Method 1 :
Method 2 :
1. HCl (150 ml, 0.7 M) was carefully added to 500 ml of 0.1 M Na2WO4 solution until the final
pH of the clear solution reached a value of 1.6.
2. The clear solution thus obtained was autoclaved at 60C for 48 h.
3. A white precipitate appeared within 1 h.
4. After 48 h of autoclaving the white precipitate was isolated by decantation an
centrifugation, washed several times with doubly distilled water and then dried in a Petri
dish at 60C for 48 h.
5. The color of this sample did not change from first appearance to its isolation.
Method 3 :
Method 1:
Reference : Preparation and Characterisation of ZnO/NiO Nanocomposite Particles for Solar Cell
Applications
PREPARATION OF CoO
Method 1
Reference : Preparation of NiO and CoO nanoparticles using M2+ -oleate (M = Ni, Co) as precursor
PREPARATION OF WO3/g-C3N4 (Catalyst preparation)
1. The chemicals used in this work, melamine (C3H), dicyanodiamide(C2H4N4), and tungstic
anhydride powder (WO6), were reagent grade
2. Metal-free g-C3N4 powders were synthesized by heating mixed melamine an dicyanodiamide
powder in a mufe furnace.
3. In a typical synthesis, 2.0 g of melamine and 2.0 g of dicyanodiamide were well mixed using
a mortar.
4. After mixing, the powder was placed in a semi-closed alumina crucible with a cover.
5. The crucible was heated to 550C and held for 4 hr at a heating rate of 2.2Cmin-1 .
6. After the reaction, the alumina crucible was cooled to room temperature.
7. The product was then collected and ground into powder.
8. The synthesized g-C3N4 and WO3 powders were mixed using an agate mortar.
9. The mixed mass ratios in this work were as follows : g-C3N4:WO3= 8:2, 6:4, 4:6, 2:8.
Reference : Preparation of graphitic carbon nitride (g-C3N4)/WO3 composites and enhanced visible-
light-driven photodegradation of acetaldehyde gas