.03 -0.6 $ -0.1 0.0 -0.3 0.0 $ -0.20 0.25 4.48
168 0.100 0.07 1.4 NDS -0.2 0.8 NDS 0.0 0.0 0.40 0.68 1.65
171 0.1 0.07 1.4 R -0.4 1.5 NDS -0.2 0.0 0.46 0.92 1.22
191 0.02 -0.01 -0.2 -1.5 -2.2 -0.6 -1.2 -2.9 -1.0 -1.37 0.93 1.20
192 0.000 -0.03 -0.6 -1.1 1.3 2.3 0.4 -0.4 $ 0.32 1.29 0.87
198 <0.85 $ -0.2 -0.5 0.9 R 0.3 0.12 0.61 1.84
212 ** 0.24 R 0.2 1.2 1.0 2.3 NDS NDS 1.17 0.87 1.29
216 0.023 -0.01 -0.1 -0.3 NDS -0.8 0.5 NDS NDS -0.18 0.54 2.07
220 <0.001 $ $ 1.9 -1.2 0.1 $ 0.27 1.56 N/A N/A
230 <0.200 $ -0.5 -0.7 -0.8 0.4 NDS -0.40 0.55 2.04
ASTM Crude Oil
Sample ID: CO1607
July 2016 175
Vanadium (mg/kg)
1603 1511 1507 1503 1411 1407
231 ** 0.499 R 2.3 -0.9 -0.3 -0.4 NDS 1.4 0.42 1.36 0.82

Legend:
R = Rejected
TPI
Comments:
The Reproducibility in D5708 addresses Vanadium in the concentration range of 50 to 500 mg/kg. The Robust Mean is outside this range,
ASTM Crude Oil
Sample ID: CO1607
July 2016 176
ICP after Acid Decomposition - D5708 Method B
Iron (mg/kg)
1603 1511 1507 1503 1411 1407
004 15.3 2.928 0.9 0.2 NDS 1.3 -0.5 0.3 1.4 0.60 0.73 1.52
006 18.5 6.128 1.9 -1.5 NDS NDS 2.8 -1.3 -0.8 0.22 1.99 0.56 X
007 ** 0.30 R 0.3 0.3 -1.3 -0.8 NDS NDS -0.38 0.81 1.37
017 11.0 -1.372 -0.4 NDS -0.6 4.3 0.3 R -1.0 0.52 2.16 0.51 X
020 14.4 2.028 0.6 0.5 1.2 0.8 1.5 0.4 0.9 0.84 0.40 2.78
029 10.7 -1.672 -0.5 1.0 -0.5 0.1 -0.3 -0.4 NDS -0.10 0.58 1.91
030 11.6 -0.772 -0.2 -0.2 0.1 0.9 -0.1 0.3 -0.9 -0.01 0.55 2.02
058 12.8 0.428 0.1 NDS 0.4 0.2 NDS R NDS 0.23 0.15 N/A N/A
067 11.1 -1.272 -0.4 0.1 0.3 -0.7 -0.7 -0.6 NDS -0.33 0.43 2.58
077 10.3 -2.072 -0.7 0.0 0.7 0.0 -0.5 0.0 0.8 0.04 0.56 1.98
087 16.3 3.928 1.2 3.6 1.3 R R R 0.4 1.62 1.38 0.80
088 7.40 -4.972 -1.6 $ -0.8 NDS 0.5 -1.0 NDS -0.73 0.88 1.26
090 9.81 -2.562 -0.8 -1.9 0.3 0.6 -0.8 1.4 0.7 -0.07 1.14 0.97
096 12.5 0.128 0.0 -0.2 0.3 0.1 -1.6 -0.2 -0.5 -0.30 0.63 1.76
099 19 6.628 2.1 3 $ -0.3 NDS 0.1 NDS NDS 0.63 1.29 N/A N/A
103 10.4 -1.972 -0.6 -0.5 -2.4 1.0 NDS -0.5 -0.2 -0.53 1.09 1.02
105 14.7 2.328 0.7 -1.0 -0.6 NDS 0.1 -3.1 1.3 -0.43 1.55 0.72 X
108 13.328 0.956 0.3 NDS NDS -3.9 -2.1 R R -1.90 2.11 N/A N/A
112 11.4 -0.972 -0.3 -0.6 -0.3 0.4 -0.8 NDS -0.8 -0.40 0.45 2.47
118 18.7 6.328 2.0 -0.2 1.3 -3.6 NDS NDS NDS -0.12 2.49 0.45 X
123 13.3 0.928 0.3 -0.1 -0.1 0.4 2.6 1.2 0.0 0.61 0.99 1.12
141 15.2 2.828 0.9 1.4 0.3 -0.2 -0.6 -0.3 0.8 0.33 0.73 1.52
144 8.8 -3.572 -1.1 NDS NDS NDS -0.8 NDS NDS -0.95 0.21 N/A N/A
147 7.4 -4.972 -1.6 -0.5 -0.2 -0.2 1.1 NDS NDS -0.28 0.96 1.16
166 13.3 0.928 0.3 0.8 -0.7 0.8 0.4 0.1 1.2 0.41 0.61 1.82
175 2.983 -9.389 -2.9 3 -0.6 0.8 NDS NDS -0.3 -1.0 -0.80 1.35 0.82
176 13.8 1.428 0.4 2.3 -1.2 R 0.3 1.5 -1.4 0.32 1.46 0.76 X
191 6.79 -5.582 -1.8 0.0 -1.5 -0.8 1.2 1.3 -0.6 -0.31 1.22 0.91
192 9.80 -2.572 -0.8 0.5 -1.7 -2.0 -0.6 -0.5 0.5 -0.66 0.97 1.14
193 11.9 -0.472 -0.1 -0.2 0.5 0.8 -0.6 3.1 0.3 0.54 1.22 0.91
210 12.1 -0.272 -0.1 -0.6 2.3 -2.6 -1.3 -0.8 -1.1 -0.60 1.50 0.74 X
213 16.9 4.528 1.4 0.3 0.7 R 0.0 -0.4 0.8 0.47 0.64 1.73
214 14.6 2.228 0.7 0.3 1.0 0.1 -0.3 NDS NDS 0.36 0.51 2.18
220 13.455 1.083 0.3 3.8 $ R NDS $ 0.4 1.50 1.99 N/A N/A
224 14.76 2.388 0.7 0.2 1.0 1.2 NDS 0.6 1.1 0.80 0.37 3.00
ASTM Crude Oil
Sample ID: CO1607
July 2016 177
Iron (mg/kg)
Legend:
R = Rejected
TPI
Comments:
The Reproducibility in D5708 addresses Iron in the range of 1 to 10 mg/kg. The Robust Mean is outside this range, therefore ASTM
Reproducibility not determined.
178
Sample ID: CO1607

Iron (mg/kg)
12.744 25.116
9.558 21.93
6.372 18.744
3.186 15.558
Deviation
0 12.372
-3.186 9.186
-6.372 6

-9.558 2.814
-12.744 -0.372
1 6 1 1 8 1 1 9 7 1 2 1 6 1 2 3 1 2 1 9 5 1 1 1 1 1 2 1 2 2 1 2 1 4 8 2 6 1 9
7 2 9 4 8 4 9 0 7 0 9 7 7 1 5 0 9 1 1 6 8 1 0 6 2 0 2 7 0 1 0 2 4 7 1 1 9
5 1 7 4 2 3 2 3 0 6 7 7 6 3 8 0 6 4 5 4 1 3 8

179
Sample ID: CO1607

Iron (mg/kg)
18
16
Median
1% 99%
14
12
Number of Labs
10
0
0.68 - 3.62 3.63 - 6.57 6.58 - 9.52 9.53 - 12.47 12.48 - 15.42 15.43 - 18.37 18.38 - 21.32
ASTM Crude Oil
Sample ID: CO1607
July 2016 180
Nickel (mg/kg)
1603 1511 1507 1503 1411 1407
004 <0.1 0.6 NDS 0.9 0.1 0.9 -0.2 0.46 0.49 2.41
006 ** 1.0 R 0.8 NDS NDS 0.0 -0.6 R 0.07 0.70 N/A N/A
007 <0.10 R 0.7 0.6 0.1 NDS NDS 0.47 0.32 N/A N/A
015 0.000 -0.031 -0.9 1.6 0.3 NDS 1.1 NDS NDS 0.52 1.09 1.08
017 <0.01 NDS -1.1 -0.4 0.5 -2.4 -0.2 -0.72 1.10 1.07
020 0.0 -0.031 -0.9 0.4 0.9 0.7 R 0.5 -1.2 0.07 0.89 1.33
025 0 -0.031 -0.9 NDS -0.9 NDS NDS NDS NDS -0.90 0.00 N/A N/A
029 0.00 -0.031 -0.9 0.4 -1.2 0.8 2.8 0.1 0.0 0.29 1.31 0.90
030 0.02 -0.011 -0.3 -0.8 -0.8 -1.4 0.2 0.3 -0.8 -0.51 0.61 1.93
057 ** 0.700 R NDS NDS R NDS NDS 2.5 2.50 0.00 N/A N/A
058 <0.1 NDS -0.1 0.4 NDS 2.3 $ 0.87 1.27 N/A N/A
067 0.000 -0.031 -0.9 -0.5 0.3 0.2 -1.1 0.2 NDS -0.30 0.62 1.90
077 <0.10 0.4 0.6 0.4 -0.2 0.7 1.3 0.53 0.49 2.41
087 0 -0.031 -0.9 1.0 1.1 0.6 3.5 -2.9 $ 0.40 2.15 0.55 X
088 <10.0 $ -0.3 NDS -0.5 -0.6 NDS -0.47 0.15 N/A N/A
090 0.261 0.230 6.8 1, 3 0.9 -0.1 -0.7 -0.5 0.4 0.3 1.01 2.61 0.45 X
096 0.00 -0.031 -0.9 0.0 0.1 0.1 0.3 0.1 0.1 -0.03 0.39 3.03
099 <1.0 $ 1.8 -0.7 0.6 NDS NDS 0.57 1.25 N/A N/A
103 ** 0.630 R 0.5 -0.2 NDS NDS 0.1 -1.0 -0.15 0.64 1.84
105 <0.100 -1.8 1.5 NDS -1.3 -1.4 0.2 -0.56 1.38 0.86
108 ** 0.371 R NDS NDS R -2.0 R R -2.00 0.00 N/A N/A
112 0.12 0.089 2.6 3 0.1 -0.8 -1.8 -0.8 NDS $ -0.14 1.67 0.71 X
117 0.150 0.119 3.5 1, 3 0.0 NDS NDS NDS NDS NDS 1.75 2.47 N/A N/A
118 0.10 0.069 2.0 -2.4 2.7 0.5 NDS NDS NDS 0.70 2.26 0.52 X
123 0.045 0.014 0.4 0.8 -0.2 -0.1 1.1 1.7 -0.2 0.50 0.73 1.62
141 0.02 -0.011 -0.3 -0.3 -0.9 -0.6 -0.6 0.1 $ -0.43 0.34 3.47
144 0 -0.031 -0.9 NDS NDS NDS 1.1 NDS NDS 0.10 1.41 N/A N/A
147 ** 0.78 R 1.1 0.7 1.0 1.0 NDS NDS 0.95 0.17 6.94
166 0.059 0.028 0.8 $ -1.1 2.5 -0.1 -1.3 $ 0.16 1.55 0.76 X
175 0.012 -0.019 -0.6 1.2 1.2 NDS NDS 1.4 -1.0 0.44 1.14 1.04
176 0.044 0.013 0.4 R -2.2 -1.2 -0.8 0.5 3.0 -0.05 1.81 0.65 X
191 0.01 -0.021 -0.6 -0.5 0.2 0.9 0.5 1.1 -1.2 0.06 0.85 1.39
192 0.0803 0.049 1.4 0.4 -0.9 -1.1 -0.2 0.1 $ -0.05 0.91 1.30
193 0.020 -0.011 -0.3 -0.1 0.1 -0.6 -1.0 1.0 -0.1 -0.14 0.62 1.90
210 0.030 -0.001 0.0 -0.1 2.7 0.9 -0.3 -1.0 0.2 0.34 1.18 1.00
213 0.041 0.010 0.3 0.3 0.7 1.2 2.3 0.3 0.4 0.79 0.74 1.59
214 <0.500 $ 0.5 0.2 0.7 NDS NDS 0.47 0.25 N/A N/A
220 0.047 0.016 0.5 $ $ -1.7 NDS $ -0.1 -0.43 1.14 N/A N/A
224 0.035 0.004 0.1 0.4 0.6 -1.1 0.4 -0.7 -0.3 -0.09 0.64 1.84
ASTM Crude Oil
Sample ID: CO1607
July 2016 181
Nickel (mg/kg)
Legend:
R = Rejected
TPI
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 182
Vanadium (mg/kg)
1603 1511 1507 1503 1411 1407
004 <0.1 -0.4 NDS 0.9 0.0 0.1 -0.5 0.02 0.55 2.87
006 0.0 -0.017 -0.7 R NDS NDS -1.0 -0.1 R -0.60 0.46 N/A N/A
007 <0.10 R -0.7 1.5 0.8 NDS NDS 0.53 1.12 N/A N/A
015 0.000 -0.017 -0.7 -0.4 0.0 NDS 1.0 NDS NDS -0.03 0.74 2.14
017 <0.1 NDS 0.5 -1.0 0.6 -0.1 $ 0.00 0.73 2.16
020 0.0 -0.017 -0.7 -0.4 0.8 0.5 R -0.1 -1.0 -0.15 0.69 2.29
025 0 -0.017 -0.7 NDS -0.7 NDS NDS NDS NDS -0.70 0.00 N/A N/A
029 0.00 -0.017 -0.7 -0.1 -0.3 NDS 3.4 0.0 -0.4 0.32 1.53 1.03
030 0.02 0.003 0.1 0.0 0.2 -1.0 0.0 0.4 -0.3 -0.09 0.46 3.43
057 ** 8.30 R NDS NDS R NDS NDS -0.4 -0.40 0.00 N/A N/A
058 <0.1 NDS 1.2 -0.7 NDS NDS $ 0.25 1.34 N/A N/A
067 0.000 -0.017 -0.7 -0.5 0.3 -0.2 -1.2 -1.2 NDS -0.58 0.58 2.72
077 <0.20 2.0 1.0 0.8 0.0 1.4 2.2 1.23 0.81 1.95
087 0 -0.017 -0.7 1.3 0.9 -0.3 0.2 $ $ 0.28 0.83 1.90
088 <50.0 $ -1.5 NDS -0.7 $ NDS -1.10 0.57 N/A N/A
090 0.162 0.145 5.8 1, 3 1.6 0.6 0.3 -1.5 R 0.5 1.22 2.46 0.64 X
096 0.00 -0.017 -0.7 0.6 0.3 0.8 0.7 -0.4 0.3 0.23 0.57 2.77
099 <1.0 R 2.8 -1.2 0.2 NDS NDS 0.60 2.03 N/A N/A
103 ** 0.560 R -0.7 -0.7 NDS NDS 0.4 -1.0 -0.50 0.62 2.55
105 <0.100 R 2.1 NDS -1.2 -1.7 -0.4 -0.30 1.69 0.93
108 0.029 0.012 0.5 NDS NDS R -1.6 -1.1 -0.5 -0.68 0.90 1.76
112 0.26 0.243 9.7 1, 3 0.1 -1.1 -2.0 -1.1 NDS $ 1.12 4.85 0.33 X
118 0.20 0.183 7.3 1, 3 0.1 1.7 0.2 NDS NDS NDS 2.32 3.40 0.46 X
123 0.0375 0.020 0.8 2.6 0.0 -0.3 0.3 2.5 0.5 0.91 1.17 1.35
141 0.00 -0.017 -0.7 -0.6 0.1 0.6 -1.0 0.1 $ -0.25 0.61 2.59
144 0 -0.017 -0.7 NDS NDS NDS 0.6 NDS NDS -0.05 0.92 N/A N/A
147 ** 1.1 R -0.2 0.5 1.0 0.9 NDS NDS 0.55 0.54 2.93
166 0.049 0.032 1.3 2.5 1.0 1.0 0.2 -1.8 $ 0.70 1.43 1.10
175 0.000 -0.017 -0.7 0.5 0.4 NDS NDS 0.9 -0.7 0.08 0.74 2.14
176 0.015 -0.002 -0.1 5.0 R -0.1 -0.1 0.6 R 1.06 2.22 0.71 X
191 0.014 -0.003 -0.1 -0.6 -0.2 -0.8 -0.5 R -1.0 -0.53 0.34 4.65
192 0.0453 0.028 1.1 -0.4 -2.5 -0.5 0.4 -0.1 $ -0.33 1.21 1.31
193 0.166 0.149 6.0 1, 3 0.0 -0.2 -0.6 -1.7 3.2 -0.5 0.89 2.72 0.58 X
210 0.005 -0.012 -0.5 0.7 R 2.0 -0.6 -0.1 -0.1 0.23 0.98 1.61
213 0 -0.017 -0.7 -0.3 0.3 -0.2 0.7 -0.2 -0.3 -0.10 0.46 3.43
214 <0.100 -0.7 0.0 1.4 0.2 NDS NDS 0.22 0.87 1.82
220 0.195 0.178 7.1 1, 3 $ $ -1.2 NDS $ 0.9 2.27 4.32 N/A N/A
224 0.010 -0.007 -0.3 -0.3 0.2 -0.9 0.6 -0.4 -0.4 -0.21 0.48 3.29
ASTM Crude Oil
Sample ID: CO1607
July 2016 183
Vanadium (mg/kg)
Legend:
R = Rejected
Anderson Darling N/A * = There is no available historical information for this program cycle
TPI
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 184
AAS (Decomposed with Acid) - D5863 Method A
Iron (mg/kg)
1603 1511 1507 1503 1411 1407
006 12.8 1.51 0.4 -1.3 NDS NDS NDS R NDS -0.45 1.20 N/A N/A
026 14 2.71 0.7 0.6 0.6 NDS NDS NDS NDS 0.63 0.06 N/A N/A
030 11 -0.29 -0.1 -0.3 0.2 0.8 -1.1 0.7 0.0 0.03 0.64 1.38
088 7.0 -4.29 -1.1 -0.7 -0.7 NDS -0.4 0.1 NDS -0.56 0.44 2.00
096 9.8 -1.49 -0.4 2.0 0.3 -0.7 -1.4 -0.3 0.7 0.03 1.10 0.80
099 17 5.71 1.5 $ 0.8 NDS 0.0 -0.1 0.6 0.56 0.65 1.35
103 6.7 -4.59 -1.2 -0.4 -2.2 NDS NDS -0.1 NDS -0.98 0.94 0.94
123 13 1.71 0.4 $ 0.2 0.9 0.3 -2.2 2.1 0.28 1.40 0.63 X
166 12.7 1.41 0.4 -0.2 NDS -0.3 -0.9 -0.5 -0.6 -0.35 0.44 2.00
173 14.90 3.61 0.9 0.0 NDS -1.5 NDS NDS NDS -0.20 1.21 N/A N/A
191 6.5 -4.79 -1.2 0.0 -1.5 -1.2 0.1 0.2 0.2 -0.49 0.77 1.14
210 13 1.71 0.4 -0.3 1.1 -0.8 -1.3 -1.2 -0.8 -0.41 0.88 1.00

Legend:
R = Rejected
TPI
Comments:
The Reproducibility in D5863 addresses Iron in the concentration range of 3 to 10 mg/kg. The Robust Mean is outside this range,
185
Sample ID: CO1607

Iron (mg/kg)
15.4 26.69
11.55 22.84
7.7 18.99
3.85 15.14
Deviation
0 11.29
-3.85 7.44
-7.7 3.59

-11.55 -0.26
-15.4 -4.11
2 1 1 8 9 3 2 1 6 1 2 1 2 1 9
1 9 0 8 6 0 2 6 1 1 2 6 7 9
9 1 3 9 6 6 0 3 3

ASTM Crude Oil
Sample ID: CO1607
July 2016 186
Nickel (mg/kg)
1603 1511 1507 1503 1411 1407
006 ** 1.0 R 0.4 NDS NDS NDS 1.9 NDS 1.15 1.06 N/A N/A
015 0.00 -0.09 -0.7 R -0.6 NDS 1.2 NDS NDS -0.03 1.07 N/A N/A
026 0 -0.09 -0.7 $ 0.7 NDS NDS NDS NDS 0.00 0.99 N/A N/A
030 0.00 -0.09 -0.7 -1.5 -1.2 -0.8 0.5 -0.1 -0.8 -0.66 0.67 1.82
088 0.00 -0.09 -0.7 -0.5 -0.9 NDS -0.3 -0.1 $ -0.50 0.32 3.81
096 0.00 -0.09 -0.7 R 0.1 -0.2 -0.2 -0.2 -0.4 -0.27 0.27 4.52
099 <1.0 $ 0.1 -1.1 -2.3 -1.2 4.2 -0.06 2.53 0.48 X
103 0.79 0.70 5.4 1, 3 0.5 -0.6 NDS -0.2 -0.1 NDS 1.00 2.49 0.49 X
123 0.40 0.31 2.4 3 $ 0.4 0.5 0.5 1.3 -0.2 0.82 0.91 1.34
166 0.00 -0.09 -0.7 -0.3 NDS -0.5 -0.2 -0.4 -0.2 -0.38 0.19 6.42
191 0.085 0.00 0.0 -0.1 -0.3 0.5 1.2 -0.3 -0.8 0.03 0.65 1.88
210 <0.10 1.7 2.2 -1.1 -0.8 -0.8 0.4 0.27 1.41 0.87
229 0.21 0.12 0.9 -1.3 NDS 0.7 NDS NDS NDS 0.10 1.22 N/A N/A

Legend:
R = Rejected
TPI
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 187
Vanadium (mg/kg)
1603 1511 1507 1503 1411 1407
006 0.0 -0.209 -0.6 -0.7 NDS NDS NDS -1.2 NDS -0.83 0.32 N/A N/A
015 0.00 -0.209 -0.6 -1.0 -2.7 NDS 1.4 NDS NDS -0.73 1.68 0.50 X
088 0.00 -0.209 -0.6 -1.0 -1.1 NDS 0.7 $ $ -0.50 0.83 1.01
096 0.00 -0.209 -0.6 3.0 0.2 0.4 1.4 -0.4 0.0 0.57 1.25 0.67 X
099 <1.0 R 0.2 -0.5 -1.4 $ $ -0.57 0.80 N/A N/A
103 0.51 0.301 0.9 -0.3 -0.7 NDS -1.1 -0.4 NDS -0.32 0.75 1.12
123 0.49 0.281 0.9 $ 1.2 -0.1 0.7 R -0.5 0.44 0.71 1.18
166 0.11 -0.099 -0.3 0.5 NDS 0.9 0.1 1.4 -0.5 0.35 0.73 1.15
191 0.00 -0.209 -0.6 -0.7 NDS -0.6 -0.8 -0.3 -1.0 -0.67 0.23 3.65
210 <0.10 0.9 R -1.0 -0.8 -0.7 0.2 -0.28 0.80 1.05

Legend:
R = Rejected
TPI
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 188
AAS (Sample Diluted with an Organic Solvent) - D5863 Method B
Nickel (mg/kg)
1603 1511 1507 1503 1411 1407
006 0.3 0.09 0.4 -1.0 2.3 NDS NDS NDS 0.8 0.62 1.36 0.86
015 ** 2.4 R 0.6 -1.2 NDS 1.1 NDS NDS 0.17 1.21 N/A N/A
023 ** 2.1 R -0.1 0.2 -0.3 -1.2 2.2 -0.6 0.03 1.16 1.01
025 0 -0.21 -0.9 NDS 1.2 NDS 2.3 -0.2 0.2 0.52 1.25 0.94
029 0.87 0.66 2.8 3 0.4 -0.6 0.1 0.5 0.2 -0.6 0.40 1.15 1.02
030 0.00 -0.21 -0.9 0.6 0.2 -1.4 -0.1 0.5 -0.6 -0.24 0.75 1.56
079 1.2 0.99 4.1 1, 3 R 0.7 NDS -1.2 NDS NDS 1.20 2.69 N/A N/A
088 0 -0.21 -0.9 -1.2 0.9 NDS -0.4 1.0 1.4 0.13 1.10 1.06
089 0.0 -0.21 -0.9 -1.2 -1.9 1.8 -1.2 1.2 -0.6 -0.40 1.37 0.85
110 <0.10 NDS 0.7 NDS NDS NDS NDS 0.70 0.00 N/A N/A
123 0.10 -0.11 -0.5 $ 0.7 -0.1 0.5 -0.5 1.2 0.22 0.69 1.70
152 1.2 0.99 4.1 1, 3 -1.2 -0.5 -1.4 -1.1 -0.5 -0.6 -0.17 1.92 0.61 X
163 <1 $ -0.3 0.6 0.5 -0.5 $ 0.08 0.56 2.09
166 0.39 0.18 0.8 0.0 NDS 1.0 1.1 -0.4 -0.5 0.33 0.72 1.62
191 0.09 -0.12 -0.5 0.3 -1.2 -0.9 -0.1 0.5 -0.6 -0.36 0.62 1.89
216 0.20 -0.01 0.0 NDS NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A

Legend:
R = Rejected
TPI
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 189
AAS (Sample Diluted with an Organic Solvent) - D5863 Method B
Vanadium (mg/kg)
1603 1511 1507 1503 1411 1407
006 0.5 0.44 4.0 1, 3 0.1 -1.4 NDS NDS NDS 1.0 0.92 2.28 0.49 X
015 0.00 -0.06 -0.5 -0.3 2.3 NDS 1.4 NDS NDS 0.72 1.35 0.83
023 0.23 0.17 1.5 0.6 0.5 1.4 -0.3 2.5 5.5 1.67 1.91 0.59 X
025 ** 0.94 R NDS 1.3 NDS -1.4 -0.2 -1.0 -0.32 1.19 0.94
029 0.06 0.00 0.0 -0.3 0.5 1.1 0.8 0.7 -1.0 0.26 0.73 1.53
079 0.0 -0.06 -0.5 2.9 0.8 NDS -0.5 NDS NDS 0.68 1.60 0.70 X
088 0 -0.06 -0.5 -0.1 -0.8 NDS -0.6 $ $ -0.50 0.29 3.86
089 0.0 -0.06 -0.5 -0.8 0.3 0.2 1.3 -1.0 -1.0 -0.21 0.86 1.30
110 <0.10 NDS -1.9 NDS NDS NDS NDS -1.90 0.00 N/A N/A
123 ** 1.1 R $ 0.1 -0.3 2.8 -0.1 1.5 0.80 1.32 0.85
152 0.0 -0.06 -0.5 -0.9 0.1 -0.5 0.2 -0.3 -1.0 -0.41 0.46 2.43
163 <1 $ -0.7 0.1 0.8 $ $ 0.07 0.75 N/A N/A
166 0.0 -0.06 -0.5 -0.2 NDS 0.7 -0.8 0.7 -0.5 -0.10 0.65 1.72
167 0.25 0.19 1.7 0.0 0.3 -2.1 -0.3 NDS NDS -0.08 1.36 0.82
191 0.00 -0.06 -0.5 -0.9 NDS -1.2 -1.1 -1.0 -1.0 -0.95 0.24 4.67
216 0.02 -0.04 -0.4 NDS NDS -0.7 NDS NDS NDS -0.55 0.21 N/A N/A

Legend:
R = Rejected
TPI
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 190
Total Vapor Pressure - D5191
(p.s.i.)
1603 1511 1507 1503 1411 1407
007 1.59 0.143 0.5 NDS NDS -0.1 -0.1 NDS NDS 0.10 0.35 N/A N/A
011 0.97 -0.477 -1.6 2 NDS -1.3 -1.6 -3.0 -1.6 -2.5 -1.93 0.66 1.17
015 1.07 -0.377 -1.3 2 -1.4 0.0 NDS -0.1 NDS NDS -0.70 0.75 1.03
017 1.17 -0.277 -0.9 2 1.2 0.3 -0.1 1.3 0.7 -0.3 0.31 0.81 0.95
026 1.47 0.023 0.1 -1.1 NDS -0.3 1.0 NDS NDS -0.08 0.87 0.89
027 1.75 0.303 1.0 2 0.9 0.2 -0.9 NDS 0.8 1.1 0.52 0.76 1.01
029 1.37 -0.077 -0.3 -1.5 2.0 NDS -0.7 NDS NDS -0.12 1.50 0.51 X
030 1.34 -0.107 -0.4 -0.6 -2.0 -0.2 -1.2 -1.7 -1.3 -1.06 0.68 1.13
045 1.40 -0.047 -0.2 0.4 0.1 -0.5 NDS NDS NDS -0.05 0.39 1.97
048 1.52 0.073 0.2 NDS NDS -0.2 -0.8 -0.8 NDS -0.40 0.49 1.57
054 1.90 0.453 1.5 2 NDS R NDS 0.2 2.3 NDS 1.33 1.06 N/A N/A
055 1.68 0.233 0.8 0.2 1.1 NDS 0.1 NDS 0.7 0.58 0.42 1.83
066 1.47 0.023 0.1 0.5 0.5 1.4 2.3 0.7 NDS 0.92 0.80 0.96
069 1.72 0.273 0.9 2 R -0.3 2.5 1.1 NDS 1.6 1.16 1.02 0.75 X
071 1.39 -0.057 -0.2 0.1 R 0.0 NDS NDS NDS -0.03 0.15 N/A N/A
076 1.54 0.093 0.3 0.3 NDS NDS 2.4 NDS NDS 1.00 1.21 N/A N/A
079 1.60 0.153 0.5 1.3 -0.8 R -0.7 NDS NDS 0.08 1.01 0.76 X
081 1.80 0.353 1.2 2 0.5 NDS 0.8 0.5 NDS NDS 0.75 0.33 2.33
087 1.17 -0.277 -0.9 2 -0.9 0.7 1.5 -0.6 $ -0.3 -0.08 0.98 0.79 X
089 ** 3.97 R 0.6 NDS NDS -0.6 1.2 -0.1 0.27 0.79 0.97
103 1.29 -0.157 -0.5 NDS NDS NDS -0.2 NDS -0.5 -0.40 0.17 N/A N/A
107 ** 2.64 R NDS 1.6 NDS 0.4 -0.3 NDS 0.57 0.96 N/A N/A
112 1.52 0.073 0.2 2.0 R 1.0 1.5 NDS 0.9 1.12 0.68 1.13
132 1.97 0.523 1.8 2 -0.5 -0.1 NDS 0.9 NDS NDS 0.52 1.03 0.75 X
134 0.92 -0.527 -1.8 2 0.1 R NDS NDS NDS NDS -0.85 1.34 N/A N/A
145 1.32 -0.127 -0.4 -0.6 -0.4 0.0 0.5 1.0 0.7 0.11 0.62 1.24
152 1.72 0.273 0.9 2 -0.1 1.2 NDS -0.1 0.3 0.4 0.43 0.53 1.45
179 1.58 0.133 0.5 -0.7 0.7 -1.3 -0.4 NDS 1.4 0.03 1.00 0.77 X
193 1.53 0.083 0.3 -0.1 -1.0 -0.6 -1.4 -0.8 0.1 -0.50 0.62 1.24
226 1.83 0.383 1.3 2 0.8 -0.3 -0.2 1.7 NDS NDS 0.66 0.89 0.87
ASTM Crude Oil
Sample ID: CO1607
July 2016 191
(p.s.i.)
Legend:
R = Rejected
TPI 0.31
Comments:

Labs: 071, 094
192
Sample ID: CO1607

(p.s.i.)
1.172 2.619
0.879 2.326
0.586 2.033
0.293 1.74
Reproducibility
Deviation
0 1.447

Reproducibility
-0.293 1.154
-0.586 0.861
-0.879 0.568
-1.172 0.275
2 1 1 1 1 1 9 1 8 1 1 3 2 2 7 4 1 1 1 6 2 4 3 1 1 7 1 7 7 1 5 1 5 1 6 2 8 2 5 1
3 4 3 7 1 5 4 7 7 0 4 0 9 4 1 5 8 5 3 6 6 8 1 1 9 6 7 9 6 6 1 5 5 9 7 1 2 4 3
4 9 4 3 3 5 1 9 6 7 2 3 9 1 7 2 6 2

193
Sample ID: CO1607

(p.s.i.)
14
Median
12 1% 99%
10
Number of Labs
0
0.56 - 0.78 0.79 - 1.01 1.02 - 1.24 1.25 - 1.47 1.48 - 1.7 1.71 - 1.93 1.94 - 2.16
ASTM Crude Oil
Sample ID: CO1607
July 2016 194
Vapor Pressure (Expansion Method) - D6377
(kPa)
1603 1511 1507 1503 1411 1407
015 9.4 -2.33 -1.5 -0.3 -0.7 NDS -1.5 NDS NDS -1.00 0.60 1.58
017 13.7 1.97 1.3 1.0 0.7 0.5 0.5 0.3 -0.6 0.53 0.60 1.58
025 10.3 -1.43 -0.9 NDS R NDS -1.0 NDS NDS -0.95 0.07 N/A N/A
029 10.3 -1.43 -0.9 -0.1 -1.2 NDS NDS NDS -0.2 -0.60 0.54 1.76
031 10.1 -1.63 -1.1 1.1 -0.7 -0.4 -0.2 NDS 0.6 -0.12 0.82 1.16
032 12.1 0.37 0.2 NDS 0.6 R 0.5 1.3 NDS 0.65 0.47 2.02
034 10.6 -1.13 -0.7 NDS -0.1 -0.2 0.1 0.0 -0.3 -0.20 0.28 3.39
037 10.5 -1.23 -0.8 NDS -0.7 -0.4 1.7 2.8 NDS 0.52 1.63 0.58 X
042 12.1 0.37 0.2 0.0 -0.5 -0.7 NDS -0.5 NDS -0.30 0.38 2.50
045 10.8 -0.93 -0.6 0.1 1.2 0.4 1.5 2.3 3.4 1.19 1.37 0.69 X
046 11.6 -0.13 -0.1 -0.5 1.1 -0.4 -0.2 NDS NDS -0.02 0.65 1.46
054 11.9 0.17 0.1 NDS R NDS R 0.0 R 0.05 0.07 N/A N/A
061 13.0 1.27 0.8 1.9 0.6 1.5 1.3 -0.1 -1.6 0.63 1.18 0.81
063 ** 2.0 R NDS 1.4 0.5 NDS NDS NDS 0.95 0.64 N/A N/A
067 11.3 -0.43 -0.3 1.0 0.5 -0.1 0.9 -0.1 0.3 0.31 0.51 1.86
077 11.2 -0.53 -0.3 -0.4 0.0 0.3 0.8 0.5 -0.2 0.10 0.45 2.11
080 12.4 0.67 0.4 0.8 0.6 1.0 NDS 0.8 0.6 0.70 0.21 4.52
087 15.5 3.77 2.5 3 1.9 0.8 3.0 0.6 -2.0 0.7 1.07 1.65 0.58 X
088 10.7 -1.03 -0.7 0.0 -0.6 -0.4 0.0 -0.4 -2.5 -0.66 0.86 1.10
090 9.6 -2.13 -1.4 -1.8 -0.6 -1.2 -0.9 -0.6 -0.9 -1.06 0.44 2.16
092 10.9 -0.83 -0.5 -1.6 -1.9 2.2 NDS -2.3 NDS -0.82 1.82 0.52 X
096 9.6 -2.13 -1.4 1.1 -0.7 -0.2 -0.7 -0.7 -0.6 -0.46 0.77 1.23
097 9.6 -2.13 -1.4 -1.5 R NDS -1.1 -1.2 R -1.30 0.18 5.28
099 13.4 1.67 1.1 1.0 0.0 NDS 1.2 0.5 1.4 0.87 0.52 1.83
105 11.6 -0.13 -0.1 1.0 -0.2 NDS 0.8 -0.2 R 0.26 0.59 1.61
109 11.7 -0.03 0.0 -0.3 NDS 0.7 R 1.8 -1.5 0.14 1.22 0.78 X
118 11.7 -0.03 0.0 -1.1 1.1 0.6 -1.7 NDS R -0.22 1.16 0.82
127 10.5 -1.23 -0.8 0.0 -1.3 -0.4 -0.3 -0.3 -0.5 -0.51 0.42 2.26
132 12.2 0.47 0.3 0.1 -0.1 NDS 1.0 NDS NDS 0.32 0.48 1.98
135 ** 44.8 R -0.1 -3.4 -1.2 -0.8 NDS NDS -1.38 1.42 0.67 X
139 ** 1.7 R -1.0 0.4 -0.4 -0.2 0.3 1.0 0.02 0.70 1.36
149 11.7 -0.03 0.0 NDS NDS 2.3 -0.8 0.0 0.0 0.30 1.17 0.81
156 9.9 -1.83 -1.2 -1.6 -2.0 NDS -0.8 -0.6 0.3 -0.98 0.81 1.17
ASTM Crude Oil
Sample ID: CO1607
July 2016 195
(kPa)
1603 1511 1507 1503 1411 1407
159 ** 26.3 R -1.0 0.2 -0.2 0.1 R 0.2 -0.14 0.51 1.86
166 12.0 0.27 0.2 0.3 NDS 3.6 0.5 NDS NDS 1.15 1.64 0.58 X
192 10.9 -0.83 -0.5 0.3 -0.7 -0.9 -0.8 -0.6 -1.0 -0.60 0.43 2.21
193 10.5 -1.23 -0.8 -0.4 -0.8 -0.5 0.2 0.7 0.1 -0.21 0.56 1.70
194 11.4 -0.33 -0.2 -1.0 -0.6 -0.8 0.0 -2.2 R -0.80 0.78 1.22
203 16.4 4.67 3.1 1, 3 R 1.0 -0.1 1.7 -0.3 -0.9 0.75 1.49 0.64 X
206 14.3 2.57 1.7 1.3 -0.1 NDS R NDS NDS 0.97 0.95 N/A N/A
209 12.0 0.27 0.2 R 1.9 0.1 -0.2 0.3 -2.7 -0.07 1.49 0.64 X
210 14.1 2.37 1.6 0.8 NDS -3.1 1.1 1.0 1.0 0.40 1.74 0.55 X
214 <25.0 $ $ -0.8 -0.4 NDS NDS -0.60 0.28 N/A N/A
216 12.4 0.67 0.4 0.6 0.0 -0.3 -0.8 NDS NDS -0.02 0.56 1.70
220 13.7 1.97 1.3 -1.0 0.2 -1.3 R -2.3 R -0.62 1.40 0.68 X
222 ** 22.0 R 2.9 0.8 0.1 1.2 0.0 0.9 0.98 1.05 0.90
226 14.9 3.17 2.1 3 0.6 2.4 -0.4 0.0 NDS NDS 0.94 1.25 0.76 X
229 12.3 0.57 0.4 0.1 -0.1 1.4 NDS NDS NDS 0.45 0.67 1.42
230 11.7 -0.03 0.0 0.6 0.0 0.8 0.8 -0.1 NDS 0.35 0.43 2.21
241 11.5 -0.23 -0.2 0.6 -0.7 1.2 -0.9 NDS NDS 0.00 0.89 1.07

Legend:
R = Rejected
TPI 1.25
Comments:

Labs: 090, 097,109,118,149,216,220,222,228.
196
Sample ID: CO1607

(kPa)
6.08 17.81
Reproducibility
4.56 16.29
3.04 14.77
1.52 13.25
Deviation
0 11.73
-1.52 10.21
-3.04 8.69
-4.56 7.17
Reproducibility
-6.08 5.65
1 1 9 9 9 1 1 3 3 2 2 3 1 2 1 3 8 4 1 9 6 7 4 6 1 2 1 2 4 1 1 1 1 2 1 5 2 2 1 3 4 1 1 2 8 2 2 6 2 6 1 9 9 2 2 1 1 2 2 2 8 2
8 5 0 6 7 2 5 1 0 5 9 7 9 2 4 8 5 9 2 8 7 1 7 9 4 7 1 6 0 0 1 4 3 4 4 0 0 6 2 2 2 3 2 0 1 1 1 2 2 4 5 9 2 2 7 6 1 0 2 7 0
9 3 6 3 7 2 4 1 5 5 9 8 9 0 8 9 0 6 2 2 9 6 3 8 6 4 0 1 0 6 6 3

197
Sample ID: CO1607

(kPa)
28
Median
24 1% 99%
20
Number of Labs
16
12
0
7.2 - 8.45 8.5 - 9.75 9.8 - 11.05 11.1 - 12.35 12.4 - 13.65 13.7 - 14.95 15 - 16.25 16.3 - 17.55
ASTM Crude Oil
Sample ID: CO1607
July 2016 198
Viscosity, Kinematic - D445 25C
(mm/s)
1603 1511 1507 1503 1411 1407
009 4.000 -0.20 -0.7 0.0 -0.2 -0.7 -0.8 -0.3 -0.6 -0.47 0.30 3.40
013 4.197 0.00 0.0 -0.8 1.6 3.4 0.7 -0.6 -2.2 0.30 1.82 0.56 X
017 4.230 0.03 0.1 0.3 0.0 0.8 -0.5 -0.1 -0.8 -0.03 0.52 1.96
021 4.076 -0.12 -0.4 0.5 0.0 1.9 0.8 -0.4 2.5 0.70 1.13 0.90
023 4.688 0.49 1.7 -0.9 0.6 1.8 -1.2 -1.4 0.2 0.11 1.33 0.77 X
030 ** 7.628 R -0.4 -0.5 R 0.0 0.0 0.8 -0.02 0.51 2.00
054 4.0321 -0.17 -0.6 NDS -2.7 NDS -0.3 2.3 NDS -0.33 2.05 0.50 X
057 4.576 0.38 1.3 R -0.5 0.7 1.0 3.5 1.1 1.18 1.30 0.78 X
058 4.028 -0.17 -0.6 NDS -0.8 NDS NDS R R -0.70 0.14 N/A N/A
060 4.493 0.30 1.0 0.9 -1.7 0.0 -1.8 -1.7 R -0.55 1.34 0.76 X
066 3.928 -0.27 -0.9 -0.8 -1.0 -0.8 -0.3 -0.6 -0.2 -0.66 0.30 3.40
074 4.737 0.54 1.9 R 1.8 1.3 -2.7 R R 0.57 2.20 0.46 X
077 4.581 0.38 1.3 -0.9 -0.2 2.5 R 0.4 1.1 0.70 1.20 0.85
080 3.874 -0.32 -1.1 -1.1 -0.4 -1.2 NDS -0.4 -1.3 -0.92 0.41 2.49
085 4.9200 0.72 2.5 3 0.0 NDS -0.9 1.1 NDS NDS 0.68 1.47 0.69 X
088 4.055 -0.14 -0.5 NDS -1.2 NDS 0.7 NDS NDS -0.33 0.96 N/A N/A
089 4.034 -0.16 -0.6 3.3 -0.3 0.4 -0.3 0.9 0.6 0.57 1.32 0.77 X
090 4.084 -0.11 -0.4 1.0 -0.8 NDS -0.2 -0.1 -0.9 -0.23 0.68 1.50
096 3.978 -0.22 -0.8 0.2 0.1 0.3 2.0 0.2 -0.2 0.26 0.86 1.19
102 3.6395 -0.56 -1.9 -2.6 -0.1 -0.5 0.9 -0.6 0.3 -0.64 1.22 0.84
107 3.493 -0.70 -2.4 3 -1.6 NDS 0.0 NDS NDS NDS -1.33 1.22 N/A N/A
123 3.966 -0.23 -0.8 -0.8 0.0 0.5 NDS NDS R -0.28 0.64 1.59
129 4.045 -0.15 -0.5 -1.0 1.0 -0.9 NDS NDS NDS -0.35 0.93 1.10
133 4.179 -0.02 -0.1 -0.1 -0.7 NDS R -1.2 -1.6 -0.74 0.67 1.52
135 3.740 -0.46 -1.6 -0.2 -0.9 1.1 -1.4 NDS NDS -0.60 1.09 0.94
138 4.195 0.00 0.0 1.8 0.0 1.8 2.7 -0.6 1.1 0.97 1.21 0.84
144 4.410 0.21 0.7 NDS R NDS NDS NDS NDS 0.70 0.00 N/A N/A
152 4.936 0.74 2.5 3 1.0 -1.0 NDS R 1.1 NDS 0.90 1.44 0.71 X
161 4.580 0.38 1.3 0.0 NDS -1.6 -0.7 NDS NDS -0.25 1.22 0.84
163 4.349 0.15 0.5 -0.9 -0.5 -0.6 -0.4 0.4 -0.6 -0.30 0.54 1.89
165 3.945 -0.25 -0.9 R NDS NDS -0.5 -0.4 -0.5 -0.57 0.22 4.64
166 4.623 0.43 1.5 NDS 0.0 -0.6 R -2.8 2.4 0.10 2.01 0.51 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 199
(mm/s)
1603 1511 1507 1503 1411 1407
178 3.954 -0.24 -0.8 -0.6 -0.4 -1.0 -1.0 -0.3 -0.8 -0.70 0.28 3.64
189 3.91 -0.29 -1.0 -0.7 0.7 -0.2 -2.5 NDS NDS -0.74 1.18 0.86
191 4.425 0.23 0.8 1.5 1.6 R 1.8 0.0 0.5 1.03 0.71 1.44
193 4.169 -0.03 -0.1 1.0 0.8 -1.0 0.8 -0.7 -0.4 0.06 0.81 1.26
209 4.0515 -0.15 -0.5 -0.9 -0.7 -1.6 -0.9 0.4 0.0 -0.60 0.65 1.57
210 4.025 -0.17 -0.6 -1.3 -1.2 -0.2 -0.6 0.6 -0.1 -0.49 0.66 1.55
211 3.910 -0.29 -1.0 -0.7 -0.7 -1.3 -0.9 -0.4 -0.3 -0.76 0.35 2.91
213 4.189 -0.01 0.0 -0.8 NDS 0.5 -0.1 0.0 R -0.08 0.47 2.17
214 ** 5.831 R 3.3 1.2 1.2 1.4 NDS NDS 1.78 1.02 1.00
223 <8 $ NDS NDS NDS 1.7 0.5 1.10 0.85 N/A N/A
234 4.234 0.04 0.1 0.6 0.9 0.7 NDS -0.4 -0.2 0.28 0.53 1.92

Legend:
R = Rejected
Reproducibility ASTM Standard "See Comment" NDS = No Data Submitted
TPI
Comments:
There is no published ASTM Reproducibility for this test method for 25C.
200
Sample ID: CO1607

(mm/s)
1.16 5.36
0.87 5.07
0.58 4.78
0.29 4.49
Deviation
0 4.2
-0.29 3.91
-0.58 3.62
-0.87 3.33
-1.16 3.04
1 1 1 1 1 8 2 1 2 6 1 1 1 9 9 2 5 5 8 1 2 1 8 1 2 9 9 1 1 4 1 1 2 1 1 1 2 1 2 1 1 2 2 1 1 1 1 1 1 6 2 1 1 5 9 1 7 1 2 7 8 1
0 0 0 3 1 0 1 8 2 6 6 7 2 6 1 4 8 9 2 0 1 8 1 1 0 3 0 8 0 9 3 1 3 3 7 3 9 1 9 4 2 3 8 9 6 6 4 9 0 2 4 2 7 4 6 7 6 3 4 5 5
7 2 8 5 1 1 9 8 5 8 3 0 9 9 6 3 8 3 3 3 8 4 7 7 0 2 7 7 9 3 2 4 1 5 9 8 1 6 2

201
Sample ID: CO1607

(mm/s)
24
Median
1% 99%
20
16
Number of Labs
12
0
3.25 - 3.45 3.5 - 3.7 3.75 - 3.95 4 - 4.2 4.25 - 4.45 4.5 - 4.7 4.75 - 4.95 5 - 5.2
ASTM Crude Oil
Sample ID: CO1607
July 2016 202
(mm/s)
1603 1511 1507 1503 1411 1407
003 2.811 -0.019 -0.4 -0.8 0.7 1.6 -0.4 -0.6 0.1 0.03 0.85 1.22
005 2.796 -0.034 -0.8 1.6 -2.3 -0.4 0.3 1.1 0.2 -0.04 1.29 0.81
006 ** 3.082 R 0.1 -0.3 0.4 0.0 -1.2 0.3 -0.12 0.58 1.79
008 2.800 -0.030 -0.7 0.1 2.7 0.9 0.2 -0.3 NDS 0.48 1.21 0.86
013 2.769 -0.061 -1.4 -0.3 2.3 3.4 0.2 1.0 -1.0 0.60 1.75 0.59 X
015 2.777 -0.053 -1.2 -1.3 -1.0 NDS 0.2 NDS NDS -0.82 0.69 1.51
017 2.788 -0.042 -1.0 -0.4 -0.1 0.0 -1.0 -0.7 -0.9 -0.59 0.42 2.48
019 2.800 -0.030 -0.7 -0.6 NDS NDS R NDS NDS -0.65 0.07 N/A N/A
020 2.867 0.037 0.8 -1.2 -1.2 -1.9 NDS 1.1 -0.8 -0.53 1.21 0.86
021 2.827 -0.003 -0.1 1.8 0.2 2.5 -0.3 -1.8 -1.3 0.14 1.55 0.67 X
023 2.971 0.141 3.2 1, 3 -0.6 0.9 0.9 -0.7 1.3 0.0 0.71 1.34 0.78 X
025 ** 3.092 R NDS NDS NDS 1.2 0.1 0.6 0.63 0.55 N/A N/A
026 2.843 0.013 0.3 -0.4 -0.3 2.5 NDS NDS NDS 0.52 1.35 0.77 X
027 2.861 0.031 0.7 0.9 NDS -3.1 NDS 0.0 0.9 -0.12 1.71 0.61 X
028 2.811 -0.019 -0.4 -0.2 1.1 0.9 -0.8 -0.6 1.7 0.24 0.97 1.07
029 2.876 0.046 1.0 -0.6 -0.9 -0.7 -0.1 -0.4 0.2 -0.21 0.65 1.60
030 2.742 -0.088 -2.0 -0.7 0.4 R 1.4 1.7 0.7 0.25 1.39 0.75 X
032 2.796 -0.034 -0.8 NDS -1.0 -1.3 -0.3 0.6 NDS -0.56 0.74 1.41
035 2.862 0.032 0.7 NDS -0.3 NDS -0.8 -0.2 0.2 -0.08 0.56 1.86
037 2.840 0.010 0.2 NDS -0.4 -1.3 -0.5 -0.8 NDS -0.56 0.55 1.89
048 ** 3.034 R NDS NDS 0.4 0.6 0.1 0.0 0.28 0.28 3.71
049 2.844 0.014 0.3 NDS NDS -1.2 NDS NDS NDS -0.45 1.06 N/A N/A
052 2.829 -0.001 0.0 1.0 NDS NDS NDS NDS NDS 0.50 0.71 N/A N/A
057 2.840 0.010 0.2 -1.6 -1.5 1.3 -2.7 R -2.8 -1.18 1.63 0.64 X
058 2.829 -0.001 0.0 0.0 -0.6 -0.2 NDS R -0.7 -0.30 0.33 3.15
060 ** 3.029 R 2.0 -0.2 -0.5 -0.7 R 0.9 0.30 1.13 0.92
062 ** 3.026 R 0.1 -1.6 0.0 NDS 1.5 R 0.00 1.27 0.82
067 2.873 0.043 1.0 1.4 0.0 -1.3 0.8 0.7 0.3 0.41 0.88 1.18
073 ** 1.530 R -0.9 -1.0 -0.3 1.1 0.0 0.7 -0.07 0.85 1.22
074 2.853 0.023 0.5 R 1.2 2.1 -1.5 R 1.9 0.84 1.45 0.72 X
077 ** 3.132 R -0.9 -0.5 1.3 0.2 0.1 -0.5 -0.05 0.78 1.33
079 2.929 0.099 2.2 3 0.5 -0.4 -0.8 -0.1 NDS NDS 0.28 1.17 0.89
080 2.769 -0.061 -1.4 -1.0 -0.3 -1.1 NDS -1.1 -1.1 -1.00 0.37 2.81
082 2.823 -0.007 -0.2 NDS 0.3 R NDS -1.0 1.0 0.02 0.84 1.24
085 2.8618 0.032 0.7 0.7 NDS -0.5 -0.5 NDS NDS 0.10 0.69 1.51
088 2.817 -0.013 -0.3 R 0.2 NDS NDS -0.2 2.9 0.65 1.52 0.68 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 203
(mm/s)
1603 1511 1507 1503 1411 1407
089 2.796 -0.034 -0.8 0.1 0.3 1.0 -0.5 0.3 2.9 0.47 1.22 0.85
090 2.820 -0.010 -0.2 0.3 -1.0 NDS -0.7 -0.6 -0.9 -0.52 0.49 2.12
091 2.779 -0.051 -1.2 -0.5 -1.0 0.0 -0.2 -0.3 R -0.53 0.47 2.21
092 2.746 -0.084 -1.9 -0.7 NDS 2.8 0.8 NDS NDS 0.25 2.03 0.51 X
093 2.9182 0.089 2.0 -0.9 NDS -1.8 -0.3 NDS NDS -0.25 1.62 0.64 X
096 2.810 -0.020 -0.5 -0.4 R 0.0 2.9 0.4 0.5 0.48 1.25 0.83
099 2.869 0.039 0.9 0.2 1.1 -0.8 1.7 2.4 -1.3 0.60 1.32 0.79 X
101 2.8290 -0.001 0.0 0.0 0.7 R -0.4 R 0.9 0.24 0.54 1.93
102 ** 2.6505 R -2.4 0.1 -0.5 0.1 -0.4 0.1 -0.50 0.97 1.07
103 2.812 -0.018 -0.4 -0.8 -0.8 2.3 -0.2 -0.8 -0.1 -0.11 1.11 0.94
105 2.729 -0.101 -2.3 3 0.1 -1.0 0.8 -0.4 -0.8 -0.3 -0.56 0.97 1.07
107 2.800 -0.030 -0.7 1.4 0.8 NDS R -0.4 NDS 0.28 0.99 1.05
108 2.757 -0.073 -1.7 NDS NDS 0.2 0.2 -0.6 0.5 -0.28 0.89 1.17
110 ** 3.176 R R -1.0 -1.6 NDS NDS NDS -1.30 0.42 N/A N/A
112 2.834 0.004 0.1 2.6 -0.4 -0.3 0.8 NDS 0.4 0.53 1.11 0.94
117 2.830 0.000 0.0 1.1 1.1 -0.1 1.4 NDS -0.8 0.45 0.87 1.20
118 2.832 0.002 0.0 -0.9 NDS -1.0 2.9 NDS NDS 0.25 1.82 0.57 X
122 2.925 0.095 2.2 3 -0.8 0.1 -0.7 NDS NDS 2.2 0.60 1.50 0.69 X
123 2.942 0.112 2.5 3 0.9 0.0 1.1 0.0 1.2 1.2 0.99 0.85 1.22
129 2.825 -0.005 -0.1 -0.9 1.4 -0.4 NDS NDS NDS 0.00 0.99 1.05
131 2.8063 -0.023 -0.5 0.1 0.3 0.6 NDS NDS NDS 0.12 0.46 2.26
132 2.721 -0.109 -2.5 3 -0.5 -0.7 NDS 0.7 NDS -1.6 -0.92 1.20 0.87
133 2.792 -0.038 -0.9 -0.3 NDS NDS 0.9 -1.8 -1.1 -0.64 1.01 1.03
134 2.828 -0.002 0.0 -0.9 1.4 NDS NDS NDS NDS 0.17 1.16 N/A N/A
135 ** 2.568 R -0.1 -1.0 1.0 NDS NDS NDS -0.03 1.00 N/A N/A
138 2.810 -0.020 -0.5 0.8 -0.3 2.9 2.9 -1.3 -0.2 0.61 1.68 0.62 X
141 2.819 -0.011 -0.2 0.5 1.1 -0.6 -1.0 -0.5 R -0.12 0.78 1.33
144 2.820 -0.010 -0.2 NDS -0.1 NDS R NDS NDS -0.15 0.07 N/A N/A
147 2.815 -0.015 -0.3 -0.2 -0.8 1.2 -0.6 NDS NDS -0.14 0.79 1.32
148 2.848 0.018 0.4 NDS -2.2 R -0.6 -0.3 R -0.68 1.10 0.95
149 2.808 -0.022 -0.5 -0.2 NDS NDS 1.2 NDS 0.0 0.12 0.75 1.39
151 2.909 0.079 1.8 NDS -0.4 NDS NDS 0.1 NDS 0.50 1.15 N/A N/A
152 2.945 0.115 2.6 3 0.4 0.3 NDS 1.1 -0.1 1.9 1.03 1.04 1.00
155 2.779 -0.051 -1.2 -0.6 -0.1 -1.4 NDS -0.7 0.5 -0.58 0.70 1.49
158 ** 4.368 R 0.2 -2.0 NDS NDS NDS NDS -0.90 1.56 N/A N/A
159 2.860 0.030 0.7 1.1 R 0.4 0.1 2.7 -0.7 0.72 1.15 0.90
160 2.939 0.109 2.5 3 NDS -1.2 0.5 NDS NDS -0.2 0.40 1.56 0.67 X
161 2.847 0.017 0.4 -0.3 NDS -1.1 -1.1 NDS NDS -0.52 0.72 1.44
ASTM Crude Oil
Sample ID: CO1607
July 2016 204
(mm/s)
1603 1511 1507 1503 1411 1407
163 2.798 -0.032 -0.7 -1.0 -1.1 -0.5 -1.1 -1.2 -0.8 -0.91 0.25 4.16
166 2.848 0.018 0.4 1.6 0.2 -1.1 R -1.9 -0.1 -0.15 1.22 0.85
167 2.851 0.021 0.5 1.7 0.2 3.3 3.4 NDS NDS 1.82 1.51 0.69 X
169 2.847 0.017 0.4 0.2 1.2 -0.1 NDS NDS NDS 0.42 0.56 1.86
170 2.833 0.003 0.1 -0.2 0.5 R -0.3 0.1 0.0 0.03 0.28 3.71
173 2.944 0.114 2.6 3 -0.4 NDS 0.3 NDS NDS NDS 0.83 1.57 N/A N/A
176 2.824 -0.006 -0.1 -1.0 -0.8 2.9 1.3 -0.3 -0.9 0.16 1.44 0.72 X
178 2.790 -0.040 -0.9 -0.7 -0.2 R -1.6 -0.7 -1.2 -0.88 0.48 2.17
179 2.885 0.055 1.2 2.4 1.4 -0.3 1.1 0.5 1.3 1.09 0.83 1.25
180 2.8567 0.027 0.6 0.6 0.5 -1.3 0.1 -0.4 0.0 0.01 0.69 1.51
182 2.83 0.000 0.0 -0.9 NDS R NDS R 3.0 0.70 2.04 N/A N/A
184 2.807 -0.023 -0.5 R -0.6 -0.5 0.2 NDS NDS -0.35 0.37 2.81
189 2.79 -0.040 -0.9 -0.6 1.4 0.0 -1.7 NDS NDS -0.36 1.16 0.90
191 2.979 0.149 3.4 1, 3 0.9 0.5 0.8 -0.9 -1.1 -0.1 0.50 1.50 0.69 X
192 2.826 -0.004 -0.1 -0.3 0.0 0.4 0.3 0.5 0.3 0.16 0.29 3.59
193 2.831 0.001 0.0 0.3 0.9 0.7 2.1 1.7 -0.1 0.80 0.84 1.24
194 ** 3.042 R -0.4 R 0.3 R -1.0 1.3 0.05 0.99 1.05
196 2.837 0.007 0.2 NDS NDS -0.6 0.3 -0.8 0.1 -0.16 0.50 2.08
201 2.8600 0.030 0.7 2.4 -0.6 -1.1 0.9 -0.7 -0.6 0.14 1.25 0.83
204 2.775 -0.055 -1.2 -0.6 -0.5 -0.6 NDS -0.7 -0.5 -0.68 0.26 4.00
208 2.76 -0.070 -1.6 -1.4 1.4 -0.4 -1.3 -0.3 -1.2 -0.69 1.05 0.99
209 2.7814 -0.048 -1.1 -1.0 -0.7 -0.8 -1.3 0.4 -0.4 -0.70 0.57 1.82
210 2.867 0.037 0.8 -0.7 -0.8 -0.2 -0.9 0.2 -0.8 -0.34 0.64 1.62
211 2.834 0.004 0.1 -0.6 -0.8 -0.3 -1.1 -0.3 -0.5 -0.50 0.39 2.67
213 2.868 0.038 0.9 -0.7 NDS -0.4 -0.6 -0.1 -0.6 -0.25 0.60 1.73
214 2.856 0.026 0.6 1.3 -0.2 2.5 0.3 NDS NDS 0.90 1.05 0.99
220 2.9700 0.140 3.2 1, 3 R 1.4 1.1 -0.2 R R 1.37 1.40 0.74 X
223 <8 $ NDS NDS NDS 2.1 0.0 1.05 1.48 N/A N/A
224 2.831 0.001 0.0 1.7 0.2 -0.1 0.9 1.8 0.8 0.76 0.78 1.33
226 2.768 -0.062 -1.4 0.5 -0.9 0.3 1.6 NDS NDS 0.02 1.19 0.87
228 2.987 0.157 3.6 1, 3 0.9 -0.6 0.1 NDS NDS NDS 1.00 1.84 0.57 X
229 2.809 -0.021 -0.5 -0.4 0.1 0.5 NDS NDS NDS -0.08 0.46 2.26
234 2.805 -0.025 -0.6 -0.5 1.1 0.3 NDS -0.6 -0.5 -0.13 0.69 1.51
239 2.832 0.002 0.0 NDS R -0.6 NDS -0.2 NDS -0.27 0.31 N/A N/A
241 2.809 -0.021 -0.5 -0.5 -0.7 -1.0 NDS NDS NDS -0.68 0.24 4.33
ASTM Crude Oil
Sample ID: CO1607
July 2016 205
(mm/s)
Legend:
R = Rejected
Reproducibility ASTM Standard "See Comment" NDS = No Data Submitted
TPI
Comments:
There is no published ASTM Reproducibility for this test method for 40C.
206
Page 1 of 2
Sample ID: CO1607
(mm/s)
0.176 3.006
0.132 2.962
0.088 2.918
0.044 2.874
Deviation
0 2.83
-0.044 2.786
-0.088 2.742
-0.132 2.698
-0.176 2.654
1 1 3 9 1 1 2 1 2 1 8 2 1 1 9 2 1 4 1 1 1 5 3 5 8 1 1 8 4 1 4 1 1 2 2 1 1 1 2 2 1 9 3 2 1 1 1 8 1 1 1 9 8 1 1 1 5 1 2 2
3 0 0 2 1 0 0 4 2 3 0 0 5 5 1 0 7 4 7 8 3 9 2 9 6 9 0 0 6 1 3 3 8 3 4 2 4 3 6 8 0 4 2 8 9 4 4 0 2 4 7 2 0 9 1 1
2 5 6 8 8 6 4 5 9 8 9 3 3 7 2 7 4 4 1 9 9 1 8 3 7 6 9 1 4 2 6 9 2 7

207
Page 2 of 2
Sample ID: CO1607
(mm/s)
0.176 3.006
0.132 2.962
0.088 2.918
0.044 2.874
Deviation
0 2.83
-0.044 2.786
-0.088 2.742
-0.132 2.698
-0.176 2.654
1 5 5 1 1 1 1 2 2 1 1 1 2 1 1 1 3 5 1 2 4 1 1 1 1 1 1 1 7 2 1 2 1 2 8 3 2 2 2 2 9 6 2 1 2 9 1 1 9 1 1 7 1 1 1 1 2 2 2 1 2
3 8 2 0 1 8 9 2 3 1 7 9 1 1 8 9 7 7 8 6 9 2 6 6 6 4 9 6 4 1 8 0 5 7 5 5 2 1 0 1 9 7 9 7 2 4 5 2 3 5 2 9 6 2 7 5 2 2 3 9 2
4 1 7 2 3 4 9 8 0 7 1 2 8 6 0 1 9 6 8 0 7 4 0 1 9 7 0 3 9 1 8 3 2 0 3 3 2 5 0 1 8

208
Sample ID: CO1607

(mm/s)
42
36 1% Median 99%
30
Number of Labs
24
18
12
0
2.7 - 2.72 2.73 - 2.75 2.76 - 2.78 2.79 - 2.81 2.82 - 2.84 2.85 - 2.87 2.88 - 2.9 2.91 - 2.93 2.94 - 2.96 2.97 - 2.99 3 - 3.02
ASTM Crude Oil
Sample ID: CO1607
July 2016 209
D7042 Kinematic Viscosity @ 40C
(mm/s)
1603 * 1511 * 1507 * 1503 * 1411 * 1407 *
002 2.871 0.0500 1.1 1.10 0.00 N/A N/A
015 2.825 0.0040 0.1 0.10 0.00 N/A N/A
017 ** 2.264 R 0.00 0.00 N/A N/A
037 2.820 -0.0010 0.0 0.00 0.00 N/A N/A
042 2.88 0.0590 1.3 1.30 0.00 N/A N/A
045 2.778 -0.0430 -0.9 -0.90 0.00 N/A N/A
046 2.847 0.0260 0.6 0.60 0.00 N/A N/A
051 2.8 -0.0210 -0.5 -0.50 0.00 N/A N/A
064 2.796 -0.0250 -0.5 -0.50 0.00 N/A N/A
075 2.8860 0.0650 1.4 1.40 0.00 N/A N/A
084 2.7147 -0.1063 -2.3 3 -2.30 0.00 N/A N/A
087 2.816 -0.0050 -0.1 -0.10 0.00 N/A N/A
089 2.772 -0.0490 -1.1 -1.10 0.00 N/A N/A
090 2.874 0.0530 1.1 1.10 0.00 N/A N/A
115 2.797 -0.0240 -0.5 -0.50 0.00 N/A N/A
117 2.833 0.0120 0.3 0.30 0.00 N/A N/A
139 2.805 -0.0160 -0.3 -0.30 0.00 N/A N/A
144 2.820 -0.0010 0.0 0.00 0.00 N/A N/A
151 2.876 0.0550 1.2 1.20 0.00 N/A N/A
161 2.949 0.1280 2.8 3 2.80 0.00 N/A N/A
164 2.7797 -0.0413 -0.9 -0.90 0.00 N/A N/A
178 2.790 -0.0310 -0.7 -0.70 0.00 N/A N/A
183 2.80 -0.0210 -0.5 -0.50 0.00 N/A N/A
198 2.746 -0.0750 -1.6 -1.60 0.00 N/A N/A
200 2.801 -0.0200 -0.4 -0.40 0.00 N/A N/A
216 2.831 0.0100 0.2 0.20 0.00 N/A N/A
220 2.8521 0.0311 0.7 0.70 0.00 N/A N/A

Legend:
R = Rejected
TPI
Comments:
210
Sample ID: CO1607

(mm/s)
0.1848 3.0058
0.1386 2.9596
0.0924 2.9134
0.0462 2.8672
Deviation
0 2.821
-0.0462 2.7748
-0.0924 2.7286

-0.1386 2.6824
-0.1848 2.6362
8 1 8 4 1 1 6 1 1 5 2 1 8 3 1 1 2 1 4 2 2 9 1 4 7 1
4 9 9 5 6 7 4 1 8 1 0 3 7 7 4 5 1 1 6 2 0 5 2 5 6
8 4 8 5 3 0 9 4 6 7 0 1 1

211
Sample ID: CO1607

(mm/s)
16
14
Median
12
10
Number of Labs
0
2.674 - 2.726 2.727 - 2.779 2.78 - 2.832 2.833 - 2.885 2.886 - 2.938 2.939 - 2.991
ASTM Crude Oil
Sample ID: CO1607
July 2016 212
D7042 Dynamic Viscosity @ 100C
(mm/s)
1603 * 1511 * 1507 * 1503 * 1411 * 1407 *
115 1.193 0.0212 0.5 0.50 0.00 N/A N/A
117 1.183 0.0112 0.3 0.30 0.00 N/A N/A
137 1.170 -0.0018 0.0 0.00 0.00 N/A N/A
183 1.15 -0.0218 -0.6 -0.60 0.00 N/A N/A
200 1.113 -0.0588 -1.5 -1.50 0.00 N/A N/A
225 1.216 0.0442 1.1 1.10 0.00 N/A N/A

Legend:
No. Valid Results 6
R = Rejected
TPI
Comments:
213
Sample ID: CO1607

D7042 Dynamic Viscosity @ 100C
(mm/s)
0.1544 1.3262
0.1158 1.2876
0.0772 1.249
0.0386 1.2104
Deviation
0 1.1718
-0.0386 1.1332
-0.0772 1.0946
-0.1158 1.056
-0.1544 1.0174
2 1 1 1 1 2
0 8 3 1 1 2
0 3 7 7 5 5

ASTM Crude Oil
Sample ID: CO1607
July 2016 214
Water - D4006
(Volume%)
1603 1511 1507 1503 1411 1407
003 0.000 -0.0082 -0.6 $ 1.0 -0.4 2.7 -0.6 -0.8 0.22 1.38 0.75 X
004 0.025 0.0168 1.2 $ NDS -0.4 -0.7 NDS $ 0.03 1.02 N/A N/A
005 0.000 -0.0082 -0.6 $ -1.5 1.0 1.0 0.9 2.6 0.57 1.43 0.72 X
006 0.025 0.0168 1.2 $ -0.9 0.5 -0.7 0.9 0.0 0.17 0.85 1.21
007 0.025 0.0168 1.2 NDS NDS NDS 1.0 NDS NDS 1.10 0.14 N/A N/A
008 0.000 -0.0082 -0.6 $ 0.7 1.5 -0.7 -0.6 NDS 0.06 0.99 1.04
013 0.000 -0.0082 -0.6 $ R -1.4 -0.7 -0.6 -0.8 -0.82 0.33 3.12
015 0.000 -0.0082 -0.6 $ -0.3 NDS 1.0 NDS NDS 0.03 0.85 N/A N/A
017 0.000 -0.0082 -0.6 $ -0.6 -1.4 -0.7 -0.6 -0.8 -0.78 0.31 3.32
023 0.000 -0.0082 -0.6 $ 1.6 1.5 -0.7 -0.6 2.6 0.63 1.44 0.72 X
024 0.025 0.0168 1.2 $ -0.6 0.5 -0.7 -0.6 -0.8 -0.17 0.82 1.26
025 0.025 0.0168 1.2 NDS R NDS -0.7 0.9 2.6 1.00 1.35 0.76 X
026 0.025 0.0168 1.2 $ 0.4 0.0 -0.7 NDS NDS 0.23 0.79 1.30
028 0.025 0.0168 1.2 R 0.4 -0.9 NDS NDS NDS 0.23 1.06 N/A N/A
029 0.000 -0.0082 -0.6 $ R -0.4 NDS -0.6 2.6 0.25 1.57 0.66 X
030 0.000 -0.0082 -0.6 $ -0.6 0.0 2.7 2.3 R 0.76 1.61 0.64 X
043 0.000 -0.0082 -0.6 NDS NDS -0.4 NDS -0.6 -0.8 -0.60 0.16 6.44
047 0.000 -0.0082 -0.6 $ -0.3 0.0 1.0 -0.6 0.9 0.07 0.72 1.43
048 0.025 0.0168 1.2 NDS NDS 0.5 1.0 -0.6 2.6 0.94 1.16 0.89
053 0.000 -0.0082 -0.6 $ -0.6 -0.9 -0.7 -0.6 -0.8 -0.70 0.13 7.92
054 ** 0.175 R NDS -0.3 1.5 1.0 0.9 0.0 0.62 0.75 1.37
058 0.025 0.0168 1.2 $ 0.4 -0.4 NDS 2.3 2.6 1.22 1.26 0.82
060 0.000 -0.0082 -0.6 $ -2.1 0.5 NDS -0.6 1.7 -0.22 1.42 0.73 X
062 0.000 -0.0082 -0.6 $ NDS 0.5 NDS $ R -0.05 0.78 N/A N/A
067 0.000 -0.0082 -0.6 $ -1.2 -1.9 -0.7 -0.6 -0.8 -0.97 0.51 2.02
072 0.000 -0.0082 -0.6 NDS 0.4 0.5 -0.7 -0.6 0.0 -0.17 0.54 1.91
073 0.000 -0.0082 -0.6 $ 0.4 0.5 R 0.9 0.0 0.24 0.57 1.81
074 <0.025 NDS 1.9 0.0 1.0 R -0.8 0.52 1.18 0.87
079 0.000 -0.0082 -0.6 $ R 1.9 -0.7 NDS NDS 0.20 1.47 N/A N/A
085 0.000 -0.0082 -0.6 $ NDS 1.0 -0.7 NDS NDS -0.10 0.95 N/A N/A
088 0.025 0.0168 1.2 NDS 1.0 -0.4 $ -0.6 -0.8 0.08 0.94 1.10
089 0.000 -0.0082 -0.6 $ 1.3 0.5 -0.7 -0.6 0.9 0.13 0.88 1.17
091 0.000 -0.0082 -0.6 $ -0.9 -1.4 -0.7 NDS NDS -0.90 0.36 2.86
092 0.000 -0.0082 -0.6 $ -2.1 -1.9 1.0 0.9 NDS -0.54 1.48 0.70 X
096 0.050 0.0418 3.1 1, 2, 3 $ 1.3 1.5 1.0 2.3 0.0 1.53 1.07 0.96
101 0.000 -0.0082 -0.6 $ NDS -0.4 1.0 NDS NDS 0.00 0.87 N/A N/A
103 0.000 -0.0082 -0.6 $ -3.0 -1.4 1.0 -0.6 0.9 -0.62 1.50 0.69 X
108 0.025 0.0168 1.2 NDS NDS $ -0.7 -0.6 -0.8 -0.22 0.95 1.08
110 0.050 0.0418 3.1 1, 2, 3 $ -2.1 -0.4 NDS NDS NDS 0.20 2.65 N/A N/A
112 ** 0.075 R R -3.0 -1.4 2.7 NDS -0.8 -0.62 2.40 0.43 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 215
Water - D4006
(Volume%)
1603 1511 1507 1503 1411 1407
117 0.000 -0.0082 -0.6 NDS 0.4 -0.4 -0.7 -0.6 0.9 -0.17 0.66 1.56
119 0.000 -0.0082 -0.6 NDS NDS $ NDS NDS NDS -0.60 0.00 N/A N/A
122 0.050 0.0418 3.1 1, 2, 3 $ -0.3 -0.4 NDS NDS -0.8 0.40 1.81 0.57 X
123 0.000 -0.0082 -0.6 $ 1.0 1.5 -0.7 0.9 0.0 0.35 0.91 1.13
124 0.000 -0.0082 -0.6 $ 0.4 -0.4 -0.7 -0.6 -0.8 -0.45 0.44 2.34
126 0.025 0.0168 1.2 $ -0.9 -0.4 1.0 -0.6 0.0 0.05 0.87 1.18
127 0.025 0.0168 1.2 $ -2.1 1.5 1.0 NDS 2.6 0.84 1.76 0.59 X
132 0.025 0.0168 1.2 $ -0.3 -0.4 1.0 NDS -0.8 0.14 0.90 1.14
133 0.000 -0.0082 -0.6 $ 1.0 NDS 1.0 2.3 -0.8 0.58 1.29 0.80
134 0.000 -0.0082 -0.6 $ 2.2 NDS NDS NDS NDS 0.80 1.98 N/A N/A
138 0.000 -0.0082 -0.6 $ -1.2 -1.9 -0.7 -0.6 -0.8 -0.97 0.51 2.02
142 0.025 0.0168 1.2 $ NDS NDS NDS NDS NDS 1.20 0.00 N/A N/A
144 0.000 -0.0082 -0.6 NDS 1.0 NDS -0.7 NDS NDS -0.10 0.95 N/A N/A
148 0.000 -0.0082 -0.6 $ R -2.3 -0.7 -0.6 -0.8 -1.00 0.73 1.41
152 0.000 -0.0082 -0.6 $ R -0.9 -0.7 -0.6 0.9 -0.38 0.73 1.41
154 0.025 0.0168 1.2 $ NDS 0.5 NDS 0.9 0.0 0.65 0.52 1.98
161 0.000 -0.0082 -0.6 $ NDS -0.9 -0.7 NDS NDS -0.73 0.15 N/A N/A
163 0.000 -0.0082 -0.6 R 0.4 0.5 -0.7 -0.6 -0.8 -0.30 0.59 1.75
166 0.025 0.0168 1.2 $ NDS -0.4 $ 2.3 NDS 1.03 1.36 N/A N/A
167 0.000 -0.0082 -0.6 $ 1.0 0.5 1.0 NDS NDS 0.48 0.75 1.37
169 0.000 -0.0082 -0.6 $ 0.4 -1.9 NDS NDS NDS -0.70 1.15 N/A N/A
170 0.025 0.0168 1.2 $ R 1.0 -0.7 -0.6 2.6 0.70 1.38 0.75 X
172 <0.050 $ -1.5 0.5 $ -0.6 0.0 -0.40 0.86 1.20
173 ** 0.750 R $ NDS 0.5 NDS NDS NDS 0.50 0.00 N/A N/A
176 0.000 -0.0082 -0.6 $ R 1.5 $ -0.6 0.9 0.30 1.07 0.96
179 0.000 -0.0082 -0.6 $ -0.3 0.0 -0.7 -0.6 -0.8 -0.50 0.30 3.43
181 0.000 -0.0082 -0.6 $ R -1.4 NDS NDS NDS -1.00 0.57 N/A N/A
184 0.000 -0.0082 -0.6 $ -0.9 -1.4 -0.7 NDS NDS -0.90 0.36 2.86
191 0.000 -0.0082 -0.6 $ 2.8 0.0 1.0 -0.6 -0.8 0.30 1.39 0.74 X
192 0.000 -0.0082 -0.6 $ -0.3 -0.4 $ $ 0.9 -0.10 0.68 1.51
193 0.000 -0.0082 -0.6 $ -1.2 -0.4 -0.7 -0.6 0.0 -0.58 0.39 2.64
194 0.000 -0.0082 -0.6 $ -0.9 0.0 -0.7 2.3 -0.8 -0.12 1.23 0.84
196 0.000 -0.0082 -0.6 NDS NDS 1.5 -0.7 -0.6 0.0 -0.08 0.93 1.11
ASTM Crude Oil
Sample ID: CO1607
July 2016 216
Water - D4006
(Volume%)
1603 1511 1507 1503 1411 1407
204 0.025 0.0168 1.2 NDS NDS NDS NDS -0.6 -0.8 -0.07 1.10 N/A N/A
207 0.025 0.0168 1.2 $ 0.4 -0.4 1.0 -0.6 0.0 0.27 0.73 1.41
210 0.000 -0.0082 -0.6 $ R NDS -0.7 -0.6 -0.8 -0.68 0.10 10.30
211 0.000 -0.0082 -0.6 $ -0.3 0.5 -0.7 $ -0.8 -0.38 0.53 1.94
213 0.000 -0.0082 -0.6 $ -0.9 -0.4 -0.7 -0.6 -0.8 -0.67 0.18 5.72
216 0.025 0.0168 1.2 NDS NDS NDS -0.7 NDS NDS 0.25 1.34 N/A N/A
218 0.025 0.0168 1.2 R NDS NDS 2.7 0.9 0.9 1.43 0.86 1.20
220 0.025 0.0168 1.2 $ -1.5 -0.4 $ -0.6 NDS -0.32 1.12 0.92
223 0.000 -0.0082 -0.6 $ NDS NDS NDS 2.3 0.9 0.87 1.45 N/A N/A
224 0.050 0.0418 3.1 1, 2, 3 $ 0.4 0.0 1.0 NDS NDS 1.12 1.38 0.75 X
226 0.000 -0.0082 -0.6 $ R -1.4 -0.7 NDS NDS -0.90 0.44 N/A N/A
229 0.000 -0.0082 -0.6 $ -0.9 -0.4 NDS NDS NDS -0.63 0.25 N/A N/A
234 0.000 -0.0082 -0.6 NDS NDS 2.4 -0.7 -0.6 -0.8 -0.06 1.38 0.75 X
239 0.000 -0.0082 -0.6 NDS -0.9 -0.4 NDS 0.9 NDS -0.25 0.79 1.30

Legend:
R = Rejected
TPI 0.93
Comments:
ASTM Crude Oil
Sample ID: CO1607
July 2016 217
Water and Sediment by Centrifuge - D4007
Total % v Water & Sediment
1603 1511 1507 1503 1411 1407
003 0.050 0.016 0.7 -0.6 0.0 0.3 -1.2 -0.8 -0.7 -0.33 0.68 1.50
004 0.025 -0.009 -0.4 -0.6 NDS -0.7 -0.2 NDS 0.0 -0.38 0.29 3.52
005 0.000 -0.034 -1.4 -0.6 0.0 0.3 -0.2 0.3 0.7 -0.13 0.70 1.46
006 0.050 0.016 0.7 -0.6 0.0 2.3 -1.2 0.3 1.4 0.41 1.19 0.86
007 0.050 0.016 0.7 1.1 0.7 2.3 0.8 NDS NDS 1.12 0.68 1.50
008 0.000 -0.034 -1.4 -0.6 1.0 2.3 -1.2 0.3 NDS 0.07 1.42 0.72 X
011 0.100 0.066 2.8 3 NDS 0.7 -0.7 0.8 $ 1.4 1.00 1.27 0.80
013 0.000 -0.034 -1.4 -0.6 -3.6 -0.7 -1.2 -0.8 0.0 -1.19 1.16 0.88
014 <0.025 $ NDS NDS NDS NDS NDS 0.00 0.00 N/A N/A
015 0.000 -0.034 -1.4 $ -0.8 NDS -0.2 NDS NDS -0.80 0.60 N/A N/A
017 0.025 -0.009 -0.4 $ 1.4 -0.7 -1.2 -0.8 $ -0.34 1.01 1.01
019 <0.050 2.7 -0.8 0.3 NDS NDS 0.0 0.55 1.51 0.68 X
020 0.025 -0.009 -0.4 -0.6 0.7 -0.7 -1.2 -0.8 0.0 -0.43 0.62 1.65
021 <0.025 $ $ $ 0.8 -0.8 R 0.00 1.13 N/A N/A
023 0.000 -0.034 -1.4 -0.6 -0.8 0.3 0.8 -0.8 1.4 -0.16 1.01 1.01
024 0.025 -0.009 -0.4 $ 0.3 1.8 -1.2 -0.8 -1.4 -0.28 1.19 0.86
025 <0.025 NDS 0.0 NDS -0.2 0.3 1.4 0.38 0.71 1.44
026 0.050 0.016 0.7 $ 0.3 -0.2 -0.2 NDS NDS 0.15 0.44 2.32
027 0.000 -0.034 -1.4 -0.6 0.0 3.3 NDS 0.3 -0.7 0.15 1.65 0.62 X
028 0.050 0.016 0.7 2.7 0.3 -0.7 0.8 1.5 0.0 0.76 1.10 0.93
029 0.025 -0.009 -0.4 -0.6 -0.8 -0.7 -0.2 0.3 1.4 -0.14 0.77 1.32
030 ** 0.125 R -0.6 R 1.3 -1.2 -0.8 0.0 -0.26 0.97 1.05
031 0.050 0.016 0.7 NDS 1.4 -1.6 0.8 1.5 0.0 0.47 1.15 0.89
032 0.050 0.016 0.7 NDS 1.4 0.3 -0.2 0.3 NDS 0.50 0.60 1.70
034 ** 0.300 R NDS -0.4 0.3 R 0.3 -0.7 -0.12 0.51 2.00
037 0.050 0.016 0.7 NDS 1.0 0.3 0.8 1.5 NDS 0.86 0.44 2.32
042 ** 0.250 R -0.6 -3.6 0.3 NDS 1.5 NDS -0.60 2.18 0.47 X
043 0.000 -0.034 -1.4 1.1 R -0.7 NDS 0.3 -1.4 -0.42 1.10 0.93
045 0.000 -0.034 -1.4 -0.6 -1.1 -0.7 -1.2 -0.8 0.0 -0.83 0.46 2.22
046 0.025 -0.009 -0.4 -0.6 1.0 -0.7 0.8 NDS NDS 0.02 0.81 1.26
047 0.000 -0.034 -1.4 -0.6 0.0 0.3 -1.2 -0.8 0.0 -0.53 0.65 1.57
048 0.000 -0.034 -1.4 NDS NDS 0.3 -1.2 -0.8 1.4 -0.34 1.17 0.87
049 0.050 0.016 0.7 -0.6 -0.8 0.3 2.8 NDS NDS 0.48 1.44 0.71 X
054 0.025 -0.009 -0.4 NDS -0.8 -0.7 -0.2 0.3 NDS -0.36 0.44 2.32
055 0.000 -0.034 -1.4 -0.6 R R -1.2 1.5 0.0 -0.34 1.17 0.87
058 0.050 0.016 0.7 $ -0.8 -0.2 NDS 1.5 0.0 0.24 0.88 1.16
060 0.000 -0.034 -1.4 -0.6 -0.8 1.3 -0.2 -0.8 0.7 -0.26 0.94 1.09
062 0.000 -0.034 -1.4 -0.6 0.7 1.3 NDS $ 2.7 0.54 1.61 0.63 X
066 0.100 0.066 2.8 3 1.1 -0.8 R 0.8 1.5 0.0 0.90 1.24 0.82
ASTM Crude Oil
Sample ID: CO1607
July 2016 218
1603 1511 1507 1503 1411 1407
067 0.050 0.016 0.7 1.1 0.1 -1.2 -0.2 -0.8 -1.4 -0.24 0.95 1.07
072 0.000 -0.034 -1.4 NDS 0.7 0.3 -0.2 -0.8 -0.7 -0.35 0.77 1.32
074 <0.025 -0.6 1.4 -0.7 0.8 R 0.0 0.18 0.91 1.12
076 0.050 0.016 0.7 -0.6 0.0 -0.7 -1.2 -0.8 0.0 -0.37 0.64 1.59
077 0.050 0.016 0.7 -0.6 0.0 0.3 -1.2 R 0.0 -0.13 0.67 1.52
078 0.050 0.016 0.7 -0.6 0.7 0.3 -0.2 -0.8 0.0 0.01 0.59 1.73
079 0.075 0.041 1.7 2.7 0.0 3.3 $ NDS NDS 1.92 1.44 0.71 X
086 0.025 -0.009 -0.4 1.1 -0.4 $ -0.2 -0.8 0.0 -0.12 0.65 1.57
088 0.050 0.016 0.7 $ 0.0 0.3 -0.2 0.3 $ 0.22 0.34 3.00
089 0.025 -0.009 -0.4 -0.6 -0.8 2.3 -0.2 -0.8 R -0.08 1.19 0.86
090 0.025 -0.009 -0.4 -0.6 0.7 -0.2 -1.2 0.3 1.4 0.00 0.87 1.17
091 0.025 -0.009 -0.4 -0.6 0.5 -0.7 -0.2 -0.8 -0.7 -0.41 0.45 2.27
092 0.025 -0.009 -0.4 -0.6 R -1.2 -0.2 0.3 NDS -0.42 0.55 1.85
093 0.000 -0.034 -1.4 1.1 -1.5 0.3 0.8 NDS NDS -0.14 1.23 0.83
096 0.025 -0.009 -0.4 2.7 0.0 1.3 -0.2 1.5 0.0 0.70 1.15 0.89
097 0.050 0.016 0.7 -0.6 -3.6 NDS -1.2 R -1.4 -1.22 1.56 0.65 X
099 0.025 -0.009 -0.4 $ 0.7 NDS NDS NDS NDS 0.15 0.78 N/A N/A
101 ** 0.250 R -0.6 -0.4 -0.7 0.8 NDS NDS -0.22 0.69 1.48
102 ** 0.400 R -0.6 2.8 R 2.8 1.5 R 1.62 1.60 0.64 X
103 0.000 -0.034 -1.4 -0.6 -1.1 -0.7 0.8 1.5 -0.7 -0.31 1.06 0.96
105 0.050 0.016 0.7 -0.6 0.7 0.3 -1.2 0.3 1.4 0.23 0.87 1.17
106 0.025 -0.009 -0.4 R R -1.6 NDS NDS NDS -1.00 0.85 N/A N/A
107 0.050 0.016 0.7 2.7 0.0 NDS -1.2 -0.8 NDS 0.28 1.54 0.66 X
108 0.050 0.016 0.7 $ NDS NDS $ -0.8 $ -0.05 1.06 N/A N/A
109 0.050 0.016 0.7 1.1 0.7 -0.7 0.8 1.5 0.0 0.59 0.73 1.40
110 0.025 -0.009 -0.4 $ -0.8 0.3 NDS NDS NDS -0.30 0.56 N/A N/A
111 0.050 0.016 0.7 1.1 0.7 0.3 NDS 1.5 NDS 0.86 0.46 2.22
112 0.050 0.016 0.7 -0.6 -0.8 0.3 0.8 NDS -1.4 -0.17 0.90 1.13
114 0.100 0.066 2.8 3 2.7 -0.8 -0.2 0.8 NDS NDS 1.06 1.65 0.62 X
118 0.025 -0.009 -0.4 1.1 NDS -0.7 0.8 NDS -0.7 0.02 0.86 1.19
119 0.050 0.016 0.7 NDS NDS 0.3 NDS NDS NDS 0.50 0.28 N/A N/A
122 0.025 -0.009 -0.4 $ -0.8 -1.2 NDS NDS $ -0.80 0.40 N/A N/A
123 0.000 -0.034 -1.4 1.1 1.4 R 2.8 -0.8 0.0 0.52 1.55 0.66 X
124 0.050 0.016 0.7 2.7 0.7 0.3 0.8 1.5 0.0 0.96 0.90 1.13
125 0.100 0.066 2.8 3 -0.6 0.7 NDS R NDS NDS 0.97 1.72 N/A N/A
126 0.025 -0.009 -0.4 -0.6 0.7 2.3 NDS -0.8 0.0 0.20 1.16 0.88
127 0.050 0.016 0.7 -0.6 -0.8 2.3 -0.2 0.3 1.4 0.44 1.12 0.91
129 <0.025 $ 1.4 0.3 -2.2 NDS NDS -0.17 1.84 N/A N/A
132 0.025 -0.009 -0.4 -0.6 0.7 0.3 -0.2 NDS $ -0.04 0.53 1.92
137 0.000 -0.034 -1.4 -0.6 NDS NDS NDS -0.8 R -0.93 0.42 N/A N/A
138 0.000 -0.034 -1.4 1.1 -0.8 0.8 0.8 -0.8 -1.4 -0.24 1.10 0.93
ASTM Crude Oil
Sample ID: CO1607
July 2016 219
1603 1511 1507 1503 1411 1407
139 0.050 0.016 0.7 1.1 1.4 R -0.2 -0.8 0.0 0.37 0.84 1.21
143 0.050 0.016 0.7 -0.6 -3.6 -0.7 0.8 -0.8 0.0 -0.60 1.48 0.69 X
144 0.050 0.016 0.7 NDS R NDS NDS NDS NDS 0.70 0.00 N/A N/A
145 0.050 0.016 0.7 1.1 R 0.3 -1.2 1.5 0.0 0.40 0.95 1.07
146 0.050 0.016 0.7 -0.6 NDS 0.3 -1.2 NDS NDS -0.20 0.86 1.19
148 0.000 -0.034 -1.4 -0.6 -0.8 -0.7 0.8 -0.8 -0.7 -0.60 0.67 1.52
149 <0.025 1.1 NDS -1.2 0.8 -2.0 $ -0.32 1.51 0.68 X
151 0.050 0.016 0.7 NDS NDS NDS NDS 1.5 NDS 1.10 0.57 N/A N/A
152 0.050 0.016 0.7 -0.6 -3.6 -0.7 -1.2 -0.8 2.7 -0.50 1.91 0.53 X
154 0.025 -0.009 -0.4 -0.6 NDS -1.6 -1.2 0.3 -1.4 -0.82 0.72 1.42
155 0.025 -0.009 -0.4 -0.6 -1.8 -1.2 -0.2 -0.8 -0.7 -0.81 0.54 1.89
158 0.000 -0.034 -1.4 NDS NDS R NDS NDS NDS -1.40 0.00 N/A N/A
161 0.025 -0.009 -0.4 $ NDS 0.3 0.8 NDS NDS 0.23 0.60 N/A N/A
163 0.025 -0.009 -0.4 1.1 0.7 0.8 $ $ 0.0 0.44 0.62 1.65
166 0.050 0.016 0.7 $ 1.4 0.3 $ 0.3 0.0 0.54 0.54 1.89
168 0.050 0.016 0.7 NDS 1.4 -0.7 NDS $ $ 0.47 1.07 N/A N/A
170 0.025 -0.009 -0.4 -0.6 -1.5 0.3 -1.2 -0.8 1.4 -0.40 0.98 1.04
172 <0.025 -0.6 -0.8 0.3 -0.2 -0.8 -0.7 -0.47 0.44 2.32
174 0.025 -0.009 -0.4 -0.6 NDS NDS -1.2 0.3 R -0.48 0.62 1.65
176 0.050 0.016 0.7 -0.6 NDS 1.3 0.8 -0.8 0.0 0.23 0.84 1.21
178 <0.025 -0.6 -0.8 0.3 $ -0.8 1.4 -0.10 0.95 1.07
179 0.050 0.016 0.7 -0.6 0.7 2.3 -1.2 -0.8 0.0 0.16 1.19 0.86
182 0.050 0.016 0.7 -0.6 NDS -1.6 NDS 0.3 0.0 -0.24 0.90 1.13
183 0.100 0.066 2.8 3 -0.6 R -0.7 -0.2 NDS 1.4 0.54 1.52 0.67 X
184 0.000 -0.034 -1.4 $ 0.0 -0.7 -1.2 NDS NDS -0.82 0.62 1.65
187 ** 0.150 R NDS NDS -1.6 -0.2 NDS NDS -0.90 0.99 N/A N/A
189 0.050 0.016 0.7 2.7 -1.1 -0.7 0.8 NDS NDS 0.48 1.50 0.68 X
191 0.050 0.016 0.7 -0.6 2.1 -0.7 0.8 -0.8 NDS 0.25 1.15 0.89
193 0.050 0.016 0.7 -0.6 0.0 0.3 0.8 1.5 1.4 0.59 0.75 1.36
194 0.025 -0.009 -0.4 -0.6 0.0 -0.2 -0.2 1.5 -0.7 -0.09 0.74 1.38
196 0.000 -0.034 -1.4 NDS NDS 2.3 -1.2 0.3 -0.7 -0.14 1.51 0.68 X
198 0.000 -0.034 -1.4 -0.6 -0.8 2.3 2.8 -0.8 -1.4 0.01 1.76 0.58 X
201 0.050 0.016 0.7 NDS NDS -0.7 NDS NDS NDS 0.00 0.99 N/A N/A
204 0.050 0.016 0.7 NDS 0.0 -0.2 NDS 0.3 0.0 0.16 0.35 2.91
206 0.075 0.041 1.7 1.1 -0.8 NDS 0.8 NDS NDS 0.70 1.07 0.95
207 0.050 0.016 0.7 2.7 -0.4 -0.7 -1.2 -0.8 -1.4 -0.16 1.43 0.71 X
208 0.025 -0.009 -0.4 1.1 0.0 -0.7 -0.2 0.3 -0.7 -0.09 0.64 1.59
209 0.025 -0.009 -0.4 1.1 0.7 0.3 -0.2 0.3 -0.7 0.16 0.63 1.62
210 0.050 0.016 0.7 -0.6 -3.6 -1.6 -1.2 -0.8 -1.4 -1.21 1.30 0.78 X
211 0.050 0.016 0.7 -0.6 -0.8 -0.7 0.8 -0.8 -1.4 -0.40 0.83 1.23
212 0.050 0.016 0.7 -0.6 -0.4 0.3 2.8 NDS NDS 0.56 1.36 0.75 X
213 0.000 -0.034 -1.4 -0.6 0.7 -0.7 $ -0.8 0.0 -0.47 0.73 1.40
214 0.050 0.016 0.7 -0.6 0.7 R 0.8 NDS NDS 0.40 0.67 1.52
ASTM Crude Oil
Sample ID: CO1607
July 2016 220
1603 1511 1507 1503 1411 1407
216 0.050 0.016 0.7 1.1 0.7 $ -1.2 NDS NDS 0.32 1.03 0.99
220 <0.025 $ NDS $ $ $ $ 0.00 0.00 N/A N/A
221 0.050 0.016 0.7 NDS -2.9 -1.6 -1.2 -0.8 0.7 -0.85 1.39 0.73 X
226 0.050 0.016 0.7 -0.6 -0.8 -0.7 -0.2 NDS NDS -0.32 0.61 1.67
228 0.025 -0.009 -0.4 2.7 -0.8 -0.7 0.8 NDS $ 0.32 1.48 0.69 X
236 0.050 0.016 0.7 1.1 NDS -0.2 0.8 NDS NDS 0.60 0.56 1.82
239 0.025 -0.009 -0.4 NDS 0.3 0.3 NDS 0.3 NDS 0.12 0.35 2.91
241 0.050 0.016 0.7 -0.6 0.0 R R -0.8 0.0 -0.14 0.59 1.73

Legend:
R = Rejected
Reproducibility ASTM Standard See Comment
0.28 NDS = No Data Submitted
TPI
Comments:
221
Page 1 of 2
Sample ID: CO1607
NOTE:3SigmaRangeLimitASTMStandard Water and Sediment by Centrifuge - D4007
Reproducibilityplottedoutsiderangeof Total % v Water & Sediment
thisgraph
0.096 0.13
0.072 0.106
0.048 0.082
0.024 0.058
Deviation
0 0.034
-0.024 0.01
-0.048 -0.014
-0.072 -0.038
-0.096 -0.062
5 2 1 1 1 1 1 1 1 1 1 9 7 6 6 5 5 4 4 4 4 2 2 1 1 8 9 4 9 1 9 9 1 8 8 1 6 2 1 1 5 2 1 2 4 1 1 2 1 2 1 2 2 1 1 1 1 2 9 3 6 7
1 9 9 8 5 4 3 3 2 0 3 2 2 0 5 0 8 7 5 3 7 3 5 3 0 2 6 6 9 7 9 6 6 4 2 5 5 4 0 9 0 6 3 2 9 7 4 2 2 0 7 1 1 0 3 1
3 8 6 4 8 8 8 7 3 3 3 0 1 8 5 4 9 4 8 2 6 4 2 8 0 6 9

222
Page 2 of 2
Sample ID: CO1607
NOTE:3SigmaRangeLimitASTMStandard Water and Sediment by Centrifuge - D4007
Reproducibilityplottedoutsiderangeof Total % v Water & Sediment
thisgraph
0.096 0.13
0.072 0.106
0.048 0.082
0.024 0.058
Deviation
0 0.034
-0.024 0.01
-0.048 -0.014
-0.072 -0.038
-0.096 -0.062
2 2 3 3 3 4 5 5 6 6 7 7 7 8 9 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 2 2 2 2 2 2 2 2 2 2 2 7 1 1 6 1 1
6 8 1 2 7 9 8 9 1 7 6 7 8 8 7 0 0 0 0 1 1 1 1 1 2 2 2 3 3 4 4 4 4 5 5 6 6 7 7 8 8 9 9 9 0 0 0 1 1 1 1 1 2 2 3 4 0 9 2 8 6 1 1
5 7 8 9 1 2 3 6 9 1 4 7 4 9 3 4 5 6 1 2 6 8 6 9 2 9 1 3 5 1 4 7 0 1 2 4 6 1 6 6 1 6 5 3 4

223
Sample ID: CO1607

70
60 Median
50
Number of Labs
40
30
20
10
0
0 0.01 0.02 0.03 0.04 0.05 0.06 0.07 0.08 0.09 0.1 0.11
ASTM Crude Oil
Sample ID: CO1607
July 2016 224
Water - D4928
(Mass%)
1603 1511 1507 1503 1411 1407
005 0.02 -0.004 -0.7 0.2 -1.0 0.8 0.4 R 0.8 0.08 0.77 1.25
006 0.03 0.006 1.0 0.2 -0.6 -1.0 1.9 1.8 -0.4 0.41 1.17 0.82
010 0.02 -0.004 -0.7 0.2 -0.1 NDS 0.4 -0.2 0.2 -0.03 0.39 2.46
011 0.02 -0.004 -0.7 NDS 0.2 0.1 0.4 -0.2 -1.1 -0.22 0.58 1.66
012 0.03 0.006 1.0 0.2 -1.6 R 1.9 NDS NDS 0.37 1.49 0.64 X
013 0.03 0.006 1.0 0.2 R 1.3 1.9 -0.2 -0.4 0.63 0.91 1.05
015 0.03 0.006 1.0 0.2 -0.7 NDS -1.0 NDS NDS -0.12 0.91 1.05
017 0.02 -0.004 -0.7 0.2 0.6 1.0 0.4 -0.2 0.2 0.21 0.55 1.75
020 0.03 0.006 1.0 0.2 0.8 0.6 R -0.2 R 0.48 0.48 2.00
025 0.02 -0.004 -0.7 NDS R NDS -1.0 1.8 0.8 0.23 1.31 0.73 X
026 0.02 -0.004 -0.7 $ 0.6 0.3 0.4 NDS NDS 0.15 0.58 1.66
028 ** 0.05 R 0.2 -0.2 -1.4 0.4 -0.2 -0.4 -0.27 0.63 1.52
029 0.03 0.006 1.0 -1.8 -2.8 -0.7 -2.4 -0.2 0.8 -0.87 1.51 0.64 X
030 0.02 -0.004 -0.7 0.2 0.7 1.2 -1.0 -0.2 -1.1 -0.13 0.88 1.09
032 0.03 0.006 1.0 NDS 0.1 0.6 0.4 -0.2 NDS 0.38 0.46 2.09
037 0.03 0.006 1.0 NDS 0.1 0.8 0.4 -0.2 NDS 0.42 0.49 1.96
038 0.03 0.006 1.0 -1.8 -1.3 -0.8 0.4 -0.2 0.2 -0.36 0.99 0.97
042 ** 0.07 R 0.2 R -0.1 NDS -2.2 NDS -0.70 1.31 N/A N/A
046 0.02 -0.004 -0.7 -1.8 0.3 -0.5 NDS NDS NDS -0.68 0.87 1.10
047 0.02 -0.004 -0.7 0.2 0.3 0.4 0.4 -0.2 -0.4 0.00 0.44 2.18
048 0.02 -0.004 -0.7 NDS NDS 0.6 0.4 -0.2 0.2 0.06 0.52 1.85
051 0.02 -0.004 -0.7 NDS -2.2 NDS 1.9 NDS NDS -0.33 2.07 N/A N/A
054 0.01 -0.014 -2.3 2, 3 NDS -1.3 0.3 -2.4 R NDS -1.42 1.25 0.77 X
058 0.01 -0.014 -2.3 2, 3 $ -0.7 NDS NDS R -1.7 -1.57 0.81 N/A N/A
062 0.03 0.006 1.0 0.2 -0.6 0.1 NDS 1.8 -0.4 0.35 0.90 1.07
068 0.02 -0.004 -0.7 0.2 -0.2 -0.1 0.4 -0.2 0.8 0.03 0.49 1.96
070 0.03 0.006 1.0 -1.8 -0.8 -1.0 -1.0 -0.2 0.8 -0.43 1.02 0.94
074 ** 0.08 R 2.2 NDS -0.8 0.4 R R 0.60 1.51 N/A N/A
077 0.02 -0.004 -0.7 0.2 -0.3 -0.7 -1.0 -0.2 0.2 -0.36 0.46 2.09
079 0.01 -0.014 -2.3 2, 3 0.2 0.1 0.4 -1.0 NDS NDS -0.52 1.13 0.85
088 0.02 -0.004 -0.7 $ 0.0 0.1 0.4 $ R -0.05 0.47 2.04
089 0.02 -0.004 -0.7 0.2 0.6 1.2 0.4 1.8 0.2 0.53 0.80 1.20
091 0.02 -0.004 -0.7 -1.8 -0.5 -1.4 -2.4 R -1.1 -1.32 0.71 1.35
092 0.02 -0.004 -0.7 0.2 -0.5 -2.1 0.4 -0.2 NDS -0.48 0.89 1.08
096 0.03 0.006 1.0 2.2 -0.7 1.3 0.4 -0.2 0.8 0.69 0.96 1.00
098 0.03 0.006 1.0 0.2 NDS 0.6 -1.0 NDS 3.3 0.82 1.58 0.61 X
100 0.02 -0.004 -0.7 0.2 NDS NDS 0.4 -0.2 -1.1 -0.28 0.62 1.55
101 0.02 -0.004 -0.7 0.2 R -1.4 -1.0 1.8 -2.3 -0.57 1.42 0.68 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 225
Water - D4928
(Mass%)
1603 1511 1507 1503 1411 1407
103 0.02 -0.004 -0.7 0.2 -1.5 -1.2 -1.0 NDS -1.7 -0.98 0.68 1.41
105 0.02 -0.004 -0.7 0.2 1.4 0.3 0.4 -0.2 0.8 0.31 0.67 1.43
109 0.02 -0.004 -0.7 0.2 0.8 R 0.4 1.8 NDS 0.50 0.91 1.05
110 0.02 -0.004 -0.7 $ -0.5 -0.3 NDS NDS NDS -0.50 0.20 N/A N/A
112 0.02 -0.004 -0.7 0.2 0.8 -1.0 -1.0 NDS -1.1 -0.47 0.78 1.23
115 0.03 0.006 1.0 0.2 NDS NDS -1.0 NDS NDS 0.07 1.01 N/A N/A
123 0.03 0.006 1.0 0.2 0.3 1.5 0.4 -0.2 0.2 0.49 0.57 1.68
124 0.02 -0.004 -0.7 0.2 -0.7 NDS 0.4 -0.2 NDS -0.20 0.50 1.92
127 0.02 -0.004 -0.7 0.2 2.4 1.3 0.4 -0.2 2.1 0.79 1.17 0.82
131 0.02 -0.004 -0.7 $ 1.3 -0.7 0.4 R -0.4 -0.02 0.86 1.12
132 0.03 0.006 1.0 -1.8 0.0 -0.3 -1.0 NDS R -0.42 1.05 0.91
138 0.03 0.006 1.0 0.2 -1.1 -0.1 0.4 -0.2 0.8 0.14 0.70 1.37
141 0.03 0.006 1.0 0.2 1.6 -1.0 -1.0 -0.2 NDS 0.10 1.06 0.91
145 0.02 -0.004 -0.7 -1.8 R -1.6 -1.0 -0.2 -0.4 -0.95 0.64 1.50
151 0.02 -0.004 -0.7 2.2 -0.6 NDS NDS -0.2 NDS 0.18 1.37 0.70 X
152 0.03 0.006 1.0 0.2 R -1.0 -1.0 -2.2 -0.4 -0.57 1.11 0.86
154 ** 0.00 R 0.2 NDS -1.2 -1.0 -2.2 R -1.05 0.98 0.98
155 0.03 0.006 1.0 -1.8 -0.2 NDS 0.4 1.8 -1.7 -0.08 1.45 0.66 X
161 0.03 0.006 1.0 0.2 NDS -0.3 -1.0 NDS NDS -0.03 0.84 1.14
166 0.03 0.006 1.0 $ 1.2 NDS 1.9 -0.2 0.8 0.94 0.76 1.26
170 0.02 -0.004 -0.7 0.2 -3.5 0.8 R 1.8 0.8 -0.10 1.86 0.52 X
173 ** 0.09 R $ NDS 0.1 NDS NDS NDS 0.10 0.00 N/A N/A
179 0.03 0.006 1.0 0.2 1.2 1.2 0.4 -0.2 0.8 0.66 0.54 1.78
181 0.03 0.006 1.0 0.2 R -1.4 0.4 1.8 -0.4 0.27 1.11 0.86
184 0.03 0.006 1.0 -1.8 -0.6 1.5 0.4 NDS NDS 0.10 1.32 0.73 X
185 0.02 -0.004 -0.7 0.2 -0.5 NDS -1.0 -0.2 -0.4 -0.43 0.41 2.34
189 0.04 0.016 2.7 2, 3 0.2 -2.3 -0.7 1.9 NDS NDS 0.36 2.00 0.48 X
191 0.02 -0.004 -0.7 0.2 2.9 -1.0 -1.0 -2.2 -1.1 -0.41 1.62 0.59 X
192 0.02 -0.004 -0.7 -1.8 1.2 -0.8 0.4 -0.2 -0.4 -0.33 0.95 1.01
193 0.03 0.006 1.0 0.2 0.1 0.8 1.9 -0.2 0.8 0.66 0.70 1.37
204 0.02 -0.004 -0.7 0.2 0.2 0.1 -1.0 -0.2 1.4 0.00 0.77 1.25
211 0.02 -0.004 -0.7 0.2 -0.6 0.8 0.4 -0.2 0.2 0.01 0.54 1.78
213 0.03 0.006 1.0 NDS NDS 0.4 0.4 -0.2 NDS 0.40 0.49 1.96
215 0.02 -0.004 -0.7 0.2 -3.3 -0.5 0.4 -0.2 0.8 -0.47 1.35 0.71 X
220 0.03 0.006 1.0 0.2 NDS -0.8 1.9 -0.2 1.4 0.58 1.02 0.94
222 0.02 -0.004 -0.7 0.2 -0.9 -0.1 0.4 -0.2 0.2 -0.16 0.49 1.96
224 0.02 -0.004 -0.7 $ -1.2 0.1 0.4 -0.2 NDS -0.32 0.64 1.50
ASTM Crude Oil
Sample ID: CO1607
July 2016 226
Water - D4928
(Mass%)
1603 1511 1507 1503 1411 1407
226 ** 0.10 R 0.2 0.5 -1.0 -1.0 NDS NDS -0.32 0.79 1.22
230 0.02 -0.004 -0.7 0.2 0.5 1.0 NDS -0.2 1.4 0.37 0.77 1.25
232 0.02 -0.004 -0.7 0.2 0.1 -0.7 NDS -0.2 0.2 -0.18 0.43 2.23
233 0.03 0.006 1.0 NDS NDS 1.7 NDS -2.2 0.8 0.32 1.73 0.55 X
234 0.02 -0.004 -0.7 NDS NDS R 0.4 NDS NDS -0.15 0.78 N/A N/A
235 0.02 -0.004 -0.7 0.2 0.0 0.3 NDS -0.2 0.8 0.07 0.50 1.92
239 0.03 0.006 1.0 NDS 0.3 0.4 NDS -0.2 NDS 0.38 0.49 1.96
241 ** 0.05 R 0.2 2.2 R -1.0 -0.2 R 0.30 1.36 0.71 X

Legend:
R = Rejected
TPI 0.53
Comments:
227
Page 1 of 2
Sample ID: CO1607
Water - D4928
(Mass%)
0.024 0.048
0.018 0.042
0.012 0.036
Reproducibility
0.006 0.03
Deviation
0 0.024
-0.006 0.018
Reproducibility
-0.012 0.012
-0.018 0.006
-0.024 0
5 1 7 5 1 1 1 2 2 3 4 4 4 4 4 5 5 6 7 8 8 9 9 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2
4 1 9 8 0 1 7 5 6 0 1 4 6 7 8 0 1 8 7 8 9 1 2 0 0 0 0 0 1 1 2 2 2 3 3 4 5 7 7 8 9 9 9 0
3 0 1 3 5 9 0 2 1 4 7 0 1 5 1 0 7 5 1 2 5 2

228
Page 2 of 2
Sample ID: CO1607
Water - D4928
(Mass%)
0.024 0.048
0.018 0.042
0.012 0.036
Reproducibility
0.006 0.03
Deviation
0 0.024
-0.006 0.018
Reproducibility
-0.012 0.012
-0.018 0.006
-0.024 0
2 2 2 2 2 2 2 2 2 5 1 6 1 1 2 2 2 2 3 3 3 5 6 7 9 9 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 1 8 1
0 1 1 2 2 3 3 3 3 2 5 3 3 3 0 9 2 7 8 6 2 0 6 8 0 1 2 3 3 4 5 5 6 6 7 8 8 9 1 2 8 6 6
4 1 5 2 4 0 2 4 5 9 3 8 5 3 2 8 1 2 5 1 6 9 1 4 3 3 0 9

229
Sample ID: CO1607

Water - D4928
(Mass%)
56
1% Median 99%
48
40
Number of Labs
32
24
16
0
-0.02 -0.01 0 0.01 0.02 0.03 0.04 0.05 0.06 0.07

ASTM Crude Oil
Sample ID: CO1607
July 2016 230
Water Content by Karl Fischer Titration - D4377
(mass%)
1603 1511 1507 1503 1411 1407
003 0.04 0.013 1.6 1.8 0.8 0.3 1.9 -0.6 -0.3 0.79 1.02 1.02
007 0.02 -0.007 -0.9 0.2 -0.6 -0.4 -1.4 NDS NDS -0.62 0.59 1.76
009 0.01 -0.017 -2.1 3 0.2 -1.0 -0.3 -0.3 -0.6 0.4 -0.53 0.84 1.24
013 0.03 0.003 0.4 -1.5 R -1.6 -0.3 -0.6 -1.0 -0.77 0.76 1.37
021 0.03 0.003 0.4 R -0.4 NDS 3.0 3.4 1.1 1.50 1.65 0.63 X
023 0.03 0.003 0.4 0.2 1.0 3.1 -0.3 -0.6 0.4 0.60 1.22 0.85
030 0.02 -0.007 -0.9 0.2 0.9 0.3 0.8 -0.6 -0.3 0.06 0.69 1.51
045 0.02 -0.007 -0.9 $ -0.4 -0.6 -0.3 $ 0.4 -0.36 0.48 2.17
057 ** 0.17 R 3.5 -2.7 2.3 R R -1.7 0.35 3.01 0.35 X
066 0.03 0.003 0.4 0.2 0.6 -0.3 0.8 -0.6 1.1 0.31 0.60 1.73
067 0.03 0.003 0.4 0.2 0.9 -0.3 R -0.6 -1.0 -0.07 0.70 1.49
072 0.03 0.003 0.4 NDS 0.8 0.8 -0.3 1.4 0.4 0.58 0.57 1.82
078 0.02 -0.007 -0.9 0.2 0.8 0.3 -0.3 -0.6 -1.0 -0.21 0.67 1.55
082 0.03 0.003 0.4 NDS 0.6 -1.9 NDS 1.4 0.4 0.18 1.23 0.85
089 0.02 -0.007 -0.9 NDS 0.8 NDS 0.8 -0.6 -1.0 -0.18 0.91 1.14
090 0.03 0.003 0.4 0.2 0.2 0.6 0.8 1.4 -1.0 0.37 0.73 1.42
099 0.02 -0.007 -0.9 $ 0.4 -1.1 -0.3 -0.6 -1.7 -0.70 0.72 1.44
111 0.03 0.003 0.4 0.2 -0.1 0.3 0.8 -0.6 NDS 0.17 0.48 2.17
117 0.03 0.003 0.4 0.2 0.4 -1.3 0.8 -0.6 -0.3 -0.06 0.72 1.44
118 0.03 0.003 0.4 1.8 0.3 3.3 0.8 -0.6 -0.3 0.81 1.34 0.78 X
123 0.03 0.003 0.4 0.2 0.7 0.8 -1.4 NDS -1.0 -0.05 0.92 1.13
127 0.02 -0.007 -0.9 NDS NDS NDS -0.3 -0.6 1.9 0.03 1.27 0.82
135 0.03 0.003 0.4 3.5 0.6 R R NDS NDS 1.50 1.73 N/A N/A
148 0.02 -0.007 -0.9 0.2 0.6 -0.8 -1.4 -0.6 -1.0 -0.56 0.71 1.46
152 0.04 0.013 1.6 1.8 -2.7 -0.9 0.8 -0.6 -0.3 -0.04 1.58 0.66 X
161 0.03 0.003 0.4 0.2 NDS -0.8 3.0 NDS NDS 0.70 1.62 0.64 X
164 0.03 0.003 0.4 NDS 1.0 NDS 3.0 NDS R 1.47 1.36 N/A N/A
165 0.03 0.003 0.4 R -0.2 NDS 0.8 1.4 0.4 0.56 0.59 1.76
166 0.04 0.013 1.6 $ 0.9 0.9 -0.3 -0.6 R 0.50 0.92 1.13
176 0.02 -0.007 -0.9 0.2 R 1.6 -0.3 -0.6 -0.3 -0.05 0.89 1.17
178 ** 0.06 R $ 0.1 0.1 0.8 -0.6 0.4 0.16 0.51 2.04
183 0.02 -0.007 -0.9 0.2 NDS NDS -0.3 1.4 -1.0 -0.12 0.98 1.06
189 0.01 -0.017 -2.1 3 0.2 -1.1 -0.9 NDS NDS NDS -0.98 0.94 1.11
191 0.02 -0.007 -0.9 -1.5 1.6 -0.4 -0.3 -2.6 -2.4 -0.93 1.43 0.73 X
ASTM Crude Oil
Sample ID: CO1607
July 2016 231
(mass%)
1603 1511 1507 1503 1411 1407
193 0.03 0.003 0.4 0.2 -0.3 0.4 R 1.4 R 0.42 0.62 1.68
194 0.01 -0.017 -2.1 3 -1.5 1.8 0.4 0.8 -0.6 1.1 -0.01 1.43 0.73 X
203 0.03 0.003 0.4 0.2 1.0 -0.8 0.8 1.4 0.4 0.49 0.70 1.49
209 0.05 0.023 2.9 3 NDS 0.4 -0.1 0.8 -0.6 1.1 0.75 1.22 0.85
210 0.04 0.013 1.6 0.2 R R 1.9 1.4 0.4 1.10 0.75 1.39
211 0.02 -0.007 -0.9 0.2 0.6 0.1 -0.3 -0.6 -0.3 -0.17 0.51 2.04
214 0.02 -0.007 -0.9 $ 0.6 1.6 -0.3 NDS NDS 0.25 1.09 0.95
224 0.02 -0.007 -0.9 NDS 0.2 NDS NDS NDS NDS -0.35 0.78 N/A N/A
228 0.02 -0.007 -0.9 1.8 -1.0 NDS NDS NDS NDS -0.03 1.59 N/A N/A

Legend:
R = Rejected
TPI 1.55
Comments:
232
Sample ID: CO1607

(mass%)
0.048 0.075
0.04 0.067
Reproducibility
0.032 0.059
0.024 0.051
0.016 0.043
0.008 0.035
Deviation
0 0.027
-0.008 0.019
-0.016 0.011
-0.024 0.003
-0.032 3 Sigma Range Limit ASTM Standard -0.005

Reproducibility
-0.04 -0.013
-0.048 -0.021
1 9 1 9 3 8 2 1 2 1 2 7 1 2 7 2 4 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 9 8 7 6 6 2 2 2 1 1 2 2 1 2 8 6 3 1 2 1 2
8 9 9 0 9 2 5 0 4 1 8 2 2 1 5 9 7 0 8 6 6 6 6 3 3 2 1 1 1 0 0 2 2 7 6 9 3 1 3 2 3 0 9 1 1 4 5 2 6 0
9 4 8 8 1 8 1 7 4 4 1 6 6 3 5 4 3 1 5 2 1 8 7 1 8 3 7 3 3 0 2 6 9

233
Sample ID: CO1607

(mass%)
28
Median
24 1% 99%
20
Number of Labs
16
12
0
0 0.01 0.02 0.03 0.04 0.05 0.06 0.07
234
Sample ID: CO1607

API Gravity
40.8
40.7
40.6
40.5
Results
40.4
40.3
40.2
40.1
235
Sample ID: CO1607

Density
0.824
0.8235
0.823
Results
0.8225
0.822
0.8215
0.821
236
Sample ID: CO1607

Iron
19.1
17.1
15.1
13.1
11.1
Results
9.1
7.1
5.1
3.1
1.1
237
Sample ID: CO1607

Nickel
1.2
0.8
Results
0.6
0.4
0.2
-0
238
Sample ID: CO1607

Nitrogen
128
108
88
Results
68
48
28
239
Sample ID: CO1607

Pour Point
17.8
15.8
13.8
11.8
9.8
Results
7.8
5.8
3.8
1.8
-0.2
240
Sample ID: CO1607

Sulfur
0.21
0.205
0.2
0.195
0.19
Results
0.185
0.18
0.175
0.17
0.165
241
Sample ID: CO1607

Vanadium
0.8
0.7
0.6
0.5
Results
0.4
0.3
0.2
0.1
-0
242
Sample ID: CO1607

Vapor Pressure
2.2
1.7
Results
1.2
0.7
0.2
243
Sample ID: CO1607

Water
0.1
0.09
0.08
0.07
0.06
Results
0.05
0.04
0.03
0.02
0.01
-0
244
Crude Oil
Sample ID: CO1607
July 2016
PARTICIPANT COMMENTS
Lab 002
The following analyses are done using other test methods which were not
referenced by PTP. The tests, results and methods are listed as follows.
We also recommend addition of these ASTM in the PT program.
Pour point: 0C (ASTM D5949)

Water content: 0.04% (ASTM E203)
Asphaltene: 0.13% (n-pentane precipitation)
API Gravity: 39.08
Asphaltenes are precipitated from the original oil using n-pentane in

excess as the precipitating medium (30 mL n-pentane per gram of oil). The
mixture is filtered through a pre-weighed 0.45 m pore filter. The filter
residue (asphaltenes) is rinsed with n-pentane, and then transferred with
the filter to a weighing boat and dried in a desiccator, to be weighted
after drying.
API gravity is calculated based on the equation:

API Gravity=[141.5/(specific gravity at 15.6 C) - 131.5]
where specific gravity of the oil density at 15.56 C is estimated by
exponential extrapolation from the 15.0 C and 0.0 C data points and is
calculated based on following equation:
Specific gravity at 15.6 C = Density at 0C exp [( ln (Density oil at
15C) - ln (Density oil at 0C) )/15 15.56 ] / Density of water at
15.56C
Lab 003
Sample (Tin) ID : 149&169 .
Unable to report D445@25 Deg C , result between 2 bulbs are out of
determinability.
Lab 026
I was entering 0.00 for D4006 but the field won't accept it.
Lab 033
The sample bottle 525 of CO1607, came our lab with 3 other bottles more
(535, 549 and 550 of CO1607), of these samples it was not possible to
include results on line, because it is only allowed to a bottle.
Lab 037
THE WEIGHT OF BOTTLE NUMBER 617 IS (765 gm)
WHILE THE WEIGHT OF BOTTLE NUMBER 398 IS (923 gm)
245
Lab 044
Did not receive CO1607 until 10/4/16.
Lab 045
Sample has pour point of +9C making it not possible to meet the
requirement of keeping sample @ temperature of 0C for test methods D5191
and D323. Our lab has performed both tests maintaining temperature just
below 10C so as to make sample in liquid state.
Lab 046
Unable to run ASTM D7042 @ 100C
Lab 047
Water by Coulometric Karl Fischer (D4928)
Please introduce the method of Preparation of Apparatus
- With Single Compartment
- Without Diaphragm and
- Using only One Kind of Reagent.
Lab 059
Thank you very much.
Lab 062
Also received can 261
Lab 072
when we received CAN from the carrier, both of them were opened and
leaked.
Lab 085
ID container# is 84 and 85
Lab 103
ASTM D6560 asphaltenes results reported below the reporting parameters of
the method.
ASTM D664 TAN results reported below the reporting parameters of the
method.
ASTM D4929 A & B reported below the reporting parameters of the method.
Lab 109
We used two sample container #159 and #168.
Lab 116
Unable to enter result 0.00% for method D4006 Waterby Distillation as
instruction. Enter <0.025 for 0.00%
ASTM Response: This field has been corrected
Lab 130
We do not investigated influences sulphur and mercaptan for the test
method D4928.
246
Lab 177
Nothing Special
Lab 178
D4007 Water and Sediment by Centrifuge result was below detection limit
and reported as <0.025%
ASTM Response: This field has been corrected
Lab 196
ASTM D3230 - Faulty Salt in Crude Analyser
Lab 202
We do not investigated influences sulphur and mercaptan for the test
method D4928.
Lab 221
My lab received 2 samples;
Sample 78-We tested D323-Vapour Pressure (RVP) only.
Sample 79- We tested D1298(Density) & D4007(Water & Sediments by

Centrifuge).
Lab 228
The first question on the Asphaltene Questionnaire is a two part
question. A yes or no answer fails to identify which part of the question
is being acknowledged.
Lab 239
Our CO1607 sample to the lab was missing in action for so long and we had
to ask for another set of sample and that had caused this delay in the
submission of the results. Hopefully the sample that we received is from
the same batch as the other CO1607 samples
247
LAB INSTRUCTIONS
CRUDE OIL
July 2016
(CO1607)
The ASTM Proficiency Testing Center will provide an interactive data collection form to you by way of a secure ASTM-PTP website
server. You will have the capability of entering your own test data on a customized electronic data form. You will be able to
electronically save your data, review it, edit it, and then submit all your results to ASTM-PTP by the closing date of the test cycle.
Test instructions are subject to change. Please read the test instructions thoroughly every test cycle. Should you have any questions
about the test instructions or during the test trial, please contact the Proficiency Testing Center at ptp@astm.org.
1. Selected tests, to be determined by the participating laboratory from the designated list of test procedures, must be performed
within the participant's laboratory facilities using the specified ASTM standards. Participants are not to have tests performed by
a subcontracting laboratory or to deviate from the standard procedure.
2. Participants are to utilize the most current available edition of the ASTM standards (see the attached Index Listing of ASTM
Standards).
3. The initial single determination by each laboratory for each test conducted is required. Unless the ASTM test method otherwise
indicates, the ASTM-PTP does not allow the reporting of averages of replicate determinations or the reporting of results from
subsequent attempts following the initial result.
4. Laboratories are encouraged to provide any and all information on any problems they identified during testing or with their
results or where the test is not clear, etc., in the general comment section of the electronic data entry form. This will help the
standardization committee responsible for the test methods in this ASTM-PTP address any issues or improvements as needed.
5. Test results are to be entered in the interactive on-line report form within the PTP Portal. For sign-on details, please see the email
that was sent to your attention at the time samples were distributed. Should your email change, please contact the Proficiency
Testing Center at ptp@astm.org immediately.
6. Test results are to be recorded according to the specified units of measurement indicated on the interactive report form. The units
of measurements requested are consistent with the relevant ASTM test methods or that required in relevant specifications.
Participants will be responsible for any conversions necessary to comply with the report form.
7. IMPORTANT NOTEThe program requires that participants report a single value for each element in accordance
with the specific method used. Report the actual numerical value for the proficiency testing data obtained by your lab.
Values reported as less than (<) or greater than (>) cannot be numerically treated.
8. Please do not use commas for decimal points otherwise your data will be invalidated.
9. Your data must be received at ASTM no later than the posted deadline. Test data received after this date will not be included in
the published statistical summary report.
10. Please be sure to click on submit all test results when you are ready to submit your final results for all tests. Otherwise,
your data will not be received at ASTM.
11. NOTEThe abilitly to select reporting units has been added to D4294. Please select the proper reporting units or the result
will be rejected.
ASTM TEST PROGRAM SCHEDULE
Test Samples Distributed . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . week ending August 19 , 2016
DEADLINE DATE FOR RECEIPT OF TEST RESULTS AT ASTM . . . . . . . . . . . . . . . . . . . .October 14 , 2016
Statistical Summary Reports will be electronically distributed from ASTM approximately

2025 business days after the Deadline Date for Receipt of Test Results.
248

PROFICIENCY TESTING PROGRAM
UTILIZED IN THE JULY2016

CRUDE OIL (CO1607)
NOTERun tests in the order prescribed below.

Due to loss of light materials during these analyses, some results may be impacted when NOT analyzed in the prescribed
order of testing below.
1. VAPOR PRESSURE:
D323, D5191, or D6377, or a combination thereof
The sample is to be cooled to 0 to 1C before being opened in the laboratory.
If vapor pressure is performed by multiple test procedures, each must be performed on separate containers, as the
methods require that Vapor Pressure be the first procedure performed and do not allow further vapor pressure testing
on the same container. Therefore it is only possible to perform a maximum of two of these tests.
Shaking is required to ensure homogeneity of the test specimen and to ensure applicability of the sample to further
testing.
2. HIGH-TEMPERATURE SIMULATED DISTILLATION:

D7169
The sample must be homogenized prior to obtaining the test specimen to ensure homogeneity of the test specimen and
to ensure applicability of the sample to further testing.
Following the procedure is critical.
3. API GRAVITY:
D287
Method requires samples to be homogenized before obtaining a test specimen.
Homogenization is critical to ensure applicability of the sample to further testing.
4. DENSITY:
D1298 or D5002, or both
Both methods require samples to be homogenized before obtaining a test specimen.
5. SALTS:
D3230 does not address homogenization of the laboratory sample. However, homogenization is necessary before
obtaining the test specimen, in order to obtain valid results.
D6470 required samples to be homogenized before obtaining a test specimen.
6. WATER:
D4006, D4007, D4377, or D4928, or a combination thereof
D4006 does not specifically address homogenization of the laboratory sample. However, homogenization is necessary
before obtaining a test specimen, to obtain valid results.
D4007 requires mixing of the sample to ensure homogeneity.
D4377 and D4928 require homogenization of the laboratory sample, before obtaining a test specimen.
249

PROFICIENCY TESTING PROGRAM
UTILIZED IN THE MARCH2015

CRUDE OIL (CO1607)
7. SEDIMENT:
D473, D4007, or D4807, or a combination thereof
D473 and D4807 require samples to be homogenized before obtaining a test specimen.
D4007 requires mixing of the sample to ensure homogeneity.
8. METALS:
Both methods require samples to be homogenized before obtaining a test specimen.
9. MICRO CARBON RESIDUE:

D4530
D4530 does not address homogenization of the laboratory sample. However, homogenization is necessary
before obtaining a test specimen, to obtain valid results.
10. ACID NUMBER:

D664
obtaining a test specimen, to obtain valid results.
11. POUR POINT:

Neither method addresses homogenization of the laboratory sample. However, homogenization is necessary before
obtaining a test specimen, to obtain valid results.
12. NITROGEN:
obtaining a test specimen, to obtain valid results. This method uses syringes, which could plug if sediment is
drawn into the needle.
D5762 requires mixing/homogenization before obtaining a test specimen. This method uses syringes, which could
plug if sediment is drawn into the needle.
13. VISCOSITY:
D445
D445 does not address homogenization of the laboratory sample. However, homogenization may be necessary before
obtaining a test specimen, to obtain valid results. Sediment may cause plugging of tubes thereby invalidating the
result.
14. ASPHALTENES:
D6560
Homogenization is required.
15. SULFUR:
Neither D4294 nor D2622 addresses homogenization. Water or sediment, or both, will interfere with these
analyses, so samples should be allowed to settle or be centrifuged prior to analysis.
Since homogenization is not recommended, further testing on this sample is not recommended.
250
USER ID COMPANY NAME
CITY STATE COUNTRY
DEADLINE FOR DATA SUBMISSION 10/14/2016

THIS FORM IS A WORKSHEET TO BE USED IN THE LAB ONLY. ALL DATA MUST BE SUBMITTED
ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
API GRAVITY
D287
(XX.X API @ 60F)
API Gravity
ASPHALTENES
D6560
IF<1.0 report to nearest 0.05% m/m%. . IF >1.0 report to nearest 0.1% m/m%
Asphaltenes
D6560 Asphaltene Questionnaire
D6560 Asphaltene Questionnaire
Are you following D6560 to the letter or do you have in-house modifications?
Do you find your crude slate more difficult to handle in the method than it
used to be?
A training video on the method will soon be available from ASTM.
Would you be interested in seeing it?
Do you use other in-house automation methods to measure asphaltene?
If so, please report data under the General Comments section.
Carbon Residue
D4530
TEST AS IS. For Values Up to 10%, report Carbon Residue Value to the Nearest 0.01%(m/m). For Values above 10% Report
Carbon Residue Value to Nearest 0.1% (m/m)
Carbon Residue
1
251
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
DENSITY
D1298
(If result initially developed in 60F, please convert your data to 15C using Petroleum Measurement Tables (Guide 1250).
NOTE: Data not repoted in C will be made outliers.
API GRAVITY
Density
(Report results at 15C AND to the nearest 0.0001 kg/L)
D5002
Report result at 15C (kg/L) to 4 signficant figures (0.XXXX) (If result initially developed in 60F, please convert your data to
15C using Petroleum Measurement Tables (Guide 1250). NOTE: Data not reported in C will be made outliers.
Density
2
252
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
HIGH TEMPERATURE SIMULATED DISTILLATION
D7169
Report ALL DATA to the nearest 0.1C. NOTE: DATA NOT REPORTED IN C WILL BE MADE OUTLIERS
IBP
5%
10%
20%
30%
40%
50%
60%
70%
80%
90%
95%
FBP
3
253
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
D7169 Questionnaire
Sample Introduction
Mass (g) of sample
Mass (g) of carbon disulphide
Injection size uL
Injector type: PTV or on-column
Oven Temperature Program
Initial Temperature
Oven Rate
Final Temperature
Injector Temperature Program
Initial Temperature
Rate
Final Temperature
Endpoint Detection
Carbon no. or automatic detection
4
254
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
D7169 Questionnaire
Calibration & Column Performance
RT Standard Hydrocarbon Range nC? To nC???
Resolution nC50/nC52
Skewness nC20
Data Collection Rate Hz
HTSD Additional Total Weight Recovery Data
D7169 Total Weight % Recovery

Report ALL data to the nearest 0.1 wt.%.
82.2C (180F)
193.3C (380F)
248.9C (480F)
343.3C (650F)
426.7C (800F)
565.6C (1050F)
596.1C (1105F)
720C (1328F)
5
255
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
METALS
D5708 (METHOD A)
(Report to 3 significant figures in mg/kg) Please, Only To 3 Significant Figures
Vanadium
Nickel
Iron
D5708 (METHOD B)
(Report to 3 significant figures in mg/kg) Please, Only To 3 Significant Figures
Vanadium
Nickel
Iron
D5863 (METHOD A)
(Report to 2 significant figures in mg/kg) Please, only to 2 significant figures.
Vanadium
Nickel
Iron
D5863 (METHOD B)
(Report to 2 significant figures in mg/kg) Please, only to 2 significant figures.
Vanadium
Nickel
6
256
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
NITROGEN
D4629
For results = or > 1mg/kg, report nitrogen concentarion to two (2) significant figures, for results < 1 mg/gk report result to
nearest 0.1 mg/kg
Nitrogen
DILUTION FACTOR
D5762
(Report to 2 significant figures to the nearest ug/g to a maximum of one decimal point)
Nitrogen
POUR POINT
D97 Pour Point

Report UPPER POUR POINT in 3C increments per Section 9.1
Upper Pour Point
D5853 Method A
(Report results in 3C increments)
Pour Point
7
257
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
SALTS
D3230
(Report salt to the nearest 0.01 lb/1000 bbl)
SALTS
D6470
(REPORT TO ONLY 2 SIGNIFICANT FIGURES, MASS %)
Salts
SEDIMENT
D473
If values >0.005 mass %, then report to nearest 0.01 mass %. If values <=0.005 mass %, then report as "0.00"
Sediment
D4807
(Report to 0.001 mass %)
Sediment
8
258
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
SULFUR
D2622
(Report in mass % to required significant figures per Section 12.)
Sulfur
Unit of Measure
Please select mg/kg or mass%
D4294
(REPORT TO 3 SIGNIFICANT FIGURES ONLY)
Sulfur
Unit of Measure
Please select mg/kg or mass%
Total Acid Number
D664
(Report in mg KOH/g to 3 significant figures)
Total Acid Number
9
259
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
VISCOSITY, KINEMATIC
D445 @ 25C
Report to 4 significant figures (mm/s).
Viscosity
D445 @ 40C
Report to 4 significant figures (mm/s). NOTE: DATA NOT REPORTED IN C WILL BE MADE OUTLIERS
Viscosity
D7042 @ 40C
Report Kinematic Viscosity(v) (mm/s) to 4 Significant Figures.Results other than Kinematic Viscosity will be rejected. Check
which instrument mode (ONLY 1) was used during testing.
Kinematic Viscosity
D7042 @ 100C
Report Kinematic Viscosity(v) (mm/s) to 4 Significant Figures.Results other than Kinematic Viscosity will be rejected.Check
which instrument mode (ONLY 1) was used during testing.
Kinematic Viscosity
10
260
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
Vapor Pressure
D323 REID VAPOR PRESSURE

(Report to nearest 0.05 p.s.i.)
Vapor Pressure
D5191*
Report total vapor pressure to nearest 0.01 p.s.i.
TVP
D6377 VAPOR PRESSURE (EXPANSION METHOD) (kPa)

Report Vapor Pressure at 37.8C (100F) and a V/L of 4:1. Report result to nearest 0.1 kPa
Vapor Pressure
Water Content
D4006
Report water content to nearst 0.025%, BUT IF result is <0.025% report as 0.00%
Water
D4928
(Report to 0.01 mass %)
Water
D4377 Water by Karl Fischer/Potentiometric Titration

Calculate the Water Content of the Sample and Report in Mass % to nearest 0.01 mass%
Water Content
11
261
CITY STATE COUNTRY

ELECTRONICALLY.
ASTM Crude Oil
Sample ID: CO1607
Water and Sediment by Centrifuge
D4007 Water and Sediment by Centrifuge

Report the combined volume of water and sediment to the nearest 0.025 vol % in accord with Section 8 of the test
Determination of Organic Chloride Content
D4929-Method A
Chloride Content
Report Chloride results in g/g
D4929-Method B
Chloride Content
Report Chloride results in g/g
GENERAL COMMENTS
General Comments:
General Comments:
12

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CommitteeD2

Sponsored by ASTM Committee D-2 on Petroleum Products and Lubricants

Report Introduction ...........................................................................................................3-7

Alphabetical Listing of Program Participants ............................................................. 8-12

Listing of ASTM Standards Used in Program ............................................................ 13

Summary of Statistics ................................................................................................. 14-15

Acid Number, D664 .........................................................................................................16-22

Asphaltenes, D6560 ..........................................................................................................34-37

Carbon Residue (Micro Method), D4530.........................................................................38-44

High Temperature Simulated Distillation, D7169 ...................................................... 58-111

Chloride Content, D4929

Reid Vapor Pressure, D323......................................................................................... 132-135

Total Vapor Pressure, D5191 ...................................................................................... 190-193

Vapor Pressure (Expansion Method), D6377 ............................................................. 194-197

Box and Whisker Graphs ..................................................................................................234-243

Participant Comments ................................................................................................. 244-246

Test Instructions and Lab Worksheet.......................................................................... 247-261

Description of the Robust Mean and Robust Standard Deviation

Calculation of Robust Mean and Robust Standard Deviation

TEST PERFORMANCE INDEX (Industry) (TPI(Industry)) - TPI(Industry) provides an index similar to

TPI (Industry) = RASTM / Robust R These Data

Robust Mean + / - 2.33 x Robust Standard Deviation

USE OF CURRENT & PAST Z-SCORES TO MONITOR LAB PERFORMANCE AND

Z-Score = X (individual lab result) - Robust Mean (These Data)

OTHER LEGEND SYMBOL DEFINITIONS/APPLICATIONS

** - Data for current trial is rejected

NDS Lab did not submit data for that trial

ND Not Detected = valid D4815 result

$ - applies to past Z-Scores possibly meaning:

* - Data was submitted, but no past Z-Scores were published because:

2. Reanalyze the sample; check for repeatability.

5. Check the instrument calibration.

9. Call the vendor for maintenance and/or repairs.

Participating in CO1607 Crude Oil

AGAT LABORATORIES AMSPEC SERVICES LLC CAMIN CARGO

CORE LABORATORIES LP (PENCOR) ESSO NORGE AS INA-RAFINERIJA NAFTE RIJEKE

ENAP REFINERIA BIO BIO EXXONMOBIL INSPECTORATE AMERICA CORPORATION

ENAP REFINERIAS CON CON FLINT HILL RESOURCES LP INSPECTORATE AMERICA

INTERTEK INTERTEK MARATHON PETROLEUM COMPANY LLC

INTERTEK INTERTEK MARATHON PETROLEUM COMPANY LLC

MONROE ENERGY PETROAMAZONAS EP PUMA ENERGY PNG REFINING LIMITED

PETROAMAZONAS EP PRI ASPHALT TECHNOLOGIES, INC. SAUDI ARAMCO SERVICES CO, #2

SINCLAIR WYOMING REFINING WYNNEWOOD REFINING

SOUTHERN PETROLEUM LABORATORIES YPF SA

ASTM PROFICIENCY TESTING PROGRAM

UTILIZED IN THE JULY2016

ASTM Customer Service Department

D97-16 Test Method for Pour Point of Petroleum Products

Results Results Results Robust Robust Anderson

Results Results Results Robust Robust Anderson

006 ** 0.14 R 1.8 R R 1.2 0.2 -0.5 0.68 1.02 0.99

045 <0.1 $ $ $ -0.5 -0.8 $ -0.65 0.21 N/A N/A

084 <0.1 -0.4 2.3 R R 1.6 0.0 0.88 1.28 0.79 X

088 <0.10 $ 0.3 0.5 1.0 -1.8 $ 0.00 1.24 0.81

Pooled Standard Deviation = 1.01

3 Sigma Range Limit These Test Data

Lab Code (Presented Vertically)

3 Sigma Range Limit These Test Data

Lab Code (Presented Vertically)

Sample ID: CO1607

Pooled Standard Deviation = 1.03

-0.48 3 Sigma Range Limit ASTM Standard

Lab Code (Presented Vertically)

-0.48 3 Sigma Range Limit ASTM Standard